data_6525 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 6525 _Entry.Title ; Backbone 1H Chemical Shift Assignments for Mungbean Defensin, VrD1 ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2005-02-28 _Entry.Accession_date 2005-02-28 _Entry.Last_release_date 2005-02-28 _Entry.Original_release_date 2005-02-28 _Entry.Origination author _Entry.NMR_STAR_version 3.1.2.6 _Entry.Original_NMR_STAR_version 3.1.2.6 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Yaw-Jen Liu . . . . 6525 2 Ping-Chiang Lyu . . . . 6525 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 6525 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '1H chemical shifts' 281 6525 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2007-11-09 2005-02-28 update BMRB 'complete entry citation' 6525 1 . . 2006-04-24 2005-02-28 original author 'original release' 6525 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 6525 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 16544327 _Citation.Full_citation . _Citation.Title ; Solution structure of the plant defensin VrD1 from mung bean and its possible role in insecticidal activity against bruchids ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev Proteins _Citation.Journal_name_full . _Citation.Journal_volume 63 _Citation.Journal_issue 4 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 777 _Citation.Page_last 786 _Citation.Year 2006 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Yaw-Jen Liu . . . . 6525 1 2 Chao-Sheng Cheng . . . . 6525 1 3 Szu-Ming Lai . . . . 6525 1 4 Ming-Pin Hsu . . . . 6525 1 5 Ching-San Chen . . . . 6525 1 6 Ping-Chiang Lyu . . . . 6525 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 6525 _Assembly.ID 1 _Assembly.Name 'Mungbean Defensin, VrD1' _Assembly.BMRB_code . _Assembly.Number_of_components 0 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites no _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state 'all disulfide bound' _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 'Mungbean Defensin, VrD1' 1 $Mungbean_defensin_VrD1 . . no native no no . . . 6525 1 stop_ loop_ _Assembly_bio_function.Biological_function _Assembly_bio_function.Entry_ID _Assembly_bio_function.Assembly_ID 'antifungal and insecticidal activities' 6525 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_Mungbean_defensin_VrD1 _Entity.Sf_category entity _Entity.Sf_framecode Mungbean_defensin_VrD1 _Entity.Entry_ID 6525 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name 'Mungbean defensin, VrD1' _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; RTCMIKKEGWGKCLIDTTCA HSCKNRGYIGGNCKGMTRTC YCLVNC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 46 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'all disulfide bound' _Entity.Src_method . _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . ARG . 6525 1 2 . THR . 6525 1 3 . CYS . 6525 1 4 . MET . 6525 1 5 . ILE . 6525 1 6 . LYS . 6525 1 7 . LYS . 6525 1 8 . GLU . 6525 1 9 . GLY . 6525 1 10 . TRP . 6525 1 11 . GLY . 6525 1 12 . LYS . 6525 1 13 . CYS . 6525 1 14 . LEU . 6525 1 15 . ILE . 6525 1 16 . ASP . 6525 1 17 . THR . 6525 1 18 . THR . 6525 1 19 . CYS . 6525 1 20 . ALA . 6525 1 21 . HIS . 6525 1 22 . SER . 6525 1 23 . CYS . 6525 1 24 . LYS . 6525 1 25 . ASN . 6525 1 26 . ARG . 6525 1 27 . GLY . 6525 1 28 . TYR . 6525 1 29 . ILE . 6525 1 30 . GLY . 6525 1 31 . GLY . 6525 1 32 . ASN . 6525 1 33 . CYS . 6525 1 34 . LYS . 6525 1 35 . GLY . 6525 1 36 . MET . 