NMRbot_cq_06266_SampleReport.20170217_2130.txt Status Report for Automated Sample Data Collection ## Host = kerry.nmrfam.wisc.edu ## ## NMRbot version 20140226 ## ## Initiated - 20170217_2130 ## - info: cq_06266 in CDCl3 at position 202 foldername => cq_06266.CDCl3.202.20170217 Exps => ZGCPPR,metabTOCSY,C13CPD_MMCD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND_MMCD,COSY45SW,HSQC_TOCSY_ADIA - instrument initialization - passed - loading sample position 202 - passed - CDCl3 solvent lock - passed - tuning probe channels - passed - topshim tuneb tunea - passed - creating exp 1 with ZGCPPR parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 114 - creating exp 2 with metabTOCSY parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 3 with C13CPD_MMCD parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 4 with C13DEPT90 parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 5 with C13DEPT135_MMCD parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 6 with HSQCETGP parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 7 with HSQCETGP parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 8 with HMBCETGPL3ND_MMCD parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 9 with COSY45SW parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 114 - creating exp 10 with HSQC_TOCSY_ADIA parameters - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - experiment folders set up - passed ## Data Acquisition ## # Exp 1 - ZGCPPR (zgcppr) - dims 1- F1 1H, SW 16.03 - start 20170217_2140 - end 20170217_2141 - passed - 1H adaptive offset determined = 4.7498 - 1H adaptive SW determined = 10.2995 # Exp 2 - metabTOCSY (mlevph) - dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21 - start 20170217_2141 - end 20170217_2300 - passed # Exp 3 - C13CPD_MMCD (zgpg30) - dims 1- F1 13C, SW 248.61 - start 20170217_2300 - end 20170217_2354 - passed # Exp 4 - C13DEPT90 (deptsp90) - dims 1- F1 13C, SW 236.77 - start 20170217_2354 - end 20170218_0008 - passed # Exp 5 - C13DEPT135_MMCD (deptsp135) - dims 1- F1 13C, SW 236.77 - start 20170218_0008 - end 20170218_0021 - passed - 13C adaptive offset determined = 70.4394 - 13C adaptive SW determined = 107.9349 # Exp 6 - HSQCETGP (hsqcetgp) - dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99 - start 20170218_0022 - end 20170218_0036 - passed # Exp 7 - HSQCETGP (hsqcetgp) - SWadapted - F1 SW changed to 107.93 - F2 SW changed to 10.30 - F1 1H offset changed to 4.75 - F2 13C offset changed to 70.44 - dims 2- F1 13C, SW 107.94; F2 1H, SW 10.31 - start 20170218_0036 - end 20170218_0050 - passed # Exp 8 - HMBCETGPL3ND_MMCD (hmbcetgpl3nd) - dims 2- F1 13C, SW 240.00; F2 1H, SW 12.02 - start 20170218_0050 - end 20170218_0132 - passed # Exp 9 - COSY45SW (cosyqf45) - dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31 - start 20170218_0132 - end 20170218_0211 - passed # Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2) - dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02 - start 20170218_0211 - end 20170218_0329 - passed ## cq_06266 Experiment Set Ended - 20170218_0329 ##