BMRB Entry 4971
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR4971
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Citation: Vranken, W.; James, S.; Bennett, H.; Ni, F.. "Solution structures of a 30 residue amino-terminal domain of the carp
granulin-1 protein and its amino-terminally truncated 3-30 subfragment:
implications for the conformational stability of the stack of two
beta-hairpins." Proteins 47, 14-24 (2002).
PubMed: 11870861
Assembly members:
truncated amino-terminal Carp Granulin-1, polymer, 28 residues, Formula weight is not available
Natural source: Common Name: carp Taxonomy ID: not available Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Caprinius carpio
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
truncated amino-terminal Carp Granulin-1: HCDAATICPDGTTCSLSPYG
VWYCSPFS
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 54 |
| 1H chemical shifts | 166 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | CG3-30 | 1 |
Entities:
Entity 1, CG3-30 28 residues - Formula weight is not available
| 1 | HIS | CYS | ASP | ALA | ALA | THR | ILE | CYS | PRO | ASP | ||||
| 2 | GLY | THR | THR | CYS | SER | LEU | SER | PRO | TYR | GLY | ||||
| 3 | VAL | TRP | TYR | CYS | SER | PRO | PHE | SER |
Samples:
sample_1: truncated amino-terminal Carp Granulin-1 2.0 mM; H2O 90%; D2O 10%
sample_2: truncated amino-terminal Carp Granulin-1 2.0 mM; D2O 100%
sample_cond_1: pH: 5.0; pressure: 1 atm; temperature: 288 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| TOCSY | not available | not available | not available |
| NOESY | not available | not available | not available |
Software:
NMRView v3.0 - Analysis
ARIA v1.0 - structure determination
NMR spectrometers:
- BRUKER DRX 500 MHz
- BRUKER AVANCE 800 MHz