6525 1 37 . THR . 6525 1 38 . ARG . 6525 1 39 . THR . 6525 1 40 . CYS . 6525 1 41 . TYR . 6525 1 42 . CYS . 6525 1 43 . LEU . 6525 1 44 . VAL . 6525 1 45 . ASN . 6525 1 46 . CYS . 6525 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . ARG 1 1 6525 1 . THR 2 2 6525 1 . CYS 3 3 6525 1 . MET 4 4 6525 1 . ILE 5 5 6525 1 . LYS 6 6 6525 1 . LYS 7 7 6525 1 . GLU 8 8 6525 1 . GLY 9 9 6525 1 . TRP 10 10 6525 1 . GLY 11 11 6525 1 . LYS 12 12 6525 1 . CYS 13 13 6525 1 . LEU 14 14 6525 1 . ILE 15 15 6525 1 . ASP 16 16 6525 1 . THR 17 17 6525 1 . THR 18 18 6525 1 . CYS 19 19 6525 1 . ALA 20 20 6525 1 . HIS 21 21 6525 1 . SER 22 22 6525 1 . CYS 23 23 6525 1 . LYS 24 24 6525 1 . ASN 25 25 6525 1 . ARG 26 26 6525 1 . GLY 27 27 6525 1 . TYR 28 28 6525 1 . ILE 29 29 6525 1 . GLY 30 30 6525 1 . GLY 31 31 6525 1 . ASN 32 32 6525 1 . CYS 33 33 6525 1 . LYS 34 34 6525 1 . GLY 35 35 6525 1 . MET 36 36 6525 1 . THR 37 37 6525 1 . ARG 38 38 6525 1 . THR 39 39 6525 1 . CYS 40 40 6525 1 . TYR 41 41 6525 1 . CYS 42 42 6525 1 . LEU 43 43 6525 1 . VAL 44 44 6525 1 . ASN 45 45 6525 1 . CYS 46 46 6525 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 6525 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $Mungbean_defensin_VrD1 . 157791 . no . 'Mung bean' . . Eukaryota Viridiplantae Vigna radiata . . . . . . . . . . . . . 6525 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 6525 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $Mungbean_defensin_VrD1 . 'Purified from the natural source' . . . . . . . . . . . . . . . . 6525 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 6525 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system . _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'Mungbean Defensin, VrD1' . . . 1 $Mungbean_defensin_VrD1 . . 2.0 . . mM . . . . 6525 1 stop_ save_ ####################### # Sample conditions # ####################### save_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode conditions_1 _Sample_condition_list.Entry_ID 6525 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.0 0.2 pH 6525 1 temperature 288 1 K 6525 1 stop_ save_ ############################ # Computer software used # ############################ save_Xwin-nmr _Software.Sf_category software _Software.Sf_framecode Xwin-nmr _Software.Entry_ID 6525 _Software.ID 1 _Software.Name Xwin-nmr _Software.Version 2.1 _Software.Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_600MHz_spectrometer _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode 600MHz_spectrometer _NMR_spectrometer.Entry_ID 6525 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ ############################# # NMR applied experiments # ############################# save_NMR_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode NMR_experiment_list _Experiment_list.Entry_ID 6525 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 DQF-COSY no . . . . . . . . . . 1 $sample_1 . . . 1 $conditions_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 6525 1 2 TOCSY no . . . . . . . . . . 1 $sample_1 . . . 1 $conditions_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 6525 1 3 NOESY no . . . . . . . . . . 1 $sample_1 . . . 1 $conditions_1 . . . 1 $600MHz_spectrometer . . . . . . . . . . . . . . . . 6525 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_referencing _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_referencing _Chem_shift_reference.Entry_ID 6525 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 DSS 'methyl protons' . . . . ppm 0.0 internal direct 1.0 . . . . . 