NMRbot_Avanti_870285_SampleReport.20140517_0243.txt Status Report for Automated Sample Data Collection ## Host = kerry.nmrfam.wisc.edu ## ## NMRbot version 20140226 ## ## Initiated - 20140517_0243 ## - info: Avanti_870285 in MMCD_mixed at position 202 foldername => Avanti_870285.MMCD_mixed.202.20140516 Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA - instrument initialization - passed - loading sample position 202 - passed - MMCD_mixed solvent lock - passed - tuning probe channels - passed - topshim tuneb tunea - passed - creating exp 1 with ZGCPPR parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 36 - creating exp 2 with metabTOCSY parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 64 - creating exp 3 with C13CPD parameters - prosol parameters loaded - NS changed to 2048 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 4 with C13DEPT90 parameters - prosol parameters loaded - NS changed to 512 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 5 with C13DEPT135_MMCD parameters - prosol parameters loaded - NS changed to 512 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 6 with HSQCETGP parameters - prosol parameters loaded - NS changed to 4 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 7 with HSQCETGP parameters - prosol parameters loaded - NS changed to 4 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 8 with HMBCETGPL3ND parameters - prosol parameters loaded - NS changed to 8 - optimizing receiver gain - passed - receiver gain set to 203 - creating exp 9 with COSY45SW parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 45.2 - creating exp 10 with HSQC_TOCSY_ADIA parameters - prosol parameters loaded - NS changed to 16 - optimizing receiver gain - passed - receiver gain set to 203 - experiment folders set up - passed ## Data Acquisition ## # Exp 1 - ZGCPPR (zgcppr) - dims 1- F1 1H, SW 16.03 - start 20140517_0254 - end 20140517_0255 - passed - 1H adaptive offset determined = 4.7498 - 1H adaptive SW determined = 8.7979 # Exp 2 - metabTOCSY (mlevph) - dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21 - start 20140517_0255 - end 20140517_0532 - passed # Exp 3 - C13CPD (zgpg30) - dims 1- F1 13C, SW 236.77 - start 20140517_0532 - end 20140517_0721 - passed # Exp 4 - C13DEPT90 (deptsp90) - dims 1- F1 13C, SW 236.77 - start 20140517_0721 - end 20140517_0748 - passed # Exp 5 - C13DEPT135_MMCD (deptsp135) - dims 1- F1 13C, SW 236.77 - start 20140517_0748 - end 20140517_0815 - passed - 13C adaptive offset determined = 94.2014 - 13C adaptive SW determined = 170.7915 # Exp 6 - HSQCETGP (hsqcetgp) - dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99 - start 20140517_0815 - end 20140517_0843 - passed # Exp 7 - HSQCETGP (hsqcetgp) - SWadapted - F1 SW changed to 170.79 - F2 SW changed to 8.80 - F1 1H offset changed to 4.75 - F2 13C offset changed to 94.20 - dims 2- F1 13C, SW 170.79; F2 1H, SW 8.81 - start 20140517_0843 - end 20140517_0911 - passed # Exp 8 - HMBCETGPL3ND (hmbcetgpl3nd) - dims 2- F1 13C, SW 221.83; F2 1H, SW 12.02 - start 20140517_0911 - end 20140517_1035 - passed # Exp 9 - COSY45SW (cosyqf45) - dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31 - start 20140517_1035 - end 20140517_1151 - passed # Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2) - dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02 - start 20140517_1151 - end 20140517_1426 - passed ## Avanti_870285 Experiment Set Ended - 20140517_1426 ##