GDP (C10H15N5O11P2)
BMRB entry bmse000270
Entry DOI: doi:10.13018/BMSE000270
Data source: Madison Metabolomics Consortium - Qiu Cui, Ian Lewis, Mark E. Anderson, John L. Markley
NMR-STAR file:
bmse000270.strNMR-STAR
interactive viewerStructure file (mol/sdf):
bmse000270.molAll files for
bmse000270Time Domain Data:
bmse000270.zipView the GISSMO record for this entry.
Sample and instrument details are given with the spectrum
Assigned chemical shifts
Set 1
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
| Atom ID | Author Nomenclature | Value | Ambiguity Code |
|---|---|---|---|
| C1 | C19 | 67.173 | 1 |
| C1 | C19 | 67.122 | 1 |
| C9 | C20 | 89.807 | 1 |
| C3 | C21 | 86.220 | 1 |
| C3 | C21 | 86.132 | 1 |
| C6 | C22 | 76.753 | 1 |
| C5 | C23 | 72.513 | 1 |
| C10 | C24 | 156.633 | 1 |
| C7 | C25 | 154.154 | 1 |
| C8 | C26 | 161.607 | 1 |
| C4 | C27 | 118.758 | 1 |
| C2 | C28 | 140.110 | 1 |
| H29 | H37 | 4.229 | 1 |
| H30 | H38 | 4.229 | 1 |
| H35 | H39 | 5.901 | 1 |
| H32 | H40 | 4.336 | 1 |
| H34 | H41 | 4.682 | 1 |
| H33 | H42 | 4.589 | 1 |
| H31 | H43 | 8.105 | 1 |
NMR experiments
1: 1D 1H
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
2: 2D [1H,1H]-TOCSY
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
![Spectrum for experiment #2: 2D [1H,1H]-TOCSY](/ftp/pub/bmrb/metabolomics/entry_directories/bmse000270/nmr/set01/spectra/HH_TOCSY.png)
3: 1D 13C
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
4: 1D DEPT90
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
5: 1D DEPT135
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
6: 2D [1H,13C]-HSQC
Sample: 100mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.4
Spectrometer: Bruker DMX - 400MHz
![Spectrum for experiment #6: 2D [1H,13C]-HSQC](/ftp/pub/bmrb/metabolomics/entry_directories/bmse000270/nmr/set01/spectra/1H_13C_HSQC.png)