6525 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_Mungbean_Defensin_VrD1_shift _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode Mungbean_Defensin_VrD1_shift _Assigned_chem_shift_list.Entry_ID 6525 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_referencing _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 DQF-COSY 1 $sample_1 anisotropic 6525 1 2 TOCSY 1 $sample_1 anisotropic 6525 1 3 NOESY 1 $sample_1 anisotropic 6525 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 ARG HA H 1 4.618 0.004 . 1 . . . . 1 ARG HA . 6525 1 2 . 1 1 1 1 ARG HB2 H 1 1.966 0.004 . 1 . . . . 1 ARG HB2 . 6525 1 3 . 1 1 1 1 ARG HB3 H 1 2.036 0.004 . 1 . . . . 1 ARG HB3 . 6525 1 4 . 1 1 1 1 ARG HG2 H 1 1.754 0.004 . 1 . . . . 1 ARG HG2 . 6525 1 5 . 1 1 1 1 ARG HG3 H 1 1.715 0.004 . 1 . . . . 1 ARG HG3 . 6525 1 6 . 1 1 1 1 ARG HD2 H 1 3.243 0.004 . 1 . . . . 1 ARG HD2 . 6525 1 7 . 1 1 1 1 ARG HD3 H 1 3.243 0.004 . 1 . . . . 1 ARG HD3 . 6525 1 8 . 1 1 1 1 ARG HE H 1 7.19 0.004 . 1 . . . . 1 ARG HE . 6525 1 9 . 1 1 2 2 THR H H 1 8.717 0.004 . 1 . . . . 2 THR H . 6525 1 10 . 1 1 2 2 THR HA H 1 5.202 0.004 . 1 . . . . 2 THR HA . 6525 1 11 . 1 1 2 2 THR HB H 1 4.043 0.004 . 1 . . . . 2 THR HB . 6525 1 12 . 1 1 2 2 THR HG21 H 1 1.167 0.004 . 1 . . . . 2 THR HG2 . 6525 1 13 . 1 1 2 2 THR HG22 H 1 1.167 0.004 . 1 . . . . 2 THR HG2 . 6525 1 14 . 1 1 2 2 THR HG23 H 1 1.167 0.004 . 1 . . . . 2 THR HG2 . 6525 1 15 . 1 1 3 3 CYS H H 1 9.311 0.004 . 1 . . . . 3 CYS H . 6525 1 16 . 1 1 3 3 CYS HA H 1 5.045 0.004 . 1 . . . . 3 CYS HA . 6525 1 17 . 1 1 3 3 CYS HB2 H 1 2.882 0.004 . 1 . . . . 3 CYS HB2 . 6525 1 18 . 1 1 3 3 CYS HB3 H 1 2.793 0.004 . 1 . . . . 3 CYS HB3 . 6525 1 19 . 1 1 4 4 MET H H 1 8.629 0.004 . 1 . . . . 4 MET H . 6525 1 20 . 1 1 4 4 MET HA H 1 5.404 0.004 . 1 . . . . 4 MET HA . 6525 1 21 . 1 1 4 4 MET HB2 H 1 2.006 0.004 . 1 . . . . 4 MET HB2 . 6525 1 22 . 1 1 4 4 MET HB3 H 1 1.863 0.004 . 1 . . . . 4 MET HB3 . 6525 1 23 . 1 1 4 4 MET HG2 H 1 2.332 0.004 . 1 . . . . 4 MET HG2 . 6525 1 24 . 1 1 4 4 MET HG3 H 1 2.496 0.004 . 1 . . . . 4 MET HG3 . 6525 1 25 . 1 1 5 5 ILE H H 1 9.463 0.004 . 1 . . . . 5 ILE H . 6525 1 26 . 1 1 5 5 ILE HA H 1 4.408 0.004 . 1 . . . . 5 ILE HA . 6525 1 27 . 1 1 5 5 ILE HB H 1 1.497 0.004 . 1 . . . . 5 ILE HB . 6525 1 28 . 1 1 5 5 ILE HG12 H 1 1.283 0.004 . 1 . . . . 5 ILE HG12 . 6525 1 29 . 1 1 5 5 ILE HG13 H 1 1.115 0.004 . 1 . . . . 5 ILE HG13 . 6525 1 30 . 1 1 5 5 ILE HG21 H 1 0.6843 0.004 . 1 . . . . 5 ILE HG2 . 6525 1 31 . 1 1 5 5 ILE HG22 H 1 0.6843 0.004 . 1 . . . . 5 ILE HG2 . 6525 1 32 . 1 1 5 5 ILE HG23 H 1 0.6843 0.004 . 1 . . . . 5 ILE HG2 . 6525 1 33 . 1 1 6 6 LYS H H 1 8.559 0.004 . 1 . . . . 6 LYS H . 6525 1 34 . 1 1 6 6 LYS HA H 1 2.832 0.004 . 1 . . . . 6 LYS HA . 6525 1 35 . 1 1 6 6 LYS HB2 H 1 1.54 0.004 . 1 . . . . 6 LYS HB2 . 6525 1 36 . 1 1 6 6 LYS HB3 H 1 1.293 0.004 . 1 . . . . 6 LYS HB3 . 6525 1 37 . 1 1 6 6 LYS HG2 H 1 0.5723 0.004 . 4 . . . . 6 LYS HG2 . 6525 1 38 . 1 1 6 6 LYS HG3 H 1 0.5723 0.004 . 4 . . . . 6 LYS HG3 . 6525 1 39 . 1 1 6 6 LYS HD2 H 1 0.9424 0.004 . 4 . . . . 6 LYS HD2 . 6525 1 40 . 1 1 6 6 LYS HD3 H 1 0.9424 0.004 . 4 . . . . 6 LYS HD3 . 6525 1 41 . 1 1 7 7 LYS H H 1 8.007 0.004 . 1 . . . . 7 LYS H . 6525 1 42 . 1 1 7 7 LYS HA H 1 4.324 0.004 . 1 . . . . 7 LYS HA . 6525 1 43 . 1 1 7 7 LYS HB2 H 1 0.8981 0.004 . 1 . . . . 7 LYS HB2 . 6525 1 44 . 