BMRB Entry 5633
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR5633
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Katayama, H.; Nagata, K.; Ohira, T.; Yumoto, F.; Tanokura, M.; Nagasawa, H.. "The solution structure of molt-inhibiting hormone from the Kuruma prawn
Marsupenaeus japonicus " J. Biol. Chem. 278, 9620-9623 (2003).
PubMed: 12519766
Assembly members:
MOLT-INHIBITING HORMONE, polymer, 78 residues, Formula weight is not available
Natural source: Common Name: Marsupenaeus japonicus Taxonomy ID: 27405 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Marsupenaeus japonicus
Experimental source: Production method: recombinant technology Host organism: Escherichia coli
Entity Sequences (FASTA):
MOLT-INHIBITING HORMONE: ASFIDNTCRGVMGNRDIYKK
VVRVCEDCTNIFRLPGLDGM
CRNRCFYNEWFLICLKAANR
EDEIEKFRVWISILNAGQ
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 628 |
| 13C chemical shifts | 343 |
| 15N chemical shifts | 97 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | molt-inhibiting hormone | 1 |
Entities:
Entity 1, molt-inhibiting hormone 78 residues - Formula weight is not available
| 1 | ALA | SER | PHE | ILE | ASP | ASN | THR | CYS | ARG | GLY | ||||
| 2 | VAL | MET | GLY | ASN | ARG | ASP | ILE | TYR | LYS | LYS | ||||
| 3 | VAL | VAL | ARG | VAL | CYS | GLU | ASP | CYS | THR | ASN | ||||
| 4 | ILE | PHE | ARG | LEU | PRO | GLY | LEU | ASP | GLY | MET | ||||
| 5 | CYS | ARG | ASN | ARG | CYS | PHE | TYR | ASN | GLU | TRP | ||||
| 6 | PHE | LEU | ILE | CYS | LEU | LYS | ALA | ALA | ASN | ARG | ||||
| 7 | GLU | ASP | GLU | ILE | GLU | LYS | PHE | ARG | VAL | TRP | ||||
| 8 | ILE | SER | ILE | LEU | ASN | ALA | GLY | GLN |
Samples:
sample_1: MOLT-INHIBITING HORMONE, [U-15N; U-13C], 2 mM; CD3CN 30%; D2O 10%; H2O 60%
sample_2: MOLT-INHIBITING HORMONE, [U-15N], 2 mM; CD3CN 30%; D2O 10%; H2O 60%
sample_cond_1: pH: 7.4; temperature: 298 K; ionic strength: 0 M; pressure: 1 atm
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 3D 13C-separated NOESY | not available | not available | not available |
| 3D 15N-separated NOESY | not available | not available | not available |
Software:
DYANA v1.4 - refinement
NMR spectrometers:
- Varian INOVA 500 MHz
Download HSQC peak lists in one of the following formats:
CSV: Backbone
or all simulated peaks
SPARKY: Backbone
or all simulated peaks