NMRbot_CID_5468522_SampleReport.20190421_1227.txt
Status Report for Automated Sample Data Collection
## Host = kerry.nmrfam.wisc.edu ##

## NMRbot version 20140226 ##

## Initiated - 20190421_1227 ##

- info:
  CID_5468522 in DMSO at position 203
  foldername => CID_5468522.DMSO.203.20190419
  Exps => ZGCPPR,metabTOCSY,C13CPD_MMCD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND_MMCD,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 203 - passed
- DMSO solvent lock - passed
-   tuning probe channels - passed
-   topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 144
- creating exp 2 with metabTOCSY parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 3 with C13CPD_MMCD parameters
-   prosol parameters loaded
-   NS changed to 4096
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 4 with C13DEPT90 parameters
-   prosol parameters loaded
-   NS changed to 1024
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 5 with C13DEPT135_MMCD parameters
-   prosol parameters loaded
-   NS changed to 1024
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 6 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 8
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 7 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 8
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 8 with HMBCETGPL3ND_MMCD parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 9 with COSY45SW parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 10 with HSQC_TOCSY_ADIA parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 203
- experiment folders set up - passed
## Data Acquisition ##
# Exp 1 - ZGCPPR (zgcppr)
- dims 1- F1 1H, SW 16.03
- start 20190421_1238
- end   20190421_1241 - passed
-   1H adaptive offset determined = 4.7000
-   1H adaptive SW determined = 15.1492
# Exp 2 - metabTOCSY (mlevph)
- dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21
- start 20190421_1241
- end   20190421_1754 - passed
# Exp 3 - C13CPD_MMCD (zgpg30)
- dims 1- F1 13C, SW 248.61
- start 20190421_1754
- end   20190421_2127 - passed
# Exp 4 - C13DEPT90 (deptsp90)
- dims 1- F1 13C, SW 236.77
- start 20190421_2127
- end   20190421_2222 - passed
# Exp 5 - C13DEPT135_MMCD (deptsp135)
- dims 1- F1 13C, SW 236.77
- start 20190421_2222
- end   20190421_2316 - passed
-   13C adaptive offset determined = 82.3602
-   13C adaptive SW determined = 145.6061
# Exp 6 - HSQCETGP (hsqcetgp)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 12.99
- start 20190421_2316
- end   20190422_0011 - passed
# Exp 7 - HSQCETGP (hsqcetgp) - SWadapted
-   F1 SW changed to 145.61
-   F2 SW changed to 15.15
-   F1 1H offset changed to 4.70
-   F2 13C offset changed to 82.36
- dims 2- F1 13C, SW 145.61; F2 1H, SW 15.16
- start 20190422_0011
- end   20190422_0105 - passed
# Exp 8 - HMBCETGPL3ND_MMCD (hmbcetgpl3nd)
- dims 2- F1 13C, SW 240.00; F2 1H, SW 12.02
- start 20190422_0105
- end   20190422_0352 - passed
# Exp 9 - COSY45SW (cosyqf45)
- dims 2- F1 1H, SW 10.00; F2 1H, SW 10.00
- start 20190422_0352
- end   20190422_0624 - passed
# Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 16.03
- start 20190422_0624
- end   20190422_1128 - passed

## CID_5468522 Experiment Set Ended - 20190422_1128 ##