1 1 7 7 LYS HB3 H 1 0.8981 0.004 . 1 . . . . 7 LYS HB3 . 6525 1 45 . 1 1 7 7 LYS HG2 H 1 -0.1806 0.004 . 4 . . . . 7 LYS HG2 . 6525 1 46 . 1 1 7 7 LYS HG3 H 1 -0.1806 0.004 . 4 . . . . 7 LYS HG3 . 6525 1 47 . 1 1 7 7 LYS HD2 H 1 0.515 0.004 . 4 . . . . 7 LYS HD2 . 6525 1 48 . 1 1 7 7 LYS HD3 H 1 0.515 0.004 . 4 . . . . 7 LYS HD3 . 6525 1 49 . 1 1 8 8 GLU H H 1 8.72 0.004 . 1 . . . . 8 GLU H . 6525 1 50 . 1 1 8 8 GLU HA H 1 4.006 0.004 . 1 . . . . 8 GLU HA . 6525 1 51 . 1 1 8 8 GLU HB2 H 1 1.922 0.004 . 1 . . . . 8 GLU HB2 . 6525 1 52 . 1 1 8 8 GLU HB3 H 1 1.922 0.004 . 1 . . . . 8 GLU HB3 . 6525 1 53 . 1 1 8 8 GLU HG2 H 1 2.236 0.004 . 1 . . . . 8 GLU HG2 . 6525 1 54 . 1 1 8 8 GLU HG3 H 1 2.236 0.004 . 1 . . . . 8 GLU HG3 . 6525 1 55 . 1 1 9 9 GLY H H 1 9.008 0.004 . 1 . . . . 9 GLY HN . 6525 1 56 . 1 1 9 9 GLY HA2 H 1 3.932 0.004 . 1 . . . . 9 GLY HA2 . 6525 1 57 . 1 1 9 9 GLY HA3 H 1 4.087 0.004 . 1 . . . . 9 GLY HA3 . 6525 1 58 . 1 1 10 10 TRP H H 1 7.461 0.004 . 1 . . . . 10 TRP HN . 6525 1 59 . 1 1 10 10 TRP HA H 1 4.955 0.004 . 1 . . . . 10 TRP HA . 6525 1 60 . 1 1 10 10 TRP HB2 H 1 3.251 0.004 . 1 . . . . 10 TRP HB1 . 6525 1 61 . 1 1 10 10 TRP HB3 H 1 3.502 0.004 . 1 . . . . 10 TRP HB2 . 6525 1 62 . 1 1 10 10 TRP HD1 H 1 6.926 0.004 . 1 . . . . 10 TRP HD1 . 6525 1 63 . 1 1 10 10 TRP HE1 H 1 10.23 0.004 . 1 . . . . 10 TRP HE1 . 6525 1 64 . 1 1 10 10 TRP HE3 H 1 7.457 0.004 . 1 . . . . 10 TRP HE3 . 6525 1 65 . 1 1 10 10 TRP HZ2 H 1 7.507 0.004 . 1 . . . . 10 TRP HZ2 . 6525 1 66 . 1 1 10 10 TRP HZ3 H 1 7.346 0.004 . 1 . . . . 10 TRP HZ3 . 6525 1 67 . 1 1 10 10 TRP HH2 H 1 6.991 0.004 . 1 . . . . 10 TRP HH2 . 6525 1 68 . 1 1 11 11 GLY H H 1 7.924 0.004 . 1 . . . . 11 GLY H . 6525 1 69 . 1 1 11 11 GLY HA2 H 1 3.925 0.004 . 1 . . . . 11 GLY HA2 . 6525 1 70 . 1 1 11 11 GLY HA3 H 1 4.312 0.004 . 1 . . . . 11 GLY HA3 . 6525 1 71 . 1 1 12 12 LYS H H 1 8.67 0.004 . 1 . . . . 12 LYS H . 6525 1 72 . 1 1 12 12 LYS HA H 1 4.375 0.004 . 1 . . . . 12 LYS HA . 6525 1 73 . 1 1 12 12 LYS HB2 H 1 1.484 0.004 . 1 . . . . 12 LYS HB2 . 6525 1 74 . 1 1 12 12 LYS HB3 H 1 1.735 0.004 . 1 . . . . 12 LYS HB3 . 6525 1 75 . 1 1 12 12 LYS HG2 H 1 1.572 0.004 . 4 . . . . 12 LYS HG2 . 6525 1 76 . 1 1 12 12 LYS HG3 H 1 1.572 0.004 . 4 . . . . 12 LYS HG3 . 6525 1 77 . 1 1 12 12 LYS HD2 H 1 1.434 0.004 . 4 . . . . 12 LYS HD2 . 6525 1 78 . 1 1 12 12 LYS HD3 H 1 1.434 0.004 . 4 . . . . 12 LYS HD3 . 6525 1 79 . 1 1 13 13 CYS H H 1 8.311 0.004 . 1 . . . . 13 CYS H . 6525 1 80 . 1 1 13 13 CYS HA H 1 4.678 0.004 . 1 . . . . 13 CYS HA . 6525 1 81 . 1 1 13 13 CYS HB2 H 1 2.992 0.004 . 1 . . . . 13 CYS HB2 . 6525 1 82 . 1 1 13 13 CYS HB3 H 1 2.54 0.004 . 1 . . . . 13 CYS HB3 . 6525 1 83 . 1 1 14 14 LEU H H 1 9.054 0.004 . 1 . . . . 14 LEU H . 6525 1 84 . 1 1 14 14 LEU HA H 1 4.536 0.004 . 1 . . . . 14 LEU HA . 6525 1 85 . 1 1 14 14 LEU HB2 H 1 1.777 0.004 . 1 . . . . 14 LEU HB2 . 6525 1 86 . 1 1 14 14 LEU HB3 H 1 1.666 0.004 . 1 . . . . 14 LEU HB3 . 6525 1 87 . 1 1 14 14 LEU HG H 1 1.626 0.004 . 1 . . . . 14 LEU HG . 6525 1 88 . 1 1 14 14 LEU HD11 H 1 0.8879 0.004 . 1 . . . . 14 LEU HD1 . 6525 1 89 . 1 1 14 14 LEU HD12 H 1 0.8879 0.004 . 1 . . . . 14 LEU HD1 . 6525 1 90 . 1 1 14 14 LEU HD13 H 1 0.8879 0.004 . 1 . . . . 14 LEU HD1 . 6525 1 91 . 1 1 14 14 LEU HD21 H 1 0.9581 0.004 . 1 . . . . 14 LEU HD2 . 6525 1 92 . 1 1 14 14 LEU HD22 H 1 0.9581 0.004 . 1 . . . . 14 LEU HD2 . 6525 1 93 . 1 1 14 14 LEU HD23 H 1 0.9581 0.004 . 1 . . . . 