data_5995 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 5995 _Entry.Title ; Temperature Dependent Spectral Density Analysis Applied to Monitoring Backbone Dynamics of Major Urinary Protein-I Complexed with the Pheromone 2-sec-Butyl-4,5-dihyrothiazole ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2003-11-05 _Entry.Accession_date 2003-11-05 _Entry.Last_release_date 2004-04-07 _Entry.Original_release_date 2004-04-07 _Entry.Origination author _Entry.NMR_STAR_version 3.1.2.6 _Entry.Original_NMR_STAR_version 2.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Hana Krizova . . . . 5995 2 Lukas Zidek . . . . 5995 3 Martin Stone . J. . . 5995 4 Milos Novotny . V. . . 5995 5 Vladimir Sklenar . . . . 5995 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 5995 heteronucl_NOEs 8 5995 heteronucl_T1_relaxation 8 5995 heteronucl_T2_relaxation 8 5995 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '15N chemical shifts' 159 5995 '1H chemical shifts' 159 5995 'T1 relaxation values' 699 5995 'T2 relaxation values' 699 5995 'heteronuclear NOE values' 699 5995 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2017-06-15 2003-11-05 update author 'update t2 data' 5995 1 . . 2004-04-07 2003-11-05 original author 'original release' 5995 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 5996 'Relaxation data of complex form' 5995 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 5995 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 14872128 _Citation.Full_citation . _Citation.Title ; Temperature-Dependent Spectral Density Analysis Applied to Monitoring Backbone Dynamics of Major Urinary Protein-I Complexed with the Pheromone 2-sec-butyl-4,5-dihyrothiazole. ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'J. Biomol. NMR' _Citation.Journal_name_full . _Citation.Journal_volume 28 _Citation.Journal_issue 4 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 369 _Citation.Page_last 384 _Citation.Year 2004 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Hana Krizova . . . . 5995 1 2 Lukas Zidek . . . . 5995 1 3 Martin Stone . J. . . 5995 1 4 Milos Novotny . V. . . 5995 1 5 Vladimir Sklenar . . . . 5995 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_system_MUP-I _Assembly.Sf_category assembly _Assembly.Sf_framecode system_MUP-I _Assembly.Entry_ID 5995 _Assembly.ID 1 _Assembly.Name 'Major Urinary Protein-I' _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state 'disulfide bound and free' _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Assembly_type.Type _Assembly_type.Entry_ID _Assembly_type.Assembly_ID monomer 5995 1 stop_ loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 MUP-I 1 $MUP-I . . . native . . . . . 5995 1 stop_ loop_ _Bond.ID _Bond.Type _Bond.Value_order _Bond.Assembly_atom_ID_1 _Bond.Entity_assembly_ID_1 _Bond.Entity_assembly_name_1 _Bond.Entity_ID_1 _Bond.Comp_ID_1 _Bond.Comp_index_ID_1 _Bond.Seq_ID_1 _Bond.Atom_ID_1 _Bond.Assembly_atom_ID_2 _Bond.Entity_assembly_ID_2 _Bond.Entity_assembly_name_2 _Bond.Entity_ID_2 _Bond.Comp_ID_2 _Bond.Comp_index_ID_2 _Bond.Seq_ID_2 _Bond.Atom_ID_2 _Bond.Auth_entity_assembly_ID_1 _Bond.Auth_entity_assembly_name_1 _Bond.Auth_seq_ID_1 _Bond.Auth_comp_ID_1 _Bond.Auth_atom_ID_1 _Bond.Auth_entity_assembly_ID_2 _Bond.Auth_entity_assembly_name_2 _Bond.Auth_seq_ID_2 _Bond.Auth_comp_ID_2 _Bond.Auth_atom_ID_2 _Bond.Entry_ID _Bond.Assembly_ID 1 disulfide single . 1 . 1 CYS 64 64 SG . 1 . 1 CYS 157 157 SG . . . . . . . . . . 5995 1 stop_ loop_ _Assembly_db_link.Author_supplied _Assembly_db_link.Database_code _Assembly_db_link.Accession_code _Assembly_db_link.Entry_mol_code _Assembly_db_link.Entry_mol_name _Assembly_db_link.Entry_experimental_method _Assembly_db_link.Entry_structure_resolution _Assembly_db_link.Entry_relation_type _Assembly_db_link.Entry_details _Assembly_db_link.Entry_ID _Assembly_db_link.Assembly_ID yes PDB 1I04 . . . . . 'Four C-terminal residues are missing in the PDB file.' 5995 1 stop_ loop_ _Assembly_common_name.Name _Assembly_common_name.Type _Assembly_common_name.Entry_ID _Assembly_common_name.Assembly_ID MUP-I abbreviation 5995 1 'Major Urinary Protein-I' system 5995 1 stop_ loop_ _Assembly_bio_function.Biological_function _Assembly_bio_function.Entry_ID _Assembly_bio_function.Assembly_ID 'pheromone binding' 5995 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_MUP-I _Entity.Sf_category entity _Entity.Sf_framecode MUP-I _Entity.Entry_ID 5995 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name 'Major Urinary Protein-I' _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; EEASSTGRNFNVEKINGEWH TIILASDKREKIEDNGNFRL FLEQIHVLENSLVLKFHTVR DEECSELSMVADKTEKAGEY SVTYDGFNTFTIPKTDYDNF LMAHLINEKDGETFQLMGLY GREPDLSSDIKERFAQLCEK HGILRENIIDLSNANRCLQA RE ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states . _Entity.Ambiguous_chem_comp_sites . _Entity.Nstd_monomer . _Entity.Nstd_chirality . _Entity.Nstd_linkage . _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 162 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'disulfide bound and free' _Entity.Src_method . _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date 2015-01-28 loop_ _Entity_db_link.Ordinal _Entity_db_link.Author_supplied _Entity_db_link.Database_code _Entity_db_link.Accession_code _Entity_db_link.Entry_mol_code _Entity_db_link.Entry_mol_name _Entity_db_link.Entry_experimental_method _Entity_db_link.Entry_structure_resolution _Entity_db_link.Entry_relation_type _Entity_db_link.Entry_details _Entity_db_link.Chimera_segment_ID _Entity_db_link.Seq_query_to_submitted_percent _Entity_db_link.Seq_subject_length _Entity_db_link.Seq_identity _Entity_db_link.Seq_positive _Entity_db_link.Seq_homology_expectation_val _Entity_db_link.Seq_align_begin _Entity_db_link.Seq_align_end _Entity_db_link.Seq_difference_details _Entity_db_link.Seq_alignment_details _Entity_db_link.Entry_ID _Entity_db_link.Entity_ID 1 no BMRB 17447 . MUP11 . . . . . 100.00 176 99.38 100.00 6.22e-114 . . . . 5995 1 2 no BMRB 4340 . rMUP . . . . . 100.00 162 98.77 99.38 2.36e-113 . . . . 5995 1 3 no BMRB 5996 . MUP-I . . . . . 100.00 162 100.00 100.00 7.39e-115 . . . . 5995 1 4 no PDB 1DF3 . 'Solution Structure Of A Recombinant Mouse Major Urinary Protein' . . . . . 100.00 162 98.77 99.38 2.36e-113 . . . . 5995 1 5 no PDB 1I04 . 'Crystal Structure Of Mouse Major Urinary Protein-I From Mouse Liver' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5995 1 6 no PDB 1I05 . 'Crystal Structure Of Mouse Major Urinary Protein (Mup-I) Complexed With Hydroxy-Methyl-Heptanone' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5995 1 7 no PDB 1I06 . 'Crystal Structure Of Mouse Major Urinary Protein (Mup-I) Complexed With Sec-Butyl-Thiazoline' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5995 1 8 no PDB 1JV4 . 'Crystal Structure Of Recombinant Major Mouse Urinary Protein (Rmup) At 1.75 A Resolution' . . . . . 100.00 162 98.77 99.38 2.36e-113 . . . . 5995 1 9 no PDB 1MUP . 'Pheromone Binding To Two Rodent Urinary Proteins Revealed By X-Ray Crystallography' . . . . . 100.00 166 99.38 100.00 5.44e-114 . . . . 5995 1 10 no PDB 1QY0 . 'Thermodynamics Of Binding Of 2-Methoxy-3-Isopropylpyrazine And 2- Methoxy-3-Isobutylpyrazine To The Major Urinary Protein' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 11 no PDB 1QY1 . 'Thermodynamics Of Binding Of 2-Methoxy-3-Isopropylpyrazine And 2- Methoxy-3-Isobutylpyrazine To The Major Urinary Protein' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 12 no PDB 1QY2 . 'Thermodynamics Of Binding Of 2-Methoxy-3-Isopropylpyrazine And 2- Methoxy-3-Isobutylpyrazine To The Major Urinary Protein' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 13 no PDB 1YP6 . 'Van Der Waals Interactions Dominate Hydrophobic Association In A Protein Binding Site Occluded From Solvent Water' . . . . . 100.00 174 98.15 99.38 2.26e-112 . . . . 5995 1 14 no PDB 1YP7 . 'Van Der Waals Interactions Dominate Hydrophobic Association In A Protein Binding Site Occluded From Solvent Water' . . . . . 100.00 174 98.15 99.38 2.26e-112 . . . . 5995 1 15 no PDB 1ZND . 'Strong Solute-solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 16 no PDB 1ZNE . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 17 no PDB 1ZNG . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 18 no PDB 1ZNH . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 19 no PDB 1ZNK . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 20 no PDB 1ZNL . 'Strong Solute-Solute Dispersive Interactions In A Protein- Ligand Complex' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 21 no PDB 2DM5 . 'Thermodynamic Penalty Arising From Burial Of A Ligand Polar Group Within A Hydrophobic Pocket Of A Protein Receptor' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 22 no PDB 2LB6 . 'Structure Of 18694da Mup, Typical To The Major Urinary Protein Family: Mup9, Mup11, Mup15, Mup18 & Mup19' . . . . . 100.00 176 99.38 100.00 6.22e-114 . . . . 5995 1 23 no PDB 2OZQ . 'Crystal Structure Of Apo-Mup' . . . . . 100.00 174 98.77 99.38 5.00e-113 . . . . 5995 1 24 no DBJ BAB28753 . 'unnamed protein product [Mus musculus]' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5995 1 25 no DBJ BAB29093 . 'unnamed protein product [Mus musculus]' . . . . . 100.00 181 98.15 100.00 8.83e-113 . . . . 5995 1 26 no EMBL CAA26953 . 'major urinary protein [Mus musculus]' . . . . . 100.00 180 98.77 99.38 3.12e-113 . . . . 5995 1 27 no EMBL CAA27227 . 'MUP [Mus musculus]' . . . . . 92.59 151 99.33 100.00 4.32e-105 . . . . 5995 1 28 no EMBL CAA27729 . 'MUP [Mus musculus]' . . . . . 83.95 136 97.06 98.53 1.96e-91 . . . . 5995 1 29 no EMBL CAC34259 . 'Major Urinary Protein [Mus musculus]' . . . . . 100.00 180 98.77 99.38 3.97e-113 . . . . 5995 1 30 no EMBL CAQ11104 . 'novel member of the major urinary protein (Mup) gene family [Mus musculus]' . . . . . 100.00 180 97.53 98.15 4.55e-111 . . . . 5995 1 31 no GB AAA39764 . 'major urinary protein [Mus musculus]' . . . . . 100.00 178 98.77 98.77 1.01e-112 . . . . 5995 1 32 no GB AAA39765 . 'major urinary protein, partial [Mus musculus]' . . . . . 92.59 151 99.33 100.00 4.32e-105 . . . . 5995 1 33 no GB AAA39767 . 'major urinary protein I [Mus musculus domesticus]' . . . . . 100.00 180 100.00 100.00 1.10e-114 . . . . 5995 1 34 no GB AAA39768 . 'major urinary protein II [Mus musculus domesticus]' . . . . . 100.00 180 98.15 99.38 2.02e-112 . . . . 5995 1 35 no GB AAB47130 . 'uMUP-VIII=18.695 kda major urinary protein [mice, Balb/c, urine, Peptide, 162 aa]' . . . . . 100.00 162 99.38 100.00 3.16e-114 . . . . 5995 1 36 no REF NP_001039015 . 'major urinary protein 2 isoform 1 precursor [Mus musculus]' . . . . . 100.00 180 98.77 100.00 1.33e-113 . . . . 5995 1 37 no REF NP_001116119 . 'major urinary protein 10 precursor [Mus musculus]' . . . . . 100.00 180 98.77 99.38 3.56e-113 . . . . 5995 1 38 no REF NP_001128116 . 'major urinary protein LOC100048885 precursor [Mus musculus]' . . . . . 100.00 180 97.53 98.15 4.55e-111 . . . . 5995 1 39 no REF NP_001128147 . 'major urinary protein 7 precursor [Mus musculus]' . . . . . 95.06 235 99.35 99.35 3.25e-106 . . . . 5995 1 40 no REF NP_001128148 . 'major urinary protein 8 precursor [Mus musculus]' . . . . . 95.06 235 98.05 98.70 4.04e-104 . . . . 5995 1 41 no SP B5X0G2 . 'RecName: Full=Major urinary protein 17; Short=MUP 17; Flags: Precursor [Mus musculus]' . . . . . 100.00 180 97.53 99.38 1.16e-111 . . . . 5995 1 42 no SP P02762 . 'RecName: Full=Major urinary protein 6; Short=MUP 6; AltName: Full=Alpha-2U-globulin; AltName: Full=Group 1, BS6; AltName: Aller' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5995 1 43 no SP P04938 . 'RecName: Full=Major urinary proteins 11 and 8; AltName: Full=MUP11 and MUP8, partial [Mus musculus]' . . . . . 92.59 151 99.33 100.00 4.32e-105 . . . . 5995 1 44 no SP P11588 . 'RecName: Full=Major urinary protein 1; Short=MUP 1; Flags: Precursor [Mus musculus]' . . . . . 100.00 180 100.00 100.00 1.10e-114 . . . . 5995 1 45 no SP P11589 . 'RecName: Full=Major urinary protein 2; Short=MUP 2; Flags: Precursor [Mus musculus]' . . . . . 100.00 180 98.15 99.38 2.02e-112 . . . . 5995 1 46 no TPG DAA06299 . 'TPA_inf: major urinary protein 3 [Mus musculus]' . . . . . 100.00 180 99.38 99.38 8.98e-114 . . . . 5995 1 47 no TPG DAA06300 . 'TPA_inf: major urinary protein 4 [Mus musculus]' . . . . . 100.00 180 98.77 100.00 1.33e-113 . . . . 5995 1 48 no TPG DAA06301 . 'TPA_inf: major urinary protein 5 [Mus musculus]' . . . . . 100.00 180 98.15 98.77 6.23e-112 . . . . 5995 1 49 no TPG DAA06302 . 'TPA_inf: major urinary protein 6 [Mus musculus]' . . . . . 100.00 180 99.38 100.00 5.87e-114 . . . . 5995 1 50 no TPG DAA06303 . 'TPA_inf: major urinary protein 7 [Mus musculus]' . . . . . 100.00 180 100.00 100.00 9.88e-115 . . . . 5995 1 stop_ loop_ _Entity_common_name.Name _Entity_common_name.Type _Entity_common_name.Entry_ID _Entity_common_name.Entity_ID MUP-I abbreviation 5995 1 'Major Urinary Protein-I' common 5995 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . GLU . 5995 1 2 . GLU . 5995 1 3 . ALA . 5995 1 4 . SER . 5995 1 5 . SER . 5995 1 6 . THR . 5995 1 7 . GLY . 5995 1 8 . ARG . 5995 1 9 . ASN . 5995 1 10 . PHE . 5995 1 11 . ASN . 5995 1 12 . VAL . 5995 1 13 . GLU . 5995 1 14 . LYS . 5995 1 15 . ILE . 5995 1 16 . ASN . 5995 1 17 . GLY . 5995 1 18 . GLU . 5995 1 19 . TRP . 5995 1 20 . HIS . 5995 1 21 . THR . 5995 1 22 . ILE . 5995 1 23 . ILE . 5995 1 24 . LEU . 5995 1 25 . ALA . 5995 1 26 . SER . 5995 1 27 . ASP . 5995 1 28 . LYS . 5995 1 29 . ARG . 5995 1 30 . GLU . 5995 1 31 . LYS . 5995 1 32 . ILE . 5995 1 33 . GLU . 5995 1 34 . ASP . 5995 1 35 . ASN . 5995 1 36 . GLY . 5995 1 37 . ASN . 5995 1 38 . PHE . 5995 1 39 . ARG . 5995 1 40 . LEU . 5995 1 41 . PHE . 5995 1 42 . LEU . 5995 1 43 . GLU . 5995 1 44 . GLN . 5995 1 45 . ILE . 5995 1 46 . HIS . 5995 1 47 . VAL . 5995 1 48 . LEU . 5995 1 49 . GLU . 5995 1 50 . ASN . 5995 1 51 . SER . 5995 1 52 . LEU . 5995 1 53 . VAL . 5995 1 54 . LEU . 5995 1 55 . LYS . 5995 1 56 . PHE . 5995 1 57 . HIS . 5995 1 58 . THR . 5995 1 59 . VAL . 5995 1 60 . ARG . 5995 1 61 . ASP . 5995 1 62 . GLU . 5995 1 63 . GLU . 5995 1 64 . CYS . 5995 1 65 . SER . 5995 1 66 . GLU . 5995 1 67 . LEU . 5995 1 68 . SER . 5995 1 69 . MET . 5995 1 70 . VAL . 5995 1 71 . ALA . 5995 1 72 . ASP . 5995 1 73 . LYS . 5995 1 74 . THR . 5995 1 75 . GLU . 5995 1 76 . LYS . 5995 1 77 . ALA . 5995 1 78 . GLY . 5995 1 79 . GLU . 5995 1 80 . TYR . 5995 1 81 . SER . 5995 1 82 . VAL . 5995 1 83 . THR . 5995 1 84 . TYR . 5995 1 85 . ASP . 5995 1 86 . GLY . 5995 1 87 . PHE . 5995 1 88 . ASN . 5995 1 89 . THR . 5995 1 90 . PHE . 5995 1 91 . THR . 5995 1 92 . ILE . 5995 1 93 . PRO . 5995 1 94 . LYS . 5995 1 95 . THR . 5995 1 96 . ASP . 5995 1 97 . TYR . 5995 1 98 . ASP . 5995 1 99 . ASN . 5995 1 100 . PHE . 5995 1 101 . LEU . 5995 1 102 . MET . 5995 1 103 . ALA . 5995 1 104 . HIS . 5995 1 105 . LEU . 5995 1 106 . ILE . 5995 1 107 . ASN . 5995 1 108 . GLU . 5995 1 109 . LYS . 5995 1 110 . ASP . 5995 1 111 . GLY . 5995 1 112 . GLU . 5995 1 113 . THR . 5995 1 114 . PHE . 5995 1 115 . GLN . 5995 1 116 . LEU . 5995 1 117 . MET . 5995 1 118 . GLY . 5995 1 119 . LEU . 5995 1 120 . TYR . 5995 1 121 . GLY . 5995 1 122 . ARG . 5995 1 123 . GLU . 5995 1 124 . PRO . 5995 1 125 . ASP . 5995 1 126 . LEU . 5995 1 127 . SER . 5995 1 128 . SER . 5995 1 129 . ASP . 5995 1 130 . ILE . 5995 1 131 . LYS . 5995 1 132 . GLU . 5995 1 133 . ARG . 5995 1 134 . PHE . 5995 1 135 . ALA . 5995 1 136 . GLN . 5995 1 137 . LEU . 5995 1 138 . CYS . 5995 1 139 . GLU . 5995 1 140 . LYS . 5995 1 141 . HIS . 5995 1 142 . GLY . 5995 1 143 . ILE . 5995 1 144 . LEU . 5995 1 145 . ARG . 5995 1 146 . GLU . 5995 1 147 . ASN . 5995 1 148 . ILE . 5995 1 149 . ILE . 5995 1 150 . ASP . 5995 1 151 . LEU . 5995 1 152 . SER . 5995 1 153 . ASN . 5995 1 154 . ALA . 5995 1 155 . ASN . 5995 1 156 . ARG . 5995 1 157 . CYS . 5995 1 158 . LEU . 5995 1 159 . GLN . 5995 1 160 . ALA . 5995 1 161 . ARG . 5995 1 162 . GLU . 5995 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . GLU 1 1 5995 1 . GLU 2 2 5995 1 . ALA 3 3 5995 1 . SER 4 4 5995 1 . SER 5 5 5995 1 . THR 6 6 5995 1 . GLY 7 7 5995 1 . ARG 8 8 5995 1 . ASN 9 9 5995 1 . PHE 10 10 5995 1 . ASN 11 11 5995 1 . VAL 12 12 5995 1 . GLU 13 13 5995 1 . LYS 14 14 5995 1 . ILE 15 15 5995 1 . ASN 16 16 5995 1 . GLY 17 17 5995 1 . GLU 18 18 5995 1 . TRP 19 19 5995 1 . HIS 20 20 5995 1 . THR 21 21 5995 1 . ILE 22 22 5995 1 . ILE 23 23 5995 1 . LEU 24 24 5995 1 . ALA 25 25 5995 1 . SER 26 26 5995 1 . ASP 27 27 5995 1 . LYS 28 28 5995 1 . ARG 29 29 5995 1 . GLU 30 30 5995 1 . LYS 31 31 5995 1 . ILE 32 32 5995 1 . GLU 33 33 5995 1 . ASP 34 34 5995 1 . ASN 35 35 5995 1 . GLY 36 36 5995 1 . ASN 37 37 5995 1 . PHE 38 38 5995 1 . ARG 39 39 5995 1 . LEU 40 40 5995 1 . PHE 41 41 5995 1 . LEU 42 42 5995 1 . GLU 43 43 5995 1 . GLN 44 44 5995 1 . ILE 45 45 5995 1 . HIS 46 46 5995 1 . VAL 47 47 5995 1 . LEU 48 48 5995 1 . GLU 49 49 5995 1 . ASN 50 50 5995 1 . SER 51 51 5995 1 . LEU 52 52 5995 1 . VAL 53 53 5995 1 . LEU 54 54 5995 1 . LYS 55 55 5995 1 . PHE 56 56 5995 1 . HIS 57 57 5995 1 . THR 58 58 5995 1 . VAL 59 59 5995 1 . ARG 60 60 5995 1 . ASP 61 61 5995 1 . GLU 62 62 5995 1 . GLU 63 63 5995 1 . CYS 64 64 5995 1 . SER 65 65 5995 1 . GLU 66 66 5995 1 . LEU 67 67 5995 1 . SER 68 68 5995 1 . MET 69 69 5995 1 . VAL 70 70 5995 1 . ALA 71 71 5995 1 . ASP 72 72 5995 1 . LYS 73 73 5995 1 . THR 74 74 5995 1 . GLU 75 75 5995 1 . LYS 76 76 5995 1 . ALA 77 77 5995 1 . GLY 78 78 5995 1 . GLU 79 79 5995 1 . TYR 80 80 5995 1 . SER 81 81 5995 1 . VAL 82 82 5995 1 . THR 83 83 5995 1 . TYR 84 84 5995 1 . ASP 85 85 5995 1 . GLY 86 86 5995 1 . PHE 87 87 5995 1 . ASN 88 88 5995 1 . THR 89 89 5995 1 . PHE 90 90 5995 1 . THR 91 91 5995 1 . ILE 92 92 5995 1 . PRO 93 93 5995 1 . LYS 94 94 5995 1 . THR 95 95 5995 1 . ASP 96 96 5995 1 . TYR 97 97 5995 1 . ASP 98 98 5995 1 . ASN 99 99 5995 1 . PHE 100 100 5995 1 . LEU 101 101 5995 1 . MET 102 102 5995 1 . ALA 103 103 5995 1 . HIS 104 104 5995 1 . LEU 105 105 5995 1 . ILE 106 106 5995 1 . ASN 107 107 5995 1 . GLU 108 108 5995 1 . LYS 109 109 5995 1 . ASP 110 110 5995 1 . GLY 111 111 5995 1 . GLU 112 112 5995 1 . THR 113 113 5995 1 . PHE 114 114 5995 1 . GLN 115 115 5995 1 . LEU 116 116 5995 1 . MET 117 117 5995 1 . GLY 118 118 5995 1 . LEU 119 119 5995 1 . TYR 120 120 5995 1 . GLY 121 121 5995 1 . ARG 122 122 5995 1 . GLU 123 123 5995 1 . PRO 124 124 5995 1 . ASP 125 125 5995 1 . LEU 126 126 5995 1 . SER 127 127 5995 1 . SER 128 128 5995 1 . ASP 129 129 5995 1 . ILE 130 130 5995 1 . LYS 131 131 5995 1 . GLU 132 132 5995 1 . ARG 133 133 5995 1 . PHE 134 134 5995 1 . ALA 135 135 5995 1 . GLN 136 136 5995 1 . LEU 137 137 5995 1 . CYS 138 138 5995 1 . GLU 139 139 5995 1 . LYS 140 140 5995 1 . HIS 141 141 5995 1 . GLY 142 142 5995 1 . ILE 143 143 5995 1 . LEU 144 144 5995 1 . ARG 145 145 5995 1 . GLU 146 146 5995 1 . ASN 147 147 5995 1 . ILE 148 148 5995 1 . ILE 149 149 5995 1 . ASP 150 150 5995 1 . LEU 151 151 5995 1 . SER 152 152 5995 1 . ASN 153 153 5995 1 . ALA 154 154 5995 1 . ASN 155 155 5995 1 . ARG 156 156 5995 1 . CYS 157 157 5995 1 . LEU 158 158 5995 1 . GLN 159 159 5995 1 . ALA 160 160 5995 1 . ARG 161 161 5995 1 . GLU 162 162 5995 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 5995 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $MUP-I . 10090 organism . 'Mus musculus' 'House mouse' . . Eukaryota Metazoa Mus musculus . . . . . . . . . . . . domesticus 5995 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 5995 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $MUP-I . 'recombinant technology' . . . . . . . . . . . . . . . . 5995 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 5995 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system . _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'Major Urinary Protein-I' '[U-95% 15N]' . . 1 $MUP-I . . 1.8 . . mM . . . . 5995 1 stop_ save_ ####################### # Sample conditions # ####################### save_283K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 283K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 1 temperature 283 1 K 5995 1 stop_ save_ save_288K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 288K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 2 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 2 temperature 288 1 K 5995 2 stop_ save_ save_293K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 293K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 3 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 3 temperature 293 1 K 5995 3 stop_ save_ save_298K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 298K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 4 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 4 temperature 298 1 K 5995 4 stop_ save_ save_303K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 303K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 5 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 5 temperature 303 1 K 5995 5 stop_ save_ save_308K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 308K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 6 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 6 temperature 308 1 K 5995 6 stop_ save_ save_291K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 291K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 7 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 7 temperature 291 1 K 5995 7 stop_ save_ save_297K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 297K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 8 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 8 temperature 297 1 K 5995 8 stop_ save_ save_302K _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode 302K _Sample_condition_list.Entry_ID 5995 _Sample_condition_list.ID 9 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.3 0.2 n/a 5995 9 temperature 302 1 K 5995 9 stop_ save_ ############################ # Computer software used # ############################ save_NMRPipe _Software.Sf_category software _Software.Sf_framecode NMRPipe _Software.Entry_ID 5995 _Software.ID 1 _Software.Name NMRPipe _Software.Version . _Software.Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 5995 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_NMR_spectrometer_2 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_2 _NMR_spectrometer.Entry_ID 5995 _NMR_spectrometer.ID 2 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DRX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 500 save_ save_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode spectrometer_list _NMR_spectrometer_list.Entry_ID 5995 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 NMR_spectrometer_1 Bruker Avance . 600 . . . 5995 1 2 NMR_spectrometer_2 Bruker DRX . 500 . . . 