# 1 "/opt/topspin/exp/stan/nmr/lists/pp/user/zg-wg3919-dec.eth" ;zg-wg3919-dec.eth ;1D sequence with watergate using 3-9-19 ;Denis Berger 14.3.2007 ;M. Piotto, V. Saudek & V. Sklenar, J. Biomol. NMR 2, 661 - 666 (1992) ;Use ZGOPTNS in AcquPars to define the flags. eg -DC13DEC or -DN15DEC ;ZGOPTNS: -DC13DEC ;13C decoupling ;ZGOPTNS: -DN15DEC ;15N decoupling ;ZGOPTNS: -DC13DEC -DN15DEC ;13C and 15N decoupling ;d1 : relaxation delay ;d5 : delay 3-9-19=1/(Hz between nulls) ;p1 : 90 degree hard pulse 1H ;pl1 : power level for hard 1H pulse p1 ;pl2 : not used (set=120) ;pl3 : not used (set=120) ;pcpd2 : 90 degree for 13C decoupling (~90us) ;pl12 : power level for 13C decoupling ;pcpd3 : 90 degree for 15N decoupling (~180us) ;pl13 : power level for 15N decoupling ;p21 : 1000u (Gradient before and after 3-9-19) ;gpz1 : 50% ;$OWNER=setup # 44 "/opt/topspin/exp/stan/nmr/lists/pp/user/zg-wg3919-dec.eth" # 1 "/opt/topspin/exp/stan/nmr/lists/pp/Avance.incl" 1 ;Avance3.incl ; for AV III ; ;avance-version (07/12/14) ; ;$CLASS=HighRes Incl ;$COMMENT= ;$Id: pulseprogram,v 1.1 2021/02/11 14:48:11 bmrbsvc Exp $ # 56 "/opt/topspin/exp/stan/nmr/lists/pp/user/zg-wg3919-dec.eth" 2 # 1 "mc_line 58 file /opt/topspin/exp/stan/nmr/lists/pp/user/zg-wg3919-dec.eth dc-measurement inserted automatically" dccorr # 58 "/opt/topspin/exp/stan/nmr/lists/pp/user/zg-wg3919-dec.eth" 1 ze 2 1m ;-------------------------------------------------------Relaxation Delay 10u do:f3 10u pl13:f3 10u setnmr3^0 d1 pl1:f1 10u setnmr3|0 ;-------------------------------------------------------Excitation (p1 ph1):f1 ;-------------------------------------------------------WG 3-9-19 10u ;mirrored delay of setnmr3^0 after 3919 10u p21:gp1 200u (p1*0.2308 ph3 d5 p1*0.6923 ph3 d5 p1*1.4615 ph3):f1 d5 (p1*1.4615 ph4 d5 p1*0.6923 ph4 d5 p1*0.2308 ph4):f1 10u p21:gp1 200u 10u setnmr3^0 ;preferably after acquisition (bruker problem) ;-------------------------------------------------------Acquisition go=2 ph0 cpd3:f3 10u do:f3 1m wr #0 10u setnmr3^0 exit ph1=0 2 ph0=0 2 2 0 ;receiver ph3=1 1 2 2 3 3 0 0 ;3-9-19 ph4=3 3 0 0 1 1 2 2 ;19-9-3 ;##/($P[1],$PL[1])= &SetPulse(f1,HP,90); ;##\$D[5]=round(1/(10*$BF1),.00001 ;##/($PCPD[2],$PL[12])=&SetPulse(f2,0.000090,90); ;##/($PCPD[3],$PL[13])=&SetPulse(f3,0.000180,90);