BMRB Entry 6652

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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR6652
MolProbity Validation Chart

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Title:
RNA helical packing in solution: NMR structure of a 30 kDa GAAA tetraloop receptor complex
Deposition date:
2005-06-01
Original release date:
2005-09-08
Authors:
Davis, Jared; Tonelli, Marco; Scott, Lincoln; James, Williamson; Butcher, Samuel
Citation:

Citation: Davis, Jared; Tonelli, Marco; Scott, Lincoln; Jaeger, Luc; Williamson, James; Butcher, Samuel. "RNA Helical Packing in Solution: NMR Structure of a 30kDa GAAA Tetraloop-Receptor Complex."  J. Mol. Biol. 351, 371-382 (2005).
PubMed: 16002091

Assembly members:

Assembly members:
GAAA tetraloop 11-nt receptor RNA, polymer, 43 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: enzymatic semisynthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
GAAA tetraloop 11-nt receptor RNA: GGGAUAUGGAAGAACCGGGG AAACUUGGUUCUUCCUAAGU CCU

Data sets:
Data typeCount
13C chemical shifts88
15N chemical shifts23
1H chemical shifts239

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
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Assembly:

Entity Assembly IDEntity NameEntity ID
1.1
2.1

Entities:

Entity 1, .

Samples:

sample_1: GAAA tetraloop 11-nt receptor RNA, [U-95% 13C; U-95% 15N], 1.2 mM; pf1 phage 17 ± 2 mM

conditions_1: pH: 6.8; temperature: 283 K

conditions_2: temperature: 303 K

Experiments:

NameSampleSample stateSample conditions
1H-1H NOESYsample_1not availablenot available
1H-1H TOCSYsample_1not availablenot available
1H-13C HSQCsample_1not availablenot available
HCCH-TOCSYsample_1not availablenot available
HCCH-COSYsample_1not availablenot available
HNN-COSYsample_1not availablenot available
1H-13C-1H NOESY HMQCsample_1not availablenot available
F2f 13C 1H-1H NOESYsample_1not availablenot available
F1f F2e 13C 1H-1H NOESY F1e F2e 13C 1H-1H NOESY F1f 13C 1H-1H NOESYsample_1not availablenot available

Software:

No software information available

NMR spectrometers:

  • Bruker DMX 500 MHz
  • Bruker DMX 600 MHz
  • Bruker DMX 750 MHz
  • Varian inova 600 MHz
  • Varian inova 800 MHz
  • Varian inova 900 MHz