Temperature: 298K; p1:13.28 ;# 90 degree 1H hard pulse SR:-40.38 ;# Chemical shift reference (DSS) SWH:3.5:9.5 ;# 1H SW SWC_ALL:0:220 ;# 13C SW (ALL) SWC_H:50:165 ;# 13C SW (only 13C with 1H attached) S/N:weak Processing log: EXPNO=1 1D-1H DONE! ******************************* Peak_list: cq_00005_1.list Spectrum_figure: cq_00005_1.pdf Parameters: sr=-40.380001 ; f1p=9.600917 ; f2p=3.600917 EXPNO=2 2D-[1H,1H]-TOCSY DONE! ******************************* Peak_list: cq_00005_2.list Spectrum_figure: cq_00005_2.pdf spectrum: cq_00005_2.ft2 Parameters: sr=-40.380001 ; f1_low=9.600917 ; f1_high=3.761358 ; f2_low=9.600917 ; f2_high=3.868092 EXPNO=3 1D-13C DONE! ******************************* Peak_list: cq_00005_3.list Spectrum_figure: cq_00005_3.pdf Parameters: sr=-238.714632 ; f1p=222.372604 ; f2p=2.372609 EXPNO=5 1D-13C-DEPT135 DONE! ******************************* Peak_list: cq_00005_5.list Spectrum_figure: cq_00005_5.pdf Parameters: sr=-238.714632 ; f1p=167.372604 ; f2p=52.372608 EXPNO=4 1D-13C-DEPT90 DONE! ******************************* Peak_list: cq_00005_4.list Spectrum_figure: cq_00005_4.pdf Parameters: sr=-238.714632 ; f1p=167.372604 ; f2p=52.372608 EXPNO=6 2D-[1H,13C]-HSQCSE DONE! ******************************* Peak_list: cq_00005_6.list Spectrum_figure: cq_00005_6.pdf spectrum: cq_00005_6.ft2 Parameters: sr=-40.380001 ; csr=-238.714632, f1_low=9.600917 ; f1_high=3.651013 ; f2_low=162.500687 ; f2_high=59.962410