5995 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 5995 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '15N T1' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5995 1 2 '15N T2' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5995 1 3 '{1H}-15N NOE' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5995 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference _Chem_shift_reference.Entry_ID 5995 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 DSS 'methyl protons' . . . . ppm 0.0 internal direct 1.0 . . . . . 5995 1 N 15 DSS 'methyl protons' . . . . ppm 0.0 . indirect 0.101329118 . . . . . 5995 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_chemical_shift_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode chemical_shift_1 _Assigned_chem_shift_list.Entry_ID 5995 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $283K _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '15N T1' 1 $sample_1 . 5995 1 2 '15N T2' 1 $sample_1 . 5995 1 3 '{1H}-15N NOE' 1 $sample_1 . 5995 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 2 2 GLU H H 1 8.399 0.01 . 1 . . . . . . . . 5995 1 2 . 1 1 2 2 GLU N N 15 119.915 0.10 . 1 . . . . . . . . 5995 1 3 . 1 1 3 3 ALA H H 1 8.832 0.01 . 1 . . . . . . . . 5995 1 4 . 1 1 3 3 ALA N N 15 124.770 0.10 . 1 . . . . . . . . 5995 1 5 . 1 1 4 4 SER H H 1 8.130 0.01 . 1 . . . . . . . . 5995 1 6 . 1 1 4 4 SER N N 15 111.840 0.10 . 1 . . . . . . . . 5995 1 7 . 1 1 5 5 SER H H 1 9.265 0.01 . 1 . . . . . . . . 5995 1 8 . 1 1 5 5 SER N N 15 120.290 0.10 . 1 . . . . . . . . 5995 1 9 . 1 1 6 6 THR H H 1 7.111 0.01 . 1 . . . . . . . . 5995 1 10 . 1 1 6 6 THR N N 15 108.350 0.10 . 1 . . . . . . . . 5995 1 11 . 1 1 7 7 GLY H H 1 7.570 0.01 . 1 . . . . . . . . 5995 1 12 . 1 1 7 7 GLY N N 15 111.128 0.10 . 1 . . . . . . . . 5995 1 13 . 1 1 8 8 ARG H H 1 8.637 0.01 . 1 . . . . . . . . 5995 1 14 . 1 1 8 8 ARG N N 15 120.540 0.10 . 1 . . . . . . . . 5995 1 15 . 1 1 9 9 ASN H H 1 8.667 0.01 . 1 . . . . . . . . 5995 1 16 . 1 1 9 9 ASN N N 15 115.099 0.10 . 1 . . . . . . . . 5995 1 17 . 1 1 10 10 PHE H H 1 7.789 0.01 . 1 . . . . . . . . 5995 1 18 . 1 1 10 10 PHE N N 15 121.591 0.10 . 1 . . . . . . . . 5995 1 19 . 1 1 11 11 ASN H H 1 7.687 0.01 . 1 . . . . . . . . 5995 1 20 . 1 1 11 11 ASN N N 15 127.700 0.10 . 1 . . . . . . . . 5995 1 21 . 1 1 12 12 VAL H H 1 8.128 0.01 . 1 . . . . . . . . 5995 1 22 . 1 1 12 12 VAL N N 15 123.270 0.10 . 1 . . . . . . . . 5995 1 23 . 1 1 13 13 GLU H H 1 8.039 0.01 . 1 . . . . . . . . 5995 1 24 . 1 1 13 13 GLU N N 15 118.050 0.10 . 1 . . . . . . . . 5995 1 25 . 1 1 14 14 LYS H H 1 7.335 0.01 . 1 . . . . . . . . 5995 1 26 . 1 1 14 14 LYS N N 15 114.570 0.10 . 1 . . . . . . . . 5995 1 27 . 1 1 15 15 ILE H H 1 7.635 0.01 . 1 . . . . . . . . 5995 1 28 . 1 1 15 15 ILE N N 15 110.100 0.10 . 1 . . . . . . . . 5995 1 29 . 1 1 16 16 ASN H H 1 7.096 0.01 . 1 . . . . . . . . 5995 1 30 . 1 1 16 16 ASN N N 15 119.050 0.10 . 1 . . . . . . . . 5995 1 31 . 1 1 17 17 GLY H H 1 9.355 0.01 . 1 . . . . . . . . 5995 1 32 . 1 1 17 17 GLY N N 15 111.590 0.10 . 1 . . . . . . . . 5995 1 33 . 1 1 18 18 GLU H H 1 8.563 0.01 . 1 . . . . . . . . 5995 1 34 . 1 1 18 18 GLU N N 15 118.800 0.10 . 1 . . . . . . . . 5995 1 35 . 1 1 19 19 TRP H H 1 10.151 0.01 . 1 . . . . . . . . 5995 1 36 . 1 1 19 19 TRP N N 15 129.087 0.10 . 1 . . . . . . . . 5995 1 37 . 1 1 20 20 HIS H H 1 8.906 0.01 . 1 . . . . . . . . 5995 1 38 . 1 1 20 20 HIS N N 15 112.327 0.10 . 1 . . . . . . . . 5995 1 39 . 1 1 21 21 THR H H 1 10.418 0.01 . 1 . . . . . . . . 5995 1 40 . 1 1 21 21 THR N N 15 122.230 0.10 . 1 . . . . . . . . 5995 1 41 . 1 1 22 22 ILE H H 1 8.957 0.01 . 1 . . . . . . . . 5995 1 42 . 1 1 22 22 ILE N N 15 127.750 0.10 . 1 . . . . . . . . 5995 1 43 . 1 1 23 23 ILE H H 1 7.470 0.01 . 1 . . . . . . . . 5995 1 44 . 1 1 23 23 ILE N N 15 114.570 0.10 . 1 . . . . . . . . 5995 1 45 . 1 1 24 24 LEU H H 1 8.263 0.01 . 1 . . . . . . . . 5995 1 46 . 1 1 24 24 LEU N N 15 122.780 0.10 . 1 . . . . . . . . 5995 1 47 . 1 1 25 25 ALA H H 1 9.040 0.01 . 1 . . . . . . . . 5995 1 48 . 1 1 25 25 ALA N N 15 122.382 0.10 . 1 . . . . . . . . 5995 1 49 . 1 1 26 26 SER H H 1 7.320 0.01 . 1 . . . . . . . . 5995 1 50 . 1 1 26 26 SER N N 15 112.080 0.10 . 1 . . . . . . . . 5995 1 51 . 1 1 27 27 ASP H H 1 8.682 0.01 . 1 . . . . . . . . 5995 1 52 . 1 1 27 27 ASP N N 15 122.780 0.10 . 1 . . . . . . . . 5995 1 53 . 1 1 28 28 LYS H H 1 8.218 0.01 . 1 . . . . . . . . 5995 1 54 . 1 1 28 28 LYS N N 15 126.257 0.10 . 1 . . . . . . . . 5995 1 55 . 1 1 29 29 ARG H H 1 8.772 0.01 . 1 . . . . . . . . 5995 1 56 . 1 1 29 29 ARG N N 15 126.928 0.10 . 1 . . . . . . . . 5995 1 57 . 1 1 30 30 GLU H H 1 9.355 0.01 . 1 . . . . . . . . 5995 1 58 . 1 1 30 30 GLU N N 15 114.558 0.10 . 1 . . . . . . . . 5995 1 59 . 1 1 31 31 LYS H H 1 7.455 0.01 . 1 . . . . . . . . 5995 1 60 . 1 1 31 31 LYS N N 15 116.046 0.10 . 1 . . . . . . . . 5995 1 61 . 1 1 32 32 ILE H H 1 7.470 0.01 . 1 . . . . . . . . 5995 1 62 . 1 1 32 32 ILE N N 15 106.444 0.10 . 1 . . . . . . . . 5995 1 63 . 1 1 33 33 GLU H H 1 6.587 0.01 . 1 . . . . . . . . 5995 1 64 . 1 1 33 33 GLU N N 15 121.040 0.10 . 1 . . . . . . . . 5995 1 65 . 1 1 34 34 ASP H H 1 8.368 0.01 . 1 . . . . . . . . 5995 1 66 . 1 1 34 34 ASP N N 15 117.939 0.10 . 1 . . . . . . . . 5995 1 67 . 1 1 35 35 ASN H H 1 8.921 0.01 . 1 . . . . . . . . 5995 1 68 . 1 1 35 35 ASN N N 15 116.560 0.10 . 1 . . . . . . . . 5995 1 69 . 1 1 36 36 GLY H H 1 8.742 0.01 . 1 . . . . . . . . 5995 1 70 . 1 1 36 36 GLY N N 15 110.100 0.10 . 1 . . . . . . . . 5995 1 71 . 1 1 37 37 ASN H H 1 9.310 0.01 . 1 . . . . . . . . 5995 1 72 . 1 1 37 37 ASN N N 15 121.185 0.10 . 1 . . . . . . . . 5995 1 73 . 1 1 38 38 PHE H H 1 8.562 0.01 . 1 . . . . . . . . 5995 1 74 . 1 1 38 38 PHE N N 15 114.964 0.10 . 1 . . . . . . . . 5995 1 75 . 1 1 39 39 ARG H H 1 7.126 0.01 . 1 . . . . . . . . 5995 1 76 . 1 1 39 39 ARG N N 15 124.025 0.10 . 1 . . . . . . . . 5995 1 77 . 1 1 40 40 LEU H H 1 6.632 0.01 . 1 . . . . . . . . 5995 1 78 . 1 1 40 40 LEU N N 15 124.020 0.10 . 1 . . . . . . . . 5995 1 79 . 1 1 41 41 PHE H H 1 8.622 0.01 . 1 . . . . . . . . 5995 1 80 . 1 1 41 41 PHE N N 15 124.020 0.10 . 1 . . . . . . . . 5995 1 81 . 1 1 42 42 LEU H H 1 8.383 0.01 . 1 . . . . . . . . 5995 1 82 . 1 1 42 42 LEU N N 15 128.990 0.10 . 1 . . . . . . . . 5995 1 83 . 1 1 43 43 GLU H H 1 8.996 0.01 . 1 . . . . . . . . 5995 1 84 . 1 1 43 43 GLU N N 15 121.020 0.10 . 1 . . . . . . . . 5995 1 85 . 1 1 44 44 GLN H H 1 7.350 0.01 . 1 . . . . . . . . 5995 1 86 . 1 1 44 44 GLN N N 15 114.558 0.10 . 1 . . . . . . . . 5995 1 87 . 1 1 45 45 ILE H H 1 8.772 0.01 . 1 . . . . . . . . 5995 1 88 . 1 1 45 45 ILE N N 15 120.577 0.10 . 1 . . . . . . . . 5995 1 89 . 1 1 46 46 HIS H H 1 9.370 0.01 . 1 . . . . . . . . 5995 1 90 . 1 1 46 46 HIS N N 15 126.595 0.10 . 1 . . . . . . . . 5995 1 91 . 1 1 47 47 VAL H H 1 8.787 0.01 . 1 . . . . . . . . 5995 1 92 . 1 1 47 47 VAL N N 15 127.338 0.10 . 1 . . . . . . . . 5995 1 93 . 1 1 48 48 LEU H H 1 8.188 0.01 . 1 . . . . . . . . 5995 1 94 . 1 1 48 48 LEU N N 15 129.740 0.10 . 1 . . . . . . . . 5995 1 95 . 1 1 49 49 GLU H H 1 8.622 0.01 . 1 . . . . . . . . 5995 1 96 . 1 1 49 49 GLU N N 15 119.790 0.10 . 1 . . . . . . . . 5995 1 97 . 1 1 50 50 ASN H H 1 8.592 0.01 . 1 . . . . . . . . 5995 1 98 . 1 1 50 50 ASN N N 15 114.840 0.10 . 1 . . . . . . . . 5995 1 99 . 1 1 51 51 SER H H 1 7.485 0.01 . 1 . . . . . . . . 5995 1 100 . 1 1 51 51 SER N N 15 111.921 0.10 . 1 . . . . . . . . 5995 1 101 . 1 1 52 52 LEU H H 1 9.086 0.01 . 1 . . . . . . . . 5995 1 102 . 1 1 52 52 LEU N N 15 119.050 0.10 . 1 . . . . . . . . 5995 1 103 . 1 1 53 53 VAL H H 1 9.161 0.01 . 1 . . . . . . . . 5995 1 104 . 1 1 53 53 VAL N N 15 122.280 0.10 . 1 . . . . . . . . 5995 1 105 . 1 1 54 54 LEU H H 1 9.086 0.01 . 1 . . . . . . . . 5995 1 106 . 1 1 54 54 LEU N N 15 128.990 0.10 . 1 . . . . . . . . 5995 1 107 . 1 1 55 55 LYS H H 1 8.113 0.01 . 1 . . . . . . . . 5995 1 108 . 1 1 55 55 LYS N N 15 122.280 0.10 . 1 . . . . . . . . 5995 1 109 . 1 1 56 56 PHE H H 1 9.191 0.01 . 1 . . . . . . . . 5995 1 110 . 1 1 56 56 PHE N N 15 122.537 0.10 . 1 . . . . . . . . 5995 1 111 . 1 1 57 57 HIS H H 1 8.981 0.01 . 1 . . . . . . . . 5995 1 112 . 1 1 57 57 HIS N N 15 113.409 0.10 . 1 . . . . . . . . 5995 1 113 . 1 1 58 58 THR H H 1 9.041 0.01 . 1 . . . . . . . . 5995 1 114 . 1 1 58 58 THR N N 15 112.462 0.10 . 1 . . . . . . . . 5995 1 115 . 1 1 59 59 VAL H H 1 9.071 0.01 . 1 . . . . . . . . 5995 1 116 . 1 1 59 59 VAL N N 15 122.061 0.10 . 1 . . . . . . . . 5995 1 117 . 1 1 60 60 ARG H H 1 8.375 0.01 . 1 . . . . . . . . 5995 1 118 . 1 1 60 60 ARG N N 15 127.265 0.10 . 1 . . . . . . . . 5995 1 119 . 1 1 61 61 ASP H H 1 9.430 0.01 . 1 . . . . . . . . 5995 1 120 . 1 1 61 61 ASP N N 15 127.193 0.10 . 1 . . . . . . . . 5995 1 121 . 1 1 62 62 GLU H H 1 8.375 0.01 . 1 . . . . . . . . 5995 1 122 . 1 1 62 62 GLU N N 15 110.434 0.10 . 1 . . . . . . . . 5995 1 123 . 1 1 63 63 GLU H H 1 7.977 0.01 . 1 . . . . . . . . 5995 1 124 . 1 1 63 63 GLU N N 15 120.540 0.10 . 1 . . . . . . . . 5995 1 125 . 1 1 64 64 CYS H H 1 8.996 0.01 . 1 . . . . . . . . 5995 1 126 . 1 1 64 64 CYS N N 15 124.160 0.10 . 1 . . . . . . . . 5995 1 127 . 1 1 65 65 SER H H 1 8.861 0.01 . 1 . . . . . . . . 5995 1 128 . 1 1 65 65 SER N N 15 118.413 0.10 . 1 . . . . . . . . 5995 1 129 . 1 1 66 66 GLU H H 1 8.708 0.01 . 1 . . . . . . . . 5995 1 130 . 1 1 66 66 GLU N N 15 124.020 0.10 . 1 . . . . . . . . 5995 1 131 . 1 1 67 67 LEU H H 1 8.582 0.01 . 1 . . . . . . . . 5995 1 132 . 1 1 67 67 LEU N N 15 124.972 0.10 . 1 . . . . . . . . 5995 1 133 . 1 1 68 68 SER H H 1 8.563 0.01 . 1 . . . . . . . . 5995 1 134 . 1 1 68 68 SER N N 15 118.751 0.10 . 1 . . . . . . . . 5995 1 135 . 1 1 69 69 MET H H 1 9.250 0.01 . 1 . . . . . . . . 5995 1 136 . 1 1 69 69 MET N N 15 120.306 0.10 . 1 . . . . . . . . 5995 1 137 . 1 1 70 70 VAL H H 1 8.592 0.01 . 1 . . . . . . . . 5995 1 138 . 1 1 70 70 VAL N N 15 122.280 0.10 . 1 . . . . . . . . 5995 1 139 . 1 1 71 71 ALA H H 1 9.475 0.01 . 1 . . . . . . . . 5995 1 140 . 1 1 71 71 ALA N N 15 130.980 0.10 . 1 . . . . . . . . 5995 1 141 . 1 1 72 72 ASP H H 1 8.891 0.01 . 1 . . . . . . . . 5995 1 142 . 1 1 72 72 ASP N N 15 123.270 0.10 . 1 . . . . . . . . 5995 1 143 . 1 1 73 73 LYS H H 1 8.188 0.01 . 1 . . . . . . . . 5995 1 144 . 1 1 73 73 LYS N N 15 120.712 0.10 . 1 . . . . . . . . 5995 1 145 . 1 1 74 74 THR H H 1 7.829 0.01 . 1 . . . . . . . . 5995 1 146 . 1 1 74 74 THR N N 15 114.570 0.10 . 1 . . . . . . . . 5995 1 147 . 1 1 75 75 GLU H H 1 8.661 0.01 . 1 . . . . . . . . 5995 1 148 . 1 1 75 75 GLU N N 15 116.560 0.10 . 1 . . . . . . . . 5995 1 149 . 1 1 76 76 LYS H H 1 7.983 0.01 . 1 . . . . . . . . 5995 1 150 . 1 1 76 76 LYS N N 15 121.780 0.10 . 1 . . . . . . . . 5995 1 151 . 1 1 77 77 ALA H H 1 8.267 0.01 . 1 . . . . . . . . 5995 1 152 . 1 1 77 77 ALA N N 15 127.750 0.10 . 1 . . . . . . . . 5995 1 153 . 1 1 78 78 GLY H H 1 8.375 0.01 . 1 . . . . . . . . 5995 1 154 . 1 1 78 78 GLY N N 15 108.276 0.10 . 1 . . . . . . . . 5995 1 155 . 1 1 79 79 GLU H H 1 7.290 0.01 . 1 . . . . . . . . 5995 1 156 . 1 1 79 79 GLU N N 15 120.290 0.10 . 1 . . . . . . . . 5995 1 157 . 1 1 80 80 TYR H H 1 8.637 0.01 . 1 . . . . . . . . 5995 1 158 . 1 1 80 80 TYR N N 15 125.510 0.10 . 1 . . . . . . . . 5995 1 159 . 1 1 81 81 SER H H 1 9.595 0.01 . 1 . . . . . . . . 5995 1 160 . 1 1 81 81 SER N N 15 114.491 0.10 . 1 . . . . . . . . 5995 1 161 . 1 1 82 82 VAL H H 1 8.592 0.01 . 1 . . . . . . . . 5995 1 162 . 1 1 82 82 VAL N N 15 117.550 0.10 . 1 . . . . . . . . 5995 1 163 . 1 1 83 83 THR H H 1 9.370 0.01 . 1 . . . . . . . . 5995 1 164 . 1 1 83 83 THR N N 15 128.250 0.10 . 1 . . . . . . . . 5995 1 165 . 1 1 84 84 TYR H H 1 8.637 0.01 . 1 . . . . . . . . 5995 1 166 . 1 1 84 84 TYR N N 15 128.490 0.10 . 1 . . . . . . . . 5995 1 167 . 1 1 85 85 ASP H H 1 8.547 0.01 . 1 . . . . . . . . 5995 1 168 . 1 1 85 85 ASP N N 15 129.990 0.10 . 1 . . . . . . . . 5995 1 169 . 1 1 86 86 GLY H H 1 7.799 0.01 . 1 . . . . . . . . 5995 1 170 . 1 1 86 86 GLY N N 15 102.880 0.10 . 1 . . . . . . . . 5995 1 171 . 1 1 87 87 PHE H H 1 8.413 0.01 . 1 . . . . . . . . 5995 1 172 . 1 1 87 87 PHE N N 15 120.441 0.10 . 1 . . . . . . . . 5995 1 173 . 1 1 88 88 ASN H H 1 7.979 0.01 . 1 . . . . . . . . 5995 1 174 . 1 1 88 88 ASN N N 15 122.780 0.10 . 1 . . . . . . . . 5995 1 175 . 1 1 89 89 THR H H 1 8.697 0.01 . 1 . . . . . . . . 5995 1 176 . 1 1 89 89 THR N N 15 113.080 0.10 . 1 . . . . . . . . 5995 1 177 . 1 1 90 90 PHE H H 1 9.350 0.01 . 1 . . . . . . . . 5995 1 178 . 1 1 90 90 PHE N N 15 120.238 0.10 . 1 . . . . . . . . 5995 1 179 . 1 1 91 91 THR H H 1 8.622 0.01 . 1 . . . . . . . . 5995 1 180 . 1 1 91 91 THR N N 15 110.340 0.10 . 1 . . . . . . . . 5995 1 181 . 1 1 92 92 ILE H H 1 8.158 0.01 . 1 . . . . . . . . 5995 1 182 . 1 1 92 92 ILE N N 15 119.050 0.10 . 1 . . . . . . . . 5995 1 183 . 1 1 94 94 LYS H H 1 6.901 0.01 . 1 . . . . . . . . 5995 1 184 . 1 1 94 94 LYS N N 15 111.340 0.10 . 1 . . . . . . . . 5995 1 185 . 1 1 95 95 THR H H 1 8.722 0.01 . 1 . . . . . . . . 5995 1 186 . 1 1 95 95 THR N N 15 119.050 0.10 . 1 . . . . . . . . 5995 1 187 . 1 1 96 96 ASP H H 1 6.872 0.01 . 1 . . . . . . . . 5995 1 188 . 1 1 96 96 ASP N N 15 124.520 0.10 . 1 . . . . . . . . 5995 1 189 . 1 1 97 97 TYR H H 1 8.742 0.01 . 1 . . . . . . . . 5995 1 190 . 1 1 97 97 TYR N N 15 115.570 0.10 . 1 . . . . . . . . 5995 1 191 . 1 1 98 98 ASP H H 1 9.310 0.01 . 1 . . . . . . . . 5995 1 192 . 1 1 98 98 ASP N N 15 119.427 0.10 . 1 . . . . . . . . 5995 1 193 . 1 1 99 99 ASN H H 1 8.891 0.01 . 1 . . . . . . . . 5995 1 194 . 1 1 99 99 ASN N N 15 116.810 0.10 . 1 . . . . . . . . 5995 1 195 . 1 1 100 100 PHE H H 1 9.804 0.01 . 1 . . . . . . . . 5995 1 196 . 1 1 100 100 PHE N N 15 117.310 0.10 . 1 . . . . . . . . 5995 1 197 . 1 1 101 101 LEU H H 1 9.323 0.01 . 1 . . . . . . . . 5995 1 198 . 1 1 101 101 LEU N N 15 126.010 0.10 . 1 . . . . . . . . 5995 1 199 . 1 1 102 102 MET H H 1 9.071 0.01 . 1 . . . . . . . . 5995 1 200 . 1 1 102 102 MET N N 15 125.039 0.10 . 1 . . . . . . . . 5995 1 201 . 1 1 103 103 ALA H H 1 9.323 0.01 . 1 . . . . . . . . 5995 1 202 . 1 1 103 103 ALA N N 15 121.780 0.10 . 1 . . . . . . . . 5995 1 203 . 1 1 104 104 HIS H H 1 8.582 0.01 . 1 . . . . . . . . 5995 1 204 . 1 1 104 104 HIS N N 15 120.849 0.10 . 1 . . . . . . . . 5995 1 205 . 1 1 105 105 LEU H H 1 9.596 0.01 . 1 . . . . . . . . 5995 1 206 . 1 1 105 105 LEU N N 15 131.939 0.10 . 1 . . . . . . . . 5995 1 207 . 1 1 106 106 ILE H H 1 8.981 0.01 . 1 . . . . . . . . 5995 1 208 . 1 1 106 106 ILE N N 15 125.039 0.10 . 1 . . . . . . . . 5995 1 209 . 1 1 107 107 ASN H H 1 8.308 0.01 . 1 . . . . . . . . 5995 1 210 . 1 1 107 107 ASN N N 15 128.260 0.10 . 1 . . . . . . . . 5995 1 211 . 1 1 108 108 GLU H H 1 8.891 0.01 . 1 . . . . . . . . 5995 1 212 . 1 1 108 108 GLU N N 15 124.020 0.10 . 1 . . . . . . . . 5995 1 213 . 1 1 109 109 LYS H H 1 8.652 0.01 . 1 . . . . . . . . 5995 1 214 . 1 1 109 109 LYS N N 15 126.054 0.10 . 1 . . . . . . . . 5995 1 215 . 1 1 110 110 ASP H H 1 9.505 0.01 . 1 . . . . . . . . 5995 1 216 . 1 1 110 110 ASP N N 15 129.010 0.10 . 1 . . . . . . . . 5995 1 217 . 1 1 111 111 GLY H H 1 8.787 0.01 . 1 . . . . . . . . 5995 1 218 . 1 1 111 111 GLY N N 15 104.130 0.10 . 1 . . . . . . . . 5995 1 219 . 1 1 112 112 GLU H H 1 7.964 0.01 . 1 . . . . . . . . 5995 1 220 . 1 1 112 112 GLU N N 15 120.540 0.10 . 1 . . . . . . . . 5995 1 221 . 1 1 113 113 THR H H 1 8.712 0.01 . 1 . . . . . . . . 5995 1 222 . 1 1 113 113 THR N N 15 117.601 0.10 . 1 . . . . . . . . 5995 1 223 . 1 1 114 114 PHE H H 1 8.443 0.01 . 1 . . . . . . . . 5995 1 224 . 1 1 114 114 PHE N N 15 120.280 0.10 . 1 . . . . . . . . 5995 1 225 . 1 1 115 115 GLN H H 1 9.977 0.01 . 1 . . . . . . . . 5995 1 226 . 1 1 115 115 GLN N N 15 118.260 0.10 . 1 . . . . . . . . 5995 1 227 . 1 1 116 116 LEU H H 1 9.490 0.01 . 1 . . . . . . . . 5995 1 228 . 1 1 116 116 LEU N N 15 125.510 0.10 . 1 . . . . . . . . 5995 1 229 . 1 1 117 117 MET H H 1 9.460 0.01 . 1 . . . . . . . . 5995 1 230 . 1 1 117 117 MET N N 15 125.010 0.10 . 1 . . . . . . . . 5995 1 231 . 1 1 118 118 GLY H H 1 8.772 0.01 . 1 . . . . . . . . 5995 1 232 . 1 1 118 118 GLY N N 15 109.555 0.10 . 1 . . . . . . . . 5995 1 233 . 1 1 119 119 LEU H H 1 8.248 0.01 . 1 . . . . . . . . 5995 1 234 . 1 1 119 119 LEU N N 15 124.270 0.10 . 1 . . . . . . . . 5995 1 235 . 1 1 120 120 TYR H H 1 9.323 0.01 . 1 . . . . . . . . 5995 1 236 . 1 1 120 120 TYR N N 15 125.981 0.10 . 1 . . . . . . . . 5995 1 237 . 1 1 121 121 GLY H H 1 9.518 0.01 . 1 . . . . . . . . 5995 1 238 . 1 1 121 121 GLY N N 15 108.276 0.10 . 1 . . . . . . . . 5995 1 239 . 1 1 122 122 ARG H H 1 8.218 0.01 . 1 . . . . . . . . 5995 1 240 . 1 1 122 122 ARG N N 15 120.712 0.10 . 1 . . . . . . . . 5995 1 241 . 1 1 123 123 GLU H H 1 8.460 0.01 . 1 . . . . . . . . 5995 1 242 . 1 1 123 123 GLU N N 15 118.528 0.10 . 1 . . . . . . . . 5995 1 243 . 1 1 125 125 ASP H H 1 7.156 0.01 . 1 . . . . . . . . 5995 1 244 . 1 1 125 125 ASP N N 15 113.820 0.10 . 1 . . . . . . . . 5995 1 245 . 1 1 126 126 LEU H H 1 8.443 0.01 . 1 . . . . . . . . 5995 1 246 . 1 1 126 126 LEU N N 15 123.484 0.10 . 1 . . . . . . . . 5995 1 247 . 1 1 127 127 SER H H 1 8.158 0.01 . 1 . . . . . . . . 5995 1 248 . 1 1 127 127 SER N N 15 114.320 0.10 . 1 . . . . . . . . 5995 1 249 . 1 1 128 128 SER H H 1 8.947 0.01 . 1 . . . . . . . . 5995 1 250 . 1 1 128 128 SER N N 15 117.820 0.10 . 1 . . . . . . . . 5995 1 251 . 1 1 129 129 ASP H H 1 8.472 0.01 . 1 . . . . . . . . 5995 1 252 . 1 1 129 129 ASP N N 15 120.790 0.10 . 1 . . . . . . . . 5995 1 253 . 1 1 130 130 ILE H H 1 7.380 0.01 . 1 . . . . . . . . 5995 1 254 . 1 1 130 130 ILE N N 15 121.530 0.10 . 1 . . . . . . . . 5995 1 255 . 1 1 131 131 LYS H H 1 7.575 0.01 . 1 . . . . . . . . 5995 1 256 . 1 1 131 131 LYS N N 15 118.818 0.10 . 1 . . . . . . . . 5995 1 257 . 1 1 132 132 GLU H H 1 8.293 0.01 . 1 . . . . . . . . 5995 1 258 . 1 1 132 132 GLU N N 15 120.712 0.10 . 1 . . . . . . . . 5995 1 259 . 1 1 133 133 ARG H H 1 7.700 0.01 . 1 . . . . . . . . 5995 1 260 . 1 1 133 133 ARG N N 15 120.790 0.10 . 1 . . . . . . . . 5995 1 261 . 1 1 134 134 PHE H H 1 8.413 0.01 . 1 . . . . . . . . 5995 1 262 . 1 1 134 134 PHE N N 15 119.900 0.10 . 1 . . . . . . . . 5995 1 263 . 1 1 135 135 ALA H H 1 8.263 0.01 . 1 . . . . . . . . 5995 1 264 . 1 1 135 135 ALA N N 15 124.270 0.10 . 1 . . . . . . . . 5995 1 265 . 1 1 136 136 GLN H H 1 8.039 0.01 . 1 . . . . . . . . 5995 1 266 . 1 1 136 136 GLN N N 15 115.776 0.10 . 1 . . . . . . . . 5995 1 267 . 1 1 137 137 LEU H H 1 7.515 0.01 . 1 . . . . . . . . 5995 1 268 . 1 1 137 137 LEU N N 15 122.740 0.10 . 1 . . . . . . . . 5995 1 269 . 1 1 138 138 CYS H H 1 8.128 0.01 . 1 . . . . . . . . 5995 1 270 . 1 1 138 138 CYS N N 15 120.577 0.10 . 1 . . . . . . . . 5995 1 271 . 1 1 139 139 GLU H H 1 7.977 0.01 . 1 . . . . . . . . 5995 1 272 . 1 1 139 139 GLU N N 15 120.455 0.10 . 1 . . . . . . . . 5995 1 273 . 1 1 140 140 LYS H H 1 7.679 0.01 . 1 . . . . . . . . 5995 1 274 . 1 1 140 140 LYS N N 15 120.374 0.10 . 1 . . . . . . . . 5995 1 275 . 1 1 141 141 HIS H H 1 7.335 0.01 . 1 . . . . . . . . 5995 1 276 . 1 1 141 141 HIS N N 15 114.694 0.10 . 1 . . . . . . . . 5995 1 277 . 1 1 142 142 GLY H H 1 7.739 0.01 . 1 . . . . . . . . 5995 1 278 . 1 1 142 142 GLY N N 15 106.610 0.10 . 1 . . . . . . . . 5995 1 279 . 1 1 143 143 ILE H H 1 7.814 0.01 . 1 . . . . . . . . 5995 1 280 . 1 1 143 143 ILE N N 15 122.030 0.10 . 1 . . . . . . . . 5995 1 281 . 1 1 144 144 LEU H H 1 7.979 0.01 . 1 . . . . . . . . 5995 1 282 . 1 1 144 144 LEU N N 15 125.010 0.10 . 1 . . . . . . . . 5995 1 283 . 1 1 145 145 ARG H H 1 8.637 0.01 . 1 . . . . . . . . 5995 1 284 . 1 1 145 145 ARG N N 15 119.427 0.10 . 1 . . . . . . . . 5995 1 285 . 1 1 146 146 GLU H H 1 8.772 0.01 . 1 . . . . . . . . 5995 1 286 . 1 1 146 146 GLU N N 15 116.560 0.10 . 1 . . . . . . . . 5995 1 287 . 1 1 147 147 ASN H H 1 8.188 0.01 . 1 . . . . . . . . 5995 1 288 . 1 1 147 147 ASN N N 15 120.540 0.10 . 1 . . . . . . . . 5995 1 289 . 1 1 148 148 ILE H H 1 7.051 0.01 . 1 . . . . . . . . 5995 1 290 . 1 1 148 148 ILE N N 15 118.300 0.10 . 1 . . . . . . . . 5995 1 291 . 1 1 149 149 ILE H H 1 9.340 0.01 . 1 . . . . . . . . 5995 1 292 . 1 1 149 149 ILE N N 15 128.285 0.10 . 1 . . . . . . . . 5995 1 293 . 1 1 150 150 ASP H H 1 8.697 0.01 . 1 . . . . . . . . 5995 1 294 . 1 1 150 150 ASP N N 15 127.250 0.10 . 1 . . . . . . . . 5995 1 295 . 1 1 151 151 LEU H H 1 8.921 0.01 . 1 . . . . . . . . 5995 1 296 . 1 1 151 151 LEU N N 15 129.840 0.10 . 1 . . . . . . . . 5995 1 297 . 1 1 152 152 SER H H 1 9.041 0.01 . 1 . . . . . . . . 5995 1 298 . 1 1 152 152 SER N N 15 118.800 0.10 . 1 . . . . . . . . 5995 1 299 . 1 1 153 153 ASN H H 1 8.400 0.01 . 1 . . . . . . . . 5995 1 300 . 1 1 153 153 ASN N N 15 117.306 0.10 . 1 . . . . . . . . 5995 1 301 . 1 1 154 154 ALA H H 1 7.790 0.01 . 1 . . . . . . . . 5995 1 302 . 1 1 154 154 ALA N N 15 122.020 0.10 . 1 . . . . . . . . 5995 1 303 . 1 1 155 155 ASN H H 1 8.009 0.01 . 1 . . . . . . . . 5995 1 304 . 1 1 155 155 ASN N N 15 117.060 0.10 . 1 . . . . . . . . 5995 1 305 . 1 1 156 156 ARG H H 1 7.883 0.01 . 1 . . . . . . . . 5995 1 306 . 1 1 156 156 ARG N N 15 121.780 0.10 . 1 . . . . . . . . 5995 1 307 . 1 1 157 157 CYS H H 1 8.293 0.01 . 1 . . . . . . . . 5995 1 308 . 1 1 157 157 CYS N N 15 118.075 0.10 . 1 . . . . . . . . 5995 1 309 . 1 1 158 158 LEU H H 1 8.068 0.01 . 1 . . . . . . . . 5995 1 310 . 1 1 158 158 LEU N N 15 122.537 0.10 . 1 . . . . . . . . 5995 1 311 . 1 1 159 159 GLN H H 1 8.282 0.01 . 1 . . . . . . . . 5995 1 312 . 1 1 159 159 GLN N N 15 120.917 0.10 . 1 . . . . . . . . 5995 1 313 . 1 1 160 160 ALA H H 1 8.233 0.01 . 1 . . . . . . . . 5995 1 314 . 1 1 160 160 ALA N N 15 125.760 0.10 . 1 . . . . . . . . 5995 1 315 . 1 1 161 161 ARG H H 1 8.218 0.01 . 1 . . . . . . . . 5995 1 316 . 1 1 161 161 ARG N N 15 120.847 0.10 . 1 . . . . . . . . 5995 1 317 . 1 1 162 162 GLU H H 1 7.964 0.01 . 1 . . . . . . . . 5995 1 318 . 1 1 162 162 GLU N N 15 126.730 0.10 . 1 . . . . . . . . 5995 1 stop_ save_ ############################## # Heteronuclear NOE values # ############################## save_283_600_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 283_600_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 1 _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $283K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 1 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.70 0.05 . . . . . . . . . . 5995 1 2 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.74 0.04 . . . . . . . . . . 5995 1 3 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.73 0.02 . . . . . . . . . . 5995 1 4 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.74 0.01 . . . . . . . . . . 5995 1 5 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.79 0.01 . . . . . . . . . . 5995 1 6 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.73 0.04 . . . . . . . . . . 5995 1 7 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.88 0.03 . . . . . . . . . . 5995 1 8 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.82 0.01 . . . . . . . . . . 5995 1 9 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.80 0.04 . . . . . . . . . . 