BMRB Entry 15978
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR15978
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Citation: Bhunia, Anirban; Bhattacharjya, Surajit. "Lipopolysaccharide Bound Structures of the Active Fragments of
Fowlicidin-1, a Cathelicidin Family of Antimicrobial and Antiendotoxic
Peptide from Chicken, Determined by Transferred Nuclear Overhauser
Effect Spectroscopy" Biopolymers 92, 9-22 (2009).
PubMed: 18844294
Assembly members:
Fowlicidin-1, polymer, 16 residues, 1867.351 Da.
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: recombinant technology Host organism: solid phase peptide synthesis Vector: solid phase peptide synthesis
Entity Sequences (FASTA):
Fowlicidin-1: RVKRVWPLVIRTVIAG
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 101 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Fowlicidin-1 | 1 |
Entities:
Entity 1, Fowlicidin-1 16 residues - 1867.351 Da.
| 1 | ARG | VAL | LYS | ARG | VAL | TRP | PRO | LEU | VAL | ILE | ||||
| 2 | ARG | THR | VAL | ILE | ALA | GLY |
Samples:
sample_1: H2O 90%; D2O 10%; entity
sample_conditions_1: pH: 4.5; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D 1H-1H NOESY | sample_1 | isotropic | sample_conditions_1 |
| 2D 1H-1H TOCSY | sample_1 | isotropic | sample_conditions_1 |
Software:
DYANA v1.5, Guntert, Braun and Wuthrich - refinement
NMR spectrometers:
- Bruker DRX 600 MHz