NMRbot_cq_pentyl_benzoate_SampleReport.20141206_0521.txt
Status Report for Automated Sample Data Collection
## Host = kerry.nmrfam.wisc.edu ##

## NMRbot version 20140226 ##

## Initiated - 20141206_0521 ##

- info:
  cq_pentyl_benzoate in MeOD at position 203
  foldername => cq_pentyl_benzoate.MeOD.203.20141205
  Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 203 - passed
- MeOD solvent lock - passed
-   tuning probe channels - passed
-   topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 90.5
- creating exp 2 with metabTOCSY parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 181
- creating exp 3 with C13CPD parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 4 with C13DEPT90 parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 5 with C13DEPT135 parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 6 with HSQCETGP parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 7 with HSQCETGP parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 8 with HMBCETGPL3ND parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- creating exp 9 with COSY45SW parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 161
- creating exp 10 with HSQC_TOCSY_ADIA parameters
-   prosol parameters loaded
-   optimizing receiver gain - passed
-   receiver gain set to 203
- experiment folders set up - passed
## Data Acquisition ##
# Exp 1 - ZGCPPR (zgcppr)
- dims 1- F1 1H, SW 16.03
- start 20141206_0532
- end   20141206_0533 - passed
-   1H adaptive offset determined = 4.7498
-   1H adaptive SW determined = 10.2419
# Exp 2 - metabTOCSY (mlevph)
- dims 2- F1 1H, SW 10.21; F2 1H, SW 10.21
- start 20141206_0533
- end   20141206_0652 - passed
# Exp 3 - C13CPD (zgpg30)
- dims 1- F1 13C, SW 236.77
- start 20141206_0652
- end   20141206_0747 - passed
# Exp 4 - C13DEPT90 (deptsp90)
- dims 1- F1 13C, SW 236.77
- start 20141206_0747
- end   20141206_0800 - passed
# Exp 5 - C13DEPT135 (deptsp135)
- dims 1- F1 13C, SW 160.40
- start 20141206_0800
- end   20141206_0816 - passed
-   13C adaptive offset determined = 70.5682
-   13C adaptive SW determined = 142.6401
# Exp 6 - HSQCETGP (hsqcetgp)
- dims 2- F1 13C, SW 165.64; F2 1H, SW 12.99
- start 20141206_0816
- end   20141206_0831 - passed
# Exp 7 - HSQCETGP (hsqcetgp) - SWadapted
-   F1 SW changed to 142.64
-   F2 SW changed to 10.24
-   F1 1H offset changed to 4.75
-   F2 13C offset changed to 70.57
- dims 2- F1 13C, SW 142.64; F2 1H, SW 10.25
- start 20141206_0831
- end   20141206_0845 - passed
# Exp 8 - HMBCETGPL3ND (hmbcetgpl3nd)
- dims 2- F1 13C, SW 221.83; F2 1H, SW 12.02
- start 20141206_0845
- end   20141206_0927 - passed
# Exp 9 - COSY45SW (cosyqf45)
- dims 2- F1 1H, SW 10.31; F2 1H, SW 10.31
- start 20141206_0927
- end   20141206_1005 - passed
# Exp 10 - HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- dims 2- F1 13C, SW 165.00; F2 1H, SW 12.02
- start 20141206_1005
- end   20141206_1124 - passed

## cq_pentyl_benzoate Experiment Set Ended - 20141206_1124 ##