5995 1 10 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.72 0.08 . . . . . . . . . . 5995 1 11 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.79 0.01 . . . . . . . . . . 5995 1 12 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.83 0.01 . . . . . . . . . . 5995 1 13 . 1 1 28 28 LYS N N 15 . 1 1 28 28 LYS H H 1 0.78 0.01 . . . . . . . . . . 5995 1 14 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.78 0.00 . . . . . . . . . . 5995 1 15 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.78 0.01 . . . . . . . . . . 5995 1 16 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.84 0.04 . . . . . . . . . . 5995 1 17 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.85 0.03 . . . . . . . . . . 5995 1 18 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.75 0.03 . . . . . . . . . . 5995 1 19 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.81 0.12 . . . . . . . . . . 5995 1 20 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.79 0.02 . . . . . . . . . . 5995 1 21 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.80 0.02 . . . . . . . . . . 5995 1 22 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.71 0.02 . . . . . . . . . . 5995 1 23 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.78 0.08 . . . . . . . . . . 5995 1 24 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.73 0.05 . . . . . . . . . . 5995 1 25 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.76 0.02 . . . . . . . . . . 5995 1 26 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.67 0.02 . . . . . . . . . . 5995 1 27 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.80 0.02 . . . . . . . . . . 5995 1 28 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.82 0.07 . . . . . . . . . . 5995 1 29 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.82 0.02 . . . . . . . . . . 5995 1 30 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.82 0.03 . . . . . . . . . . 5995 1 31 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.85 0.00 . . . . . . . . . . 5995 1 32 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.85 0.02 . . . . . . . . . . 5995 1 33 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.75 0.09 . . . . . . . . . . 5995 1 34 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.77 0.01 . . . . . . . . . . 5995 1 35 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.86 0.05 . . . . . . . . . . 5995 1 36 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.86 0.05 . . . . . . . . . . 5995 1 37 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.81 0.04 . . . . . . . . . . 5995 1 38 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.80 0.08 . . . . . . . . . . 5995 1 39 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.78 0.01 . . . . . . . . . . 5995 1 40 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.83 0.03 . . . . . . . . . . 5995 1 41 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.83 0.10 . . . . . . . . . . 5995 1 42 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.83 0.01 . . . . . . . . . . 5995 1 43 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.72 0.02 . . . . . . . . . . 5995 1 44 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.80 0.00 . . . . . . . . . . 5995 1 45 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.81 0.01 . . . . . . . . . . 5995 1 46 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.88 0.02 . . . . . . . . . . 5995 1 47 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.85 0.09 . . . . . . . . . . 5995 1 48 . 1 1 119 119 LEU N N 15 . 1 1 119 119 LEU H H 1 0.82 0.07 . . . . . . . . . . 5995 1 49 . 1 1 120 120 TYR N N 15 . 1 1 120 120 TYR H H 1 0.86 0.05 . . . . . . . . . . 5995 1 50 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.87 0.03 . . . . . . . . . . 5995 1 51 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.79 0.01 . . . . . . . . . . 5995 1 52 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.72 0.02 . . . . . . . . . . 5995 1 53 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.80 0.01 . . . . . . . . . . 5995 1 54 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.81 0.02 . . . . . . . . . . 5995 1 55 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.80 0.02 . . . . . . . . . . 5995 1 56 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.83 0.01 . . . . . . . . . . 5995 1 57 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.83 0.01 . . . . . . . . . . 5995 1 58 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.79 0.01 . . . . . . . . . . 5995 1 59 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.81 0.02 . . . . . . . . . . 5995 1 60 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.80 0.02 . . . . . . . . . . 5995 1 61 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.79 0.01 . . . . . . . . . . 5995 1 62 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.79 0.00 . . . . . . . . . . 5995 1 63 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.78 0.02 . . . . . . . . . . 5995 1 64 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.62 0.02 . . . . . . . . . . 5995 1 65 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.78 0.01 . . . . . . . . . . 5995 1 66 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.82 0.05 . . . . . . . . . . 5995 1 67 . 1 1 160 160 ALA N N 15 . 1 1 160 160 ALA H H 1 0.12 0.00 . . . . . . . . . . 5995 1 68 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.29 0.07 . . . . . . . . . . 5995 1 stop_ save_ save_288_600_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 288_600_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 2 _Heteronucl_NOE_list.Sample_condition_list_ID 2 _Heteronucl_NOE_list.Sample_condition_list_label $288K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 2 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.75 0.04 . . . . . . . . . . 5995 2 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.72 0.03 . . . . . . . . . . 5995 2 3 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.78 0.02 . . . . . . . . . . 5995 2 4 . 1 1 10 10 PHE N N 15 . 1 1 10 10 PHE H H 1 0.57 0.02 . . . . . . . . . . 5995 2 5 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.81 0.02 . . . . . . . . . . 5995 2 6 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.77 0.03 . . . . . . . . . . 5995 2 7 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.83 0.01 . . . . . . . . . . 5995 2 8 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.83 0.02 . . . . . . . . . . 5995 2 9 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.80 0.03 . . . . . . . . . . 5995 2 10 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.80 0.02 . . . . . . . . . . 5995 2 11 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.84 0.02 . . . . . . . . . . 5995 2 12 . 1 1 24 24 LEU N N 15 . 1 1 24 24 LEU H H 1 0.79 0.03 . . . . . . . . . . 5995 2 13 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.83 0.02 . . . . . . . . . . 5995 2 14 . 1 1 28 28 LYS N N 15 . 1 1 28 28 LYS H H 1 0.78 0.02 . . . . . . . . . . 5995 2 15 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.76 0.04 . . . . . . . . . . 5995 2 16 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.83 0.01 . . . . . . . . . . 5995 2 17 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.84 0.03 . . . . . . . . . . 5995 2 18 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.85 0.06 . . . . . . . . . . 5995 2 19 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.79 0.02 . . . . . . . . . . 5995 2 20 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.77 0.04 . . . . . . . . . . 5995 2 21 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.79 0.12 . . . . . . . . . . 5995 2 22 . 1 1 38 38 PHE N N 15 . 1 1 38 38 PHE H H 1 0.82 0.05 . . . . . . . . . . 5995 2 23 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.81 0.06 . . . . . . . . . . 5995 2 24 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.78 0.01 . . . . . . . . . . 5995 2 25 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.83 0.02 . . . . . . . . . . 5995 2 26 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.80 0.01 . . . . . . . . . . 5995 2 27 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.73 0.02 . . . . . . . . . . 5995 2 28 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.80 0.02 . . . . . . . . . . 5995 2 29 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.78 0.02 . . . . . . . . . . 5995 2 30 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.88 0.09 . . . . . . . . . . 5995 2 31 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.80 0.02 . . . . . . . . . . 5995 2 32 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.68 0.02 . . . . . . . . . . 5995 2 33 . 1 1 61 61 ASP N N 15 . 1 1 61 61 ASP H H 1 0.68 0.03 . . . . . . . . . . 5995 2 34 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.70 0.02 . . . . . . . . . . 5995 2 35 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.65 0.03 . . . . . . . . . . 5995 2 36 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.67 0.03 . . . . . . . . . . 5995 2 37 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.71 0.02 . . . . . . . . . . 5995 2 38 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.73 0.03 . . . . . . . . . . 5995 2 39 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.79 0.02 . . . . . . . . . . 5995 2 40 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.81 0.02 . . . . . . . . . . 5995 2 41 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.71 0.03 . . . . . . . . . . 5995 2 42 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.69 0.03 . . . . . . . . . . 5995 2 43 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.77 0.02 . . . . . . . . . . 5995 2 44 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.78 0.10 . . . . . . . . . . 5995 2 45 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.81 0.04 . . . . . . . . . . 5995 2 46 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.84 0.04 . . . . . . . . . . 5995 2 47 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.81 0.05 . . . . . . . . . . 5995 2 48 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.87 0.07 . . . . . . . . . . 5995 2 49 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.81 0.02 . . . . . . . . . . 5995 2 50 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.83 0.02 . . . . . . . . . . 5995 2 51 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.80 0.01 . . . . . . . . . . 5995 2 52 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.80 0.02 . . . . . . . . . . 5995 2 53 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.85 0.05 . . . . . . . . . . 5995 2 54 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.84 0.09 . . . . . . . . . . 5995 2 55 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.82 0.04 . . . . . . . . . . 5995 2 56 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.84 0.03 . . . . . . . . . . 5995 2 57 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.81 0.02 . . . . . . . . . . 5995 2 58 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.81 0.08 . . . . . . . . . . 5995 2 59 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.81 0.02 . . . . . . . . . . 5995 2 60 . 1 1 99 99 ASN N N 15 . 1 1 99 99 ASN H H 1 0.76 0.03 . . . . . . . . . . 5995 2 61 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.81 0.06 . . . . . . . . . . 5995 2 62 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.84 0.04 . . . . . . . . . . 5995 2 63 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.80 0.02 . . . . . . . . . . 5995 2 64 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.80 0.02 . . . . . . . . . . 5995 2 65 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.84 0.02 . . . . . . . . . . 5995 2 66 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.79 0.03 . . . . . . . . . . 5995 2 67 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.81 0.02 . . . . . . . . . . 5995 2 68 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.74 0.02 . . . . . . . . . . 5995 2 69 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.77 0.02 . . . . . . . . . . 5995 2 70 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.79 0.02 . . . . . . . . . . 5995 2 71 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.79 0.02 . . . . . . . . . . 5995 2 72 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.78 0.02 . . . . . . . . . . 5995 2 73 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.84 0.02 . . . . . . . . . . 5995 2 74 . 1 1 119 119 LEU N N 15 . 1 1 119 119 LEU H H 1 0.78 0.03 . . . . . . . . . . 5995 2 75 . 1 1 120 120 TYR N N 15 . 1 1 120 120 TYR H H 1 0.82 0.03 . . . . . . . . . . 5995 2 76 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.83 0.03 . . . . . . . . . . 5995 2 77 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.74 0.03 . . . . . . . . . . 5995 2 78 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.75 0.02 . . . . . . . . . . 5995 2 79 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.80 0.02 . . . . . . . . . . 5995 2 80 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.83 0.06 . . . . . . . . . . 5995 2 81 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.85 0.03 . . . . . . . . . . 5995 2 82 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.84 0.04 . . . . . . . . . . 5995 2 83 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.84 0.04 . . . . . . . . . . 5995 2 84 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.83 0.02 . . . . . . . . . . 5995 2 85 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.82 0.02 . . . . . . . . . . 5995 2 86 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.82 0.03 . . . . . . . . . . 5995 2 87 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.79 0.02 . . . . . . . . . . 5995 2 88 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.82 0.02 . . . . . . . . . . 5995 2 89 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.78 0.03 . . . . . . . . . . 5995 2 90 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.66 0.02 . . . . . . . . . . 5995 2 91 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.71 0.02 . . . . . . . . . . 5995 2 92 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.80 0.02 . . . . . . . . . . 5995 2 93 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.82 0.04 . . . . . . . . . . 5995 2 94 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.78 0.02 . . . . . . . . . . 5995 2 95 . 1 1 155 155 ASN N N 15 . 1 1 155 155 ASN H H 1 0.79 0.04 . . . . . . . . . . 5995 2 96 . 1 1 157 157 CYS N N 15 . 1 1 157 157 CYS H H 1 0.76 0.01 . . . . . . . . . . 5995 2 97 . 1 1 158 158 LEU N N 15 . 1 1 158 158 LEU H H 1 0.74 0.05 . . . . . . . . . . 5995 2 98 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 0.06 0.02 . . . . . . . . . . 5995 2 stop_ save_ save_298_600_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 298_600_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 3 _Heteronucl_NOE_list.Sample_condition_list_ID 4 _Heteronucl_NOE_list.Sample_condition_list_label $298K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 3 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.83 0.01 . . . . . . . . . . 5995 3 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.70 0.01 . . . . . . . . . . 5995 3 3 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.75 0.01 . . . . . . . . . . 5995 3 4 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.78 0.01 . . . . . . . . . . 5995 3 5 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.81 0.01 . . . . . . . . . . 5995 3 6 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.83 0.01 . . . . . . . . . . 5995 3 7 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.77 0.02 . . . . . . . . . . 5995 3 8 . 1 1 18 18 GLU N N 15 . 1 1 18 18 GLU H H 1 0.75 0.07 . . . . . . . . . . 5995 3 9 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.81 0.01 . . . . . . . . . . 5995 3 10 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.78 0.01 . . . . . . . . . . 5995 3 11 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.83 0.07 . . . . . . . . . . 5995 3 12 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.82 0.01 . . . . . . . . . . 5995 3 13 . 1 1 24 24 LEU N N 15 . 1 1 24 24 LEU H H 1 0.77 0.01 . . . . . . . . . . 5995 3 14 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.80 0.02 . . . . . . . . . . 5995 3 15 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.77 0.01 . . . . . . . . . . 5995 3 16 . 1 1 28 28 LYS N N 15 . 1 1 28 28 LYS H H 1 0.72 0.01 . . . . . . . . . . 5995 3 17 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.78 0.01 . . . . . . . . . . 5995 3 18 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.81 0.02 . . . . . . . . . . 5995 3 19 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.81 0.02 . . . . . . . . . . 5995 3 20 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.79 0.01 . . . . . . . . . . 5995 3 21 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.78 0.02 . . . . . . . . . . 5995 3 22 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.69 0.05 . . . . . . . . . . 5995 3 23 . 1 1 38 38 PHE N N 15 . 1 1 38 38 PHE H H 1 0.83 0.01 . . . . . . . . . . 5995 3 24 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.87 0.02 . . . . . . . . . . 5995 3 25 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.85 0.05 . . . . . . . . . . 5995 3 26 . 1 1 41 41 PHE N N 15 . 1 1 41 41 PHE H H 1 0.74 0.03 . . . . . . . . . . 5995 3 27 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.79 0.01 . . . . . . . . . . 5995 3 28 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.74 0.01 . . . . . . . . . . 5995 3 29 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.79 0.03 . . . . . . . . . . 5995 3 30 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.81 0.03 . . . . . . . . . . 5995 3 31 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.78 0.01 . . . . . . . . . . 5995 3 32 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.74 0.01 . . . . . . . . . . 5995 3 33 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.80 0.08 . . . . . . . . . . 5995 3 34 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.72 0.01 . . . . . . . . . . 5995 3 35 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.71 0.01 . . . . . . . . . . 5995 3 36 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.79 0.01 . . . . . . . . . . 5995 3 37 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.67 0.02 . . . . . . . . . . 5995 3 38 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.71 0.01 . . . . . . . . . . 5995 3 39 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.75 0.04 . . . . . . . . . . 5995 3 40 . 1 1 70 70 VAL N N 15 . 1 1 70 70 VAL H H 1 0.71 0.02 . . . . . . . . . . 5995 3 41 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.79 0.02 . . . . . . . . . . 5995 3 42 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.75 0.04 . . . . . . . . . . 5995 3 43 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.74 0.02 . . . . . . . . . . 5995 3 44 . 1 1 75 75 GLU N N 15 . 1 1 75 75 GLU H H 1 0.71 0.03 . . . . . . . . . . 5995 3 45 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.72 0.01 . . . . . . . . . . 5995 3 46 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.77 0.01 . . . . . . . . . . 5995 3 47 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.78 0.03 . . . . . . . . . . 5995 3 48 . 1 1 82 82 VAL N N 15 . 1 1 82 82 VAL H H 1 0.79 0.01 . . . . . . . . . . 5995 3 49 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.76 0.04 . . . . . . . . . . 5995 3 50 . 1 1 85 85 ASP N N 15 . 1 1 85 85 ASP H H 1 0.76 0.01 . . . . . . . . . . 5995 3 51 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.83 0.01 . . . . . . . . . . 5995 3 52 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.76 0.01 . . . . . . . . . . 5995 3 53 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.78 0.03 . . . . . . . . . . 5995 3 54 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.74 0.07 . . . . . . . . . . 5995 3 55 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.78 0.01 . . . . . . . . . . 5995 3 56 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.79 0.01 . . . . . . . . . . 5995 3 57 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.82 0.03 . . . . . . . . . . 5995 3 58 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.85 0.05 . . . . . . . . . . 5995 3 59 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.81 0.04 . . . . . . . . . . 5995 3 60 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.83 0.03 . . . . . . . . . . 5995 3 61 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.83 0.05 . . . . . . . . . . 5995 3 62 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.76 0.03 . . . . . . . . . . 5995 3 63 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.84 0.04 . . . . . . . . . . 5995 3 64 . 1 1 106 106 ILE N N 15 . 1 1 106 106 ILE H H 1 0.82 0.02 . . . . . . . . . . 5995 3 65 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.80 0.02 . . . . . . . . . . 5995 3 66 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.71 0.04 . . . . . . . . . . 5995 3 67 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.78 0.01 . . . . . . . . . . 5995 3 68 . 1 1 114 114 PHE N N 15 . 1 1 114 114 PHE H H 1 0.77 0.01 . . . . . . . . . . 5995 3 69 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.82 0.02 . . . . . . . . . . 5995 3 70 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.78 0.03 . . . . . . . . . . 5995 3 71 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.83 0.03 . . . . . . . . . . 5995 3 72 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.82 0.01 . . . . . . . . . . 5995 3 73 . 1 1 119 119 LEU N N 15 . 1 1 119 119 LEU H H 1 0.77 0.02 . . . . . . . . . . 5995 3 74 . 1 1 120 120 TYR N N 15 . 1 1 120 120 TYR H H 1 0.83 0.02 . . . . . . . . . . 5995 3 75 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.82 0.01 . . . . . . . . . . 5995 3 76 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.75 0.01 . . . . . . . . . . 5995 3 77 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.77 0.01 . . . . . . . . . . 5995 3 78 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.82 0.01 . . . . . . . . . . 5995 3 79 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.79 0.01 . . . . . . . . . . 5995 3 80 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.78 0.02 . . . . . . . . . . 5995 3 81 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.72 0.01 . . . . . . . . . . 5995 3 82 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.80 0.01 . . . . . . . . . . 5995 3 83 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.78 0.03 . . . . . . . . . . 5995 3 84 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.80 0.01 . . . . . . . . . . 5995 3 85 . 1 1 134 134 PHE N N 15 . 1 1 134 134 PHE H H 1 0.83 0.01 . . . . . . . . . . 5995 3 86 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.82 0.01 . . . . . . . . . . 5995 3 87 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.81 0.01 . . . . . . . . . . 5995 3 88 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.79 0.01 . . . . . . . . . . 