14 LEU HD2 . 6525 1 94 . 1 1 15 15 ILE H H 1 7.956 0.004 . 1 . . . . 15 ILE H . 6525 1 95 . 1 1 15 15 ILE HA H 1 4.529 0.004 . 1 . . . . 15 ILE HA . 6525 1 96 . 1 1 15 15 ILE HB H 1 2.074 0.004 . 1 . . . . 15 ILE HB . 6525 1 97 . 1 1 15 15 ILE HG12 H 1 1.534 0.004 . 1 . . . . 15 ILE HG12 . 6525 1 98 . 1 1 15 15 ILE HG13 H 1 1.223 0.004 . 1 . . . . 15 ILE HG13 . 6525 1 99 . 1 1 15 15 ILE HG21 H 1 1.068 0.004 . 1 . . . . 15 ILE HG2 . 6525 1 100 . 1 1 15 15 ILE HG22 H 1 1.068 0.004 . 1 . . . . 15 ILE HG2 . 6525 1 101 . 1 1 15 15 ILE HG23 H 1 1.068 0.004 . 1 . . . . 15 ILE HG2 . 6525 1 102 . 1 1 15 15 ILE HD11 H 1 0.9123 0.004 . 1 . . . . 15 ILE HD1 . 6525 1 103 . 1 1 15 15 ILE HD12 H 1 0.9123 0.004 . 1 . . . . 15 ILE HD1 . 6525 1 104 . 1 1 15 15 ILE HD13 H 1 0.9123 0.004 . 1 . . . . 15 ILE HD1 . 6525 1 105 . 1 1 16 16 ASP H H 1 9.017 0.004 . 1 . . . . 16 ASP H . 6525 1 106 . 1 1 16 16 ASP HA H 1 4.912 0.004 . 9 . . . . 16 ASP HA . 6525 1 107 . 1 1 16 16 ASP HB2 H 1 2.802 0.004 . 1 . . . . 16 ASP HB2 . 6525 1 108 . 1 1 16 16 ASP HB3 H 1 2.908 0.004 . 1 . . . . 16 ASP HB3 . 6525 1 109 . 1 1 17 17 THR H H 1 8.062 0.004 . 1 . . . . 17 THR H . 6525 1 110 . 1 1 17 17 THR HA H 1 4.083 0.004 . 1 . . . . 17 THR HA . 6525 1 111 . 1 1 17 17 THR HB H 1 4.162 0.004 . 1 . . . . 17 THR HB . 6525 1 112 . 1 1 17 17 THR HG21 H 1 1.313 0.004 . 1 . . . . 17 THR HG2 . 6525 1 113 . 1 1 17 17 THR HG22 H 1 1.313 0.004 . 1 . . . . 17 THR HG2 . 6525 1 114 . 1 1 17 17 THR HG23 H 1 1.313 0.004 . 1 . . . . 17 THR HG2 . 6525 1 115 . 1 1 18 18 THR H H 1 7.316 0.004 . 1 . . . . 18 THR H . 6525 1 116 . 1 1 18 18 THR HA H 1 4.162 0.004 . 1 . . . . 18 THR HA . 6525 1 117 . 1 1 18 18 THR HB H 1 4.406 0.004 . 1 . . . . 18 THR HB . 6525 1 118 . 1 1 18 18 THR HG21 H 1 1.333 0.004 . 1 . . . . 18 THR HG2 . 6525 1 119 . 1 1 18 18 THR HG22 H 1 1.333 0.004 . 1 . . . . 18 THR HG2 . 6525 1 120 . 1 1 18 18 THR HG23 H 1 1.333 0.004 . 1 . . . . 18 THR HG2 . 6525 1 121 . 1 1 19 19 CYS H H 1 7.057 0.004 . 1 . . . . 19 CYS H . 6525 1 122 . 1 1 19 19 CYS HA H 1 4.706 0.004 . 1 . . . . 19 CYS HA . 6525 1 123 . 1 1 19 19 CYS HB2 H 1 3.595 0.004 . 1 . . . . 19 CYS HB2 . 6525 1 124 . 1 1 19 19 CYS HB3 H 1 2.753 0.004 . 1 . . . . 19 CYS HB3 . 6525 1 125 . 1 1 20 20 ALA H H 1 8.868 0.004 . 1 . . . . 20 ALA H . 6525 1 126 . 1 1 20 20 ALA HA H 1 3.646 0.004 . 1 . . . . 20 ALA HA . 6525 1 127 . 1 1 20 20 ALA HB1 H 1 1.627 0.004 . 1 . . . . 20 ALA HB . 6525 1 128 . 1 1 20 20 ALA HB2 H 1 1.627 0.004 . 1 . . . . 20 ALA HB . 6525 1 129 . 1 1 20 20 ALA HB3 H 1 1.627 0.004 . 1 . . . . 20 ALA HB . 6525 1 130 . 1 1 21 21 HIS H H 1 8.292 0.004 . 1 . . . . 21 HIS H . 6525 1 131 . 1 1 21 21 HIS HA H 1 4.35 0.004 . 1 . . . . 21 HIS HA . 6525 1 132 . 1 1 21 21 HIS HB2 H 1 3.39 0.004 . 1 . . . . 21 HIS HB2 . 6525 1 133 . 1 1 21 21 HIS HB3 H 1 3.428 0.004 . 1 . . . . 21 HIS HB3 . 6525 1 134 . 1 1 21 21 HIS HD2 H 1 7.314 0.004 . 1 . . . . 21 HIS HD2 . 6525 1 135 . 1 1 21 21 HIS HE1 H 1 8.517 0.004 . 1 . . . . 21 HIS HE1 . 6525 1 136 . 1 1 22 22 SER H H 1 8.435 0.004 . 1 . . . . 22 SER H . 6525 1 137 . 1 1 22 22 SER HA H 1 4.061 0.004 . 1 . . . . 22 SER HA . 6525 1 138 . 1 1 22 22 SER HB2 H 1 3.325 0.004 . 1 . . . . 22 SER HB2 . 6525 1 139 . 1 1 22 22 SER HB3 H 1 3.325 0.004 . 1 . . . . 22 SER HB3 . 6525 1 140 . 1 1 23 23 CYS H H 1 9.088 0.004 . 1 . . . . 23 CYS H . 6525 1 141 . 1 1 23 23 CYS HA H 1 4.681 0.004 . 1 . . . . 23 CYS HA . 6525 1 142 . 1 1 23 23 CYS HB2 H 1 2.97 0.004 . 