NMRbot_CID197204_NSC_284437_SampleReport.20180915_1428.txt Status Report for Automated Sample Data Collection ## Host = kerry.nmrfam.wisc.edu ## ## NMRbot version 20140226 ## ## Initiated - 20180915_1428 ## - info: CID197204_NSC_284437 in DMSO at position 202 foldername => CID197204_NSC_284437.DMSO.202.20180914 Exps => ZGCPPR,metabTOCSY,C13CPD_MMCD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND_MMCD,COSY45SW,HSQC_TOCSY_ADIA - instrument initialization - passed - loading sample position 202 - passed - DMSO solvent lock - passed - tuning probe channels - passed - topshim tuneb tunea - passed - creating exp 1 with ZGCPPR parameters - prosol parameters loaded - NS changed to 32 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 2 with metabTOCSY parameters - prosol parameters loaded - NS changed to 32 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 3 with C13CPD_MMCD parameters - prosol parameters loaded - NS changed to 4096 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 4 with C13DEPT90 parameters - prosol parameters loaded - NS changed to 1024 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 5 with C13DEPT135_MMCD parameters - prosol parameters loaded - NS changed to 1024 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 6 with HSQCETGP parameters - prosol parameters loaded - NS changed to 8 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 7 with HSQCETGP parameters - prosol parameters loaded - NS changed to 8 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 8 with HMBCETGPL3ND_MMCD parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 9 with COSY45SW parameters - prosol parameters loaded - NS changed to 32 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 10 with HSQC_TOCSY_ADIA parameters - prosol parameters loaded - NS changed to 32 - optimizing receiver gain - passed - receiver gain set to 203 - experiment folders set up - passed ## Data Acquisition ## # Exp 1 - ZGCPPR (zgcppr) - dims 1- F1 1H, SW 16.03 - start 20180915_1440 - end 20180915_1442 - passed - 1H adaptive offset determined = 4.7000 - 1H adaptive SW determined = 17.0285 # Exp 2 - metabTOCSY (mlevph) - dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21 - start 20180915_1443 - end 20180915_1956 - passed # Exp 3 - C13CPD_MMCD (zgpg30) - dims 1- F1 13C, SW 248.61 - start 20180915_1956 - end 20180915_2329 - passed # Exp 4 - C13DEPT90 (deptsp90) - dims 1- F1 13C, SW 236.77 - start 20180915_2329 - end 20180916_0023 - passed # Exp 5 - C13DEPT135_MMCD (deptsp135) - dims 1- F1 13C, SW 236.77 - start 20180916_0023 - end 20180916_0117 - passed - 13C adaptive offset determined = 108.9993 - 13C adaptive SW determined = 226.8241 # Exp 6 - HSQCETGP (hsqcetgp) - dims 2- F1 13C, SW 165.00; F2 1H, SW 12.99 - start 20180916_0117 - end 20180916_0212 - passed # Exp 7 - HSQCETGP (hsqcetgp) - SWadapted - F1 SW changed to 226.82 - F2 SW changed to 17.03 - F1 1H offset changed to 4.70 - F2 13C offset changed to 109.00 - dims 2- F1 13C, SW 226.82; F2 1H, SW 17.01 - start 20180916_0212 - end 20180916_0307 - passed # Exp 8 - HMBCETGPL3ND_MMCD (hmbcetgpl3nd) - dims 2- F1 13C, SW 240.00; F2 1H, SW 12.02 - start 20180916_0307 - end 20180916_0553 - passed # Exp 9 - COSY45SW (cosyqf45) - dims 2- F1 1H, SW 10.00; F2 1H, SW 10.00 - start 20180916_0553 - end 20180916_0825 - passed # Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2) - dims 2- F1 13C, SW 165.00; F2 1H, SW 16.03 - start 20180916_0825 - end 20180916_1329 - passed ## CID197204_NSC_284437 Experiment Set Ended - 20180916_1329 ##