BMRB Entry 16489
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR16489
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Citation: Galloux, Marie; Libersou, Sonia; Alves, Isabel; Marquant, Rodrigue; Salgado, Gilmar; Rezaei, Human; Lepault, Jean; Delmas, Bernard; Bouaziz, Serge; Morellet, Nelly. "NMR structure of a viral peptide inserted in artificial membranes: a view on the early steps of the birnavirus entry process." J. Biol. Chem. 285, 19409-19421 (2010).
PubMed: 20385550
Assembly members:
IBDV_pep46, polymer, 46 residues, Formula weight is not available
Natural source: Common Name: Birnavirus Taxonomy ID: 39742 Superkingdom: Viruses Kingdom: not available Genus/species: Birnavirus not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
IBDV_pep46: FGFKDIIRAIRRIAVPVVST
LFPPAAPLAHAIGEGVDYLL
GDEAQA
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 292 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | IBDV_pep46 | 1 |
Entities:
Entity 1, IBDV_pep46 46 residues - Formula weight is not available
| 1 | PHE | GLY | PHE | LYS | ASP | ILE | ILE | ARG | ALA | ILE | ||||
| 2 | ARG | ARG | ILE | ALA | VAL | PRO | VAL | VAL | SER | THR | ||||
| 3 | LEU | PHE | PRO | PRO | ALA | ALA | PRO | LEU | ALA | HIS | ||||
| 4 | ALA | ILE | GLY | GLU | GLY | VAL | ASP | TYR | LEU | LEU | ||||
| 5 | GLY | ASP | GLU | ALA | GLN | ALA |
Samples:
sample_1: IBDV pep46 1 mM
sample_conditions_1: pH: 3.5; pressure: 1 atm; temperature: 293 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF-COSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
Software:
X-PLOR v3.84, Brunger - structure solution
NMR spectrometers:
- Bruker Avance 600 MHz