;inv4prst ;MANUFACTURER: Bruker ;MODEL: DMX ;AUTHOR: Charles G. Hoogstraten ;DESCRIPTION: 2D H-1/X correlation via heteronuclear zero and double quantum ; coherence ;phase sensitive using States-TPPI method ;BMRB Pulse Sequence Accession Number: 23 ;A. Bax, R.H. Griffey & B.L. Hawkins, J. Magn. Reson. 55, 301 (1983) #include p2=p1*2 p4=p3*2 d4=2.3m d3=2.7m 1 ze 2 d11 do:f2 3 d11 4 4u d12 pl9:f1 d1 cw:f1 d13 do:f1 d12 pl1:f1 p1 ph1 d4 pl2:f2 ;reduced from 1/4J for proton T2 (p4 ph1):f2 (p2 ph1) d4 p7 ph1 (p1 ph3) (p3 ph2):f2 d3 ; 1/4J exactly (p4 ph1):f2 (p2 ph1) d3 d12 pl11:f2 8 d13 (p15 ph2):f2 d13 lo to 8 times l8 d0 p2 ph1 d0 d3 pl2:f2 (p4 ph1):f2 (p2 ph1) d3 (p1 ph5) (p3 ph4):f2 d4 (p2 ph1) (p4 ph1):f2 d4 pl12:f2 p7*1.3 ph1 go=2 ph31 cpd2:f2 d11 do:f2 wr #0 if #0 ip2 zd lo to 3 times 2 d11 id0 ip31*2 lo to 4 times l3 exit ph2=0 ph1=0 ph3=1 3 ph4=0 0 2 2 ph5=0 0 0 0 2 2 2 2 ph31=0 2 2 0 2 0 0 2 ;pl1 : f1 channel - power level for pulse (default) ;pl2 : f2 channel - power level for pulse (default) ;pl9 : f1 channel - power level for presaturation ;pl12: f2 channel - power level for CPD/BB decoupling ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p3 : f2 channel - 90 degree high power pulse ;p31: - 90 degree pulse for decoupling sequence ;d0 : incremented delay (2D) [3 usec] ;d1 : relaxation delay; 1-5 * T1 ;d2 : 1/(2J)XH ;d11: delay for disk I/O [30 msec] ;d12: delay for power switching [20 usec] ;d13: short delay [3 usec] ;L3: loop for phase sensitive 2D using States-TPPI method: l3 = td1/2 ;in0: 1/(2 * SW(X)) = DW(X) ;nd0: 2 ;NS: 4 * n ;DS: 16 ;td1: number of experiments ;MC2: States-TPPI ;cpd2: decoupling according to sequence defined by cpdprg2