BMRB Entry 6618
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR6618
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Martins, Rafael; Sforca, Mauricio; Amino, Rogerio; Juliano, Maria; Oyama, Sergio; Juliano, Luiz; Pertinhez, Thelma; Spisni, Alberto; Schenkman, Sergio. "Lytic Activity and Structural Differences of Amphipathic Peptides Derived from
Trialysin" Biochemistry 45, 1765-1774 (2006).
PubMed: 16460023
Assembly members:
P6, polymer, 32 residues, 3510.4 Da.
Natural source: Common Name: Triatoma infestans Taxonomy ID: 30076 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Triatoma infestans
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
P6: FKIKPGKVLDKFGKIVGKVL
KQLKKVSAVAKV
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 201 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | peptide P6 | 1 |
Entities:
Entity 1, peptide P6 32 residues - 3510.4 Da.
| 1 | PHE | LYS | ILE | LYS | PRO | GLY | LYS | VAL | LEU | ASP | ||||
| 2 | LYS | PHE | GLY | LYS | ILE | VAL | GLY | LYS | VAL | LEU | ||||
| 3 | LYS | GLN | LEU | LYS | LYS | VAL | SER | ALA | VAL | ALA | ||||
| 4 | LYS | VAL |
Samples:
sample_1: P6 1.2 mM; TFE 30 % (vol); D2O 5 % (vol); H2O 65 % (vol)
P6_conditions: pH: 4; temperature: 310 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1H TOCSY | sample_1 | not available | P6_conditions |
| 1H COSY | sample_1 | not available | P6_conditions |
| 1H NOESY | sample_1 | not available | P6_conditions |
| 1H ROESY | sample_1 | not available | P6_conditions |
Software:
NMRView5 v5, One Moon Scientific Inc. - chemical shift assignment, spectrum analysis
NMR spectrometers:
- Varian Unity 500 MHz