NMRbot_cq_20061_SampleReport.20130528_1126.txt
Status Report for Automated Sample Data Collection
# Host = kerry.nmrfam.wisc.edu

# Initiated - 20130528_1126

- info:
cq_20061.CDCl3.203.20130528 = cq_20061 in CDCl3 at position 203
   Exps => ZGCPPR,metabTOCSY,C13CPD,C13DEPT90,C13DEPT135_MMCD,HSQCETGP,HSQCETGP,HMBCETGPL3ND,COSY45SW,HSQC_TOCSY_ADIA
- instrument initialization - passed
- loading sample position 203 - passed
- sample solvent lock - passed
- tuning probe channels - passed
- topshim tuneb tunea - passed
- creating exp 1 with ZGCPPR parameters - passed
- prosol parameters loaded
- NS changed to 40
- creating exp 2 with metabTOCSY parameters - passed
- prosol parameters loaded
- NS changed to 40
- creating exp 3 with C13CPD parameters - passed
- prosol parameters loaded
- NS changed to 5120
- creating exp 4 with C13DEPT90 parameters - passed
- prosol parameters loaded
- NS changed to 1280
- creating exp 5 with C13DEPT135_MMCD parameters - passed
- prosol parameters loaded
- NS changed to 1280
- creating exp 6 with HSQCETGP parameters - passed
- prosol parameters loaded
- NS changed to 10
- creating exp 7 with HSQCETGP parameters - passed
- prosol parameters loaded
- NS changed to 10
- creating exp 8 with HMBCETGPL3ND parameters - passed
- prosol parameters loaded
- NS changed to 20
- creating exp 9 with COSY45SW parameters - passed
- prosol parameters loaded
- NS changed to 40
- creating exp 10 with HSQC_TOCSY_ADIA parameters - passed
- prosol parameters loaded
- NS changed to 40
- experiment folders set up - passed
# Exp 1 started - 20130528_1133
- ZGCPPR (zgcppr)
- optimizing receiver gain - passed
- receiver gain set to 36
# Exp 1 ended - 20130528_1136 - passed
- 1H adaptive offset determined = 4.7498
- 1H adaptive SW determined = 12.3027
# Exp 2 started - 20130528_1136
- metabTOCSY (mlevph)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 2 ended - 20130528_1808 - passed
# Exp 3 started - 20130528_1808
- C13CPD (zgpg30)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 3 ended - 20130528_2239 - passed
# Exp 4 started - 20130528_2239
- C13DEPT90 (dept90)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 4 ended - 20130528_2346 - passed
# Exp 5 started - 20130528_2346
- C13DEPT135_MMCD (deptsp135)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 5 ended - 20130529_0054 - passed
- 13C adaptive offset determined = 103.1723
- 13C adaptive SW determined = 199.6440
# Exp 6 started - 20130529_0054
- HSQCETGP (hsqcetgp)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 6 ended - 20130529_0202 - passed
# Exp 7 started - 20130529_0202
- HSQCETGP (hsqcetgp)
- 1 SW changed to 199.6440
- 2 SW changed to 12.3027
- 1H offset changed to 4.7498
- 13C offset changed to 103.1723
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 7 ended - 20130529_0311 - passed
# Exp 8 started - 20130529_0311
- HMBCETGPL3ND (hmbcetgpl3nd)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 8 ended - 20130529_0639 - passed
# Exp 9 started - 20130529_0639
- COSY45SW (cosyqf45)
- optimizing receiver gain - passed
- receiver gain set to 71.8
# Exp 9 ended - 20130529_0949 - passed
# Exp 10 started - 20130529_0949
- HSQC_TOCSY_ADIA (hsqcdietgpsisp.2)
- optimizing receiver gain - passed
- receiver gain set to 203
# Exp 10 ended - 20130529_1615 - passed

# cq_20061 Experiment Set Ended - 20130529_1615