5995 3 89 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.76 0.01 . . . . . . . . . . 5995 3 90 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.81 0.01 . . . . . . . . . . 5995 3 91 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.77 0.01 . . . . . . . . . . 5995 3 92 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.77 0.01 . . . . . . . . . . 5995 3 93 . 1 1 143 143 ILE N N 15 . 1 1 143 143 ILE H H 1 0.80 0.01 . . . . . . . . . . 5995 3 94 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.67 0.02 . . . . . . . . . . 5995 3 95 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.73 0.01 . . . . . . . . . . 5995 3 96 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.80 0.01 . . . . . . . . . . 5995 3 97 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.82 0.01 . . . . . . . . . . 5995 3 98 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.79 0.01 . . . . . . . . . . 5995 3 99 . 1 1 158 158 LEU N N 15 . 1 1 158 158 LEU H H 1 0.79 0.01 . . . . . . . . . . 5995 3 100 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 0.02 0.01 . . . . . . . . . . 5995 3 stop_ save_ save_303_600_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 303_600_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 4 _Heteronucl_NOE_list.Sample_condition_list_ID 5 _Heteronucl_NOE_list.Sample_condition_list_label $303K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 4 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.69 0.01 . . . . . . . . . . 5995 4 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.66 0.02 . . . . . . . . . . 5995 4 3 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.80 0.01 . . . . . . . . . . 5995 4 4 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.81 0.01 . . . . . . . . . . 5995 4 5 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.80 0.01 . . . . . . . . . . 5995 4 6 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.82 0.03 . . . . . . . . . . 5995 4 7 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.84 0.02 . . . . . . . . . . 5995 4 8 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.80 0.02 . . . . . . . . . . 5995 4 9 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.81 0.04 . . . . . . . . . . 5995 4 10 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.80 0.02 . . . . . . . . . . 5995 4 11 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.84 0.07 . . . . . . . . . . 5995 4 12 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.80 0.01 . . . . . . . . . . 5995 4 13 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.83 0.01 . . . . . . . . . . 5995 4 14 . 1 1 24 24 LEU N N 15 . 1 1 24 24 LEU H H 1 0.82 0.01 . . . . . . . . . . 5995 4 15 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.80 0.01 . . . . . . . . . . 5995 4 16 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.81 0.02 . . . . . . . . . . 5995 4 17 . 1 1 28 28 LYS N N 15 . 1 1 28 28 LYS H H 1 0.75 0.01 . . . . . . . . . . 5995 4 18 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.82 0.01 . . . . . . . . . . 5995 4 19 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.81 0.01 . . . . . . . . . . 5995 4 20 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.83 0.01 . . . . . . . . . . 5995 4 21 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.80 0.01 . . . . . . . . . . 5995 4 22 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.77 0.03 . . . . . . . . . . 5995 4 23 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.78 0.01 . . . . . . . . . . 5995 4 24 . 1 1 38 38 PHE N N 15 . 1 1 38 38 PHE H H 1 0.83 0.01 . . . . . . . . . . 5995 4 25 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.82 0.01 . . . . . . . . . . 5995 4 26 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.82 0.02 . . . . . . . . . . 5995 4 27 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.83 0.01 . . . . . . . . . . 5995 4 28 . 1 1 46 46 HIS N N 15 . 1 1 46 46 HIS H H 1 0.82 0.01 . . . . . . . . . . 5995 4 29 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.79 0.01 . . . . . . . . . . 5995 4 30 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.75 0.01 . . . . . . . . . . 5995 4 31 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.76 0.02 . . . . . . . . . . 5995 4 32 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.79 0.02 . . . . . . . . . . 5995 4 33 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.81 0.01 . . . . . . . . . . 5995 4 34 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.80 0.01 . . . . . . . . . . 5995 4 35 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.77 0.02 . . . . . . . . . . 5995 4 36 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.79 0.01 . . . . . . . . . . 5995 4 37 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.70 0.01 . . . . . . . . . . 5995 4 38 . 1 1 62 62 GLU N N 15 . 1 1 62 62 GLU H H 1 0.72 0.01 . . . . . . . . . . 5995 4 39 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.80 0.01 . . . . . . . . . . 5995 4 40 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.76 0.01 . . . . . . . . . . 5995 4 41 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.74 0.01 . . . . . . . . . . 5995 4 42 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.75 0.01 . . . . . . . . . . 5995 4 43 . 1 1 70 70 VAL N N 15 . 1 1 70 70 VAL H H 1 0.73 0.02 . . . . . . . . . . 5995 4 44 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.78 0.01 . . . . . . . . . . 5995 4 45 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.77 0.01 . . . . . . . . . . 5995 4 46 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.71 0.01 . . . . . . . . . . 5995 4 47 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.77 0.01 . . . . . . . . . . 5995 4 48 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.70 0.03 . . . . . . . . . . 5995 4 49 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.78 0.01 . . . . . . . . . . 5995 4 50 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.79 0.02 . . . . . . . . . . 5995 4 51 . 1 1 84 84 TYR N N 15 . 1 1 84 84 TYR H H 1 0.77 0.01 . . . . . . . . . . 5995 4 52 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.80 0.01 . . . . . . . . . . 5995 4 53 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.79 0.01 . . . . . . . . . . 5995 4 54 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.84 0.01 . . . . . . . . . . 5995 4 55 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.79 0.02 . . . . . . . . . . 5995 4 56 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.79 0.02 . . . . . . . . . . 5995 4 57 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.82 0.01 . . . . . . . . . . 5995 4 58 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.81 0.02 . . . . . . . . . . 5995 4 59 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.81 0.02 . . . . . . . . . . 5995 4 60 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.78 0.01 . . . . . . . . . . 5995 4 61 . 1 1 99 99 ASN N N 15 . 1 1 99 99 ASN H H 1 0.79 0.01 . . . . . . . . . . 5995 4 62 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.84 0.01 . . . . . . . . . . 5995 4 63 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.84 0.02 . . . . . . . . . . 5995 4 64 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.81 0.01 . . . . . . . . . . 5995 4 65 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.81 0.01 . . . . . . . . . . 5995 4 66 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.81 0.01 . . . . . . . . . . 5995 4 67 . 1 1 106 106 ILE N N 15 . 1 1 106 106 ILE H H 1 0.81 0.01 . . . . . . . . . . 5995 4 68 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.82 0.02 . . . . . . . . . . 5995 4 69 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.82 0.01 . . . . . . . . . . 5995 4 70 . 1 1 110 110 ASP N N 15 . 1 1 110 110 ASP H H 1 0.81 0.01 . . . . . . . . . . 5995 4 71 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.74 0.01 . . . . . . . . . . 5995 4 72 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.76 0.01 . . . . . . . . . . 5995 4 73 . 1 1 114 114 PHE N N 15 . 1 1 114 114 PHE H H 1 0.81 0.01 . . . . . . . . . . 5995 4 74 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.81 0.01 . . . . . . . . . . 5995 4 75 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.79 0.01 . . . . . . . . . . 5995 4 76 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.83 0.01 . . . . . . . . . . 5995 4 77 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.80 0.01 . . . . . . . . . . 5995 4 78 . 1 1 119 119 LEU N N 15 . 1 1 119 119 LEU H H 1 0.81 0.02 . . . . . . . . . . 5995 4 79 . 1 1 120 120 TYR N N 15 . 1 1 120 120 TYR H H 1 0.83 0.01 . . . . . . . . . . 5995 4 80 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.82 0.02 . . . . . . . . . . 5995 4 81 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.79 0.01 . . . . . . . . . . 5995 4 82 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.76 0.01 . . . . . . . . . . 5995 4 83 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.78 0.01 . . . . . . . . . . 5995 4 84 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.78 0.01 . . . . . . . . . . 5995 4 85 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.80 0.02 . . . . . . . . . . 5995 4 86 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.72 0.02 . . . . . . . . . . 5995 4 87 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.79 0.01 . . . . . . . . . . 5995 4 88 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.80 0.03 . . . . . . . . . . 5995 4 89 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.82 0.02 . . . . . . . . . . 5995 4 90 . 1 1 135 135 ALA N N 15 . 1 1 135 135 ALA H H 1 0.82 0.01 . . . . . . . . . . 5995 4 91 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.82 0.01 . . . . . . . . . . 5995 4 92 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.81 0.02 . . . . . . . . . . 5995 4 93 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.84 0.01 . . . . . . . . . . 5995 4 94 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.80 0.01 . . . . . . . . . . 5995 4 95 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.79 0.01 . . . . . . . . . . 5995 4 96 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.79 0.01 . . . . . . . . . . 5995 4 97 . 1 1 143 143 ILE N N 15 . 1 1 143 143 ILE H H 1 0.80 0.03 . . . . . . . . . . 5995 4 98 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.69 0.01 . . . . . . . . . . 5995 4 99 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.73 0.01 . . . . . . . . . . 5995 4 100 . 1 1 146 146 GLU N N 15 . 1 1 146 146 GLU H H 1 0.79 0.01 . . . . . . . . . . 5995 4 101 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.81 0.01 . . . . . . . . . . 5995 4 102 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.78 0.01 . . . . . . . . . . 5995 4 103 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.78 0.01 . . . . . . . . . . 5995 4 104 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.79 0.01 . . . . . . . . . . 5995 4 105 . 1 1 157 157 CYS N N 15 . 1 1 157 157 CYS H H 1 0.77 0.02 . . . . . . . . . . 5995 4 106 . 1 1 158 158 LEU N N 15 . 1 1 158 158 LEU H H 1 0.78 0.01 . . . . . . . . . . 5995 4 107 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.09 0.01 . . . . . . . . . . 5995 4 stop_ save_ save_308_600_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 308_600_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 5 _Heteronucl_NOE_list.Sample_condition_list_ID 6 _Heteronucl_NOE_list.Sample_condition_list_label $308K _Heteronucl_NOE_list.Spectrometer_frequency_1H 600 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 5 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.63 0.04 . . . . . . . . . . 5995 5 2 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.75 0.01 . . . . . . . . . . 5995 5 3 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.75 0.02 . . . . . . . . . . 5995 5 4 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.78 0.01 . . . . . . . . . . 5995 5 5 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.82 0.02 . . . . . . . . . . 5995 5 6 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.74 0.04 . . . . . . . . . . 5995 5 7 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.76 0.02 . . . . . . . . . . 5995 5 8 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.76 0.02 . . . . . . . . . . 5995 5 9 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.74 0.01 . . . . . . . . . . 5995 5 10 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.76 0.00 . . . . . . . . . . 5995 5 11 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.77 0.02 . . . . . . . . . . 5995 5 12 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.73 0.03 . . . . . . . . . . 5995 5 13 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.73 0.02 . . . . . . . . . . 5995 5 14 . 1 1 38 38 PHE N N 15 . 1 1 38 38 PHE H H 1 0.75 0.02 . . . . . . . . . . 5995 5 15 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.77 0.02 . . . . . . . . . . 5995 5 16 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.72 0.02 . . . . . . . . . . 5995 5 17 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.74 0.02 . . . . . . . . . . 5995 5 18 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.67 0.03 . . . . . . . . . . 5995 5 19 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.74 0.02 . . . . . . . . . . 5995 5 20 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.76 0.00 . . . . . . . . . . 5995 5 21 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.74 0.05 . . . . . . . . . . 5995 5 22 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.63 0.02 . . . . . . . . . . 5995 5 23 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.68 0.01 . . . . . . . . . . 5995 5 24 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.69 0.05 . . . . . . . . . . 5995 5 25 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.71 0.01 . . . . . . . . . . 5995 5 26 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.65 0.03 . . . . . . . . . . 5995 5 27 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.74 0.02 . . . . . . . . . . 5995 5 28 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.75 0.03 . . . . . . . . . . 5995 5 29 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.75 0.02 . . . . . . . . . . 5995 5 30 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.78 0.01 . . . . . . . . . . 5995 5 31 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.72 0.01 . . . . . . . . . . 5995 5 32 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.75 0.01 . . . . . . . . . . 5995 5 33 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.75 0.01 . . . . . . . . . . 5995 5 34 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.77 0.01 . . . . . . . . . . 5995 5 35 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.77 0.02 . . . . . . . . . . 5995 5 36 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.75 0.05 . . . . . . . . . . 5995 5 37 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.77 0.02 . . . . . . . . . . 5995 5 38 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.77 0.05 . . . . . . . . . . 5995 5 39 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.67 0.03 . . . . . . . . . . 5995 5 40 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.77 0.01 . . . . . . . . . . 5995 5 41 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.72 0.03 . . . . . . . . . . 5995 5 42 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.73 0.01 . . . . . . . . . . 5995 5 43 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.78 0.03 . . . . . . . . . . 5995 5 44 . 1 1 120 120 TYR N N 15 . 1 1 120 120 TYR H H 1 0.76 0.00 . . . . . . . . . . 5995 5 45 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.75 0.01 . . . . . . . . . . 5995 5 46 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.71 0.01 . . . . . . . . . . 5995 5 47 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.68 0.01 . . . . . . . . . . 5995 5 48 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.68 0.03 . . . . . . . . . . 5995 5 49 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.70 0.02 . . . . . . . . . . 5995 5 50 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.75 0.01 . . . . . . . . . . 5995 5 51 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.76 0.01 . . . . . . . . . . 5995 5 52 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.76 0.02 . . . . . . . . . . 5995 5 53 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.73 0.01 . . . . . . . . . . 5995 5 54 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.75 0.03 . . . . . . . . . . 5995 5 55 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.75 0.03 . . . . . . . . . . 5995 5 56 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.74 0.03 . . . . . . . . . . 5995 5 57 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.74 0.01 . . . . . . . . . . 5995 5 58 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.67 0.03 . . . . . . . . . . 5995 5 59 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.69 0.02 . . . . . . . . . . 5995 5 60 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.75 0.03 . . . . . . . . . . 5995 5 61 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.73 0.01 . . . . . . . . . . 5995 5 62 . 1 1 162 162 GLU N N 15 . 1 1 162 162 GLU H H 1 -0.08 0.01 . . . . . . . . . . 5995 5 stop_ save_ save_291_500_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 291_500_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 6 _Heteronucl_NOE_list.Sample_condition_list_ID 7 _Heteronucl_NOE_list.Sample_condition_list_label $291K _Heteronucl_NOE_list.Spectrometer_frequency_1H 500 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 6 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.66 0.02 . . . . . . . . . . 5995 6 2 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.71 0.02 . . . . . . . . . . 5995 6 3 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.62 0.02 . . . . . . . . . . 5995 6 4 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.73 0.02 . . . . . . . . . . 5995 6 5 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.69 0.04 . . . . . . . . . . 5995 6 6 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.66 0.03 . . . . . . . . . . 5995 6 7 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.73 0.03 . . . . . . . . . . 5995 6 8 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.75 0.02 . . . . . . . . . . 5995 6 9 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.75 0.04 . . . . . . . . . . 5995 6 10 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.63 0.00 . . . . . . . . . . 5995 6 11 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.75 0.02 . . . . . . . . . . 5995 6 12 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.72 0.02 . . . . . . . . . . 5995 6 13 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.70 0.02 . . . . . . . . . . 5995 6 14 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.70 0.04 . . . . . . . . . . 5995 6 15 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.73 0.02 . . . . . . . . . . 5995 6 16 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.79 0.02 . . . . . . . . . . 5995 6 17 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.74 0.02 . . . . . . . . . . 5995 6 18 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.75 0.05 . . . . . . . . . . 5995 6 19 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.71 0.02 . . . . . . . . . . 5995 6 20 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.69 0.04 . . . . . . . . . . 5995 6 21 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.76 0.03 . . . . . . . . . . 5995 6 22 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.69 0.03 . . . . . . . . . . 5995 6 23 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.72 0.03 . . . . . . . . . . 5995 6 24 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.66 0.02 . . . . . . . . . . 5995 6 25 . 1 1 53 53 VAL N N 15 . 1 1 53 53 VAL H H 1 0.68 0.04 . . . . . . . . . . 5995 6 26 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.74 0.04 . . . . . . . . . . 5995 6 27 . 1 1 55 55 LYS N N 15 . 1 1 55 55 LYS H H 1 0.76 0.04 . . . . . . . . . . 5995 6 28 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.65 0.03 . . . . . . . . . . 5995 6 29 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.59 0.04 . . . . . . . . . . 5995 6 30 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.69 0.04 . . . . . . . . . . 5995 6 31 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.67 0.03 . . . . . . . . . . 5995 6 32 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.68 0.03 . . . . . . . . . . 5995 6 33 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.69 0.03 . . . . . . . . . . 5995 6 34 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.74 0.04 . . . . . . . . . . 5995 6 35 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.65 0.04 . . . . . . . . . . 5995 6 36 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.64 0.02 . . . . . . . . . . 5995 6 37 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.62 0.04 . . . . . . . . . . 5995 6 38 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.71 0.02 . . . . . . . . . . 5995 6 39 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.66 0.02 . . . . . . . . . . 5995 6 40 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.78 0.02 . . . . . . . . . . 5995 6 41 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.72 0.02 . . . . . . . . . . 5995 6 42 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.76 0.04 . . . . . . . . . . 5995 6 43 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.79 0.02 . . . . . . . . . . 5995 6 44 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.70 0.02 . . . . . . . . . . 5995 6 45 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.72 0.02 . . . . . . . . . . 5995 6 46 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.01 0.02 . . . . . . . . . . 5995 6 47 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.75 0.03 . . . . . . . . . . 5995 6 48 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.82 0.03 . . . . . . . . . . 5995 6 49 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.69 0.03 . . . . . . . . . . 5995 6 50 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.81 0.02 . . . . . . . . . . 5995 6 51 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.78 0.03 . . . . . . . . . . 5995 6 52 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.73 0.02 . . . . . . . . . . 5995 6 53 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.74 0.02 . . . . . . . . . . 5995 6 54 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.78 0.03 . . . . . . . . . . 5995 6 55 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.71 0.02 . . . . . . . . . . 5995 6 56 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.75 0.03 . . . . . . . . . . 5995 6 57 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.75 0.02 . . . . . . . . . . 5995 6 58 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.69 0.02 . . . . . . . . . . 5995 6 59 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.70 0.02 . . . . . . . . . . 5995 6 60 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.64 0.02 . . . . . . . . . . 