NMRbot_PC9301_SampleReport.20170128_2142.txt
Status Report for Automated Sample Data Collection
## Host = kerry.nmrfam.wisc.edu ##

## NMRbot version 20140226 ##

## Initiated - 20170128_2142 ##

- info:
  PC9301 in D2O at position 204
  foldername => PC9301.D2O.204.20170127
  Exps => ZGCPPR,metabTOCSY,C13CPD_MMCD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND_MMCD,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 204 - passed
- D2O solvent lock - passed
-   tuning probe channels - passed
-   topshim tuneb tunea - passed
-   determined 1H offset = 4.7029
- creating exp 1 with ZGCPPR parameters
-   prosol parameters loaded
-   1H offset changed to 4.7029
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 2 with metabTOCSY parameters
-   prosol parameters loaded
-   1H offset changed to 4.7029
-   1H offset changed to 4.7029
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 3 with C13CPD_MMCD parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 4 with C13DEPT90 parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 5 with C13DEPT135_MMCD parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 6 with HSQCETGP parameters
-   prosol parameters loaded
-   1H offset changed to 4.7029
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 7 with HSQCETGP parameters
-   prosol parameters loaded
-   1H offset changed to 4.7029
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 8 with HMBCETGPL3ND_MMCD parameters
-   prosol parameters loaded
-   1H offset changed to 4.7029
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 9 with COSY45SW parameters
-   prosol parameters loaded
-   1H offset changed to 4.7029
-   1H offset changed to 4.7029
-   optimizing receiver gain - passed
-   receiver gain set to 161
- creating exp 10 with HSQC_TOCSY_ADIA parameters
-   prosol parameters loaded
-   1H offset changed to 4.7029
-   optimizing receiver gain - passed
-   receiver gain set to 203
- experiment folders set up - passed
## Data Acquisition ##
# Exp 1 - ZGCPPR (zgcppr)
- dims 1- F1 1H, SW 16.03
- start 20170128_2157
- end   20170128_2158 - passed
-   1H adaptive offset determined = 4.7029
-   1H adaptive SW determined = 9.4514
# Exp 2 - metabTOCSY (mlevph)
- dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21
- start 20170128_2158
- end   20170128_2317 - passed
# Exp 3 - C13CPD_MMCD (zgpg30)
- dims 1- F1 13C, SW 248.61
- start 20170128_2317
- end   20170129_0010 - passed
# Exp 4 - C13DEPT90 (deptsp90)
- dims 1- F1 13C, SW 236.77
- start 20170129_0010
- end   20170129_0024 - passed
# Exp 5 - C13DEPT135_MMCD (deptsp135)
- dims 1- F1 13C, SW 236.77
- start 20170129_0024
- end   20170129_0038 - passed
-   13C adaptive offset determined = 80.3720
-   13C adaptive SW determined = 125.4739
# Exp 6 - HSQCETGP (hsqcetgp)
- dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99
- start 20170129_0038
- end   20170129_0052 - passed
# Exp 7 - HSQCETGP (hsqcetgp) - SWadapted
-   F1 SW changed to 125.47
-   F2 SW changed to 9.45
-   F1 1H offset changed to 4.70
-   F2 13C offset changed to 80.37
- dims 2- F1 13C, SW 125.47; F2 1H, SW 9.45
- start 20170129_0052
- end   20170129_0106 - passed
# Exp 8 - HMBCETGPL3ND_MMCD (hmbcetgpl3nd)
- dims 2- F1 13C, SW 240.00; F2 1H, SW 12.02
- start 20170129_0107
- end   20170129_0149 - passed
# Exp 9 - COSY45SW (cosyqf45)
- dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31
- start 20170129_0149
- end   20170129_0227 - passed
# Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02
- start 20170129_0227
- end   20170129_0345 - passed

## PC9301 Experiment Set Ended - 20170129_0345 ##