NMRbot_cq_04332_SampleReport.20160507_0740.txt
Status Report for Automated Sample Data Collection
## Host = kerry.nmrfam.wisc.edu ##

## NMRbot version 20140226 ##

## Initiated - 20160507_0740 ##

- info:
  cq_04332 in CDCl3 at position 204
  foldername => cq_04332.CDCl3.204.20160506
  Exps => ZGCPPR,metabTOCSY,C13CPD_MMCD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND_MMCD,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 204 - passed
- CDCl3 solvent lock - passed
-   tuning probe channels - passed
-   topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 2 with metabTOCSY parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 3 with C13CPD_MMCD parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 4 with C13DEPT90 parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 5 with C13DEPT135_MMCD parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 6 with HSQCETGP parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 7 with HSQCETGP parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 8 with HMBCETGPL3ND_MMCD parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 9 with COSY45SW parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 10 with HSQC_TOCSY_ADIA parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- experiment folders set up - passed
## Data Acquisition ##
# Exp 1 - ZGCPPR (zgcppr)
- dims 1- F1 1H, SW 16.03
- start 20160507_0749
- end   20160507_0750 - passed
-   1H adaptive offset determined = 4.7498
-   1H adaptive SW determined = 14.3871
# Exp 2 - metabTOCSY (mlevph)
- dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21
- start 20160507_0750
- end   20160507_0909 - passed
# Exp 3 - C13CPD_MMCD (zgpg30)
- dims 1- F1 13C, SW 248.61
- start 20160507_0909
- end   20160507_1003 - passed
# Exp 4 - C13DEPT90 (deptsp90)
- dims 1- F1 13C, SW 236.77
- start 20160507_1003
- end   20160507_1016 - passed
# Exp 5 - C13DEPT135_MMCD (deptsp135)
- dims 1- F1 13C, SW 236.77
- start 20160507_1017
- end   20160507_1030 - passed
-   13C adaptive offset determined = 109.7410
-   13C adaptive SW determined = 196.6665
# Exp 6 - HSQCETGP (hsqcetgp)
- dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99
- start 20160507_1030
- end   20160507_1045 - passed
# Exp 7 - HSQCETGP (hsqcetgp) - SWadapted
-   F1 SW changed to 196.67
-   F2 SW changed to 14.39
-   F1 1H offset changed to 4.75
-   F2 13C offset changed to 109.74
- dims 2- F1 13C, SW 196.66; F2 1H, SW 14.37
- start 20160507_1045
- end   20160507_1059 - passed
# Exp 8 - HMBCETGPL3ND_MMCD (hmbcetgpl3nd)
- dims 2- F1 13C, SW 240.00; F2 1H, SW 12.02
- start 20160507_1059
- end   20160507_1141 - passed
# Exp 9 - COSY45SW (cosyqf45)
- dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31
- start 20160507_1141
- end   20160507_1219 - passed
# Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02
- start 20160507_1219
- end   20160507_1337 - passed

## cq_04332 Experiment Set Ended - 20160507_1337 ##