NMRbot_cq_03424_SampleReport.20130527_0919.txt
Status Report for Automated Sample Data Collection
# Host = kerry.nmrfam.wisc.edu

# Initiated - 20130527_0919

- info:
cq_03424.CDCl3.201.20130527 = cq_03424 in CDCl3 at position 201
   Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 201 - passed
- sample solvent lock - passed
- tuning probe channels - passed
- topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters - passed
- prosol parameters loaded
- NS changed to 16
- creating exp 2 with metabTOCSY parameters - passed
- prosol parameters loaded
- NS changed to 16
- creating exp 3 with C13CPD parameters - passed
- prosol parameters loaded
- NS changed to 2048
- creating exp 4 with C13DEPT90 parameters - passed
- prosol parameters loaded
- NS changed to 512
- creating exp 5 with C13DEPT135_MMCD parameters - passed
- prosol parameters loaded
- NS changed to 512
- creating exp 6 with HSQCETGP parameters - passed
- prosol parameters loaded
- NS changed to 4
- creating exp 7 with HSQCETGP parameters - passed
- prosol parameters loaded
- NS changed to 4
- creating exp 8 with HMBCETGPL3ND parameters - passed
- prosol parameters loaded
- NS changed to 8
- creating exp 9 with COSY45SW parameters - passed
- prosol parameters loaded
- NS changed to 16
- creating exp 10 with HSQC_TOCSY_ADIA parameters - passed
- prosol parameters loaded
- NS changed to 16
- experiment folders set up - passed
# Exp 1 started - 20130527_0926
- ZGCPPR (zgcppr)
- optimizing receiver gain - passed
- receiver gain set to 32
# Exp 1 ended - 20130527_0927 - passed
- 1H adaptive offset determined = 4.7498
- 1H adaptive SW determined = 10.2331
# Exp 2 started - 20130527_0928
- metabTOCSY (mlevph)
- optimizing receiver gain - passed
- receiver gain set to 114
# Exp 2 ended - 20130527_1205 - passed
# Exp 3 started - 20130527_1205
- C13CPD (zgpg30)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 3 ended - 20130527_1353 - passed
# Exp 4 started - 20130527_1353
- C13DEPT90 (dept90)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 4 ended - 20130527_1421 - passed
# Exp 5 started - 20130527_1421
- C13DEPT135_MMCD (deptsp135)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 5 ended - 20130527_1448 - passed
- 13C adaptive offset determined = 77.1679
- 13C adaptive SW determined = 133.0536
# Exp 6 started - 20130527_1448
- HSQCETGP (hsqcetgp)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 6 ended - 20130527_1516 - passed
# Exp 7 started - 20130527_1516
- HSQCETGP (hsqcetgp)
- 1 SW changed to 133.0536
- 2 SW changed to 10.2331
- 1H offset changed to 4.7498
- 13C offset changed to 77.1679
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 7 ended - 20130527_1544 - passed
# Exp 8 started - 20130527_1544
- HMBCETGPL3ND (hmbcetgpl3nd)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 8 ended - 20130527_1708 - passed
# Exp 9 started - 20130527_1708
- COSY45SW (cosyqf45)
- optimizing receiver gain - passed
- receiver gain set to 50.8
# Exp 9 ended - 20130527_1824 - passed
# Exp 10 started - 20130527_1824
- HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 10 ended - 20130527_2100 - passed

# cq_03424 Experiment Set Ended - 20130527_2100