D-(+)-Galactose (C6H12O6)

D-(+)-Galactose bmse000013 - Data bmse001006 - Data

View large 3D structure

BMRB entry bmse001006

Entry DOI: doi:10.13018/BMSE001006
Data source: National Magnetic Facility at Madison - Francisca Jofre, Mark E. Anderson, John L. Markley

NMR-STAR file:

bmse001006.str

NMR-STAR

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Structure file (mol/sdf):

bmse001006.mol

All files for

bmse001006

Time Domain Data:

bmse001006.zip

Sample and instrument details are given with the spectrum

Assigned chemical shifts

Set 1
Sample:
Conditions:
Spectrometer:

Atom ID	Author Nomenclature	Value	Ambiguity Code
C6	C1	99.185	1
C6	C1	95.014	1
C5	C2	74.591	4
C5	C2	71.066	4
C5	C2	75.518	4
C5	C2	71.890	4
C5	C2	72.032	4
C5	C2	71.471	4
C5	C2	77.897	4
C5	C2	73.218	4
C4	C3	74.591	4
C4	C3	71.066	4
C4	C3	75.518	4
C4	C3	71.890	4
C4	C3	72.032	4
C4	C3	71.471	4
C4	C3	77.897	4
C4	C3	73.218	4
C3	C4	74.591	4
C3	C4	71.066	4
C3	C4	75.518	4
C3	C4	71.890	4
C3	C4	72.032	4
C3	C4	71.471	4
C3	C4	77.897	4
C3	C4	73.218	4
C2	C5	74.591	4
C2	C5	71.066	4
C2	C5	75.518	4
C2	C5	71.890	4
C2	C5	72.032	4
C2	C5	71.471	4
C2	C5	77.897	4
C2	C5	73.218	4
C1	C6	63.921	1
C1	C6	63.716	1
H19	H13	5.254	1
H19	H13	4.575	1
H18	H14	4.079	4
H18	H14	3.975	4
H18	H14	3.918	4
H18	H14	3.820	4
H18	H14	3.727	4
H18	H14	3.639	4
H18	H14	3.480	4
H17	H15	4.079	4
H17	H15	3.975	4
H17	H15	3.918	4
H17	H15	3.820	4
H17	H15	3.727	4
H17	H15	3.639	4
H17	H15	3.480	4
H16	H16	4.079	4
H16	H16	3.975	4
H16	H16	3.918	4
H16	H16	3.820	4
H16	H16	3.727	4
H16	H16	3.639	4
H16	H16	3.480	4
H15	H17	4.079	4
H15	H17	3.975	4
H15	H17	3.918	4
H15	H17	3.820	4
H15	H17	3.727	4
H15	H17	3.639	4
H15	H17	3.480	4
H13	H18	3.727	4
H14	H19	3.727	4

NMR experiments

1: 1D 1H
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Download time domain data: bmse001006_1.zip

2: 2D [1H,1H]-TOCSY
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Spectrum for experiment #2: 2D [1H,1H]-TOCSY

Download time domain data: bmse001006_2.zip

3: 1D DEPT90
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Download time domain data: bmse001006_3.zip

4: 1D DEPT135
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Download time domain data: bmse001006_4.zip

5: 2D [1H,13C]-HSQC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Spectrum for experiment #5: 2D [1H,13C]-HSQC

Download time domain data: bmse001006_5.zip

6: 2D [1H,13C]-HMBC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Spectrum for experiment #6: 2D [1H,13C]-HMBC

Download time domain data: bmse001006_6.zip

7: 2D [1H,1H]-COSY
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Spectrum for experiment #7: 2D [1H,1H]-COSY

Download time domain data: bmse001006_7.zip

8: 2D [1H,13C]-HMQC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Spectrum for experiment #8: 2D [1H,13C]-HMQC

Download time domain data: bmse001006_8.zip

9: 2D [1H,13C]-HSQC SW small
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 600MHz

Spectrum for experiment #9: 2D [1H,13C]-HSQC SW small

Download time domain data: bmse001006_9.zip