5995 6 61 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.74 0.02 . . . . . . . . . . 5995 6 62 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.79 0.03 . . . . . . . . . . 5995 6 63 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.80 0.03 . . . . . . . . . . 5995 6 64 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.74 0.02 . . . . . . . . . . 5995 6 65 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.69 0.03 . . . . . . . . . . 5995 6 66 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.69 0.02 . . . . . . . . . . 5995 6 67 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.74 0.03 . . . . . . . . . . 5995 6 68 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.70 0.03 . . . . . . . . . . 5995 6 69 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.76 0.03 . . . . . . . . . . 5995 6 70 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.72 0.03 . . . . . . . . . . 5995 6 71 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.75 0.03 . . . . . . . . . . 5995 6 72 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.69 0.03 . . . . . . . . . . 5995 6 73 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.77 0.03 . . . . . . . . . . 5995 6 74 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.72 0.05 . . . . . . . . . . 5995 6 75 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.72 0.02 . . . . . . . . . . 5995 6 76 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.77 0.03 . . . . . . . . . . 5995 6 77 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.71 0.02 . . . . . . . . . . 5995 6 78 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.67 0.02 . . . . . . . . . . 5995 6 79 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.65 0.03 . . . . . . . . . . 5995 6 80 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.63 0.03 . . . . . . . . . . 5995 6 81 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.72 0.01 . . . . . . . . . . 5995 6 82 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.64 0.02 . . . . . . . . . . 5995 6 83 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.73 0.02 . . . . . . . . . . 5995 6 84 . 1 1 158 158 LEU N N 15 . 1 1 158 158 LEU H H 1 0.70 0.02 . . . . . . . . . . 5995 6 stop_ save_ save_297_500_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 297_500_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 7 _Heteronucl_NOE_list.Sample_condition_list_ID 8 _Heteronucl_NOE_list.Sample_condition_list_label $297K _Heteronucl_NOE_list.Spectrometer_frequency_1H 500 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 7 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.62 0.02 . . . . . . . . . . 5995 7 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.68 0.02 . . . . . . . . . . 5995 7 3 . 1 1 6 6 THR N N 15 . 1 1 6 6 THR H H 1 0.72 0.02 . . . . . . . . . . 5995 7 4 . 1 1 7 7 GLY N N 15 . 1 1 7 7 GLY H H 1 0.62 0.02 . . . . . . . . . . 5995 7 5 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.72 0.02 . . . . . . . . . . 5995 7 6 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.74 0.04 . . . . . . . . . . 5995 7 7 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.72 0.03 . . . . . . . . . . 5995 7 8 . 1 1 15 15 ILE N N 15 . 1 1 15 15 ILE H H 1 0.75 0.03 . . . . . . . . . . 5995 7 9 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.77 0.02 . . . . . . . . . . 5995 7 10 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.78 0.04 . . . . . . . . . . 5995 7 11 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.72 0.03 . . . . . . . . . . 5995 7 12 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.69 0.00 . . . . . . . . . . 5995 7 13 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.76 0.02 . . . . . . . . . . 5995 7 14 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.75 0.02 . . . . . . . . . . 5995 7 15 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.71 0.02 . . . . . . . . . . 5995 7 16 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.72 0.04 . . . . . . . . . . 5995 7 17 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.71 0.02 . . . . . . . . . . 5995 7 18 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.78 0.02 . . . . . . . . . . 5995 7 19 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.76 0.02 . . . . . . . . . . 5995 7 20 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.74 0.05 . . . . . . . . . . 5995 7 21 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.71 0.02 . . . . . . . . . . 5995 7 22 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.78 0.04 . . . . . . . . . . 5995 7 23 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.77 0.03 . . . . . . . . . . 5995 7 24 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.74 0.07 . . . . . . . . . . 5995 7 25 . 1 1 47 47 VAL N N 15 . 1 1 47 47 VAL H H 1 0.71 0.03 . . . . . . . . . . 5995 7 26 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.72 0.03 . . . . . . . . . . 5995 7 27 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 0.68 0.02 . . . . . . . . . . 5995 7 28 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.73 0.04 . . . . . . . . . . 5995 7 29 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.75 0.04 . . . . . . . . . . 5995 7 30 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.76 0.04 . . . . . . . . . . 5995 7 31 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.65 0.03 . . . . . . . . . . 5995 7 32 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.61 0.04 . . . . . . . . . . 5995 7 33 . 1 1 65 65 SER N N 15 . 1 1 65 65 SER H H 1 0.73 0.05 . . . . . . . . . . 5995 7 34 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.68 0.03 . . . . . . . . . . 5995 7 35 . 1 1 67 67 LEU N N 15 . 1 1 67 67 LEU H H 1 0.71 0.04 . . . . . . . . . . 5995 7 36 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.69 0.03 . . . . . . . . . . 5995 7 37 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.72 0.03 . . . . . . . . . . 5995 7 38 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.72 0.03 . . . . . . . . . . 5995 7 39 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.76 0.04 . . . . . . . . . . 5995 7 40 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.66 0.04 . . . . . . . . . . 5995 7 41 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.64 0.04 . . . . . . . . . . 5995 7 42 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.78 0.02 . . . . . . . . . . 5995 7 43 . 1 1 80 80 TYR N N 15 . 1 1 80 80 TYR H H 1 0.68 0.02 . . . . . . . . . . 5995 7 44 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.75 0.02 . . . . . . . . . . 5995 7 45 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.74 0.02 . . . . . . . . . . 5995 7 46 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.77 0.04 . . . . . . . . . . 5995 7 47 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.79 0.02 . . . . . . . . . . 5995 7 48 . 1 1 91 91 THR N N 15 . 1 1 91 91 THR H H 1 0.72 0.02 . . . . . . . . . . 5995 7 49 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.74 0.02 . . . . . . . . . . 5995 7 50 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.75 0.02 . . . . . . . . . . 5995 7 51 . 1 1 95 95 THR N N 15 . 1 1 95 95 THR H H 1 0.73 0.02 . . . . . . . . . . 5995 7 52 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.78 0.03 . . . . . . . . . . 5995 7 53 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.75 0.03 . . . . . . . . . . 5995 7 54 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.81 0.02 . . . . . . . . . . 5995 7 55 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.79 0.03 . . . . . . . . . . 5995 7 56 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.75 0.02 . . . . . . . . . . 5995 7 57 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.76 0.02 . . . . . . . . . . 5995 7 58 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.67 0.03 . . . . . . . . . . 5995 7 59 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.74 0.02 . . . . . . . . . . 5995 7 60 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.73 0.03 . . . . . . . . . . 5995 7 61 . 1 1 108 108 GLU N N 15 . 1 1 108 108 GLU H H 1 0.75 0.02 . . . . . . . . . . 5995 7 62 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.67 0.02 . . . . . . . . . . 5995 7 63 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.69 0.02 . . . . . . . . . . 5995 7 64 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.68 0.02 . . . . . . . . . . 5995 7 65 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.74 0.02 . . . . . . . . . . 5995 7 66 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.78 0.03 . . . . . . . . . . 5995 7 67 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.82 0.03 . . . . . . . . . . 5995 7 68 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.76 0.02 . . . . . . . . . . 5995 7 69 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.70 0.03 . . . . . . . . . . 5995 7 70 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.71 0.02 . . . . . . . . . . 5995 7 71 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.72 0.03 . . . . . . . . . . 5995 7 72 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.72 0.03 . . . . . . . . . . 5995 7 73 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.76 0.03 . . . . . . . . . . 5995 7 74 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.75 0.03 . . . . . . . . . . 5995 7 75 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.80 0.03 . . . . . . . . . . 5995 7 76 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.74 0.03 . . . . . . . . . . 5995 7 77 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.77 0.03 . . . . . . . . . . 5995 7 78 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.74 0.05 . . . . . . . . . . 5995 7 79 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.76 0.02 . . . . . . . . . . 5995 7 80 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.78 0.03 . . . . . . . . . . 5995 7 81 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.73 0.02 . . . . . . . . . . 5995 7 82 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.70 0.02 . . . . . . . . . . 5995 7 83 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.66 0.03 . . . . . . . . . . 5995 7 84 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.64 0.03 . . . . . . . . . . 5995 7 85 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.74 0.01 . . . . . . . . . . 5995 7 86 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.67 0.02 . . . . . . . . . . 5995 7 87 . 1 1 152 152 SER N N 15 . 1 1 152 152 SER H H 1 0.68 0.02 . . . . . . . . . . 5995 7 88 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.72 0.02 . . . . . . . . . . 5995 7 89 . 1 1 155 155 ASN N N 15 . 1 1 155 155 ASN H H 1 0.69 0.02 . . . . . . . . . . 5995 7 stop_ save_ save_302_500_free_noe _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode 302_500_free_noe _Heteronucl_NOE_list.Entry_ID 5995 _Heteronucl_NOE_list.ID 8 _Heteronucl_NOE_list.Sample_condition_list_ID 9 _Heteronucl_NOE_list.Sample_condition_list_label $302K _Heteronucl_NOE_list.Spectrometer_frequency_1H 500 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'relative intensities' _Heteronucl_NOE_list.NOE_ref_val . _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '{1H}-15N NOE' 1 $sample_1 . 5995 8 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 ALA N N 15 . 1 1 3 3 ALA H H 1 0.62 0.01 . . . . . . . . . . 5995 8 2 . 1 1 4 4 SER N N 15 . 1 1 4 4 SER H H 1 0.59 0.01 . . . . . . . . . . 5995 8 3 . 1 1 11 11 ASN N N 15 . 1 1 11 11 ASN H H 1 0.74 0.01 . . . . . . . . . . 5995 8 4 . 1 1 12 12 VAL N N 15 . 1 1 12 12 VAL H H 1 0.65 0.01 . . . . . . . . . . 5995 8 5 . 1 1 13 13 GLU N N 15 . 1 1 13 13 GLU H H 1 0.69 0.02 . . . . . . . . . . 5995 8 6 . 1 1 16 16 ASN N N 15 . 1 1 16 16 ASN H H 1 0.74 0.02 . . . . . . . . . . 5995 8 7 . 1 1 17 17 GLY N N 15 . 1 1 17 17 GLY H H 1 0.73 0.01 . . . . . . . . . . 5995 8 8 . 1 1 19 19 TRP N N 15 . 1 1 19 19 TRP H H 1 0.73 0.01 . . . . . . . . . . 5995 8 9 . 1 1 20 20 HIS N N 15 . 1 1 20 20 HIS H H 1 0.73 0.02 . . . . . . . . . . 5995 8 10 . 1 1 21 21 THR N N 15 . 1 1 21 21 THR H H 1 0.71 0.04 . . . . . . . . . . 5995 8 11 . 1 1 22 22 ILE N N 15 . 1 1 22 22 ILE H H 1 0.71 0.02 . . . . . . . . . . 5995 8 12 . 1 1 23 23 ILE N N 15 . 1 1 23 23 ILE H H 1 0.72 0.02 . . . . . . . . . . 5995 8 13 . 1 1 26 26 SER N N 15 . 1 1 26 26 SER H H 1 0.74 0.01 . . . . . . . . . . 5995 8 14 . 1 1 27 27 ASP N N 15 . 1 1 27 27 ASP H H 1 0.72 0.01 . . . . . . . . . . 5995 8 15 . 1 1 30 30 GLU N N 15 . 1 1 30 30 GLU H H 1 0.68 0.01 . . . . . . . . . . 5995 8 16 . 1 1 31 31 LYS N N 15 . 1 1 31 31 LYS H H 1 0.62 0.02 . . . . . . . . . . 5995 8 17 . 1 1 32 32 ILE N N 15 . 1 1 32 32 ILE H H 1 0.76 0.04 . . . . . . . . . . 5995 8 18 . 1 1 33 33 GLU N N 15 . 1 1 33 33 GLU H H 1 0.72 0.01 . . . . . . . . . . 5995 8 19 . 1 1 35 35 ASN N N 15 . 1 1 35 35 ASN H H 1 0.68 0.01 . . . . . . . . . . 5995 8 20 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.72 0.01 . . . . . . . . . . 5995 8 21 . 1 1 37 37 ASN N N 15 . 1 1 37 37 ASN H H 1 0.73 0.01 . . . . . . . . . . 5995 8 22 . 1 1 39 39 ARG N N 15 . 1 1 39 39 ARG H H 1 0.73 0.01 . . . . . . . . . . 5995 8 23 . 1 1 40 40 LEU N N 15 . 1 1 40 40 LEU H H 1 0.71 0.03 . . . . . . . . . . 5995 8 24 . 1 1 41 41 PHE N N 15 . 1 1 41 41 PHE H H 1 0.65 0.01 . . . . . . . . . . 5995 8 25 . 1 1 42 42 LEU N N 15 . 1 1 42 42 LEU H H 1 0.73 0.03 . . . . . . . . . . 5995 8 26 . 1 1 48 48 LEU N N 15 . 1 1 48 48 LEU H H 1 0.72 0.01 . . . . . . . . . . 5995 8 27 . 1 1 51 51 SER N N 15 . 1 1 51 51 SER H H 1 1.26 0.03 . . . . . . . . . . 5995 8 28 . 1 1 52 52 LEU N N 15 . 1 1 52 52 LEU H H 1 0.70 0.01 . . . . . . . . . . 5995 8 29 . 1 1 54 54 LEU N N 15 . 1 1 54 54 LEU H H 1 0.76 0.01 . . . . . . . . . . 5995 8 30 . 1 1 57 57 HIS N N 15 . 1 1 57 57 HIS H H 1 0.72 0.01 . . . . . . . . . . 5995 8 31 . 1 1 58 58 THR N N 15 . 1 1 58 58 THR H H 1 0.75 0.05 . . . . . . . . . . 5995 8 32 . 1 1 60 60 ARG N N 15 . 1 1 60 60 ARG H H 1 0.64 0.01 . . . . . . . . . . 5995 8 33 . 1 1 64 64 CYS N N 15 . 1 1 64 64 CYS H H 1 0.60 0.02 . . . . . . . . . . 5995 8 34 . 1 1 65 65 SER N N 15 . 1 1 65 65 SER H H 1 0.67 0.01 . . . . . . . . . . 5995 8 35 . 1 1 66 66 GLU N N 15 . 1 1 66 66 GLU H H 1 0.67 0.02 . . . . . . . . . . 5995 8 36 . 1 1 68 68 SER N N 15 . 1 1 68 68 SER H H 1 0.66 0.01 . . . . . . . . . . 5995 8 37 . 1 1 69 69 MET N N 15 . 1 1 69 69 MET H H 1 0.68 0.01 . . . . . . . . . . 5995 8 38 . 1 1 70 70 VAL N N 15 . 1 1 70 70 VAL H H 1 0.73 0.03 . . . . . . . . . . 5995 8 39 . 1 1 71 71 ALA N N 15 . 1 1 71 71 ALA H H 1 0.72 0.02 . . . . . . . . . . 5995 8 40 . 1 1 72 72 ASP N N 15 . 1 1 72 72 ASP H H 1 0.67 0.01 . . . . . . . . . . 5995 8 41 . 1 1 74 74 THR N N 15 . 1 1 74 74 THR H H 1 0.63 0.01 . . . . . . . . . . 5995 8 42 . 1 1 76 76 LYS N N 15 . 1 1 76 76 LYS H H 1 0.66 0.01 . . . . . . . . . . 5995 8 43 . 1 1 77 77 ALA N N 15 . 1 1 77 77 ALA H H 1 0.65 0.01 . . . . . . . . . . 5995 8 44 . 1 1 79 79 GLU N N 15 . 1 1 79 79 GLU H H 1 0.70 0.01 . . . . . . . . . . 5995 8 45 . 1 1 81 81 SER N N 15 . 1 1 81 81 SER H H 1 0.75 0.02 . . . . . . . . . . 5995 8 46 . 1 1 86 86 GLY N N 15 . 1 1 86 86 GLY H H 1 0.71 0.02 . . . . . . . . . . 5995 8 47 . 1 1 88 88 ASN N N 15 . 1 1 88 88 ASN H H 1 0.73 0.01 . . . . . . . . . . 5995 8 48 . 1 1 89 89 THR N N 15 . 1 1 89 89 THR H H 1 0.75 0.01 . . . . . . . . . . 5995 8 49 . 1 1 92 92 ILE N N 15 . 1 1 92 92 ILE H H 1 0.77 0.02 . . . . . . . . . . 5995 8 50 . 1 1 94 94 LYS N N 15 . 1 1 94 94 LYS H H 1 0.73 0.01 . . . . . . . . . . 5995 8 51 . 1 1 96 96 ASP N N 15 . 1 1 96 96 ASP H H 1 0.74 0.02 . . . . . . . . . . 5995 8 52 . 1 1 97 97 TYR N N 15 . 1 1 97 97 TYR H H 1 0.77 0.05 . . . . . . . . . . 5995 8 53 . 1 1 99 99 ASN N N 15 . 1 1 99 99 ASN H H 1 0.73 0.02 . . . . . . . . . . 5995 8 54 . 1 1 100 100 PHE N N 15 . 1 1 100 100 PHE H H 1 0.73 0.02 . . . . . . . . . . 5995 8 55 . 1 1 101 101 LEU N N 15 . 1 1 101 101 LEU H H 1 0.75 0.01 . . . . . . . . . . 5995 8 56 . 1 1 102 102 MET N N 15 . 1 1 102 102 MET H H 1 0.77 0.02 . . . . . . . . . . 5995 8 57 . 1 1 103 103 ALA N N 15 . 1 1 103 103 ALA H H 1 0.73 0.01 . . . . . . . . . . 5995 8 58 . 1 1 104 104 HIS N N 15 . 1 1 104 104 HIS H H 1 0.85 0.10 . . . . . . . . . . 5995 8 59 . 1 1 105 105 LEU N N 15 . 1 1 105 105 LEU H H 1 0.71 0.01 . . . . . . . . . . 5995 8 60 . 1 1 106 106 ILE N N 15 . 1 1 106 106 ILE H H 1 0.73 0.01 . . . . . . . . . . 5995 8 61 . 1 1 107 107 ASN N N 15 . 1 1 107 107 ASN H H 1 0.78 0.01 . . . . . . . . . . 5995 8 62 . 1 1 111 111 GLY N N 15 . 1 1 111 111 GLY H H 1 0.69 0.01 . . . . . . . . . . 5995 8 63 . 1 1 113 113 THR N N 15 . 1 1 113 113 THR H H 1 0.68 0.02 . . . . . . . . . . 5995 8 64 . 1 1 115 115 GLN N N 15 . 1 1 115 115 GLN H H 1 0.71 0.01 . . . . . . . . . . 5995 8 65 . 1 1 116 116 LEU N N 15 . 1 1 116 116 LEU H H 1 0.74 0.03 . . . . . . . . . . 5995 8 66 . 1 1 117 117 MET N N 15 . 1 1 117 117 MET H H 1 0.74 0.04 . . . . . . . . . . 5995 8 67 . 1 1 118 118 GLY N N 15 . 1 1 118 118 GLY H H 1 0.76 0.02 . . . . . . . . . . 5995 8 68 . 1 1 120 120 TYR N N 15 . 1 1 120 120 TYR H H 1 0.75 0.01 . . . . . . . . . . 5995 8 69 . 1 1 121 121 GLY N N 15 . 1 1 121 121 GLY H H 1 0.77 0.01 . . . . . . . . . . 5995 8 70 . 1 1 123 123 GLU N N 15 . 1 1 123 123 GLU H H 1 0.70 0.01 . . . . . . . . . . 5995 8 71 . 1 1 125 125 ASP N N 15 . 1 1 125 125 ASP H H 1 0.71 0.02 . . . . . . . . . . 5995 8 72 . 1 1 126 126 LEU N N 15 . 1 1 126 126 LEU H H 1 0.70 0.02 . . . . . . . . . . 5995 8 73 . 1 1 127 127 SER N N 15 . 1 1 127 127 SER H H 1 0.69 0.01 . . . . . . . . . . 5995 8 74 . 1 1 128 128 SER N N 15 . 1 1 128 128 SER H H 1 0.73 0.01 . . . . . . . . . . 5995 8 75 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.71 0.01 . . . . . . . . . . 5995 8 76 . 1 1 130 130 ILE N N 15 . 1 1 130 130 ILE H H 1 0.68 0.01 . . . . . . . . . . 5995 8 77 . 1 1 131 131 LYS N N 15 . 1 1 131 131 LYS H H 1 0.75 0.02 . . . . . . . . . . 5995 8 78 . 1 1 133 133 ARG N N 15 . 1 1 133 133 ARG H H 1 0.73 0.02 . . . . . . . . . . 5995 8 79 . 1 1 136 136 GLN N N 15 . 1 1 136 136 GLN H H 1 0.73 0.01 . . . . . . . . . . 5995 8 80 . 1 1 137 137 LEU N N 15 . 1 1 137 137 LEU H H 1 0.72 0.01 . . . . . . . . . . 5995 8 81 . 1 1 138 138 CYS N N 15 . 1 1 138 138 CYS H H 1 0.76 0.01 . . . . . . . . . . 5995 8 82 . 1 1 140 140 LYS N N 15 . 1 1 140 140 LYS H H 1 0.72 0.01 . . . . . . . . . . 5995 8 83 . 1 1 141 141 HIS N N 15 . 1 1 141 141 HIS H H 1 0.71 0.01 . . . . . . . . . . 5995 8 84 . 1 1 142 142 GLY N N 15 . 1 1 142 142 GLY H H 1 0.69 0.02 . . . . . . . . . . 5995 8 85 . 1 1 143 143 ILE N N 15 . 1 1 143 143 ILE H H 1 0.69 0.01 . . . . . . . . . . 5995 8 86 . 1 1 144 144 LEU N N 15 . 1 1 144 144 LEU H H 1 0.69 0.02 . . . . . . . . . . 5995 8 87 . 1 1 145 145 ARG N N 15 . 1 1 145 145 ARG H H 1 0.65 0.02 . . . . . . . . . . 5995 8 88 . 1 1 148 148 ILE N N 15 . 1 1 148 148 ILE H H 1 0.73 0.01 . . . . . . . . . . 5995 8 89 . 1 1 151 151 LEU N N 15 . 1 1 151 151 LEU H H 1 0.70 0.02 . . . . . . . . . . 5995 8 90 . 1 1 153 153 ASN N N 15 . 1 1 153 153 ASN H H 1 0.72 0.03 . . . . . . . . . . 5995 8 91 . 1 1 157 157 CYS N N 15 . 1 1 157 157 CYS H H 1 0.64 0.01 . . . . . . . . . . 5995 8 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_283_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 283_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $283K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 SER N N 15 964.99 51.89 . . . . . 5995 1 2 . 1 1 6 6 THR N N 15 845.49 67.59 . . . . . 5995 1 3 . 1 1 7 7 GLY N N 15 864.40 30.67 . . . . . 5995 1 4 . 1 1 11 11 ASN N N 15 902.21 27.08 . . . . . 5995 1 5 . 1 1 12 12 VAL N N 15 1050.7 20.74 . . . . . 5995 1 6 . 1 1 13 13 GLU N N 15 1055.8 33.58 . . . . . 5995 1 7 . 1 1 15 15 ILE N N 15 1042.9 21.53 . . . . . 5995 1 8 . 1 1 16 16 ASN N N 15 1042.9 32.33 . . . . . 5995 1 9 . 1 1 17 17 GLY N N 15 1038.9 38.36 . . . . . 5995 1 10 . 1 1 22 22 ILE N N 15 958.37 39.94 . . . . . 5995 1 11 . 1 1 23 23 ILE N N 15 1045.2 31.69 . . . . . 5995 1 12 . 1 1 26 26 SER N N 15 1046.9 27.14 . . . . . 5995 1 13 . 1 1 28 28 LYS N N 15 993.97 19.01 . . . . . 5995 1 14 . 1 1 30 30 GLU N N 15 891.38 32.23 . . . . . 5995 1 15 . 1 1 31 31 LYS N N 15 963.94 34.67 . . . . . 5995 1 16 . 1 1 32 32 ILE N N 15 956.89 42.70 . . . . . 5995 1 17 . 1 1 33 33 GLU N N 15 970.01 37.11 . . . . . 5995 1 18 . 1 1 36 36 GLY N N 15 913.30 19.86 . . . . . 5995 1 19 . 1 1 37 37 ASN N N 15 830.80 60.93 . . . . . 5995 1 20 . 1 1 39 39 ARG N N 15 977.28 33.34 . . . . . 5995 1 21 . 1 1 48 48 LEU N N 15 990.00 23.89 . . . . . 5995 1 22 . 1 1 51 51 SER N N 15 897.50 32.90 . . . . . 5995 1 23 . 1 1 54 54 LEU N N 15 1008.0 26.44 . . . . . 5995 1 24 . 1 1 61 61 ASP N N 15 889.94 73.26 . . . . . 5995 1 25 . 1 1 71 71 ALA N N 15 1013.9 34.91 . . . . . 5995 1 26 . 1 1 74 74 THR N N 15 907.06 24.94 . . . . . 5995 1 27 . 1 1 79 79 GLU N N 15 917.54 21.81 . . . . . 5995 1 28 . 1 1 81 81 SER N N 15 984.77 41.84 . . . . . 5995 1 29 . 1 1 84 84 TYR N N 15 1003.3 43.82 . . . . . 5995 1 30 . 1 1 85 85 ASP N N 15 889.19 71.06 . . . . . 5995 1 31 . 1 1 86 86 GLY N N 15 1002.2 24.37 . . . . . 5995 1 32 . 1 1 89 89 THR N N 15 964.39 24.66 . . . . . 5995 1 33 . 1 1 91 91 THR N N 15 1133.9 40.17 . . . . . 5995 1 34 . 1 1 92 92 ILE N N 15 1017.8 56.77 . . . . . 5995 1 35 . 1 1 94 94 LYS N N 15 1065.3 34.91 . . . . . 5995 1 36 . 1 1 96 96 ASP N N 15 1070.4 45.70 . . . . . 5995 1 37 . 1 1 97 97 TYR N N 15 1029.5 15.84 . . . . . 5995 1 38 . 1 1 100 100 PHE N N 15 1105.0 34.08 . . . . . 5995 1 39 . 1 1 101 101 LEU N N 15 1083.0 27.43 . . . . . 5995 1 40 . 1 1 103 103 ALA N N 15 1086.8 35.75 . . . . . 5995 1 41 . 1 1 105 105 LEU N N 15 1041.4 50.46 . . . . . 5995 1 42 . 1 1 107 107 ASN N N 15 954.94 31.14 . . . . . 5995 1 43 . 1 1 111 111 GLY N N 15 906.94 65.49 . . . . . 5995 1 44 . 1 1 115 115 GLN N N 15 1026.6 29.61 . . . . . 5995 1 45 . 1 1 116 116 LEU N N 15 1049.2 39.63 . . . . . 5995 1 46 . 1 1 117 117 MET N N 15 1091.5 54.07 . . . . . 5995 1 47 . 1 1 118 118 GLY N N 15 1044.4 35.00 . . . . . 5995 1 48 . 1 1 119 119 LEU N N 15 1033.4 25.50 . . . . . 5995 1 49 . 1 1 120 120 TYR N N 15 1076.6 19.75 . . . . . 5995 1 50 . 1 1 121 121 GLY N N 15 979.98 30.71 . . . . . 5995 1 51 . 1 1 125 125 ASP N N 15 1004.9 40.68 . . . . . 5995 1 52 . 1 1 126 126 LEU N N 15 1025.4 38.84 . . . . . 5995 1 53 . 1 1 127 127 SER N N 15 959.45 49.60 . . . . . 5995 1 54 . 1 1 130 130 ILE N N 15 937.98 29.23 . . . . . 5995 1 55 . 1 1 131 131 LYS N N 15 975.99 19.84 . . . . . 5995 1 56 . 1 1 133 133 ARG N N 15 983.31 19.71 . . . . . 5995 1 57 . 1 1 135 135 ALA N N 15 993.81 26.11 . . . . . 5995 1 58 . 1 1 136 136 GLN N N 15 1014.2 27.05 . . . . . 5995 1 59 . 1 1 137 137 LEU N N 15 1014.7 35.86 . . . . . 5995 1 60 . 1 1 138 138 CYS N N 15 1018.6 34.36 . . . . . 5995 1 61 . 1 1 140 140 LYS N N 15 1023.1 30.36 . . . . . 5995 1 62 . 1 1 141 141 HIS N N 15 1066.4 31.35 . . . . . 5995 1 63 . 1 1 142 142 GLY N N 15 997.53 31.09 . . . . . 5995 1 64 . 1 1 144 144 LEU N N 15 1048.1 28.83 . . . . . 5995 1 65 . 