1 . . . . 23 CYS HB2 . 6525 1 143 . 1 1 23 23 CYS HB3 H 1 2.884 0.004 . 1 . . . . 23 CYS HB3 . 6525 1 144 . 1 1 24 24 LYS H H 1 8.844 0.004 . 1 . . . . 24 LYS H . 6525 1 145 . 1 1 24 24 LYS HA H 1 4.493 0.004 . 1 . . . . 24 LYS HA . 6525 1 146 . 1 1 24 24 LYS HB2 H 1 1.963 0.004 . 1 . . . . 24 LYS HB2 . 6525 1 147 . 1 1 24 24 LYS HB3 H 1 1.872 0.004 . 1 . . . . 24 LYS HB3 . 6525 1 148 . 1 1 25 25 ASN H H 1 8.295 0.004 . 1 . . . . 25 ASN H . 6525 1 149 . 1 1 25 25 ASN HA H 1 4.538 0.004 . 1 . . . . 25 ASN HA . 6525 1 150 . 1 1 25 25 ASN HB2 H 1 2.874 0.004 . 1 . . . . 25 ASN HB2 . 6525 1 151 . 1 1 25 25 ASN HB3 H 1 2.874 0.004 . 1 . . . . 25 ASN HB3 . 6525 1 152 . 1 1 25 25 ASN HD21 H 1 7.578 0.004 . 1 . . . . 25 ASN HD21 . 6525 1 153 . 1 1 25 25 ASN HD22 H 1 6.689 0.004 . 1 . . . . 25 ASN HD22 . 6525 1 154 . 1 1 26 26 ARG H H 1 7.442 0.004 . 1 . . . . 26 ARG H . 6525 1 155 . 1 1 26 26 ARG HA H 1 4.533 0.004 . 1 . . . . 26 ARG HA . 6525 1 156 . 1 1 26 26 ARG HB2 H 1 2.406 0.004 . 1 . . . . 26 ARG HB2 . 6525 1 157 . 1 1 26 26 ARG HB3 H 1 2.015 0.004 . 1 . . . . 26 ARG HB3 . 6525 1 158 . 1 1 26 26 ARG HG2 H 1 1.937 0.004 . 1 . . . . 26 ARG HG2 . 6525 1 159 . 1 1 26 26 ARG HG3 H 1 1.937 0.004 . 1 . . . . 26 ARG HG3 . 6525 1 160 . 1 1 26 26 ARG HD2 H 1 3.25 0.004 . 1 . . . . 26 ARG HD2 . 6525 1 161 . 1 1 26 26 ARG HD3 H 1 3.25 0.004 . 1 . . . . 26 ARG HD3 . 6525 1 162 . 1 1 26 26 ARG HE H 1 7.413 0.004 . 1 . . . . 26 ARG HE . 6525 1 163 . 1 1 27 27 GLY H H 1 7.846 0.004 . 1 . . . . 27 GLY H . 6525 1 164 . 1 1 27 27 GLY HA2 H 1 3.754 0.004 . 1 . . . . 27 GLY HA2 . 6525 1 165 . 1 1 27 27 GLY HA3 H 1 4.154 0.004 . 1 . . . . 27 GLY HA3 . 6525 1 166 . 1 1 28 28 TYR H H 1 7.793 0.004 . 1 . . . . 28 TYR H . 6525 1 167 . 1 1 28 28 TYR HA H 1 5.03 0.004 . 1 . . . . 28 TYR HA . 6525 1 168 . 1 1 28 28 TYR HB2 H 1 3.96 0.004 . 1 . . . . 28 TYR HB2 . 6525 1 169 . 1 1 28 28 TYR HB3 H 1 2.618 0.004 . 1 . . . . 28 TYR HB3 . 6525 1 170 . 1 1 28 28 TYR HD1 H 1 7.459 0.004 . 1 . . . . 28 TYR HD1 . 6525 1 171 . 1 1 28 28 TYR HD2 H 1 7.459 0.004 . 1 . . . . 28 TYR HD2 . 6525 1 172 . 1 1 28 28 TYR HE1 H 1 6.775 0.004 . 1 . . . . 28 TYR HE1 . 6525 1 173 . 1 1 28 28 TYR HE2 H 1 6.775 0.004 . 1 . . . . 28 TYR HE2 . 6525 1 174 . 1 1 29 29 ILE H H 1 8.327 0.004 . 1 . . . . 29 ILE H . 6525 1 175 . 1 1 29 29 ILE HA H 1 4.147 0.004 . 1 . . . . 29 ILE HA . 6525 1 176 . 1 1 29 29 ILE HB H 1 1.847 0.004 . 1 . . . . 29 ILE HB . 6525 1 177 . 1 1 29 29 ILE HG12 H 1 1.516 0.004 . 1 . . . . 29 ILE HG12 . 6525 1 178 . 1 1 29 29 ILE HG13 H 1 1.144 0.004 . 1 . . . . 29 ILE HG13 . 6525 1 179 . 1 1 29 29 ILE HG21 H 1 0.9784 0.004 . 1 . . . . 29 ILE HG2 . 6525 1 180 . 1 1 29 29 ILE HG22 H 1 0.9784 0.004 . 1 . . . . 29 ILE HG2 . 6525 1 181 . 1 1 29 29 ILE HG23 H 1 0.9784 0.004 . 1 . . . . 29 ILE HG2 . 6525 1 182 . 1 1 29 29 ILE HD11 H 1 0.8174 0.004 . 1 . . . . 29 ILE HD1 . 6525 1 183 . 1 1 29 29 ILE HD12 H 1 0.8174 0.004 . 1 . . . . 29 ILE HD1 . 6525 1 184 . 1 1 29 29 ILE HD13 H 1 0.8174 0.004 . 1 . . . . 29 ILE HD1 . 6525 1 185 . 1 1 30 30 GLY H H 1 7.403 0.004 . 1 . . . . 30 GLY H . 6525 1 186 . 1 1 30 30 GLY HA2 H 1 4.418 0.004 . 1 . . . . 30 GLY HA2 . 6525 1 187 . 1 1 30 30 GLY HA3 H 1 3.859 0.004 . 1 . . . . 30 GLY HA3 . 6525 1 188 . 1 1 31 31 GLY H H 1 8.661 0.004 . 1 . . . . 31 GLY H . 6525 1 189 . 1 1 31 31 GLY HA2 H 1 4.63 0.004 . 1 . . . . 31 GLY HA2 . 6525 1 190 . 1 1 31 31 GLY HA3 H 1 4.63 0.004 . 1 . . . . 31 GLY HA3 . 