NMRbot_cq_02338_SampleReport.20140208_0205.txt Status Report for Automated Sample Data Collection ## Host = kerry.nmrfam.wisc.edu ## ## NMRbot version 20140114 ## ## Initiated - 20140208_0205 ## - info: cq_02338 in CDCl3 at position 202 foldername => cq_02338.CDCl3.202.20140207 Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA - instrument initialization - passed - loading sample position 202 - passed - sample solvent lock - passed - tuning probe channels - passed - topshim tuneb tunea - passed - creating exp 1 with ZGCPPR parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 36 - creating exp 2 with metabTOCSY parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 144 - creating exp 3 with C13CPD parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 4 with C13DEPT90 parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 5 with C13DEPT135_MMCD parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 6 with HSQCETGP parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 7 with HSQCETGP parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 8 with HMBCETGPL3ND parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 9 with COSY45SW parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 50.8 - creating exp 10 with HSQC_TOCSY_ADIA parameters - passed - prosol parameters loaded - optimizing receiver gain - passed - receiver gain set to 203 - experiment folders set up - passed ## Data Acquisition ## # Exp 1 - ZGCPPR (zgcppr) - dims 1- F1 1H, SW 16.0307 - start 20140208_0215 - end 20140208_0216 - passed - 1H adaptive offset determined = 4.7498 - 1H adaptive SW determined = 10.2313 # Exp 2 - metabTOCSY (mlevph) - dims 2- F1 1H, SW 10.2073; F2 1H, SW 10.2073 - start 20140208_0216 - end 20140208_0335 - passed # Exp 3 - C13CPD (zgpg30) - dims 1- F1 13C, SW 236.7742 - start 20140208_0335 - end 20140208_0429 - passed # Exp 4 - C13DEPT90 (dept90) - dims 1- F1 13C, SW 236.7742 - start 20140208_0429 - end 20140208_0443 - passed # Exp 5 - C13DEPT135_MMCD (deptsp135) - dims 1- F1 13C, SW 236.7742 - start 20140208_0443 - end 20140208_0457 - passed - 13C adaptive offset determined = 76.1962 - 13C adaptive SW determined = 147.6437 # Exp 6 - HSQCETGP (hsqcetgp) - dims 2- F1 13C, SW 165.6393; F2 1H, SW 13.3375 - start 20140208_0457 - end 20140208_0511 - passed # Exp 7 - HSQCETGP (hsqcetgp) - SWadapted - dims 2- F1 13C, SW 165.6393; F2 1H, SW 13.3375 - F1 SW changed to 147.6437 - F2 SW changed to 10.2313 - F1 1H offset changed to 4.7498 - F2 13C offset changed to 76.1962 - start 20140208_0511 - end 20140208_0525 - passed # Exp 8 - HMBCETGPL3ND (hmbcetgpl3nd) - dims 2- F1 13C, SW 221.8327; F2 1H, SW 12.0230 - start 20140208_0525 - end 20140208_0607 - passed # Exp 9 - COSY45SW (cosyqf45) - dims 2- F1 1H, SW 10.3125; F2 1H, SW 10.3125 - start 20140208_0607 - end 20140208_0646 - passed # Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2) - dims 2- F1 13C, SW 165.6580; F2 1H, SW 11.9655 - start 20140208_0646 - end 20140208_0804 - passed ## cq_02338 Experiment Set Ended - 20140208_0804 ##