1 1 148 148 ILE N N 15 988.60 32.98 . . . . . 5995 1 66 . 1 1 151 151 LEU N N 15 1016.3 64.05 . . . . . 5995 1 67 . 1 1 160 160 ALA N N 15 678.35 22.73 . . . . . 5995 1 68 . 1 1 162 162 GLU N N 15 697.88 18.80 . . . . . 5995 1 stop_ save_ save_288_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 288_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Sample_condition_list_ID 2 _Heteronucl_T1_list.Sample_condition_list_label $288K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 2 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 901.18 29.93 . . . . . 5995 2 2 . 1 1 4 4 SER N N 15 913.94 41.60 . . . . . 5995 2 3 . 1 1 6 6 THR N N 15 785.19 42.00 . . . . . 5995 2 4 . 1 1 10 10 PHE N N 15 919.79 44.36 . . . . . 5995 2 5 . 1 1 11 11 ASN N N 15 864.18 35.43 . . . . . 5995 2 6 . 1 1 12 12 VAL N N 15 1008.8 26.53 . . . . . 5995 2 7 . 1 1 13 13 GLU N N 15 947.04 17.93 . . . . . 5995 2 8 . 1 1 16 16 ASN N N 15 954.55 24.81 . . . . . 5995 2 9 . 1 1 17 17 GLY N N 15 953.75 24.66 . . . . . 5995 2 10 . 1 1 22 22 ILE N N 15 954.51 26.37 . . . . . 5995 2 11 . 1 1 23 23 ILE N N 15 988.22 16.85 . . . . . 5995 2 12 . 1 1 24 24 LEU N N 15 967.27 23.88 . . . . . 5995 2 13 . 1 1 26 26 SER N N 15 965.41 18.26 . . . . . 5995 2 14 . 1 1 28 28 LYS N N 15 974.58 27.90 . . . . . 5995 2 15 . 1 1 30 30 GLU N N 15 850.14 20.94 . . . . . 5995 2 16 . 1 1 31 31 LYS N N 15 917.18 14.87 . . . . . 5995 2 17 . 1 1 32 32 ILE N N 15 882.21 19.86 . . . . . 5995 2 18 . 1 1 33 33 GLU N N 15 917.53 26.08 . . . . . 5995 2 19 . 1 1 35 35 ASN N N 15 968.10 20.76 . . . . . 5995 2 20 . 1 1 36 36 GLY N N 15 828.53 22.59 . . . . . 5995 2 21 . 1 1 37 37 ASN N N 15 833.18 29.01 . . . . . 5995 2 22 . 1 1 38 38 PHE N N 15 871.92 19.55 . . . . . 5995 2 23 . 1 1 39 39 ARG N N 15 942.60 32.82 . . . . . 5995 2 24 . 1 1 40 40 LEU N N 15 988.58 23.27 . . . . . 5995 2 25 . 1 1 46 46 HIS N N 15 949.54 16.66 . . . . . 5995 2 26 . 1 1 48 48 LEU N N 15 944.17 26.64 . . . . . 5995 2 27 . 1 1 51 51 SER N N 15 842.34 23.36 . . . . . 5995 2 28 . 1 1 53 53 VAL N N 15 1010.4 12.11 . . . . . 5995 2 29 . 1 1 54 54 LEU N N 15 959.97 21.16 . . . . . 5995 2 30 . 1 1 55 55 LYS N N 15 973.34 16.53 . . . . . 5995 2 31 . 1 1 58 58 THR N N 15 898.92 21.00 . . . . . 5995 2 32 . 1 1 60 60 ARG N N 15 904.37 25.17 . . . . . 5995 2 33 . 1 1 61 61 ASP N N 15 861.89 45.18 . . . . . 5995 2 34 . 1 1 62 62 GLU N N 15 860.53 22.63 . . . . . 5995 2 35 . 1 1 64 64 CYS N N 15 927.25 51.04 . . . . . 5995 2 36 . 1 1 66 66 GLU N N 15 872.46 29.34 . . . . . 5995 2 37 . 1 1 68 68 SER N N 15 945.88 21.66 . . . . . 5995 2 38 . 1 1 69 69 MET N N 15 974.01 20.53 . . . . . 5995 2 39 . 1 1 71 71 ALA N N 15 937.92 26.34 . . . . . 5995 2 40 . 1 1 72 72 ASP N N 15 1037.7 36.37 . . . . . 5995 2 41 . 1 1 74 74 THR N N 15 877.45 23.71 . . . . . 5995 2 42 . 1 1 75 75 GLU N N 15 872.33 54.33 . . . . . 5995 2 43 . 1 1 76 76 LYS N N 15 956.42 27.34 . . . . . 5995 2 44 . 1 1 77 77 ALA N N 15 939.33 101.4 . . . . . 5995 2 45 . 1 1 79 79 GLU N N 15 870.85 25.37 . . . . . 5995 2 46 . 1 1 80 80 TYR N N 15 910.63 14.33 . . . . . 5995 2 47 . 1 1 81 81 SER N N 15 950.37 25.3 . . . . . 5995 2 48 . 1 1 82 82 VAL N N 15 916.86 29.25 . . . . . 5995 2 49 . 1 1 84 84 TYR N N 15 980.29 18.51 . . . . . 5995 2 50 . 1 1 85 85 ASP N N 15 852.94 39.54 . . . . . 5995 2 51 . 1 1 86 86 GLY N N 15 921.54 20.87 . . . . . 5995 2 52 . 1 1 88 88 ASN N N 15 977.53 18.92 . . . . . 5995 2 53 . 1 1 89 89 THR N N 15 923.25 25.18 . . . . . 5995 2 54 . 1 1 91 91 THR N N 15 891.44 41.66 . . . . . 5995 2 55 . 1 1 92 92 ILE N N 15 937.66 32.53 . . . . . 5995 2 56 . 1 1 94 94 LYS N N 15 970.63 30.49 . . . . . 5995 2 57 . 1 1 95 95 THR N N 15 979.12 31.15 . . . . . 5995 2 58 . 1 1 96 96 ASP N N 15 947.53 20.55 . . . . . 5995 2 59 . 1 1 97 97 TYR N N 15 928.12 45.36 . . . . . 5995 2 60 . 1 1 99 99 ASN N N 15 857.21 53.45 . . . . . 5995 2 61 . 1 1 100 100 PHE N N 15 1014.1 12.83 . . . . . 5995 2 62 . 1 1 101 101 LEU N N 15 991.55 21.21 . . . . . 5995 2 63 . 1 1 102 102 MET N N 15 982.05 22.61 . . . . . 5995 2 64 . 1 1 103 103 ALA N N 15 996.75 17.16 . . . . . 5995 2 65 . 1 1 105 105 LEU N N 15 944.55 23.79 . . . . . 5995 2 66 . 1 1 107 107 ASN N N 15 911.95 26.21 . . . . . 5995 2 67 . 1 1 108 108 GLU N N 15 929.41 20.59 . . . . . 5995 2 68 . 1 1 111 111 GLY N N 15 822.93 46.74 . . . . . 5995 2 69 . 1 1 113 113 THR N N 15 883.08 27.35 . . . . . 5995 2 70 . 1 1 115 115 GLN N N 15 924.15 23.10 . . . . . 5995 2 71 . 1 1 116 116 LEU N N 15 965.39 24.42 . . . . . 5995 2 72 . 1 1 117 117 MET N N 15 979.25 30.60 . . . . . 5995 2 73 . 1 1 118 118 GLY N N 15 987.33 15.52 . . . . . 5995 2 74 . 1 1 119 119 LEU N N 15 981.57 16.25 . . . . . 5995 2 75 . 1 1 120 120 TYR N N 15 987.07 13.57 . . . . . 5995 2 76 . 1 1 121 121 GLY N N 15 949.24 15.50 . . . . . 5995 2 77 . 1 1 125 125 ASP N N 15 908.58 19.28 . . . . . 5995 2 78 . 1 1 126 126 LEU N N 15 966.15 14.52 . . . . . 5995 2 79 . 1 1 127 127 SER N N 15 904.95 31.29 . . . . . 5995 2 80 . 1 1 130 130 ILE N N 15 907.98 27.62 . . . . . 5995 2 81 . 1 1 131 131 LYS N N 15 893.79 23.19 . . . . . 5995 2 82 . 1 1 133 133 ARG N N 15 927.38 28.12 . . . . . 5995 2 83 . 1 1 135 135 ALA N N 15 901.67 24.20 . . . . . 5995 2 84 . 1 1 136 136 GLN N N 15 934.39 21.44 . . . . . 5995 2 85 . 1 1 137 137 LEU N N 15 936.71 23.43 . . . . . 5995 2 86 . 1 1 138 138 CYS N N 15 929.29 18.69 . . . . . 5995 2 87 . 1 1 140 140 LYS N N 15 947.99 25.22 . . . . . 5995 2 88 . 1 1 141 141 HIS N N 15 956.48 10.48 . . . . . 5995 2 89 . 1 1 142 142 GLY N N 15 939.07 22.06 . . . . . 5995 2 90 . 1 1 144 144 LEU N N 15 993.16 19.69 . . . . . 5995 2 91 . 1 1 145 145 ARG N N 15 959.39 20.79 . . . . . 5995 2 92 . 1 1 146 146 GLU N N 15 863.24 38.48 . . . . . 5995 2 93 . 1 1 148 148 ILE N N 15 939.94 22.82 . . . . . 5995 2 94 . 1 1 151 151 LEU N N 15 979.48 31.60 . . . . . 5995 2 95 . 1 1 155 155 ASN N N 15 961.72 22.88 . . . . . 5995 2 96 . 1 1 157 157 CYS N N 15 979.33 26.60 . . . . . 5995 2 97 . 1 1 158 158 LEU N N 15 970.03 15.26 . . . . . 5995 2 98 . 1 1 162 162 GLU N N 15 688.37 15.70 . . . . . 5995 2 stop_ save_ save_298_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 298_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 3 _Heteronucl_T1_list.Sample_condition_list_ID 4 _Heteronucl_T1_list.Sample_condition_list_label $298K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 3 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 736.03 13.27 . . . . . 5995 3 2 . 1 1 4 4 SER N N 15 674.35 41.11 . . . . . 5995 3 3 . 1 1 11 11 ASN N N 15 651.68 34.69 . . . . . 5995 3 4 . 1 1 12 12 VAL N N 15 759.17 22.32 . . . . . 5995 3 5 . 1 1 13 13 GLU N N 15 753.74 13.09 . . . . . 5995 3 6 . 1 1 16 16 ASN N N 15 756.46 7.279 . . . . . 5995 3 7 . 1 1 17 17 GLY N N 15 746.54 11.82 . . . . . 5995 3 8 . 1 1 18 18 GLU N N 15 798.67 35.61 . . . . . 5995 3 9 . 1 1 19 19 TRP N N 15 731.97 19.00 . . . . . 5995 3 10 . 1 1 20 20 HIS N N 15 720.22 12.10 . . . . . 5995 3 11 . 1 1 22 22 ILE N N 15 745.39 13.87 . . . . . 5995 3 12 . 1 1 23 23 ILE N N 15 772.34 9.415 . . . . . 5995 3 13 . 1 1 24 24 LEU N N 15 766.44 9.429 . . . . . 5995 3 14 . 1 1 26 26 SER N N 15 755.65 7.373 . . . . . 5995 3 15 . 1 1 27 27 ASP N N 15 734.82 14.62 . . . . . 5995 3 16 . 1 1 28 28 LYS N N 15 747.91 12.08 . . . . . 5995 3 17 . 1 1 30 30 GLU N N 15 620.98 25.04 . . . . . 5995 3 18 . 1 1 31 31 LYS N N 15 683.17 10.15 . . . . . 5995 3 19 . 1 1 32 32 ILE N N 15 706.68 11.31 . . . . . 5995 3 20 . 1 1 33 33 GLU N N 15 720.84 11.79 . . . . . 5995 3 21 . 1 1 36 36 GLY N N 15 648.01 19.03 . . . . . 5995 3 22 . 1 1 37 37 ASN N N 15 726.10 20.93 . . . . . 5995 3 23 . 1 1 38 38 PHE N N 15 696.68 15.81 . . . . . 5995 3 24 . 1 1 39 39 ARG N N 15 701.33 14.53 . . . . . 5995 3 25 . 1 1 40 40 LEU N N 15 760.03 18.49 . . . . . 5995 3 26 . 1 1 41 41 PHE N N 15 732.28 16.63 . . . . . 5995 3 27 . 1 1 48 48 LEU N N 15 751.53 16.45 . . . . . 5995 3 28 . 1 1 51 51 SER N N 15 627.33 20.09 . . . . . 5995 3 29 . 1 1 53 53 VAL N N 15 798.01 7.482 . . . . . 5995 3 30 . 1 1 54 54 LEU N N 15 772.15 13.66 . . . . . 5995 3 31 . 1 1 55 55 LYS N N 15 754.74 12.78 . . . . . 5995 3 32 . 1 1 57 57 HIS N N 15 735.43 17.22 . . . . . 5995 3 33 . 1 1 58 58 THR N N 15 769.52 23.73 . . . . . 5995 3 34 . 1 1 60 60 ARG N N 15 682.87 11.77 . . . . . 5995 3 35 . 1 1 62 62 GLU N N 15 669.51 22.49 . . . . . 5995 3 36 . 1 1 64 64 CYS N N 15 727.66 16.19 . . . . . 5995 3 37 . 1 1 66 66 GLU N N 15 678.88 32.27 . . . . . 5995 3 38 . 1 1 68 68 SER N N 15 682.53 28.74 . . . . . 5995 3 39 . 1 1 69 69 MET N N 15 787.15 10.93 . . . . . 5995 3 40 . 1 1 70 70 VAL N N 15 681.70 38.08 . . . . . 5995 3 41 . 1 1 71 71 ALA N N 15 756.05 20.04 . . . . . 5995 3 42 . 1 1 72 72 ASP N N 15 768.90 10.90 . . . . . 5995 3 43 . 1 1 74 74 THR N N 15 649.59 22.00 . . . . . 5995 3 44 . 1 1 75 75 GLU N N 15 657.87 28.80 . . . . . 5995 3 45 . 1 1 76 76 LYS N N 15 721.45 15.28 . . . . . 5995 3 46 . 1 1 79 79 GLU N N 15 675.73 9.531 . . . . . 5995 3 47 . 1 1 81 81 SER N N 15 726.80 11.42 . . . . . 5995 3 48 . 1 1 82 82 VAL N N 15 719.82 20.37 . . . . . 5995 3 49 . 1 1 84 84 TYR N N 15 751.74 12.70 . . . . . 5995 3 50 . 1 1 85 85 ASP N N 15 696.72 23.24 . . . . . 5995 3 51 . 1 1 86 86 GLY N N 15 712.04 14.52 . . . . . 5995 3 52 . 1 1 88 88 ASN N N 15 784.50 9.011 . . . . . 5995 3 53 . 1 1 89 89 THR N N 15 722.28 18.64 . . . . . 5995 3 54 . 1 1 91 91 THR N N 15 743.76 36.05 . . . . . 5995 3 55 . 1 1 92 92 ILE N N 15 743.85 27.33 . . . . . 5995 3 56 . 1 1 94 94 LYS N N 15 775.56 12.71 . . . . . 5995 3 57 . 1 1 96 96 ASP N N 15 751.25 16.00 . . . . . 5995 3 58 . 1 1 97 97 TYR N N 15 723.57 17.35 . . . . . 5995 3 59 . 1 1 100 100 PHE N N 15 827.86 21.74 . . . . . 5995 3 60 . 1 1 101 101 LEU N N 15 784.81 17.52 . . . . . 5995 3 61 . 1 1 103 103 ALA N N 15 793.94 29.08 . . . . . 5995 3 62 . 1 1 104 104 HIS N N 15 780.79 9.724 . . . . . 5995 3 63 . 1 1 105 105 LEU N N 15 752.35 17.82 . . . . . 5995 3 64 . 1 1 106 106 ILE N N 15 790.22 17.26 . . . . . 5995 3 65 . 1 1 107 107 ASN N N 15 731.97 16.15 . . . . . 5995 3 66 . 1 1 111 111 GLY N N 15 647.65 37.49 . . . . . 5995 3 67 . 1 1 113 113 THR N N 15 746.05 21.35 . . . . . 5995 3 68 . 1 1 114 114 PHE N N 15 743.98 9.151 . . . . . 5995 3 69 . 1 1 115 115 GLN N N 15 753.26 16.01 . . . . . 5995 3 70 . 1 1 116 116 LEU N N 15 768.75 12.98 . . . . . 5995 3 71 . 1 1 117 117 MET N N 15 795.66 16.78 . . . . . 5995 3 72 . 1 1 118 118 GLY N N 15 763.21 17.53 . . . . . 5995 3 73 . 1 1 119 119 LEU N N 15 771.38 11.51 . . . . . 5995 3 74 . 1 1 120 120 TYR N N 15 802.90 21.64 . . . . . 5995 3 75 . 1 1 121 121 GLY N N 15 756.73 16.37 . . . . . 5995 3 76 . 1 1 123 123 GLU N N 15 794.18 17.22 . . . . . 5995 3 77 . 1 1 125 125 ASP N N 15 717.87 18.22 . . . . . 5995 3 78 . 1 1 126 126 LEU N N 15 755.65 12.88 . . . . . 5995 3 79 . 1 1 127 127 SER N N 15 681.84 33.04 . . . . . 5995 3 80 . 1 1 128 128 SER N N 15 656.19 16.85 . . . . . 5995 3 81 . 1 1 129 129 ASP N N 15 828.27 8.724 . . . . . 5995 3 82 . 1 1 130 130 ILE N N 15 681.92 16.09 . . . . . 5995 3 83 . 1 1 131 131 LYS N N 15 713.62 15.03 . . . . . 5995 3 84 . 1 1 133 133 ARG N N 15 735.36 9.642 . . . . . 5995 3 85 . 1 1 134 134 PHE N N 15 719.19 12.33 . . . . . 5995 3 86 . 1 1 135 135 ALA N N 15 710.16 11.92 . . . . . 5995 3 87 . 1 1 136 136 GLN N N 15 751.75 9.767 . . . . . 5995 3 88 . 1 1 137 137 LEU N N 15 758.25 10.08 . . . . . 5995 3 89 . 1 1 138 138 CYS N N 15 735.38 8.301 . . . . . 5995 3 90 . 1 1 140 140 LYS N N 15 757.20 11.13 . . . . . 5995 3 91 . 1 1 141 141 HIS N N 15 793.54 9.562 . . . . . 5995 3 92 . 1 1 142 142 GLY N N 15 701.77 13.18 . . . . . 5995 3 93 . 1 1 143 143 ILE N N 15 684.93 20.87 . . . . . 5995 3 94 . 1 1 144 144 LEU N N 15 796.12 10.80 . . . . . 5995 3 95 . 1 1 145 145 ARG N N 15 713.77 19.30 . . . . . 5995 3 96 . 1 1 146 146 GLU N N 15 641.91 40.11 . . . . . 5995 3 97 . 1 1 148 148 ILE N N 15 751.66 11.91 . . . . . 5995 3 98 . 1 1 151 151 LEU N N 15 786.38 20.09 . . . . . 5995 3 99 . 1 1 158 158 LEU N N 15 741.72 16.73 . . . . . 5995 3 100 . 1 1 162 162 GLU N N 15 672.26 11.25 . . . . . 5995 3 stop_ save_ save_303_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 303_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 4 _Heteronucl_T1_list.Sample_condition_list_ID 5 _Heteronucl_T1_list.Sample_condition_list_label $303K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 4 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 693.16 15.60 . . . . . 5995 4 2 . 1 1 4 4 SER N N 15 626.41 41.09 . . . . . 5995 4 3 . 1 1 6 6 THR N N 15 572.46 33.45 . . . . . 5995 4 4 . 1 1 11 11 ASN N N 15 636.37 19.08 . . . . . 5995 4 5 . 1 1 12 12 VAL N N 15 734.34 5.511 . . . . . 5995 4 6 . 1 1 13 13 GLU N N 15 689.13 8.133 . . . . . 5995 4 7 . 1 1 16 16 ASN N N 15 708.41 8.800 . . . . . 5995 4 8 . 1 1 17 17 GLY N N 15 706.99 13.62 . . . . . 5995 4 9 . 1 1 19 19 TRP N N 15 696.41 8.728 . . . . . 5995 4 10 . 1 1 20 20 HIS N N 15 724.85 15.99 . . . . . 5995 4 11 . 1 1 21 21 THR N N 15 631.23 23.39 . . . . . 5995 4 12 . 1 1 22 22 ILE N N 15 693.06 4.859 . . . . . 5995 4 13 . 1 1 23 23 ILE N N 15 710.53 10.67 . . . . . 5995 4 14 . 1 1 24 24 LEU N N 15 704.78 8.992 . . . . . 5995 4 15 . 1 1 26 26 SER N N 15 701.72 12.22 . . . . . 5995 4 16 . 1 1 27 27 ASP N N 15 653.87 13.38 . . . . . 5995 4 17 . 1 1 28 28 LYS N N 15 760.60 11.51 . . . . . 5995 4 18 . 1 1 30 30 GLU N N 15 586.56 9.525 . . . . . 5995 4 19 . 1 1 31 31 LYS N N 15 650.87 6.777 . . . . . 5995 4 20 . 1 1 32 32 ILE N N 15 639.04 5.560 . . . . . 5995 4 21 . 1 1 33 33 GLU N N 15 650.32 10.64 . . . . . 5995 4 22 . 1 1 35 35 ASN N N 15 707.41 14.79 . . . . . 5995 4 23 . 1 1 36 36 GLY N N 15 628.19 3.859 . . . . . 5995 4 24 . 1 1 38 38 PHE N N 15 631.38 6.642 . . . . . 5995 4 25 . 1 1 39 39 ARG N N 15 664.39 7.511 . . . . . 5995 4 26 . 1 1 40 40 LEU N N 15 710.90 9.957 . . . . . 5995 4 27 . 1 1 42 42 LEU N N 15 701.77 8.900 . . . . . 5995 4 28 . 1 1 46 46 HIS N N 15 711.37 7.089 . . . . . 5995 4 29 . 1 1 48 48 LEU N N 15 693.20 10.85 . . . . . 5995 4 30 . 1 1 51 51 SER N N 15 608.07 6.784 . . . . . 5995 4 31 . 1 1 52 52 LEU N N 15 701.95 12.98 . . . . . 5995 4 32 . 1 1 53 53 VAL N N 15 745.17 11.89 . . . . . 5995 4 33 . 1 1 54 54 LEU N N 15 717.70 5.001 . . . . . 5995 4 34 . 1 1 55 55 LYS N N 15 693.21 11.08 . . . . . 5995 4 35 . 1 1 57 57 HIS N N 15 662.92 12.74 . . . . . 5995 4 36 . 1 1 58 58 THR N N 15 665.44 6.330 . . . . . 5995 4 37 . 1 1 60 60 ARG N N 15 720.52 4.747 . . . . . 5995 4 38 . 1 1 62 62 GLU N N 15 642.69 7.138 . . . . . 5995 4 39 . 1 1 64 64 CYS N N 15 678.44 11.10 . . . . . 5995 4 40 . 1 1 67 67 LEU N N 15 674.75 8.381 . . . . . 5995 4 41 . 1 1 68 68 SER N N 15 673.68 14.94 . . . . . 5995 4 42 . 1 1 69 69 MET N N 15 732.87 8.362 . . . . . 5995 4 43 . 1 1 70 70 VAL N N 15 651.95 25.00 . . . . . 5995 4 44 . 1 1 71 71 ALA N N 15 702.74 13.04 . . . . . 5995 4 45 . 1 1 72 72 ASP N N 15 723.77 11.66 . . . . . 5995 4 46 . 1 1 74 74 THR N N 15 652.93 8.470 . . . . . 5995 4 47 . 1 1 76 76 LYS N N 15 702.56 7.116 . . . . . 5995 4 48 . 1 1 77 77 ALA N N 15 733.56 33.59 . . . . . 5995 4 49 . 1 1 79 79 GLU N N 15 625.58 7.597 . . . . . 5995 4 50 . 1 1 81 81 SER N N 15 704.73 9.472 . . . . . 5995 4 51 . 1 1 84 84 TYR N N 15 741.87 6.212 . . . . . 5995 4 52 . 1 1 86 86 GLY N N 15 683.81 4.781 . . . . . 5995 4 53 . 1 1 88 88 ASN N N 15 733.62 9.969 . . . . . 5995 4 54 . 1 1 89 89 THR N N 15 681.94 11.99 . . . . . 5995 4 55 . 1 1 92 92 ILE N N 15 707.91 7.377 . . . . . 5995 4 56 . 1 1 94 94 LYS N N 15 698.04 10.19 . . . . . 5995 4 57 . 1 1 95 95 THR N N 15 716.00 8.562 . . . . . 5995 4 58 . 1 1 96 96 ASP N N 15 716.21 10.51 . . . . . 5995 4 59 . 1 1 97 97 TYR N N 15 673.24 9.319 . . . . . 5995 4 60 . 1 1 98 98 ASP N N 15 771.47 16.05 . . . . . 5995 4 61 . 1 1 99 99 ASN N N 15 731.53 5.300 . . . . . 5995 4 62 . 1 1 101 101 LEU N N 15 723.75 8.378 . . . . . 5995 4 63 . 1 1 102 102 MET N N 15 736.05 12.52 . . . . . 5995 4 64 . 1 1 103 103 ALA N N 15 743.35 11.43 . . . . . 5995 4 65 . 1 1 104 104 HIS N N 15 715.56 6.722 . . . . . 5995 4 66 . 1 1 105 105 LEU N N 15 710.57 12.86 . . . . . 5995 4 67 . 1 1 106 106 ILE N N 15 750.07 14.37 . . . . . 5995 4 68 . 1 1 107 107 ASN N N 15 673.99 8.740 . . . . . 5995 4 69 . 1 1 108 108 GLU N N 15 700.36 12.57 . . . . . 5995 4 70 . 1 1 110 110 ASP N N 15 744.22 11.16 . . . . . 5995 4 71 . 1 1 111 111 GLY N N 15 624.45 25.17 . . . . . 5995 4 72 . 1 1 113 113 THR N N 15 660.39 13.24 . . . . . 5995 4 73 . 1 1 114 114 PHE N N 15 702.85 5.705 . . . . . 5995 4 74 . 1 1 115 115 GLN N N 15 687.02 13.84 . . . . . 5995 4 75 . 1 1 116 116 LEU N N 15 720.69 11.74 . . . . . 5995 4 76 . 1 1 117 117 MET N N 15 734.83 13.66 . . . . . 5995 4 77 . 1 1 118 118 GLY N N 15 733.56 5.058 . . . . . 5995 4 78 . 1 1 119 119 LEU N N 15 775.64 21.80 . . . . . 5995 4 79 . 1 1 120 120 TYR N N 15 735.00 14.50 . . . . . 5995 4 80 . 1 1 121 121 GLY N N 15 714.40 12.04 . . . . . 5995 4 81 . 1 1 123 123 GLU N N 15 729.45 6.006 . . . . . 5995 4 82 . 1 1 125 125 ASP N N 15 687.20 8.610 . . . . . 5995 4 83 . 1 1 126 126 LEU N N 15 717.66 10.81 . . . . . 5995 4 84 . 1 1 127 127 SER N N 15 657.59 19.01 . . . . . 5995 4 85 . 1 1 128 128 SER N N 15 620.60 9.998 . . . . . 5995 4 86 . 1 1 129 129 ASP N N 15 787.13 5.809 . . . . . 5995 4 87 . 1 1 130 130 ILE N N 15 651.85 6.650 . . . . . 5995 4 88 . 1 1 131 131 LYS N N 15 672.06 7.273 . . . . . 5995 4 89 . 1 1 133 133 ARG N N 15 696.57 3.732 . . . . . 5995 4 90 . 1 1 135 135 ALA N N 15 647.70 8.966 . . . . . 5995 4 91 . 1 1 136 136 GLN N N 15 677.39 9.179 . . . . . 5995 4 92 . 1 1 137 137 LEU N N 15 697.81 12.97 . . . . . 5995 4 93 . 1 1 138 138 CYS N N 15 669.76 8.708 . . . . . 5995 4 94 . 1 1 140 140 LYS N N 15 697.30 10.09 . . . . . 5995 4 95 . 1 1 141 141 HIS N N 15 714.96 13.68 . . . . . 5995 4 96 . 1 1 142 142 GLY N N 15 674.15 9.983 . . . . . 5995 4 97 . 1 1 143 143 ILE N N 15 708.38 5.978 . . . . . 5995 4 98 . 1 1 144 144 LEU N N 15 737.35 12.70 . . . . . 5995 4 99 . 1 1 145 145 ARG N N 15 702.88 8.019 . . . . . 5995 4 100 . 1 1 146 146 GLU N N 15 643.91 22.75 . . . . . 5995 4 101 . 1 1 148 148 ILE N N 15 688.03 8.541 . . . . . 5995 4 102 . 1 1 151 151 LEU N N 15 748.67 10.82 . . . . . 5995 4 103 . 1 1 152 152 SER N N 15 730.77 13.45 . . . . . 5995 4 104 . 1 1 153 153 ASN N N 15 618.03 12.30 . . . . . 5995 4 105 . 1 1 157 157 CYS N N 15 696.53 9.016 . . . . . 5995 4 106 . 1 1 158 158 LEU N N 15 704.14 16.25 . . . . . 5995 4 107 . 1 1 162 162 GLU N N 15 724.13 7.893 . . . . . 5995 4 stop_ save_ save_308_600_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 308_600_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 5 _Heteronucl_T1_list.Sample_condition_list_ID 6 _Heteronucl_T1_list.Sample_condition_list_label $308K _Heteronucl_T1_list.Spectrometer_frequency_1H 600 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 5 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 SER N N 15 552.20 34.06 . . . . . 5995 5 2 . 1 1 13 13 GLU N N 15 631.74 2.738 . . . . . 5995 5 3 . 1 1 16 16 ASN N N 15 631.40 12.54 . . . . . 5995 5 4 . 1 1 17 17 GLY N N 15 636.25 5.679 . . . . . 5995 5 5 . 1 1 19 19 TRP N N 15 617.86 11.95 . . . . . 5995 5 6 . 1 1 22 22 ILE N N 15 620.38 15.04 . . . . . 5995 5 7 . 1 1 23 23 ILE N N 15 654.20 5.380 . . . . . 5995 5 8 . 1 1 26 26 SER N N 15 657.86 6.680 . . . . . 5995 5 9 . 1 1 30 30 GLU N N 15 531.74 24.25 . . . . . 5995 5 10 . 1 1 31 31 LYS N N 15 602.49 6.573 . . . . . 5995 5 11 . 1 1 32 32 ILE N N 15 604.25 4.094 . . . . . 5995 5 12 . 1 1 33 33 GLU N N 15 612.20 23.86 . . . . . 5995 5 13 . 1 1 36 36 GLY N N 15 562.89 8.659 . . . . . 5995 5 14 . 1 1 38 38 PHE N N 15 587.17 14.64 . . . . . 5995 5 15 . 1 1 39 39 ARG N N 15 594.73 13.39 . . . . . 5995 5 16 . 1 1 40 40 LEU N N 15 652.35 14.56 . . . . . 5995 5 17 . 1 1 48 48 LEU N N 15 647.13 4.022 . . . . . 5995 5 18 . 1 1 51 51 SER N N 15 539.86 17.36 . . . . . 5995 5 19 . 1 1 53 53 VAL N N 15 665.19 3.095 . . . . . 5995 5 20 . 1 1 54 54 LEU N N 15 637.25 14.75 . . . . . 5995 5 21 . 1 1 57 57 HIS N N 15 655.29 12.64 . . . . . 5995 5 22 . 1 1 60 60 ARG N N 15 576.43 22.80 . . . . . 5995 5 23 . 1 1 68 68 SER N N 15 567.41 32.79 . . . . . 5995 5 24 . 1 1 69 69 MET N N 15 663.33 21.72 . . . . . 5995 5 25 . 1 1 71 71 ALA N N 15 646.56 9.557 . . . . . 5995 5 26 . 1 1 74 74 THR N N 15 543.97 31.12 . . . . . 5995 5 27 . 1 1 79 79 GLU N N 15 552.79 13.52 . . . . . 5995 5 28 . 1 1 81 81 SER N N 15 606.03 7.765 . . . . . 5995 5 29 . 1 1 86 86 GLY N N 15 599.62 19.56 . . . . . 5995 5 30 . 1 1 89 89 THR N N 15 647.57 8.290 . . . . . 5995 5 31 . 1 1 92 92 ILE N N 15 632.77 10.86 . . . . . 5995 5 32 . 1 1 94 94 LYS N N 15 640.85 4.608 . . . . . 5995 5 33 . 1 1 96 96 ASP N N 15 642.56 5.491 . . . . . 5995 5 34 . 1 1 100 100 PHE N N 15 685.38 21.29 . . . . . 5995 5 35 . 1 1 101 101 LEU N N 15 664.76 8.433 . . . . . 5995 5 36 . 1 1 103 103 ALA N N 15 687.78 9.088 . . . . . 5995 5 37 . 1 1 105 105 LEU N N 15 645.20 12.88 . . . . . 5995 5 38 . 1 1 107 107 ASN N N 15 608.87 11.56 . . . . . 5995 5 39 . 1 1 111 111 GLY N N 15 567.71 41.93 . . . . . 5995 5 40 . 1 1 115 115 GLN N N 15 627.71 7.097 . . . . . 5995 5 41 . 1 1 116 116 LEU N N 15 646.29 6.840 . . . . . 5995 5 42 . 1 1 117 117 MET N N 15 668.43 8.982 . . . . . 5995 5 43 . 1 1 118 118 GLY N N 15 658.04 20.02 . . . . . 5995 5 44 . 1 1 120 120 TYR N N 15 658.24 11.38 . . . . . 5995 5 45 . 1 1 121 121 GLY N N 15 632.90 25.80 . . . . . 5995 5 46 . 1 1 123 123 GLU N N 15 538.07 35.47 . . . . . 5995 5 47 . 1 1 125 125 ASP N N 15 636.08 17.74 . . . . . 5995 5 48 . 1 1 126 126 LEU N N 15 644.99 20.80 . . . . . 5995 5 49 . 1 1 127 127 SER N N 15 593.21 34.71 . . . . . 5995 5 50 . 1 1 130 130 ILE N N 15 575.07 10.72 . . . . . 5995 5 51 . 1 1 133 133 ARG N N 15 629.27 17.04 . . . . . 5995 5 52 . 1 1 136 136 GLN N N 15 639.00 3.991 . . . . . 5995 5 53 . 1 1 137 137 LEU N N 15 641.37 6.181 . . . . . 5995 5 54 . 1 1 138 138 CYS N N 15 643.60 12.51 . . . . . 5995 5 55 . 1 1 140 140 LYS N N 15 634.60 7.735 . . . . . 5995 5 56 . 1 1 141 141 HIS N N 15 670.61 4.806 . . . . . 5995 5 57 . 1 1 142 142 GLY N N 15 565.94 21.62 . . . . . 5995 5 58 . 1 1 144 144 LEU N N 15 681.82 4.879 . . . . . 5995 5 59 . 1 1 145 145 ARG N N 15 596.62 17.93 . . . . . 5995 5 60 . 1 1 148 148 ILE N N 15 641.37 7.472 . . . . . 5995 5 61 . 1 1 151 151 LEU N N 15 651.38 18.40 . . . . . 5995 5 62 . 1 1 162 162 GLU N N 15 693.89 12.36 . . . . . 5995 5 stop_ save_ save_291_500_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 291_500_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 6 _Heteronucl_T1_list.Sample_condition_list_ID 7 _Heteronucl_T1_list.Sample_condition_list_label $291K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 6 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 4 4 SER N N 15 811.85 54.57 . . . . . 5995 6 2 . 1 1 6 6 THR N N 15 767.55 67.60 . . . . . 5995 6 3 . 1 1 7 7 GLY N N 15 821.77 56.27 . . . . . 5995 6 4 . 1 1 11 11 ASN N N 15 942.45 63.18 . . . . . 5995 6 5 . 1 1 12 12 VAL N N 15 831.62 25.49 . . . . . 5995 6 6 . 