NMRbot_CID54683839_NSC307981_SampleReport.20180225_1304.txt
Status Report for Automated Sample Data Collection
## Host = kerry.nmrfam.wisc.edu ##

## NMRbot version 20140226 ##

## Initiated - 20180225_1304 ##

- info:
  CID54683839_NSC307981 in CDCl3 at position 203
  foldername => CID54683839_NSC307981.CDCl3.203.20180223
  Exps => ZGCPPR,metabTOCSY,C13CPD_MMCD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND_MMCD,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 203 - passed
- CDCl3 solvent lock - passed
-   tuning probe channels - passed
-   topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 2 with metabTOCSY parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 3 with C13CPD_MMCD parameters
-   prosol parameters loaded
-   NS changed to 4096
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 4 with C13DEPT90 parameters
-   prosol parameters loaded
-   NS changed to 1024
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 5 with C13DEPT135_MMCD parameters
-   prosol parameters loaded
-   NS changed to 1024
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 6 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 8
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 7 with HSQCETGP parameters
-   prosol parameters loaded
-   NS changed to 8
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 8 with HMBCETGPL3ND_MMCD parameters
-   prosol parameters loaded
-   NS changed to 16
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 9 with COSY45SW parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 10 with HSQC_TOCSY_ADIA parameters
-   prosol parameters loaded
-   NS changed to 32
-   optimizing receiver gain - passed
-   receiver gain set to 203
- experiment folders set up - passed
## Data Acquisition ##
# Exp 1 - ZGCPPR (zgcppr)
- dims 1- F1 1H, SW 16.03
- start 20180225_1315
- end   20180225_1318 - passed
-   1H adaptive offset determined = 4.7000
-   1H adaptive SW determined = 15.7486
# Exp 2 - metabTOCSY (mlevph)
- dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21
- start 20180225_1318
- end   20180225_1831 - passed
# Exp 3 - C13CPD_MMCD (zgpg30)
- dims 1- F1 13C, SW 248.61
- start 20180225_1832
- end   20180225_2204 - passed
# Exp 4 - C13DEPT90 (deptsp90)
- dims 1- F1 13C, SW 236.77
- start 20180225_2204
- end   20180225_2259 - passed
# Exp 5 - C13DEPT135_MMCD (deptsp135)
- dims 1- F1 13C, SW 236.77
- start 20180225_2259
- end   20180225_2353 - passed
-   13C adaptive offset determined = 73.3154
-   13C adaptive SW determined = 128.2546
# Exp 6 - HSQCETGP (hsqcetgp)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 12.99
- start 20180225_2353
- end   20180226_0048 - passed
# Exp 7 - HSQCETGP (hsqcetgp) - SWadapted
-   F1 SW changed to 128.25
-   F2 SW changed to 15.75
-   F1 1H offset changed to 4.70
-   F2 13C offset changed to 73.32
- dims 2- F1 13C, SW 128.25; F2 1H, SW 15.76
- start 20180226_0048
- end   20180226_0142 - passed
# Exp 8 - HMBCETGPL3ND_MMCD (hmbcetgpl3nd)
- dims 2- F1 13C, SW 240.00; F2 1H, SW 12.02
- start 20180226_0142
- end   20180226_0429 - passed
# Exp 9 - COSY45SW (cosyqf45)
- dims 2- F1 1H, SW 10.00; F2 1H, SW 10.00
- start 20180226_0429
- end   20180226_0701 - passed
# Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 16.03
- start 20180226_0701
- end   20180226_1205 - passed

## CID54683839_NSC307981 Experiment Set Ended - 20180226_1205 ##