NMRbot_cq_06302_SampleReport.20161024_1535.txt
Status Report for Automated Sample Data Collection
## Host = kerry.nmrfam.wisc.edu ##

## NMRbot version 20140226 ##

## Initiated - 20161024_1535 ##

- info:
  cq_06302 in MeOD at position 201
  foldername => cq_06302.MeOD.201.20161024
  Exps => ZGCPPR,metabTOCSY,C13CPD_MMCD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND_MMCD,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 201 - passed
- MeOD solvent lock - passed
-   tuning probe channels - passed
-   topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 64
- creating exp 2 with metabTOCSY parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 64
- creating exp 3 with C13CPD_MMCD parameters
-   prosol parameters loaded
-   NS changed to 2048
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 4 with C13DEPT90 parameters
-   prosol parameters loaded
-   NS changed to 512
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 5 with C13DEPT135_MMCD parameters
-   prosol parameters loaded
-   NS changed to 512
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 6 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 4
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 7 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 4
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 8 with HMBCETGPL3ND_MMCD parameters
-   prosol parameters loaded
-   NS changed to 8
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 9 with COSY45SW parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 101
- creating exp 10 with HSQC_TOCSY_ADIA parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 203
- experiment folders set up - passed
## Data Acquisition ##
# Exp 1 - ZGCPPR (zgcppr)
- dims 1- F1 1H, SW 16.03
- start 20161024_1548
- end   20161024_1549 - passed
-   1H adaptive offset determined = 4.7498
-   1H adaptive SW determined = 16.3629
# Exp 2 - metabTOCSY (mlevph)
- dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21
- start 20161024_1549
- end   20161024_1826 - passed
# Exp 3 - C13CPD_MMCD (zgpg30)
- dims 1- F1 13C, SW 248.61
- start 20161024_1827
- end   20161024_2013 - passed
# Exp 4 - C13DEPT90 (deptsp90)
- dims 1- F1 13C, SW 236.77
- start 20161024_2013
- end   20161024_2040 - passed
# Exp 5 - C13DEPT135_MMCD (deptsp135)
- dims 1- F1 13C, SW 236.77
- start 20161024_2040
- end   20161024_2107 - passed
-   13C adaptive offset determined = 82.7882
-   13C adaptive SW determined = 153.1187
# Exp 6 - HSQCETGP (hsqcetgp)
- dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99
- start 20161024_2108
- end   20161024_2135 - passed
# Exp 7 - HSQCETGP (hsqcetgp) - SWadapted
-   F1 SW changed to 153.12
-   F2 SW changed to 16.36
-   F1 1H offset changed to 4.75
-   F2 13C offset changed to 82.79
- dims 2- F1 13C, SW 153.12; F2 1H, SW 16.35
- start 20161024_2135
- end   20161024_2203 - passed
# Exp 8 - HMBCETGPL3ND_MMCD (hmbcetgpl3nd)
- dims 2- F1 13C, SW 240.00; F2 1H, SW 12.02
- start 20161024_2203
- end   20161024_2326 - passed
# Exp 9 - COSY45SW (cosyqf45)
- dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31
- start 20161024_2327
- end   20161025_0042 - passed
# Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02
- start 20161025_0042
- end   20161025_0318 - passed

## cq_06302 Experiment Set Ended - 20161025_0318 ##

