;pep_z_hsqc.bv ;Bruker DMX version ;2D 15N-1H Sensitivity-enhanced HSQC ;two experiments, due to echo-antiecho ;15N evolution phases ;last modified 9/15/95 by BFV ;Arthur G. Palmer III et al., JMR (1994), v. 104, 298-302. ;sequence by Brian Volkman, volkman@nmrfam.wisc.edu ;* see also nopephs3d.bv, 3D NOESY-HSQC version* ;BMRB Pulse Sequence Accession Number: 3 d6=3u d8=aq d11=50m d12=5m d25=p3-p1 1 ze ;*************** first experiment ************ ;********************************************** 2 d12*5 pl2:f2 d12 do:f2 3 10u pl9:f1 p18 ph0 10u pl1:f1 p1 ph1 p21 ph4 ;Messerle pulse 0.5-1.5ms d4 pl2:f2 (d25 p1*2 ph2) (p2*2 ph5):f2 d4 p22 ph1 ;Messerle pulse = 1.8 msec (d25 p1 ph2) (p2 ph5):f2 ;1H 90, X 90 (w/quad. inc.) d0 (p1 ph2 d6 p1*2 ph1 d6 p1 ph2) ;refocusing composite 180 1H d0 (d25 p1 ph11) (p2 ph14):f2 d4 (d25 p1*2 ph12) (p2*2 ph14):f2 d4 (d25 p1 ph12) (p2 ph15):f2 d4 (d25 p1*2 ph12) (p2*2 ph15):f2 d4 pl16:f2 p1 ph13 go=2 ph31 cpd2:f2 d11 do:f2 wr #0 if #0 zd ;write to disk ;**************** second experiment *********** 4 d12*5 d12 do:f2 10u pl9:f1 p18 ph0 10u pl1:f1 p1 ph1 p21 ph4 ;Messerle pulse 0.5-1.5ms d4 pl2:f2 (d25 p1*2 ph2) (p2*2 ph5):f2 d4 p22 ph1 ;Messerle pulse = 1.8 msec (d25 p1 ph2) (p2 ph5):f2 ;1H 90, X 90 (w/quad. inc.) d0 (p1 ph2 d6 p1*2 ph1 d6 p1 ph2) ;refocusing composite 180 1H d0 (d25 p1 ph11) (p2 ph24):f2 d4 (d25 p1*2 ph12) (p2*2 ph24):f2 d4 (d25 p1 ph12) (p2 ph25):f2 d4 (d25 p1*2 ph12) (p2*2 ph25):f2 d4 pl16:f2 p1 ph13 go=4 ph31 cpd2:f2 d11 do:f2 wr #0 if #0 zd ;write to disk ;*********************************************** d12 ip31 d12 ip31 d12 ip5 d12 ip5 d12 id0 lo to 3 times l3 exit ph0=1 ph1=0 ph2=3 ph3=0 2 ph4=1 ph5=0 0 2 2 ph11=1 0 ph12=0 3 ph13=3 2 ph14=2 1 ph24=0 1 ph15=1 0 ph25=1 2 ph31=0 2 2 0