1 1 13 13 GLU N N 15 745.23 27.16 . . . . . 5995 6 7 . 1 1 15 15 ILE N N 15 729.62 28.18 . . . . . 5995 6 8 . 1 1 16 16 ASN N N 15 744.16 13.63 . . . . . 5995 6 9 . 1 1 17 17 GLY N N 15 711.84 41.38 . . . . . 5995 6 10 . 1 1 22 22 ILE N N 15 822.83 79.08 . . . . . 5995 6 11 . 1 1 23 23 ILE N N 15 723.82 38.98 . . . . . 5995 6 12 . 1 1 26 26 SER N N 15 738.63 8.208 . . . . . 5995 6 13 . 1 1 27 27 ASP N N 15 804.05 50.74 . . . . . 5995 6 14 . 1 1 30 30 GLU N N 15 712.60 14.09 . . . . . 5995 6 15 . 1 1 31 31 LYS N N 15 712.19 42.29 . . . . . 5995 6 16 . 1 1 32 32 ILE N N 15 704.44 22.03 . . . . . 5995 6 17 . 1 1 33 33 GLU N N 15 766.72 16.48 . . . . . 5995 6 18 . 1 1 36 36 GLY N N 15 805.59 38.74 . . . . . 5995 6 19 . 1 1 37 37 ASN N N 15 716.76 69.80 . . . . . 5995 6 20 . 1 1 39 39 ARG N N 15 755.61 25.32 . . . . . 5995 6 21 . 1 1 40 40 LEU N N 15 829.17 51.40 . . . . . 5995 6 22 . 1 1 47 47 VAL N N 15 739.21 13.56 . . . . . 5995 6 23 . 1 1 48 48 LEU N N 15 733.25 30.34 . . . . . 5995 6 24 . 1 1 51 51 SER N N 15 767.89 23.36 . . . . . 5995 6 25 . 1 1 53 53 VAL N N 15 772.55 11.47 . . . . . 5995 6 26 . 1 1 54 54 LEU N N 15 743.76 18.61 . . . . . 5995 6 27 . 1 1 55 55 LYS N N 15 762.62 23.86 . . . . . 5995 6 28 . 1 1 60 60 ARG N N 15 745.68 16.33 . . . . . 5995 6 29 . 1 1 64 64 CYS N N 15 869.85 116.1 . . . . . 5995 6 30 . 1 1 67 67 LEU N N 15 762.26 32.42 . . . . . 5995 6 31 . 1 1 68 68 SER N N 15 803.23 26.80 . . . . . 5995 6 32 . 1 1 69 69 MET N N 15 781.20 21.51 . . . . . 5995 6 33 . 1 1 71 71 ALA N N 15 734.25 26.22 . . . . . 5995 6 34 . 1 1 72 72 ASP N N 15 788.51 19.89 . . . . . 5995 6 35 . 1 1 74 74 THR N N 15 692.82 30.35 . . . . . 5995 6 36 . 1 1 76 76 LYS N N 15 827.63 24.59 . . . . . 5995 6 37 . 1 1 77 77 ALA N N 15 1149.5 218.1 . . . . . 5995 6 38 . 1 1 79 79 GLU N N 15 781.00 31.94 . . . . . 5995 6 39 . 1 1 80 80 TYR N N 15 752.85 65.51 . . . . . 5995 6 40 . 1 1 81 81 SER N N 15 714.54 20.43 . . . . . 5995 6 41 . 1 1 86 86 GLY N N 15 783.62 20.06 . . . . . 5995 6 42 . 1 1 88 88 ASN N N 15 759.11 17.56 . . . . . 5995 6 43 . 1 1 89 89 THR N N 15 712.96 28.72 . . . . . 5995 6 44 . 1 1 91 91 THR N N 15 630.74 93.85 . . . . . 5995 6 45 . 1 1 92 92 ILE N N 15 925.06 76.43 . . . . . 5995 6 46 . 1 1 94 94 LYS N N 15 765.60 23.15 . . . . . 5995 6 47 . 1 1 96 96 ASP N N 15 736.94 36.81 . . . . . 5995 6 48 . 1 1 97 97 TYR N N 15 711.25 25.78 . . . . . 5995 6 49 . 1 1 98 98 ASP N N 15 751.13 57.83 . . . . . 5995 6 50 . 1 1 100 100 PHE N N 15 804.66 31.37 . . . . . 5995 6 51 . 1 1 101 101 LEU N N 15 804.96 31.38 . . . . . 5995 6 52 . 1 1 102 102 MET N N 15 798.00 31.32 . . . . . 5995 6 53 . 1 1 103 103 ALA N N 15 701.67 30.53 . . . . . 5995 6 54 . 1 1 104 104 HIS N N 15 709.43 12.63 . . . . . 5995 6 55 . 1 1 105 105 LEU N N 15 704.09 50.48 . . . . . 5995 6 56 . 1 1 107 107 ASN N N 15 736.72 32.40 . . . . . 5995 6 57 . 1 1 108 108 GLU N N 15 735.05 24.54 . . . . . 5995 6 58 . 1 1 111 111 GLY N N 15 891.03 42.36 . . . . . 5995 6 59 . 1 1 113 113 THR N N 15 772.34 16.07 . . . . . 5995 6 60 . 1 1 115 115 GLN N N 15 778.00 12.14 . . . . . 5995 6 61 . 1 1 116 116 LEU N N 15 767.50 32.72 . . . . . 5995 6 62 . 1 1 117 117 MET N N 15 766.55 36.88 . . . . . 5995 6 63 . 1 1 118 118 GLY N N 15 761.97 19.09 . . . . . 5995 6 64 . 1 1 121 121 GLY N N 15 775.78 37.22 . . . . . 5995 6 65 . 1 1 123 123 GLU N N 15 723.26 47.33 . . . . . 5995 6 66 . 1 1 125 125 ASP N N 15 756.32 25.58 . . . . . 5995 6 67 . 1 1 126 126 LEU N N 15 823.30 28.05 . . . . . 5995 6 68 . 1 1 127 127 SER N N 15 760.24 28.41 . . . . . 5995 6 69 . 1 1 129 129 ASP N N 15 806.87 32.86 . . . . . 5995 6 70 . 1 1 130 130 ILE N N 15 779.06 22.47 . . . . . 5995 6 71 . 1 1 131 131 LYS N N 15 746.78 29.04 . . . . . 5995 6 72 . 1 1 133 133 ARG N N 15 721.75 16.69 . . . . . 5995 6 73 . 1 1 136 136 GLN N N 15 730.24 11.91 . . . . . 5995 6 74 . 1 1 137 137 LEU N N 15 737.33 15.03 . . . . . 5995 6 75 . 1 1 138 138 CYS N N 15 684.57 21.96 . . . . . 5995 6 76 . 1 1 140 140 LYS N N 15 725.02 13.25 . . . . . 5995 6 77 . 1 1 141 141 HIS N N 15 749.84 23.90 . . . . . 5995 6 78 . 1 1 142 142 GLY N N 15 725.01 16.32 . . . . . 5995 6 79 . 1 1 144 144 LEU N N 15 746.46 12.53 . . . . . 5995 6 80 . 1 1 145 145 ARG N N 15 733.20 15.75 . . . . . 5995 6 81 . 1 1 148 148 ILE N N 15 771.80 12.21 . . . . . 5995 6 82 . 1 1 151 151 LEU N N 15 802.69 47.95 . . . . . 5995 6 83 . 1 1 153 153 ASN N N 15 794.19 23.94 . . . . . 5995 6 84 . 1 1 158 158 LEU N N 15 745.11 36.55 . . . . . 5995 6 stop_ save_ save_297_500_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 297_500_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 7 _Heteronucl_T1_list.Sample_condition_list_ID 8 _Heteronucl_T1_list.Sample_condition_list_label $297K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 7 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 701.34 48.16 . . . . . 5995 7 2 . 1 1 4 4 SER N N 15 699.79 46.31 . . . . . 5995 7 3 . 1 1 6 6 THR N N 15 505.28 40.61 . . . . . 5995 7 4 . 1 1 7 7 GLY N N 15 714.30 30.04 . . . . . 5995 7 5 . 1 1 11 11 ASN N N 15 713.42 85.43 . . . . . 5995 7 6 . 1 1 12 12 VAL N N 15 678.17 11.23 . . . . . 5995 7 7 . 1 1 13 13 GLU N N 15 657.10 11.03 . . . . . 5995 7 8 . 1 1 15 15 ILE N N 15 654.09 10.60 . . . . . 5995 7 9 . 1 1 16 16 ASN N N 15 663.11 13.27 . . . . . 5995 7 10 . 1 1 17 17 GLY N N 15 620.52 25.73 . . . . . 5995 7 11 . 1 1 21 21 THR N N 15 709.89 126.8 . . . . . 5995 7 12 . 1 1 22 22 ILE N N 15 614.52 31.71 . . . . . 5995 7 13 . 1 1 23 23 ILE N N 15 703.28 16.45 . . . . . 5995 7 14 . 1 1 26 26 SER N N 15 653.68 29.57 . . . . . 5995 7 15 . 1 1 27 27 ASP N N 15 684.60 11.51 . . . . . 5995 7 16 . 1 1 30 30 GLU N N 15 646.75 28.48 . . . . . 5995 7 17 . 1 1 31 31 LYS N N 15 639.58 20.43 . . . . . 5995 7 18 . 1 1 32 32 ILE N N 15 628.22 22.21 . . . . . 5995 7 19 . 1 1 33 33 GLU N N 15 683.55 14.05 . . . . . 5995 7 20 . 1 1 36 36 GLY N N 15 671.35 14.14 . . . . . 5995 7 21 . 1 1 37 37 ASN N N 15 673.92 13.40 . . . . . 5995 7 22 . 1 1 39 39 ARG N N 15 704.56 23.95 . . . . . 5995 7 23 . 1 1 40 40 LEU N N 15 730.90 38.04 . . . . . 5995 7 24 . 1 1 42 42 LEU N N 15 710.51 41.79 . . . . . 5995 7 25 . 1 1 47 47 VAL N N 15 652.07 18.00 . . . . . 5995 7 26 . 1 1 48 48 LEU N N 15 636.63 15.08 . . . . . 5995 7 27 . 1 1 51 51 SER N N 15 663.85 13.84 . . . . . 5995 7 28 . 1 1 52 52 LEU N N 15 702.15 27.67 . . . . . 5995 7 29 . 1 1 54 54 LEU N N 15 643.21 7.902 . . . . . 5995 7 30 . 1 1 57 57 HIS N N 15 707.31 40.80 . . . . . 5995 7 31 . 1 1 60 60 ARG N N 15 742.09 21.71 . . . . . 5995 7 32 . 1 1 64 64 CYS N N 15 651.68 15.93 . . . . . 5995 7 33 . 1 1 65 65 SER N N 15 671.60 14.72 . . . . . 5995 7 34 . 1 1 66 66 GLU N N 15 629.70 11.55 . . . . . 5995 7 35 . 1 1 67 67 LEU N N 15 671.21 22.49 . . . . . 5995 7 36 . 1 1 68 68 SER N N 15 702.22 16.11 . . . . . 5995 7 37 . 1 1 69 69 MET N N 15 659.47 10.76 . . . . . 5995 7 38 . 1 1 71 71 ALA N N 15 664.71 11.32 . . . . . 5995 7 39 . 1 1 72 72 ASP N N 15 686.23 27.01 . . . . . 5995 7 40 . 1 1 74 74 THR N N 15 700.49 20.05 . . . . . 5995 7 41 . 1 1 77 77 ALA N N 15 637.43 16.21 . . . . . 5995 7 42 . 1 1 79 79 GLU N N 15 679.25 21.81 . . . . . 5995 7 43 . 1 1 80 80 TYR N N 15 715.94 45.10 . . . . . 5995 7 44 . 1 1 81 81 SER N N 15 688.72 28.25 . . . . . 5995 7 45 . 1 1 86 86 GLY N N 15 658.17 18.83 . . . . . 5995 7 46 . 1 1 88 88 ASN N N 15 663.09 12.48 . . . . . 5995 7 47 . 1 1 89 89 THR N N 15 683.73 26.26 . . . . . 5995 7 48 . 1 1 91 91 THR N N 15 627.62 63.43 . . . . . 5995 7 49 . 1 1 92 92 ILE N N 15 702.46 59.55 . . . . . 5995 7 50 . 1 1 94 94 LYS N N 15 662.17 28.33 . . . . . 5995 7 51 . 1 1 95 95 THR N N 15 704.84 47.93 . . . . . 5995 7 52 . 1 1 96 96 ASP N N 15 648.59 21.70 . . . . . 5995 7 53 . 1 1 97 97 TYR N N 15 648.01 21.22 . . . . . 5995 7 54 . 1 1 100 100 PHE N N 15 668.51 34.68 . . . . . 5995 7 55 . 1 1 101 101 LEU N N 15 675.79 22.13 . . . . . 5995 7 56 . 1 1 102 102 MET N N 15 698.46 7.334 . . . . . 5995 7 57 . 1 1 103 103 ALA N N 15 640.72 35.23 . . . . . 5995 7 58 . 1 1 104 104 HIS N N 15 659.31 15.05 . . . . . 5995 7 59 . 1 1 105 105 LEU N N 15 617.96 27.45 . . . . . 5995 7 60 . 1 1 107 107 ASN N N 15 665.56 14.38 . . . . . 5995 7 61 . 1 1 108 108 GLU N N 15 679.22 40.87 . . . . . 5995 7 62 . 1 1 111 111 GLY N N 15 769.13 48.54 . . . . . 5995 7 63 . 1 1 113 113 THR N N 15 628.13 23.55 . . . . . 5995 7 64 . 1 1 115 115 GLN N N 15 639.30 16.20 . . . . . 5995 7 65 . 1 1 116 116 LEU N N 15 651.76 14.97 . . . . . 5995 7 66 . 1 1 117 117 MET N N 15 658.37 19.65 . . . . . 5995 7 67 . 1 1 118 118 GLY N N 15 674.46 21.46 . . . . . 5995 7 68 . 1 1 121 121 GLY N N 15 644.63 18.13 . . . . . 5995 7 69 . 1 1 123 123 GLU N N 15 691.78 29.06 . . . . . 5995 7 70 . 1 1 125 125 ASP N N 15 696.51 12.58 . . . . . 5995 7 71 . 1 1 126 126 LEU N N 15 730.02 18.06 . . . . . 5995 7 72 . 1 1 127 127 SER N N 15 721.90 29.37 . . . . . 5995 7 73 . 1 1 129 129 ASP N N 15 656.09 10.38 . . . . . 5995 7 74 . 1 1 130 130 ILE N N 15 668.40 11.23 . . . . . 5995 7 75 . 1 1 131 131 LYS N N 15 619.79 22.79 . . . . . 5995 7 76 . 1 1 133 133 ARG N N 15 633.45 19.29 . . . . . 5995 7 77 . 1 1 136 136 GLN N N 15 636.89 7.609 . . . . . 5995 7 78 . 1 1 137 137 LEU N N 15 630.09 12.33 . . . . . 5995 7 79 . 1 1 138 138 CYS N N 15 614.82 11.43 . . . . . 5995 7 80 . 1 1 140 140 LYS N N 15 637.57 4.869 . . . . . 5995 7 81 . 1 1 141 141 HIS N N 15 677.46 16.16 . . . . . 5995 7 82 . 1 1 142 142 GLY N N 15 637.73 15.04 . . . . . 5995 7 83 . 1 1 144 144 LEU N N 15 667.92 10.42 . . . . . 5995 7 84 . 1 1 145 145 ARG N N 15 651.78 11.77 . . . . . 5995 7 85 . 1 1 148 148 ILE N N 15 640.75 11.56 . . . . . 5995 7 86 . 1 1 151 151 LEU N N 15 676.15 25.90 . . . . . 5995 7 87 . 1 1 152 152 SER N N 15 644.90 9.480 . . . . . 5995 7 88 . 1 1 153 153 ASN N N 15 661.92 20.04 . . . . . 5995 7 89 . 1 1 155 155 ASN N N 15 643.03 16.10 . . . . . 5995 7 stop_ save_ save_302_500_free_t1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode 302_500_free_t1 _Heteronucl_T1_list.Entry_ID 5995 _Heteronucl_T1_list.ID 8 _Heteronucl_T1_list.Sample_condition_list_ID 9 _Heteronucl_T1_list.Sample_condition_list_label $302K _Heteronucl_T1_list.Spectrometer_frequency_1H 500 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units ms _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 1 '15N T1' 1 $sample_1 . 5995 8 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 ALA N N 15 606.66 38.51 . . . . . 5995 8 2 . 1 1 4 4 SER N N 15 676.35 59.52 . . . . . 5995 8 3 . 1 1 11 11 ASN N N 15 635.67 53.59 . . . . . 5995 8 4 . 1 1 12 12 VAL N N 15 573.52 18.40 . . . . . 5995 8 5 . 1 1 13 13 GLU N N 15 555.92 17.81 . . . . . 5995 8 6 . 1 1 16 16 ASN N N 15 571.02 10.76 . . . . . 5995 8 7 . 1 1 17 17 GLY N N 15 546.61 24.99 . . . . . 5995 8 8 . 1 1 19 19 TRP N N 15 610.35 16.67 . . . . . 5995 8 9 . 1 1 20 20 HIS N N 15 576.19 24.00 . . . . . 5995 8 10 . 1 1 21 21 THR N N 15 632.84 79.69 . . . . . 5995 8 11 . 1 1 22 22 ILE N N 15 572.39 26.95 . . . . . 5995 8 12 . 1 1 23 23 ILE N N 15 583.98 12.17 . . . . . 5995 8 13 . 1 1 26 26 SER N N 15 548.14 21.40 . . . . . 5995 8 14 . 1 1 27 27 ASP N N 15 615.39 5.014 . . . . . 5995 8 15 . 1 1 30 30 GLU N N 15 555.69 17.25 . . . . . 5995 8 16 . 1 1 31 31 LYS N N 15 534.41 16.46 . . . . . 5995 8 17 . 1 1 32 32 ILE N N 15 564.66 14.46 . . . . . 5995 8 18 . 1 1 33 33 GLU N N 15 579.61 12.38 . . . . . 5995 8 19 . 1 1 35 35 ASN N N 15 602.21 42.13 . . . . . 5995 8 20 . 1 1 36 36 GLY N N 15 572.15 13.72 . . . . . 5995 8 21 . 1 1 37 37 ASN N N 15 549.25 16.81 . . . . . 5995 8 22 . 1 1 39 39 ARG N N 15 600.14 21.73 . . . . . 5995 8 23 . 1 1 40 40 LEU N N 15 650.55 31.26 . . . . . 5995 8 24 . 1 1 41 41 PHE N N 15 632.12 54.40 . . . . . 5995 8 25 . 1 1 42 42 LEU N N 15 614.53 45.01 . . . . . 5995 8 26 . 1 1 48 48 LEU N N 15 557.55 8.453 . . . . . 5995 8 27 . 1 1 51 51 SER N N 15 592.96 13.20 . . . . . 5995 8 28 . 1 1 52 52 LEU N N 15 631.31 19.81 . . . . . 5995 8 29 . 1 1 54 54 LEU N N 15 577.83 13.35 . . . . . 5995 8 30 . 1 1 57 57 HIS N N 15 638.77 12.53 . . . . . 5995 8 31 . 1 1 58 58 THR N N 15 597.50 10.32 . . . . . 5995 8 32 . 1 1 60 60 ARG N N 15 577.59 19.30 . . . . . 5995 8 33 . 1 1 64 64 CYS N N 15 554.77 18.69 . . . . . 5995 8 34 . 1 1 65 65 SER N N 15 581.93 34.05 . . . . . 5995 8 35 . 1 1 66 66 GLU N N 15 554.96 21.31 . . . . . 5995 8 36 . 1 1 68 68 SER N N 15 631.03 34.58 . . . . . 5995 8 37 . 1 1 69 69 MET N N 15 620.06 8.210 . . . . . 5995 8 38 . 1 1 70 70 VAL N N 15 533.04 14.36 . . . . . 5995 8 39 . 1 1 71 71 ALA N N 15 537.02 26.70 . . . . . 5995 8 40 . 1 1 72 72 ASP N N 15 459.50 61.78 . . . . . 5995 8 41 . 1 1 74 74 THR N N 15 574.95 27.19 . . . . . 5995 8 42 . 1 1 76 76 LYS N N 15 619.86 12.38 . . . . . 5995 8 43 . 1 1 77 77 ALA N N 15 576.38 9.525 . . . . . 5995 8 44 . 1 1 79 79 GLU N N 15 576.27 18.86 . . . . . 5995 8 45 . 1 1 81 81 SER N N 15 549.86 22.53 . . . . . 5995 8 46 . 1 1 86 86 GLY N N 15 579.59 18.92 . . . . . 5995 8 47 . 1 1 88 88 ASN N N 15 591.05 3.924 . . . . . 5995 8 48 . 1 1 89 89 THR N N 15 593.22 13.58 . . . . . 5995 8 49 . 1 1 92 92 ILE N N 15 725.26 56.74 . . . . . 5995 8 50 . 1 1 94 94 LYS N N 15 570.47 15.22 . . . . . 5995 8 51 . 1 1 96 96 ASP N N 15 549.52 16.19 . . . . . 5995 8 52 . 1 1 97 97 TYR N N 15 535.26 18.80 . . . . . 5995 8 53 . 1 1 99 99 ASN N N 15 545.78 20.55 . . . . . 5995 8 54 . 1 1 100 100 PHE N N 15 586.02 13.53 . . . . . 5995 8 55 . 1 1 101 101 LEU N N 15 592.79 15.56 . . . . . 5995 8 56 . 1 1 102 102 MET N N 15 590.68 23.99 . . . . . 5995 8 57 . 1 1 103 103 ALA N N 15 531.04 21.81 . . . . . 5995 8 58 . 1 1 104 104 HIS N N 15 529.05 11.74 . . . . . 5995 8 59 . 1 1 105 105 LEU N N 15 569.66 18.82 . . . . . 5995 8 60 . 1 1 106 106 ILE N N 15 574.93 16.49 . . . . . 5995 8 61 . 1 1 107 107 ASN N N 15 538.01 18.56 . . . . . 5995 8 62 . 1 1 111 111 GLY N N 15 653.63 61.36 . . . . . 5995 8 63 . 1 1 113 113 THR N N 15 580.02 22.49 . . . . . 5995 8 64 . 1 1 115 115 GLN N N 15 556.98 8.826 . . . . . 5995 8 65 . 1 1 116 116 LEU N N 15 569.42 17.56 . . . . . 5995 8 66 . 1 1 117 117 MET N N 15 566.03 16.99 . . . . . 5995 8 67 . 1 1 118 118 GLY N N 15 567.12 11.22 . . . . . 5995 8 68 . 1 1 120 120 TYR N N 15 577.95 18.49 . . . . . 5995 8 69 . 1 1 121 121 GLY N N 15 581.25 13.07 . . . . . 5995 8 70 . 1 1 123 123 GLU N N 15 635.58 17.87 . . . . . 5995 8 71 . 1 1 125 125 ASP N N 15 603.42 5.533 . . . . . 5995 8 72 . 1 1 126 126 LEU N N 15 646.28 11.05 . . . . . 5995 8 73 . 1 1 127 127 SER N N 15 648.04 46.42 . . . . . 5995 8 74 . 1 1 128 128 SER N N 15 614.96 16.07 . . . . . 5995 8 75 . 1 1 129 129 ASP N N 15 567.66 4.495 . . . . . 5995 8 76 . 1 1 130 130 ILE N N 15 558.89 15.65 . . . . . 5995 8 77 . 1 1 131 131 LYS N N 15 560.12 26.28 . . . . . 5995 8 78 . 1 1 133 133 ARG N N 15 580.34 14.45 . . . . . 5995 8 79 . 1 1 136 136 GLN N N 15 547.55 10.55 . . . . . 5995 8 80 . 1 1 137 137 LEU N N 15 558.47 10.16 . . . . . 5995 8 81 . 1 1 138 138 CYS N N 15 566.91 8.943 . . . . . 5995 8 82 . 1 1 140 140 LYS N N 15 551.99 7.600 . . . . . 5995 8 83 . 1 1 141 141 HIS N N 15 588.38 8.594 . . . . . 5995 8 84 . 1 1 142 142 GLY N N 15 568.44 6.729 . . . . . 5995 8 85 . 1 1 143 143 ILE N N 15 685.55 40.55 . . . . . 5995 8 86 . 1 1 144 144 LEU N N 15 597.81 18.97 . . . . . 5995 8 87 . 1 1 145 145 ARG N N 15 587.37 12.71 . . . . . 5995 8 88 . 1 1 148 148 ILE N N 15 551.23 10.02 . . . . . 5995 8 89 . 1 1 151 151 LEU N N 15 608.44 20.65 . . . . . 5995 8 90 . 1 1 153 153 ASN N N 15 594.95 24.68 . . . . . 5995 8 91 . 1 1 157 157 CYS N N 15 549.95 19.70 . . . . . 5995 8 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_283_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 283_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $283K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 4 4 SER N N 15 57.28 3.30 . . . . . . . 5995 1 2 . 1 1 6 6 THR N N 15 53.50 2.67 . . . . . . . 5995 1 3 . 1 1 7 7 GLY N N 15 53.45 2.29 . . . . . . . 5995 1 4 . 1 1 11 11 ASN N N 15 54.60 7.99 . . . . . . . 5995 1 5 . 1 1 12 12 VAL N N 15 59.21 4.10 . . . . . . . 5995 1 6 . 1 1 13 13 GLU N N 15 53.82 2.29 . . . . . . . 5995 1 7 . 1 1 15 15 ILE N N 15 59.13 3.25 . . . . . . . 5995 1 8 . 1 1 16 16 ASN N N 15 51.90 2.18 . . . . . . . 5995 1 9 . 1 1 17 17 GLY N N 15 52.33 3.60 . . . . . . . 5995 1 10 . 1 1 22 22 ILE N N 15 47.62 4.97 . . . . . . . 5995 1 11 . 1 1 23 23 ILE N N 15 53.86 3.25 . . . . . . . 5995 1 12 . 1 1 26 26 SER N N 15 59.63 5.26 . . . . . . . 5995 1 13 . 1 1 28 28 LYS N N 15 58.33 4.27 . . . . . . . 5995 1 14 . 1 1 30 30 GLU N N 15 54.78 1.57 . . . . . . . 5995 1 15 . 1 1 31 31 LYS N N 15 52.30 4.02 . . . . . . . 5995 1 16 . 1 1 32 32 ILE N N 15 52.68 1.48 . . . . . . . 5995 1 17 . 1 1 33 33 GLU N N 15 54.65 4.76 . . . . . . . 5995 1 18 . 1 1 36 36 GLY N N 15 56.15 3.52 . . . . . . . 5995 1 19 . 1 1 37 37 ASN N N 15 45.66 2.92 . . . . . . . 5995 1 20 . 1 1 39 39 ARG N N 15 50.03 3.46 . . . . . . . 5995 1 21 . 1 1 48 48 LEU N N 15 58.46 3.30 . . . . . . . 5995 1 22 . 1 1 51 51 SER N N 15 62.90 3.57 . . . . . . . 5995 1 23 . 1 1 54 54 LEU N N 15 63.52 4.88 . . . . . . . 5995 1 24 . 1 1 61 61 ASP N N 15 49.55 5.04 . . . . . . . 5995 1 25 . 1 1 71 71 ALA N N 15 60.24 3.88 . . . . . . . 5995 1 26 . 1 1 74 74 THR N N 15 63.21 3.02 . . . . . . . 5995 1 27 . 1 1 79 79 GLU N N 15 53.24 2.30 . . . . . . . 5995 1 28 . 1 1 81 81 SER N N 15 55.61 3.33 . . . . . . . 5995 1 29 . 1 1 84 84 TYR N N 15 59.79 3.91 . . . . . . . 5995 1 30 . 1 1 85 85 ASP N N 15 55.66 6.36 . . . . . . . 5995 1 31 . 1 1 86 86 GLY N N 15 54.72 3.35 . . . . . . . 5995 1 32 . 1 1 89 89 THR N N 15 49.17 2.42 . . . . . . . 5995 1 33 . 1 1 91 91 THR N N 15 44.38 4.14 . . . . . . . 5995 1 34 . 1 1 92 92 ILE N N 15 55.48 8.02 . . . . . . . 5995 1 35 . 1 1 94 94 LYS N N 15 49.70 2.28 . . . . . . . 5995 1 36 . 1 1 96 96 ASP N N 15 52.95 4.60 . . . . . . . 5995 1 37 . 1 1 97 97 TYR N N 15 55.78 3.20 . . . . . . . 5995 1 38 . 1 1 100 100 PHE N N 15 48.30 4.53 . . . . . . . 5995 1 39 . 1 1 101 101 LEU N N 15 50.04 0.46 . . . . . . . 5995 1 40 . 1 1 103 103 ALA N N 15 52.58 5.69 . . . . . . . 5995 1 41 . 1 1 105 105 LEU N N 15 53.03 3.37 . . . . . . . 5995 1 42 . 1 1 107 107 ASN N N 15 60.22 6.23 . . . . . . . 5995 1 43 . 1 1 111 111 GLY N N 15 53.34 3.38 . . . . . . . 5995 1 44 . 1 1 115 115 GLN N N 15 58.13 1.60 . . . . . . . 5995 1 45 . 1 1 116 116 LEU N N 15 48.16 6.07 . . . . . . . 5995 1 46 . 1 1 117 117 MET N N 15 49.98 3.30 . . . . . . . 5995 1 47 . 1 1 118 118 GLY N N 15 49.96 1.66 . . . . . . . 5995 1 48 . 1 1 119 119 LEU N N 15 50.46 3.45 . . . . . . . 5995 1 49 . 1 1 120 120 TYR N N 15 57.69 4.21 . . . . . . . 5995 1 50 . 1 1 121 121 GLY N N 15 55.93 5.93 . . . . . . . 5995 1 51 . 1 1 125 125 ASP N N 15 50.45 1.94 . . . . . . . 5995 1 52 . 1 1 126 126 LEU N N 15 54.95 2.63 . . . . . . . 5995 1 53 . 1 1 127 127 SER N N 15 57.45 3.89 . . . . . . . 5995 1 54 . 1 1 130 130 ILE N N 15 56.24 3.12 . . . . . . . 5995 1 55 . 1 1 131 131 LYS N N 15 53.97 2.19 . . . . . . . 5995 1 56 . 1 1 133 133 ARG N N 15 55.27 3.31 . . . . . . . 5995 1 57 . 1 1 135 135 ALA N N 15 56.38 2.31 . . . . . . . 5995 1 58 . 1 1 136 136 GLN N N 15 59.11 2.63 . . . . . . . 5995 1 59 . 1 1 137 137 LEU N N 15 54.44 3.29 . . . . . . . 5995 1 60 . 1 1 138 138 CYS N N 15 46.63 1.09 . . . . . . . 5995 1 61 . 1 1 140 140 LYS N N 15 54.90 3.90 . . . . . . . 5995 1 62 . 1 1 141 141 HIS N N 15 60.96 3.22 . . . . . . . 5995 1 63 . 1 1 142 142 GLY N N 15 55.38 2.05 . . . . . . . 5995 1 64 . 1 1 144 144 LEU N N 15 62.23 4.46 . . . . . . . 5995 1 65 . 1 1 148 148 ILE N N 15 58.20 3.05 . . . . . . . 5995 1 66 . 1 1 151 151 LEU N N 15 53.01 7.22 . . . . . . . 5995 1 67 . 1 1 160 160 ALA N N 15 95.94 7.32 . . . . . . . 5995 1 68 . 1 1 162 162 GLU N N 15 197.47 16.57 . . . . . . . 5995 1 stop_ save_ save_288_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 288_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Sample_condition_list_ID 2 _Heteronucl_T2_list.Sample_condition_list_label $288K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 66.08 4.67 . . . . . . . 5995 2 2 . 1 1 4 4 SER N N 15 73.39 3.93 . . . . . . . 5995 2 3 . 1 1 6 6 THR N N 15 61.84 3.71 . . . . . . . 5995 2 4 . 1 1 10 10 PHE N N 15 63.94 2.88 . . . . . . . 5995 2 5 . 1 1 11 11 ASN N N 15 58.87 2.99 . . . . . . . 5995 2 6 . 1 1 12 12 VAL N N 15 71.56 0.53 . . . . . . . 5995 2 7 . 1 1 13 13 GLU N N 15 61.22 5.83 . . . . . . . 5995 2 8 . 1 1 16 16 ASN N N 15 52.87 3.46 . . . . . . . 5995 2 9 . 1 1 17 17 GLY N N 15 66.70 1.43 . . . . . . . 5995 2 10 . 1 1 22 22 ILE N N 15 61.12 7.42 . . . . . . . 5995 2 11 . 1 1 23 23 ILE N N 15 71.59 10.62 . . . . . . . 5995 2 12 . 1 1 24 24 LEU N N 15 62.46 5.12 . . . . . . . 5995 2 13 . 1 1 26 26 SER N N 15 75.20 4.81 . . . . . . . 5995 2 14 . 1 1 28 28 LYS N N 15 64.48 2.55 . . . . . . . 5995 2 15 . 1 1 30 30 GLU N N 15 67.07 3.70 . . . . . . . 5995 2 16 . 1 1 31 31 LYS N N 15 57.78 5.67 . . . . . . . 5995 2 17 . 1 1 32 32 ILE N N 15 57.06 4.02 . . . . . . . 5995 2 18 . 1 1 33 33 GLU N N 15 66.75 3.78 . . . . . . . 5995 2 19 . 1 1 35 35 ASN N N 15 64.28 2.47 . . . . . . . 5995 2 20 . 1 1 36 36 GLY N N 15 63.74 2.76 . . . . . . . 5995 2 21 . 1 1 37 37 ASN N N 15 57.06 4.83 . . . . . . . 5995 2 22 . 1 1 38 38 PHE N N 15 60.02 1.73 . . . . . . . 5995 2 23 . 1 1 39 39 ARG N N 15 56.10 3.75 . . . . . . . 5995 2 24 . 1 1 40 40 LEU N N 15 50.26 4.72 . . . . . . . 5995 2 25 . 1 1 46 46 HIS N N 15 67.06 2.59 . . . . . . . 5995 2 26 . 1 1 48 48 LEU N N 15 69.63 5.53 . . . . . . . 5995 2 27 . 1 1 51 51 SER N N 15 69.12 3.09 . . . . . . . 5995 2 28 . 1 1 53 53 VAL N N 15 66.78 3.02 . . . . . . . 5995 2 29 . 1 1 54 54 LEU N N 15 74.51 0.41 . . . . . . . 5995 2 30 . 1 1 55 55 LYS N N 15 63.38 2.66 . . . . . . . 5995 2 31 . 1 1 58 58 THR N N 15 37.24 2.34 . . . . . . . 5995 2 32 . 1 1 60 60 ARG N N 15 63.37 2.49 . . . . . . . 5995 2 33 . 1 1 61 61 ASP N N 15 58.62 5.16 . . . . . . . 5995 2 34 . 1 1 62 62 GLU N N 15 24.18 4.72 . . . . . . . 5995 2 35 . 1 1 64 64 CYS N N 15 55.26 3.68 . . . . . . . 5995 2 36 . 1 1 66 66 GLU N N 15 48.51 2.84 . . . . . . . 5995 2 37 . 1 1 68 68 SER N N 15 65.66 5.05 . . . . . . . 5995 2 38 . 1 1 69 69 MET N N 15 63.62 2.76 . . . . . . . 5995 2 39 . 1 1 71 71 ALA N N 15 68.50 2.54 . . . . . . . 5995 2 40 . 1 1 72 72 ASP N N 15 71.91 6.51 . . . . . . . 5995 2 41 . 1 1 74 74 THR N N 15 73.37 5.72 . . . . . . . 5995 2 42 . 1 1 75 75 GLU N N 15 74.48 3.68 . . . . . . . 5995 2 43 . 1 1 76 76 LYS N N 15 63.09 5.00 . . . . . . . 5995 2 44 . 1 1 77 77 ALA N N 15 63.62 5.40 . . . . . . . 5995 2 45 . 1 1 79 79 GLU N N 15 60.17 3.08 . . . . . . . 5995 2 46 . 1 1 80 80 TYR N N 15 62.49 3.02 . . . . . . . 5995 2 47 . 1 1 81 81 SER N N 15 66.07 2.80 . . . . . . . 5995 2 48 . 1 1 82 82 VAL N N 15 56.62 10.61 . . . . . . . 5995 2 49 . 1 1 84 84 TYR N N 15 70.71 4.76 . . . . . . . 5995 2 50 . 1 1 85 85 ASP N N 15 63.62 2.07 . . . . . . . 5995 2 51 . 1 1 86 86 GLY N N 15 66.54 5.45 . . . . . . . 5995 2 52 . 1 1 88 88 ASN N N 15 68.06 5.18 . . . . . . . 5995 2 53 . 