6525 1 191 . 1 1 32 32 ASN H H 1 8.88 0.004 . 1 . . . . 32 ASN H . 6525 1 192 . 1 1 32 32 ASN HA H 1 4.673 0.004 . 1 . . . . 32 ASN HA . 6525 1 193 . 1 1 32 32 ASN HB2 H 1 2.565 0.004 . 1 . . . . 32 ASN HB2 . 6525 1 194 . 1 1 32 32 ASN HB3 H 1 2.897 0.004 . 1 . . . . 32 ASN HB3 . 6525 1 195 . 1 1 32 32 ASN HD21 H 1 7.263 0.004 . 1 . . . . 32 ASN HD21 . 6525 1 196 . 1 1 32 32 ASN HD22 H 1 6.576 0.004 . 1 . . . . 32 ASN HD22 . 6525 1 197 . 1 1 33 33 CYS H H 1 9.12 0.004 . 1 . . . . 33 CYS H . 6525 1 198 . 1 1 33 33 CYS HA H 1 5.393 0.004 . 1 . . . . 33 CYS HA . 6525 1 199 . 1 1 33 33 CYS HB2 H 1 2.88 0.004 . 1 . . . . 33 CYS HB2 . 6525 1 200 . 1 1 33 33 CYS HB3 H 1 2.922 0.004 . 1 . . . . 33 CYS HB3 . 6525 1 201 . 1 1 34 34 LYS H H 1 8.798 0.004 . 1 . . . . 34 LYS H . 6525 1 202 . 1 1 34 34 LYS HA H 1 4.44 0.004 . 1 . . . . 34 LYS HA . 6525 1 203 . 1 1 34 34 LYS HB2 H 1 1.72 0.004 . 1 . . . . 34 LYS HB2 . 6525 1 204 . 1 1 34 34 LYS HB3 H 1 1.43 0.004 . 1 . . . . 34 LYS HB3 . 6525 1 205 . 1 1 34 34 LYS HG2 H 1 1.141 0.004 . 4 . . . . 34 LYS HG2 . 6525 1 206 . 1 1 34 34 LYS HG3 H 1 1.141 0.004 . 4 . . . . 34 LYS HG3 . 6525 1 207 . 1 1 34 34 LYS HD2 H 1 1.08 0.004 . 4 . . . . 34 LYS HD2 . 6525 1 208 . 1 1 34 34 LYS HD3 H 1 1.08 0.004 . 4 . . . . 34 LYS HD3 . 6525 1 209 . 1 1 35 35 GLY H H 1 8.797 0.004 . 1 . . . . 35 GLY H . 6525 1 210 . 1 1 35 35 GLY HA2 H 1 4.252 0.004 . 1 . . . . 35 GLY HA2 . 6525 1 211 . 1 1 35 35 GLY HA3 H 1 3.866 0.004 . 1 . . . . 35 GLY HA3 . 6525 1 212 . 1 1 36 36 MET H H 1 8.94 0.004 . 1 . . . . 36 MET H . 6525 1 213 . 1 1 36 36 MET HA H 1 4.508 0.004 . 1 . . . . 36 MET HA . 6525 1 214 . 1 1 36 36 MET HB2 H 1 2.094 0.004 . 1 . . . . 36 MET HB2 . 6525 1 215 . 1 1 36 36 MET HB3 H 1 2.214 0.004 . 1 . . . . 36 MET HB3 . 6525 1 216 . 1 1 36 36 MET HG2 H 1 2.607 0.004 . 1 . . . . 36 MET HG2 . 6525 1 217 . 1 1 36 36 MET HG3 H 1 2.697 0.004 . 1 . . . . 36 MET HG3 . 6525 1 218 . 1 1 37 37 THR H H 1 8.098 0.004 . 1 . . . . 37 THR H . 6525 1 219 . 1 1 37 37 THR HA H 1 4.275 0.004 . 1 . . . . 37 THR HA . 6525 1 220 . 1 1 37 37 THR HB H 1 4.384 0.004 . 9 . . . . 37 THR HB . 6525 1 221 . 1 1 37 37 THR HG21 H 1 1.286 0.004 . 1 . . . . 37 THR HG2 . 6525 1 222 . 1 1 37 37 THR HG22 H 1 1.286 0.004 . 1 . . . . 37 THR HG2 . 6525 1 223 . 1 1 37 37 THR HG23 H 1 1.286 0.004 . 1 . . . . 37 THR HG2 . 6525 1 224 . 1 1 38 38 ARG H H 1 8.705 0.004 . 1 . . . . 38 ARG H . 6525 1 225 . 1 1 38 38 ARG HA H 1 3.978 0.004 . 1 . . . . 38 ARG HA . 6525 1 226 . 1 1 38 38 ARG HB2 H 1 2.163 0.004 . 1 . . . . 38 ARG HB2 . 6525 1 227 . 1 1 38 38 ARG HB3 H 1 1.965 0.004 . 1 . . . . 38 ARG HB3 . 6525 1 228 . 1 1 38 38 ARG HG2 H 1 1.721 0.004 . 1 . . . . 38 ARG HG2 . 6525 1 229 . 1 1 38 38 ARG HG3 H 1 1.721 0.004 . 1 . . . . 38 ARG HG3 . 6525 1 230 . 1 1 38 38 ARG HD2 H 1 3.225 0.004 . 1 . . . . 38 ARG HD2 . 6525 1 231 . 1 1 38 38 ARG HD3 H 1 3.225 0.004 . 1 . . . . 38 ARG HD3 . 6525 1 232 . 1 1 38 38 ARG HE H 1 3.892 0.004 . 1 . . . . 38 ARG HE . 6525 1 233 . 1 1 39 39 THR H H 1 8.41 0.004 . 1 . . . . 39 THR H . 6525 1 234 . 1 1 39 39 THR HA H 1 4.625 0.004 . 1 . . . . 39 THR HA . 6525 1 235 . 1 1 39 39 THR HB H 1 4.009 0.004 . 1 . . . . 39 THR HB . 6525 1 236 . 1 1 39 39 THR HG21 H 1 0.961 0.004 . 1 . . . . 39 THR HG2 . 6525 1 237 . 1 1 39 39 THR HG22 H 1 0.961 0.004 . 1 . . . . 39 THR HG2 . 6525 1 238 . 1 1 39 39 THR HG23 H 1 0.961 0.004 . 1 . . . . 39 THR HG2 . 6525 1 239 . 1 1 40 40 CYS H H 1 9.478 0.004 . 1 . . . . 