Guanosine (C10H13N5O5)
BMRB entry bmse000091
Entry DOI: doi:10.13018/BMSE000091
Data source: Madison Metabolomics Consortium - Francisca Jofre, Mark E. Anderson, John L. Markley, Melanie E. Ulrich
NMR-STAR file:
bmse000091.strNMR-STAR
interactive viewerStructure file (mol/sdf):
bmse000091.molAll files for
bmse000091Time Domain Data:
bmse000091.zipView the GISSMO record for this entry.
Sample and instrument details are given with the spectrum
Assigned chemical shifts
Set 1
Sample: multiple; see NMR-STAR file
Conditions: multiple; see NMR-STAR file
Spectrometer: multiple; see NMR-STAR file
| Atom ID | Author Nomenclature | Value | Ambiguity Code |
|---|---|---|---|
| C9 | C11 | 64.61 | 1 |
| C6 | C12 | 90.985 | 1 |
| C5 | C13 | 88.699 | 1 |
| C3 | C14 | 75.910 | 1 |
| C1 | C15 | 73.897 | 1 |
| C7 | C16 | 163.653 | 1 |
| C2 | C17 | 153.590 | 1 |
| C4 | C18 | 170.871 | 1 |
| C8 | C19 | 121.098 | 1 |
| C10 | C20 | 139.399 | 1 |
| H33 | H27 | 3.854 | 1 |
| H23 | H28 | 3.854 | 1 |
| H32 | H29 | 5.869 | 1 |
| H30 | H30 | 4.265 | 1 |
| H31 | H31 | 4.797 | 1 |
| H28 | H32 | 4.403 | 1 |
| H29 | H33 | 7.849 | 1 |
NMR experiments
1: 1D 1H, 0.5 mM
Sample: 0.5mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 7.69
Spectrometer: Bruker DMX - 500MHz
2: 1D 1H, 2.0 mM
Sample: 2.0mM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 10.70
Spectrometer: Bruker DMX - 500MHz
3: 1D 1H
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
4: 2D [1H,1H]-TOCSY
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
![Spectrum for experiment #4: 2D [1H,1H]-TOCSY](/ftp/pub/bmrb/metabolomics/entry_directories/bmse000091/nmr/set01/spectra/HH_TOCSY/00.png)
5: 1D 13C
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
6: 1D DEPT90
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
7: 1D DEPT135
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
8: 2D [1H,13C]-HSQC
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
![Spectrum for experiment #8: 2D [1H,13C]-HSQC](/ftp/pub/bmrb/metabolomics/entry_directories/bmse000091/nmr/set01/spectra/1H_13C_HSQC/00.png)
9: 2D [1H,13C]-HMBC
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
![Spectrum for experiment #9: 2D [1H,13C]-HMBC](/ftp/pub/bmrb/metabolomics/entry_directories/bmse000091/nmr/set01/spectra/1H_13C_HMBC/00.png)
10: 2D [1H,1H]-COSY
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 11.36
Spectrometer: Bruker DMX - 500MHz
![Spectrum for experiment #10: 2D [1H,1H]-COSY](/ftp/pub/bmrb/metabolomics/entry_directories/bmse000091/nmr/set01/spectra/HH_COSY/00.png)
11: 2D [1H,13C]-HSQC SW small
Sample: saturatedmM in D2O, ref: DSS
Conditions: temperature: 298K, pH: 10.5
Spectrometer: Bruker DMX - 400MHz
![Spectrum for experiment #11: 2D [1H,13C]-HSQC SW small](/ftp/pub/bmrb/metabolomics/entry_directories/bmse000091/nmr/set04/spectra/1H_13C_HSQC_SW_small/00.png)