BMRB Entry 4971

Title:
NMR data for the Carp Granulin 1 3-30 subfragment
Deposition date:
2001-03-14
Original release date:
2002-04-08
Authors:
Vranken, W.; James, S.; Bennett, H.; Ni, F.
Citation:

Citation: Vranken, W.; James, S.; Bennett, H.; Ni, F.. "Solution structures of a 30 residue amino-terminal domain of the carp granulin-1 protein and its amino-terminally truncated 3-30 subfragment: implications for the conformational stability of the stack of two beta-hairpins."  Proteins 47, 14-24 (2002).
PubMed: 11870861

Assembly members:

Assembly members:
truncated amino-terminal Carp Granulin-1, polymer, 28 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: carp   Taxonomy ID: not available   Superkingdom: Eukaryota   Kingdom: Metazoa   Genus/species: Caprinius carpio

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
truncated amino-terminal Carp Granulin-1: HCDAATICPDGTTCSLSPYG VWYCSPFS

Data sets:
Data typeCount
13C chemical shifts54
1H chemical shifts166

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1CG3-301

Entities:

Entity 1, CG3-30 28 residues - Formula weight is not available

1   HISCYSASPALAALATHRILECYSPROASP
2   GLYTHRTHRCYSSERLEUSERPROTYRGLY
3   VALTRPTYRCYSSERPROPHESER

Samples:

sample_1: truncated amino-terminal Carp Granulin-1 2.0 mM; H2O 90%; D2O 10%

sample_2: truncated amino-terminal Carp Granulin-1 2.0 mM; D2O 100%

sample_cond_1: pH: 5.0; pressure: 1 atm; temperature: 288 K

Experiments:

NameSampleSample stateSample conditions
TOCSYnot availablenot availablenot available
NOESYnot availablenot availablenot available

Software:

NMRView v3.0 - Analysis

ARIA v1.0 - structure determination

NMR spectrometers:

  • BRUKER DRX 500 MHz
  • BRUKER AVANCE 800 MHz

Related Database Links:

BMRB 4351
PDB