NMRbot_cq_17682_SampleReport.20131001_1405.txt Status Report for Automated Sample Data Collection ## Host = kerry.nmrfam.wisc.edu ## ## Initiated - 20131001_1405 ## - info: cq_17682 in D2O at position 201 foldername => cq_17682.D2O.201.20131001 Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA - instrument initialization - passed - loading sample position 201 - passed - sample solvent lock - passed - tuning probe channels - passed - topshim tuneb tunea - passed - determined 1H offset = 4.6989 - creating exp 1 with ZGCPPR parameters - passed - prosol parameters loaded - NS changed to 16 - 1H offset changed to 4.6989 - optimizing receiver gain - passed - receiver gain set to 36 - creating exp 2 with metabTOCSY parameters - passed - prosol parameters loaded - NS changed to 16 - 1H offset changed to 4.6989 - 1H offset changed to 4.6989 - optimizing receiver gain - passed - receiver gain set to 144 - creating exp 3 with C13CPD parameters - passed - prosol parameters loaded - NS changed to 2048 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 4 with C13DEPT90 parameters - passed - prosol parameters loaded - NS changed to 512 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 5 with C13DEPT135_MMCD parameters - passed - prosol parameters loaded - NS changed to 512 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 6 with HSQCETGP parameters - passed - prosol parameters loaded - NS changed to 4 - 1H offset changed to 4.6989 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 7 with HSQCETGP parameters - passed - prosol parameters loaded - NS changed to 4 - 1H offset changed to 4.6989 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 8 with HMBCETGPL3ND parameters - passed - prosol parameters loaded - NS changed to 8 - 1H offset changed to 4.6989 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 9 with COSY45SW parameters - passed - prosol parameters loaded - NS changed to 16 - 1H offset changed to 4.6989 - 1H offset changed to 4.6989 - optimizing receiver gain - passed - receiver gain set to 64 - creating exp 10 with HSQC_TOCSY_ADIA parameters - passed - prosol parameters loaded - NS changed to 16 - 1H offset changed to 4.6989 - optimizing receiver gain - passed - receiver gain set to 203 - experiment folders set up - passed ## Data Acquisition ## # Exp 1 - ZGCPPR (zgcppr) - dims 1- F1 1H, SW 16.0307 - start 20131001_1417 - end 20131001_1418 - passed - 1H adaptive offset determined = 4.6989 - 1H adaptive SW determined = 9.4882 # Exp 2 - metabTOCSY (mlevph) - dims 2- F1 1H, SW 10.2073; F2 1H, SW 10.2073 - start 20131001_1418 - end 20131001_1656 - passed # Exp 3 - C13CPD (zgpg30) - dims 1- F1 13C, SW 236.7742 - start 20131001_1656 - end 20131001_1844 - passed # Exp 4 - C13DEPT90 (dept90) - dims 1- F1 13C, SW 236.7742 - start 20131001_1844 - end 20131001_1911 - passed # Exp 5 - C13DEPT135_MMCD (deptsp135) - dims 1- F1 13C, SW 236.7742 - start 20131001_1911 - end 20131001_1938 - passed - 13C adaptive offset determined = 41.2382 - 13C adaptive SW determined = 62.7695 # Exp 6 - HSQCETGP (hsqcetgp) - dims 2- F1 13C, SW 165.6393; F2 1H, SW 13.3375 - start 20131001_1938 - end 20131001_2006 - passed # Exp 7 - HSQCETGP (hsqcetgp) - SWadapted - dims 2- F1 13C, SW 165.6393; F2 1H, SW 13.3375 - F1 SW changed to 62.7695 - F2 SW changed to 9.4882 - F1 1H offset changed to 4.6989 - F2 13C offset changed to 41.2382 - start 20131001_2006 - end 20131001_2035 - passed # Exp 8 - HMBCETGPL3ND (hmbcetgpl3nd) - dims 2- F1 13C, SW 221.8327; F2 1H, SW 12.0230 - start 20131001_2035 - end 20131001_2158 - passed # Exp 9 - COSY45SW (cosyqf45) - dims 2- F1 1H, SW 10.3125; F2 1H, SW 10.3125 - start 20131001_2158 - end 20131001_2314 - passed # Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2) - dims 2- F1 13C, SW 165.6580; F2 1H, SW 11.9655 - start 20131001_2314 - end 20131002_0149 - passed ## cq_17682 Experiment Set Ended - 20131002_0149 ##