40 CYS H . 6525 1 240 . 1 1 40 40 CYS HA H 1 4.982 0.004 . 1 . . . . 40 CYS HA . 6525 1 241 . 1 1 40 40 CYS HB2 H 1 2.6 0.004 . 1 . . . . 40 CYS HB2 . 6525 1 242 . 1 1 40 40 CYS HB3 H 1 3.265 0.004 . 1 . . . . 40 CYS HB3 . 6525 1 243 . 1 1 41 41 TYR H H 1 8.725 0.004 . 1 . . . . 41 TYR H . 6525 1 244 . 1 1 41 41 TYR HA H 1 5.006 0.004 . 1 . . . . 41 TYR HA . 6525 1 245 . 1 1 41 41 TYR HB2 H 1 2.941 0.004 . 1 . . . . 41 TYR HB2 . 6525 1 246 . 1 1 41 41 TYR HB3 H 1 2.357 0.004 . 1 . . . . 41 TYR HB3 . 6525 1 247 . 1 1 41 41 TYR HD1 H 1 6.994 0.004 . 1 . . . . 41 TYR HD1 . 6525 1 248 . 1 1 41 41 TYR HD2 H 1 6.994 0.004 . 1 . . . . 41 TYR HD2 . 6525 1 249 . 1 1 41 41 TYR HE1 H 1 6.717 0.004 . 1 . . . . 41 TYR HE1 . 6525 1 250 . 1 1 41 41 TYR HE2 H 1 6.717 0.004 . 1 . . . . 41 TYR HE2 . 6525 1 251 . 1 1 42 42 CYS H H 1 8.574 0.004 . 1 . . . . 42 CYS H . 6525 1 252 . 1 1 42 42 CYS HA H 1 5.589 0.004 . 1 . . . . 42 CYS HA . 6525 1 253 . 1 1 42 42 CYS HB2 H 1 2.601 0.004 . 1 . . . . 42 CYS HB2 . 6525 1 254 . 1 1 42 42 CYS HB3 H 1 1.356 0.004 . 1 . . . . 42 CYS HB3 . 6525 1 255 . 1 1 43 43 LEU H H 1 8.246 0.004 . 1 . . . . 43 LEU H . 6525 1 256 . 1 1 43 43 LEU HA H 1 5.118 0.004 . 1 . . . . 43 LEU HA . 6525 1 257 . 1 1 43 43 LEU HB2 H 1 1.318 0.004 . 1 . . . . 43 LEU HB2 . 6525 1 258 . 1 1 43 43 LEU HB3 H 1 1.318 0.004 . 1 . . . . 43 LEU HB3 . 6525 1 259 . 1 1 43 43 LEU HG H 1 1.397 0.004 . 1 . . . . 43 LEU HG . 6525 1 260 . 1 1 43 43 LEU HD11 H 1 0.803 0.004 . 4 . . . . 43 LEU HD1 . 6525 1 261 . 1 1 43 43 LEU HD12 H 1 0.803 0.004 . 4 . . . . 43 LEU HD1 . 6525 1 262 . 1 1 43 43 LEU HD13 H 1 0.803 0.004 . 4 . . . . 43 LEU HD1 . 6525 1 263 . 1 1 44 44 VAL H H 1 8.855 0.004 . 1 . . . . 44 VAL H . 6525 1 264 . 1 1 44 44 VAL HA H 1 4.84 0.004 . 1 . . . . 44 VAL HA . 6525 1 265 . 1 1 44 44 VAL HB H 1 2.151 0.004 . 1 . . . . 44 VAL HB . 6525 1 266 . 1 1 44 44 VAL HG11 H 1 0.902 0.004 . 1 . . . . 44 VAL HG1 . 6525 1 267 . 1 1 44 44 VAL HG12 H 1 0.902 0.004 . 1 . . . . 44 VAL HG1 . 6525 1 268 . 1 1 44 44 VAL HG13 H 1 0.902 0.004 . 1 . . . . 44 VAL HG1 . 6525 1 269 . 1 1 44 44 VAL HG21 H 1 1.006 0.004 . 1 . . . . 44 VAL HG2 . 6525 1 270 . 1 1 44 44 VAL HG22 H 1 1.006 0.004 . 1 . . . . 44 VAL HG2 . 6525 1 271 . 1 1 44 44 VAL HG23 H 1 1.006 0.004 . 1 . . . . 44 VAL HG2 . 6525 1 272 . 1 1 45 45 ASN H H 1 8.914 0.004 . 1 . . . . 45 ASN H . 6525 1 273 . 1 1 45 45 ASN HA H 1 5.121 0.004 . 1 . . . . 45 ASN HA . 6525 1 274 . 1 1 45 45 ASN HB2 H 1 2.738 0.004 . 1 . . . . 45 ASN HB2 . 6525 1 275 . 1 1 45 45 ASN HB3 H 1 2.878 0.004 . 1 . . . . 45 ASN HB3 . 6525 1 276 . 1 1 45 45 ASN HD21 H 1 7.692 0.004 . 1 . . . . 45 ASN HD21 . 6525 1 277 . 1 1 45 45 ASN HD22 H 1 7.053 0.004 . 1 . . . . 45 ASN HD22 . 6525 1 278 . 1 1 46 46 CYS H H 1 8.509 0.004 . 1 . . . . 46 CYS H . 6525 1 279 . 1 1 46 46 CYS HA H 1 4.651 0.004 . 1 . . . . 46 CYS HA . 6525 1 280 . 1 1 46 46 CYS HB2 H 1 3.186 0.004 . 1 . . . . 46 CYS HB2 . 6525 1 281 . 1 1 46 46 CYS HB3 H 1 3.315 0.004 . 1 . . . . 46 CYS HB3 . 6525 1 stop_ loop_ _Ambiguous_atom_chem_shift.Ambiguous_shift_set_ID _Ambiguous_atom_chem_shift.Atom_chem_shift_ID _Ambiguous_atom_chem_shift.Entry_ID _Ambiguous_atom_chem_shift.Assigned_chem_shift_list_ID 1 37 6525 1 1 38 6525 1 1 39 6525 1 1 40 6525 1 2 45 6525 1 2 46 6525 1 2 47 6525 1 2 48 6525 1 3 75 6525 1 3 76 6525 1 3 77 6525 1 3 78 6525 1 4 205 6525 1 4 206 6525 1 4 207 6525 1 4 208 6525 1 5 260 6525 1 5 261 6525 1 5 262 6525 1 stop_ save_