2'-Deoxyguanosine 5'-monophosphate (C10H14N5O7P)

2'-Deoxyguanosine 5'-monophosphate bmse000824 - Data bmse000879 - Data

View large 3D structure

BMRB entry bmse000824

Entry DOI: doi:10.13018/BMSE000824
Data source: National Magnetic Facility at Madison - Francisca Jofre, Mark E. Anderson, John L. Markley, Melanie E. Ulrich

NMR-STAR file:

bmse000824.str

NMR-STAR

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Structure file (mol/sdf):

bmse000824.mol

All files for

bmse000824

Time Domain Data:

bmse000824.zip

View the GISSMO record for this entry.

Sample and instrument details are given with the spectrum

Assigned chemical shifts

Set 1
Sample: multiple; see NMR-STAR file
Conditions: multiple; see NMR-STAR file
Spectrometer: Bruker DMX - 500MHz

Atom ID	Author Nomenclature	Value	Ambiguity Code
C6	C14	86.051	1
C4	C15	74.254	1
C1	C16	41.648	1
C5	C17	89.025	1
C5	C17	88.958	1
C2	C18	66.738	1
C2	C18	66.702	1
C8	C19	153.868	1
C3	C20	140.187	1
C7	C21	118.638	1
C9	C22	161.455	1
C10	C23	156.526	1
H31	H24	6.243	1
H29	H25	4.705	1
H24	H26	2.762	2
H24	H26	2.533	2
H25	H27	2.762	2
H25	H27	2.533	2
H30	H28	4.229	1
H26	H29	3.972	1
H27	H30	3.972	1
H28	H32	8.121	1

NMR experiments

1: 1D 1H
Sample: 0.5mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_1.zip

2: 1D 1H
Sample: 2.0mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_2.zip

3: 1D 1H
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_3.zip

4: 2D [1H,1H]-TOCSY
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #4: 2D [1H,1H]-TOCSY

Download time domain data: bmse000824_4.zip

5: 1D 13C
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_5.zip

6: 1D DEPT90
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_6.zip

7: 1D DEPT135
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_7.zip

8: 2D [1H,13C]-HSQC
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #8: 2D [1H,13C]-HSQC

Download time domain data: bmse000824_8.zip

9: 2D [1H,13C]-HMBC
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #9: 2D [1H,13C]-HMBC

Download time domain data: bmse000824_9.zip

10: 2D [1H,1H]-COSY
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #10: 2D [1H,1H]-COSY

Download time domain data: bmse000824_10.zip

11: 2D [1H,13C]-HSQC
Sample: Saturatedn/a in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_11.zip

12: 1D 1H
Sample: 0.5mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.33
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_12.zip

13: 1D 1H
Sample: 2.0mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.40
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_13.zip

14: 1D 1H
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_14.zip

15: 2D [1H,1H]-TOCSY
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #15: 2D [1H,1H]-TOCSY

Download time domain data: bmse000824_15.zip

16: 1D 13C
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_16.zip

17: 1D DEPT90
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_17.zip

18: 1D DEPT135
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_18.zip

19: 2D [1H,13C]-HSQC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #19: 2D [1H,13C]-HSQC

Download time domain data: bmse000824_19.zip

20: 2D [1H,13C]-HMBC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #20: 2D [1H,13C]-HMBC

Download time domain data: bmse000824_20.zip

21: 2D [1H,1H]-COSY
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Spectrum for experiment #21: 2D [1H,1H]-COSY

Download time domain data: bmse000824_21.zip

22: 2D [1H,13C]-HSQC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.17
Spectrometer: Bruker DMX - 500MHz

Download time domain data: bmse000824_22.zip