1 1 89 89 THR N N 15 68.16 3.82 . . . . . . . 5995 2 54 . 1 1 91 91 THR N N 15 40.40 3.45 . . . . . . . 5995 2 55 . 1 1 92 92 ILE N N 15 60.34 2.85 . . . . . . . 5995 2 56 . 1 1 94 94 LYS N N 15 56.09 2.99 . . . . . . . 5995 2 57 . 1 1 95 95 THR N N 15 50.92 3.66 . . . . . . . 5995 2 58 . 1 1 96 96 ASP N N 15 64.26 3.55 . . . . . . . 5995 2 59 . 1 1 97 97 TYR N N 15 63.55 5.20 . . . . . . . 5995 2 60 . 1 1 99 99 ASN N N 15 83.59 4.58 . . . . . . . 5995 2 61 . 1 1 100 100 PHE N N 15 62.95 9.41 . . . . . . . 5995 2 62 . 1 1 101 101 LEU N N 15 57.55 4.38 . . . . . . . 5995 2 63 . 1 1 102 102 MET N N 15 65.06 4.17 . . . . . . . 5995 2 64 . 1 1 103 103 ALA N N 15 64.40 3.99 . . . . . . . 5995 2 65 . 1 1 105 105 LEU N N 15 53.72 1.69 . . . . . . . 5995 2 66 . 1 1 107 107 ASN N N 15 66.77 2.55 . . . . . . . 5995 2 67 . 1 1 108 108 GLU N N 15 74.67 2.27 . . . . . . . 5995 2 68 . 1 1 111 111 GLY N N 15 66.10 5.24 . . . . . . . 5995 2 69 . 1 1 113 113 THR N N 15 73.22 4.83 . . . . . . . 5995 2 70 . 1 1 115 115 GLN N N 15 73.63 4.35 . . . . . . . 5995 2 71 . 1 1 116 116 LEU N N 15 67.34 4.88 . . . . . . . 5995 2 72 . 1 1 117 117 MET N N 15 48.37 6.46 . . . . . . . 5995 2 73 . 1 1 118 118 GLY N N 15 61.49 2.24 . . . . . . . 5995 2 74 . 1 1 119 119 LEU N N 15 57.14 3.69 . . . . . . . 5995 2 75 . 1 1 120 120 TYR N N 15 59.24 2.85 . . . . . . . 5995 2 76 . 1 1 121 121 GLY N N 15 54.12 3.85 . . . . . . . 5995 2 77 . 1 1 125 125 ASP N N 15 52.40 3.73 . . . . . . . 5995 2 78 . 1 1 126 126 LEU N N 15 68.70 2.37 . . . . . . . 5995 2 79 . 1 1 127 127 SER N N 15 71.83 9.50 . . . . . . . 5995 2 80 . 1 1 130 130 ILE N N 15 60.77 4.26 . . . . . . . 5995 2 81 . 1 1 131 131 LYS N N 15 68.89 1.16 . . . . . . . 5995 2 82 . 1 1 133 133 ARG N N 15 61.99 2.99 . . . . . . . 5995 2 83 . 1 1 135 135 ALA N N 15 65.11 3.83 . . . . . . . 5995 2 84 . 1 1 136 136 GLN N N 15 64.41 6.25 . . . . . . . 5995 2 85 . 1 1 137 137 LEU N N 15 60.88 3.46 . . . . . . . 5995 2 86 . 1 1 138 138 CYS N N 15 64.24 3.18 . . . . . . . 5995 2 87 . 1 1 140 140 LYS N N 15 63.96 2.89 . . . . . . . 5995 2 88 . 1 1 141 141 HIS N N 15 78.70 3.08 . . . . . . . 5995 2 89 . 1 1 142 142 GLY N N 15 61.61 2.77 . . . . . . . 5995 2 90 . 1 1 144 144 LEU N N 15 77.05 2.06 . . . . . . . 5995 2 91 . 1 1 145 145 ARG N N 15 66.03 2.25 . . . . . . . 5995 2 92 . 1 1 146 146 GLU N N 15 62.15 6.05 . . . . . . . 5995 2 93 . 1 1 148 148 ILE N N 15 70.58 3.75 . . . . . . . 5995 2 94 . 1 1 151 151 LEU N N 15 63.03 5.67 . . . . . . . 5995 2 95 . 1 1 155 155 ASN N N 15 50.56 4.58 . . . . . . . 5995 2 96 . 1 1 157 157 CYS N N 15 67.42 3.78 . . . . . . . 5995 2 97 . 1 1 158 158 LEU N N 15 70.61 6.30 . . . . . . . 5995 2 98 . 1 1 162 162 GLU N N 15 112.02 2.17 . . . . . . . 5995 2 stop_ save_ save_298_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 298_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Sample_condition_list_ID 4 _Heteronucl_T2_list.Sample_condition_list_label $298K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 70.93 4.31 . . . . . . . 5995 3 2 . 1 1 4 4 SER N N 15 90.48 9.50 . . . . . . . 5995 3 3 . 1 1 11 11 ASN N N 15 86.89 4.75 . . . . . . . 5995 3 4 . 1 1 12 12 VAL N N 15 85.37 5.14 . . . . . . . 5995 3 5 . 1 1 13 13 GLU N N 15 72.79 3.63 . . . . . . . 5995 3 6 . 1 1 16 16 ASN N N 15 73.54 2.74 . . . . . . . 5995 3 7 . 1 1 17 17 GLY N N 15 84.17 2.49 . . . . . . . 5995 3 8 . 1 1 18 18 GLU N N 15 50.38 2.34 . . . . . . . 5995 3 9 . 1 1 19 19 TRP N N 15 50.06 2.23 . . . . . . . 5995 3 10 . 1 1 20 20 HIS N N 15 61.70 1.63 . . . . . . . 5995 3 11 . 1 1 22 22 ILE N N 15 77.94 5.23 . . . . . . . 5995 3 12 . 1 1 23 23 ILE N N 15 85.40 2.93 . . . . . . . 5995 3 13 . 1 1 24 24 LEU N N 15 79.50 3.63 . . . . . . . 5995 3 14 . 1 1 26 26 SER N N 15 88.45 4.52 . . . . . . . 5995 3 15 . 1 1 27 27 ASP N N 15 82.69 3.70 . . . . . . . 5995 3 16 . 1 1 28 28 LYS N N 15 86.29 4.37 . . . . . . . 5995 3 17 . 1 1 30 30 GLU N N 15 85.93 2.18 . . . . . . . 5995 3 18 . 1 1 31 31 LYS N N 15 78.33 2.66 . . . . . . . 5995 3 19 . 1 1 32 32 ILE N N 15 77.42 4.15 . . . . . . . 5995 3 20 . 1 1 33 33 GLU N N 15 82.87 4.28 . . . . . . . 5995 3 21 . 1 1 36 36 GLY N N 15 88.96 4.55 . . . . . . . 5995 3 22 . 1 1 37 37 ASN N N 15 38.02 2.01 . . . . . . . 5995 3 23 . 1 1 38 38 PHE N N 15 82.80 4.58 . . . . . . . 5995 3 24 . 1 1 39 39 ARG N N 15 78.58 3.63 . . . . . . . 5995 3 25 . 1 1 40 40 LEU N N 15 71.50 2.93 . . . . . . . 5995 3 26 . 1 1 41 41 PHE N N 15 91.38 4.08 . . . . . . . 5995 3 27 . 1 1 48 48 LEU N N 15 89.78 2.87 . . . . . . . 5995 3 28 . 1 1 51 51 SER N N 15 94.44 6.05 . . . . . . . 5995 3 29 . 1 1 53 53 VAL N N 15 81.83 3.28 . . . . . . . 5995 3 30 . 1 1 54 54 LEU N N 15 89.99 4.69 . . . . . . . 5995 3 31 . 1 1 55 55 LYS N N 15 80.44 3.34 . . . . . . . 5995 3 32 . 1 1 57 57 HIS N N 15 51.15 3.20 . . . . . . . 5995 3 33 . 1 1 58 58 THR N N 15 64.99 1.97 . . . . . . . 5995 3 34 . 1 1 60 60 ARG N N 15 92.03 2.74 . . . . . . . 5995 3 35 . 1 1 62 62 GLU N N 15 39.55 3.33 . . . . . . . 5995 3 36 . 1 1 64 64 CYS N N 15 86.70 3.75 . . . . . . . 5995 3 37 . 1 1 66 66 GLU N N 15 89.16 2.02 . . . . . . . 5995 3 38 . 1 1 68 68 SER N N 15 83.47 3.70 . . . . . . . 5995 3 39 . 1 1 69 69 MET N N 15 79.47 3.94 . . . . . . . 5995 3 40 . 1 1 70 70 VAL N N 15 68.91 3.38 . . . . . . . 5995 3 41 . 1 1 71 71 ALA N N 15 87.38 3.60 . . . . . . . 5995 3 42 . 1 1 72 72 ASP N N 15 87.78 4.24 . . . . . . . 5995 3 43 . 1 1 74 74 THR N N 15 95.05 4.05 . . . . . . . 5995 3 44 . 1 1 75 75 GLU N N 15 89.53 5.26 . . . . . . . 5995 3 45 . 1 1 76 76 LYS N N 15 82.14 3.59 . . . . . . . 5995 3 46 . 1 1 79 79 GLU N N 15 78.81 3.23 . . . . . . . 5995 3 47 . 1 1 81 81 SER N N 15 84.35 4.06 . . . . . . . 5995 3 48 . 1 1 82 82 VAL N N 15 80.26 2.89 . . . . . . . 5995 3 49 . 1 1 84 84 TYR N N 15 90.88 2.99 . . . . . . . 5995 3 50 . 1 1 85 85 ASP N N 15 67.40 3.26 . . . . . . . 5995 3 51 . 1 1 86 86 GLY N N 15 85.83 4.22 . . . . . . . 5995 3 52 . 1 1 88 88 ASN N N 15 82.12 2.86 . . . . . . . 5995 3 53 . 1 1 89 89 THR N N 15 83.48 3.65 . . . . . . . 5995 3 54 . 1 1 91 91 THR N N 15 65.08 7.07 . . . . . . . 5995 3 55 . 1 1 92 92 ILE N N 15 79.45 4.69 . . . . . . . 5995 3 56 . 1 1 94 94 LYS N N 15 78.52 3.61 . . . . . . . 5995 3 57 . 1 1 96 96 ASP N N 15 80.64 3.59 . . . . . . . 5995 3 58 . 1 1 97 97 TYR N N 15 80.10 4.17 . . . . . . . 5995 3 59 . 1 1 100 100 PHE N N 15 77.70 3.52 . . . . . . . 5995 3 60 . 1 1 101 101 LEU N N 15 82.14 3.53 . . . . . . . 5995 3 61 . 1 1 103 103 ALA N N 15 80.62 4.30 . . . . . . . 5995 3 62 . 1 1 104 104 HIS N N 15 80.68 3.93 . . . . . . . 5995 3 63 . 1 1 105 105 LEU N N 15 74.55 3.28 . . . . . . . 5995 3 64 . 1 1 106 106 ILE N N 15 81.67 4.32 . . . . . . . 5995 3 65 . 1 1 107 107 ASN N N 15 87.63 4.42 . . . . . . . 5995 3 66 . 1 1 111 111 GLY N N 15 87.88 3.28 . . . . . . . 5995 3 67 . 1 1 113 113 THR N N 15 77.80 4.44 . . . . . . . 5995 3 68 . 1 1 114 114 PHE N N 15 80.61 3.44 . . . . . . . 5995 3 69 . 1 1 115 115 GLN N N 15 84.02 3.82 . . . . . . . 5995 3 70 . 1 1 116 116 LEU N N 15 83.66 3.86 . . . . . . . 5995 3 71 . 1 1 117 117 MET N N 15 79.27 3.85 . . . . . . . 5995 3 72 . 1 1 118 118 GLY N N 15 80.30 2.93 . . . . . . . 5995 3 73 . 1 1 119 119 LEU N N 15 77.27 3.45 . . . . . . . 5995 3 74 . 1 1 120 120 TYR N N 15 78.61 3.02 . . . . . . . 5995 3 75 . 1 1 121 121 GLY N N 15 72.62 3.27 . . . . . . . 5995 3 76 . 1 1 123 123 GLU N N 15 84.49 4.04 . . . . . . . 5995 3 77 . 1 1 125 125 ASP N N 15 77.60 2.67 . . . . . . . 5995 3 78 . 1 1 126 126 LEU N N 15 85.47 3.59 . . . . . . . 5995 3 79 . 1 1 127 127 SER N N 15 91.14 2.46 . . . . . . . 5995 3 80 . 1 1 128 128 SER N N 15 45.81 2.61 . . . . . . . 5995 3 81 . 1 1 129 129 ASP N N 15 88.83 3.69 . . . . . . . 5995 3 82 . 1 1 130 130 ILE N N 15 82.11 4.88 . . . . . . . 5995 3 83 . 1 1 131 131 LYS N N 15 81.57 3.08 . . . . . . . 5995 3 84 . 1 1 133 133 ARG N N 15 81.05 3.14 . . . . . . . 5995 3 85 . 1 1 134 134 PHE N N 15 82.06 3.97 . . . . . . . 5995 3 86 . 1 1 135 135 ALA N N 15 81.45 3.46 . . . . . . . 5995 3 87 . 1 1 136 136 GLN N N 15 88.15 4.38 . . . . . . . 5995 3 88 . 1 1 137 137 LEU N N 15 80.89 3.78 . . . . . . . 5995 3 89 . 1 1 138 138 CYS N N 15 76.65 3.17 . . . . . . . 5995 3 90 . 1 1 140 140 LYS N N 15 79.56 3.27 . . . . . . . 5995 3 91 . 1 1 141 141 HIS N N 15 92.58 3.64 . . . . . . . 5995 3 92 . 1 1 142 142 GLY N N 15 79.94 3.61 . . . . . . . 5995 3 93 . 1 1 143 143 ILE N N 15 40.04 2.90 . . . . . . . 5995 3 94 . 1 1 144 144 LEU N N 15 94.11 4.10 . . . . . . . 5995 3 95 . 1 1 145 145 ARG N N 15 84.17 3.03 . . . . . . . 5995 3 96 . 1 1 146 146 GLU N N 15 83.39 4.27 . . . . . . . 5995 3 97 . 1 1 148 148 ILE N N 15 87.19 3.11 . . . . . . . 5995 3 98 . 1 1 151 151 LEU N N 15 85.32 4.45 . . . . . . . 5995 3 99 . 1 1 158 158 LEU N N 15 84.44 3.52 . . . . . . . 5995 3 100 . 1 1 162 162 GLU N N 15 158.89 5.71 . . . . . . . 5995 3 stop_ save_ save_303_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 303_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Sample_condition_list_ID 5 _Heteronucl_T2_list.Sample_condition_list_label $303K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 92.55 3.45 . . . . . . . 5995 4 2 . 1 1 4 4 SER N N 15 87.57 3.18 . . . . . . . 5995 4 3 . 1 1 6 6 THR N N 15 66.30 1.71 . . . . . . . 5995 4 4 . 1 1 11 11 ASN N N 15 78.65 5.55 . . . . . . . 5995 4 5 . 1 1 12 12 VAL N N 15 109.01 4.35 . . . . . . . 5995 4 6 . 1 1 13 13 GLU N N 15 76.44 6.91 . . . . . . . 5995 4 7 . 1 1 16 16 ASN N N 15 62.81 5.09 . . . . . . . 5995 4 8 . 1 1 17 17 GLY N N 15 98.37 4.90 . . . . . . . 5995 4 9 . 1 1 19 19 TRP N N 15 109.17 3.45 . . . . . . . 5995 4 10 . 1 1 20 20 HIS N N 15 52.30 4.73 . . . . . . . 5995 4 11 . 1 1 21 21 THR N N 15 112.76 4.82 . . . . . . . 5995 4 12 . 1 1 22 22 ILE N N 15 99.72 5.08 . . . . . . . 5995 4 13 . 1 1 23 23 ILE N N 15 86.30 5.12 . . . . . . . 5995 4 14 . 1 1 24 24 LEU N N 15 84.58 4.28 . . . . . . . 5995 4 15 . 1 1 26 26 SER N N 15 82.98 5.35 . . . . . . . 5995 4 16 . 1 1 27 27 ASP N N 15 53.48 3.26 . . . . . . . 5995 4 17 . 1 1 28 28 LYS N N 15 77.33 9.39 . . . . . . . 5995 4 18 . 1 1 30 30 GLU N N 15 99.85 5.40 . . . . . . . 5995 4 19 . 1 1 31 31 LYS N N 15 81.93 12.20 . . . . . . . 5995 4 20 . 1 1 32 32 ILE N N 15 76.18 4.85 . . . . . . . 5995 4 21 . 1 1 33 33 GLU N N 15 43.98 5.24 . . . . . . . 5995 4 22 . 1 1 35 35 ASN N N 15 82.45 2.27 . . . . . . . 5995 4 23 . 1 1 36 36 GLY N N 15 100.87 4.43 . . . . . . . 5995 4 24 . 1 1 38 38 PHE N N 15 43.23 7.25 . . . . . . . 5995 4 25 . 1 1 39 39 ARG N N 15 56.57 2.87 . . . . . . . 5995 4 26 . 1 1 40 40 LEU N N 15 49.08 2.65 . . . . . . . 5995 4 27 . 1 1 42 42 LEU N N 15 99.31 6.91 . . . . . . . 5995 4 28 . 1 1 46 46 HIS N N 15 89.63 6.22 . . . . . . . 5995 4 29 . 1 1 48 48 LEU N N 15 89.00 2.72 . . . . . . . 5995 4 30 . 1 1 51 51 SER N N 15 76.91 7.50 . . . . . . . 5995 4 31 . 1 1 52 52 LEU N N 15 108.89 2.42 . . . . . . . 5995 4 32 . 1 1 53 53 VAL N N 15 90.55 7.62 . . . . . . . 5995 4 33 . 1 1 54 54 LEU N N 15 98.66 3.73 . . . . . . . 5995 4 34 . 1 1 55 55 LYS N N 15 116.71 3.10 . . . . . . . 5995 4 35 . 1 1 57 57 HIS N N 15 59.41 3.95 . . . . . . . 5995 4 36 . 1 1 58 58 THR N N 15 66.12 1.55 . . . . . . . 5995 4 37 . 1 1 60 60 ARG N N 15 76.40 3.00 . . . . . . . 5995 4 38 . 1 1 62 62 GLU N N 15 55.95 2.82 . . . . . . . 5995 4 39 . 1 1 64 64 CYS N N 15 92.53 6.85 . . . . . . . 5995 4 40 . 1 1 67 67 LEU N N 15 76.81 7.00 . . . . . . . 5995 4 41 . 1 1 68 68 SER N N 15 96.95 7.05 . . . . . . . 5995 4 42 . 1 1 69 69 MET N N 15 75.41 5.37 . . . . . . . 5995 4 43 . 1 1 70 70 VAL N N 15 84.43 6.57 . . . . . . . 5995 4 44 . 1 1 71 71 ALA N N 15 90.94 7.60 . . . . . . . 5995 4 45 . 1 1 72 72 ASP N N 15 97.30 8.44 . . . . . . . 5995 4 46 . 1 1 74 74 THR N N 15 81.76 5.27 . . . . . . . 5995 4 47 . 1 1 76 76 LYS N N 15 80.66 5.45 . . . . . . . 5995 4 48 . 1 1 77 77 ALA N N 15 71.20 3.84 . . . . . . . 5995 4 49 . 1 1 79 79 GLU N N 15 53.05 3.26 . . . . . . . 5995 4 50 . 1 1 81 81 SER N N 15 78.30 10.87 . . . . . . . 5995 4 51 . 1 1 84 84 TYR N N 15 114.15 6.27 . . . . . . . 5995 4 52 . 1 1 86 86 GLY N N 15 103.63 5.45 . . . . . . . 5995 4 53 . 1 1 88 88 ASN N N 15 77.20 6.98 . . . . . . . 5995 4 54 . 1 1 89 89 THR N N 15 70.33 1.96 . . . . . . . 5995 4 55 . 1 1 92 92 ILE N N 15 98.14 2.66 . . . . . . . 5995 4 56 . 1 1 94 94 LYS N N 15 59.20 2.47 . . . . . . . 5995 4 57 . 1 1 95 95 THR N N 15 85.27 3.66 . . . . . . . 5995 4 58 . 1 1 96 96 ASP N N 15 76.91 3.88 . . . . . . . 5995 4 59 . 1 1 97 97 TYR N N 15 81.00 3.10 . . . . . . . 5995 4 60 . 1 1 98 98 ASP N N 15 82.40 5.00 . . . . . . . 5995 4 61 . 1 1 99 99 ASN N N 15 63.99 3.39 . . . . . . . 5995 4 62 . 1 1 101 101 LEU N N 15 83.13 3.41 . . . . . . . 5995 4 63 . 1 1 102 102 MET N N 15 96.85 7.79 . . . . . . . 5995 4 64 . 1 1 103 103 ALA N N 15 96.91 4.38 . . . . . . . 5995 4 65 . 1 1 104 104 HIS N N 15 79.85 4.05 . . . . . . . 5995 4 66 . 1 1 105 105 LEU N N 15 84.86 4.38 . . . . . . . 5995 4 67 . 1 1 106 106 ILE N N 15 84.60 5.41 . . . . . . . 5995 4 68 . 1 1 107 107 ASN N N 15 82.90 5.37 . . . . . . . 5995 4 69 . 1 1 108 108 GLU N N 15 88.57 5.97 . . . . . . . 5995 4 70 . 1 1 110 110 ASP N N 15 77.30 4.03 . . . . . . . 5995 4 71 . 1 1 111 111 GLY N N 15 88.83 4.12 . . . . . . . 5995 4 72 . 1 1 113 113 THR N N 15 106.70 3.80 . . . . . . . 5995 4 73 . 1 1 114 114 PHE N N 15 92.29 5.23 . . . . . . . 5995 4 74 . 1 1 115 115 GLN N N 15 80.73 3.36 . . . . . . . 5995 4 75 . 1 1 116 116 LEU N N 15 90.98 4.61 . . . . . . . 5995 4 76 . 1 1 117 117 MET N N 15 83.36 4.86 . . . . . . . 5995 4 77 . 1 1 118 118 GLY N N 15 84.62 5.71 . . . . . . . 5995 4 78 . 1 1 119 119 LEU N N 15 103.59 8.99 . . . . . . . 5995 4 79 . 1 1 120 120 TYR N N 15 81.32 3.98 . . . . . . . 5995 4 80 . 1 1 121 121 GLY N N 15 81.55 5.50 . . . . . . . 5995 4 81 . 1 1 123 123 GLU N N 15 119.82 4.03 . . . . . . . 5995 4 82 . 1 1 125 125 ASP N N 15 59.12 1.53 . . . . . . . 5995 4 83 . 1 1 126 126 LEU N N 15 85.55 5.33 . . . . . . . 5995 4 84 . 1 1 127 127 SER N N 15 93.88 3.57 . . . . . . . 5995 4 85 . 1 1 128 128 SER N N 15 71.20 1.67 . . . . . . . 5995 4 86 . 1 1 129 129 ASP N N 15 109.07 2.57 . . . . . . . 5995 4 87 . 1 1 130 130 ILE N N 15 78.84 2.79 . . . . . . . 5995 4 88 . 1 1 131 131 LYS N N 15 92.06 4.90 . . . . . . . 5995 4 89 . 1 1 133 133 ARG N N 15 75.72 1.51 . . . . . . . 5995 4 90 . 1 1 135 135 ALA N N 15 79.41 5.87 . . . . . . . 5995 4 91 . 1 1 136 136 GLN N N 15 81.22 6.30 . . . . . . . 5995 4 92 . 1 1 137 137 LEU N N 15 58.44 4.40 . . . . . . . 5995 4 93 . 1 1 138 138 CYS N N 15 56.47 14.64 . . . . . . . 5995 4 94 . 1 1 140 140 LYS N N 15 60.12 1.63 . . . . . . . 5995 4 95 . 1 1 141 141 HIS N N 15 44.76 14.16 . . . . . . . 5995 4 96 . 1 1 142 142 GLY N N 15 58.74 1.27 . . . . . . . 5995 4 97 . 1 1 143 143 ILE N N 15 57.57 2.03 . . . . . . . 5995 4 98 . 1 1 144 144 LEU N N 15 97.85 5.83 . . . . . . . 5995 4 99 . 1 1 145 145 ARG N N 15 93.36 6.07 . . . . . . . 5995 4 100 . 1 1 146 146 GLU N N 15 82.93 2.98 . . . . . . . 5995 4 101 . 1 1 148 148 ILE N N 15 79.68 4.16 . . . . . . . 5995 4 102 . 1 1 151 151 LEU N N 15 101.01 5.90 . . . . . . . 5995 4 103 . 1 1 152 152 SER N N 15 94.98 1.65 . . . . . . . 5995 4 104 . 1 1 153 153 ASN N N 15 81.21 5.16 . . . . . . . 5995 4 105 . 1 1 157 157 CYS N N 15 90.56 6.88 . . . . . . . 5995 4 106 . 1 1 158 158 LEU N N 15 85.55 8.34 . . . . . . . 5995 4 107 . 1 1 162 162 GLU N N 15 200.01 7.39 . . . . . . . 5995 4 stop_ save_ save_308_600_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 308_600_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Sample_condition_list_ID 6 _Heteronucl_T2_list.Sample_condition_list_label $308K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 600 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 4 4 SER N N 15 69.42 3.55 . . . . . . . 5995 5 2 . 1 1 13 13 GLU N N 15 89.17 6.27 . . . . . . . 5995 5 3 . 1 1 16 16 ASN N N 15 84.83 4.50 . . . . . . . 5995 5 4 . 1 1 17 17 GLY N N 15 101.96 2.91 . . . . . . . 5995 5 5 . 1 1 19 19 TRP N N 15 78.09 4.82 . . . . . . . 5995 5 6 . 1 1 22 22 ILE N N 15 96.79 8.13 . . . . . . . 5995 5 7 . 1 1 23 23 ILE N N 15 100.90 5.95 . . . . . . . 5995 5 8 . 1 1 26 26 SER N N 15 98.48 3.43 . . . . . . . 5995 5 9 . 1 1 30 30 GLU N N 15 100.72 6.51 . . . . . . . 5995 5 10 . 1 1 31 31 LYS N N 15 95.97 6.18 . . . . . . . 5995 5 11 . 1 1 32 32 ILE N N 15 87.28 4.37 . . . . . . . 5995 5 12 . 1 1 33 33 GLU N N 15 88.22 6.77 . . . . . . . 5995 5 13 . 1 1 36 36 GLY N N 15 111.28 4.62 . . . . . . . 5995 5 14 . 1 1 38 38 PHE N N 15 99.28 7.08 . . . . . . . 5995 5 15 . 1 1 39 39 ARG N N 15 89.53 5.78 . . . . . . . 5995 5 16 . 1 1 40 40 LEU N N 15 87.59 2.93 . . . . . . . 5995 5 17 . 1 1 48 48 LEU N N 15 105.15 5.81 . . . . . . . 5995 5 18 . 1 1 51 51 SER N N 15 104.14 7.16 . . . . . . . 5995 5 19 . 1 1 53 53 VAL N N 15 97.24 4.39 . . . . . . . 5995 5 20 . 1 1 54 54 LEU N N 15 104.82 5.89 . . . . . . . 5995 5 21 . 1 1 57 57 HIS N N 15 83.84 5.64 . . . . . . . 5995 5 22 . 1 1 60 60 ARG N N 15 101.84 6.04 . . . . . . . 5995 5 23 . 1 1 68 68 SER N N 15 106.45 1.89 . . . . . . . 5995 5 24 . 1 1 69 69 MET N N 15 94.63 5.70 . . . . . . . 5995 5 25 . 1 1 71 71 ALA N N 15 101.87 6.14 . . . . . . . 5995 5 26 . 1 1 74 74 THR N N 15 108.16 6.94 . . . . . . . 5995 5 27 . 1 1 79 79 GLU N N 15 87.51 3.49 . . . . . . . 5995 5 28 . 1 1 81 81 SER N N 15 99.49 4.67 . . . . . . . 5995 5 29 . 1 1 86 86 GLY N N 15 107.48 4.43 . . . . . . . 5995 5 30 . 1 1 89 89 THR N N 15 94.44 10.81 . . . . . . . 5995 5 31 . 1 1 92 92 ILE N N 15 101.91 6.07 . . . . . . . 5995 5 32 . 1 1 94 94 LYS N N 15 108.65 4.12 . . . . . . . 5995 5 33 . 1 1 96 96 ASP N N 15 93.82 7.88 . . . . . . . 5995 5 34 . 1 1 100 100 PHE N N 15 88.94 5.51 . . . . . . . 5995 5 35 . 1 1 101 101 LEU N N 15 97.67 4.37 . . . . . . . 5995 5 36 . 1 1 103 103 ALA N N 15 97.16 3.42 . . . . . . . 5995 5 37 . 1 1 105 105 LEU N N 15 89.63 6.42 . . . . . . . 5995 5 38 . 1 1 107 107 ASN N N 15 95.09 4.10 . . . . . . . 5995 5 39 . 1 1 111 111 GLY N N 15 111.73 14.27 . . . . . . . 5995 5 40 . 1 1 115 115 GLN N N 15 99.90 7.32 . . . . . . . 5995 5 41 . 1 1 116 116 LEU N N 15 103.61 3.98 . . . . . . . 5995 5 42 . 1 1 117 117 MET N N 15 94.11 4.14 . . . . . . . 5995 5 43 . 1 1 118 118 GLY N N 15 95.50 4.01 . . . . . . . 5995 5 44 . 1 1 120 120 TYR N N 15 96.12 3.51 . . . . . . . 5995 5 45 . 1 1 121 121 GLY N N 15 89.74 4.86 . . . . . . . 5995 5 46 . 1 1 123 123 GLU N N 15 112.51 9.63 . . . . . . . 5995 5 47 . 1 1 125 125 ASP N N 15 96.14 5.86 . . . . . . . 5995 5 48 . 1 1 126 126 LEU N N 15 102.18 4.44 . . . . . . . 5995 5 49 . 1 1 127 127 SER N N 15 113.23 6.53 . . . . . . . 5995 5 50 . 1 1 130 130 ILE N N 15 95.09 6.10 . . . . . . . 5995 5 51 . 1 1 133 133 ARG N N 15 91.09 5.08 . . . . . . . 5995 5 52 . 1 1 136 136 GLN N N 15 96.62 5.35 . . . . . . . 5995 5 53 . 1 1 137 137 LEU N N 15 89.94 5.96 . . . . . . . 5995 5 54 . 1 1 138 138 CYS N N 15 85.22 5.45 . . . . . . . 5995 5 55 . 1 1 140 140 LYS N N 15 93.44 6.83 . . . . . . . 5995 5 56 . 1 1 141 141 HIS N N 15 93.32 7.59 . . . . . . . 5995 5 57 . 1 1 142 142 GLY N N 15 91.21 7.83 . . . . . . . 5995 5 58 . 1 1 144 144 LEU N N 15 113.18 4.93 . . . . . . . 5995 5 59 . 1 1 145 145 ARG N N 15 102.95 4.53 . . . . . . . 5995 5 60 . 1 1 148 148 ILE N N 15 100.12 5.50 . . . . . . . 5995 5 61 . 1 1 151 151 LEU N N 15 101.89 3.78 . . . . . . . 5995 5 62 . 1 1 162 162 GLU N N 15 230.75 7.13 . . . . . . . 5995 5 stop_ save_ save_291_500_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 291_500_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Sample_condition_list_ID 7 _Heteronucl_T2_list.Sample_condition_list_label $291K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 4 4 SER N N 15 81.61 5.66 . . . . . . . 5995 6 2 . 1 1 6 6 THR N N 15 64.49 3.54 . . . . . . . 5995 6 3 . 1 1 7 7 GLY N N 15 79.78 3.99 . . . . . . . 5995 6 4 . 1 1 11 11 ASN N N 15 77.08 3.44 . . . . . . . 5995 6 5 . 1 1 12 12 VAL N N 15 74.47 4.27 . . . . . . . 5995 6 6 . 1 1 13 13 GLU N N 15 67.26 4.98 . . . . . . . 5995 6 7 . 1 1 15 15 ILE N N 15 76.07 4.40 . . . . . . . 5995 6 8 . 1 1 16 16 ASN N N 15 66.50 1.50 . . . . . . . 5995 6 9 . 1 1 17 17 GLY N N 15 77.19 5.73 . . . . . . . 5995 6 10 . 1 1 22 22 ILE N N 15 59.48 2.89 . . . . . . . 5995 6 11 . 1 1 23 23 ILE N N 15 72.48 2.77 . . . . . . . 5995 6 12 . 1 1 26 26 SER N N 15 77.43 4.37 . . . . . . . 5995 6 13 . 1 1 27 27 ASP N N 15 60.89 3.50 . . . . . . . 5995 6 14 . 1 1 30 30 GLU N N 15 77.30 2.30 . . . . . . . 5995 6 15 . 1 1 31 31 LYS N N 15 70.73 4.33 . . . . . . . 5995 6 16 . 1 1 32 32 ILE N N 15 80.48 8.05 . . . . . . . 5995 6 17 . 1 1 33 33 GLU N N 15 78.73 4.48 . . . . . . . 5995 6 18 . 1 1 36 36 GLY N N 15 80.64 5.51 . . . . . . . 5995 6 19 . 1 1 37 37 ASN N N 15 64.00 6.57 . . . . . . . 5995 6 20 . 1 1 39 39 ARG N N 15 78.38 2.08 . . . . . . . 5995 6 21 . 1 1 40 40 LEU N N 15 61.62 6.47 . . . . . . . 5995 6 22 . 1 1 47 47 VAL N N 15 80.08 1.80 . . . . . . . 5995 6 23 . 1 1 48 48 LEU N N 15 77.27 4.86 . . . . . . . 5995 6 24 . 1 1 51 51 SER N N 15 84.34 3.46 . . . . . . . 5995 6 25 . 1 1 53 53 VAL N N 15 70.42 3.58 . . . . . . . 5995 6 26 . 1 1 54 54 LEU N N 15 75.35 4.83 . . . . . . . 5995 6 27 . 1 1 55 55 LYS N N 15 73.64 3.89 . . . . . . . 5995 6 28 . 1 1 60 60 ARG N N 15 81.60 2.68 . . . . . . . 5995 6 29 . 1 1 64 64 CYS N N 15 60.26 2.66 . . . . . . . 5995 6 30 . 1 1 67 67 LEU N N 15 74.53 2.76 . . . . . . . 5995 6 31 . 1 1 68 68 SER N N 15 74.68 2.19 . . . . . . . 5995 6 32 . 1 1 69 69 MET N N 15 73.81 6.10 . . . . . . . 5995 6 33 . 1 1 71 71 ALA N N 15 77.80 5.16 . . . . . . . 5995 6 34 . 1 1 72 72 ASP N N 15 74.16 4.08 . . . . . . . 5995 6 35 . 1 1 74 74 THR N N 15 82.89 6.82 . . . . . . . 5995 6 36 . 1 1 76 76 LYS N N 15 73.96 3.35 . . . . . . . 5995 6 37 . 1 1 77 77 ALA N N 15 86.25 7.30 . . . . . . . 5995 6 38 . 1 1 79 79 GLU N N 15 75.51 3.30 . . . . . . . 5995 6 39 . 1 1 80 80 TYR N N 15 75.59 6.26 . . . . . . . 5995 6 40 . 1 1 81 81 SER N N 15 79.55 3.85 . . . . . . . 5995 6 41 . 1 1 86 86 GLY N N 15 77.90 3.75 . . . . . . . 5995 6 42 . 1 1 88 88 ASN N N 15 75.12 2.78 . . . . . . . 5995 6 43 . 1 1 89 89 THR N N 15 64.09 7.83 . . . . . . . 5995 6 44 . 1 1 91 91 THR N N 15 70.62 11.0 . . . . . . . 5995 6 45 . 1 1 92 92 ILE N N 15 70.44 5.89 . . . . . . . 5995 6 46 . 1 1 94 94 LYS N N 15 69.50 5.01 . . . . . . . 5995 6 47 . 1 1 96 96 ASP N N 15 81.23 5.82 . . . . . . . 5995 6 48 . 1 1 97 97 TYR N N 15 72.21 6.38 . . . . . . . 5995 6 49 . 1 1 98 98 ASP N N 15 64.85 5.16 . . . . . . . 5995 6 50 . 1 1 100 100 PHE N N 15 63.03 2.88 . . . . . . . 5995 6 51 . 1 1 101 101 LEU N N 15 70.02 4.27 . . . . . . . 5995 6 52 . 1 1 102 102 MET N N 15 71.75 3.94 . . . . . . . 5995 6 53 . 1 1 103 103 ALA N N 15 72.61 2.85 . . . . . . . 5995 6 54 . 1 1 104 104 HIS N N 15 76.75 5.84 . . . . . . . 5995 6 55 . 1 1 105 105 LEU N N 15 68.88 5.25 . . . . . . . 5995 6 56 . 1 1 107 107 ASN N N 15 70.30 2.80 . . . . . . . 5995 6 57 . 1 1 108 108 GLU N N 15 77.65 2.21 . . . . . . . 5995 6 58 . 1 1 111 111 GLY N N 15 84.46 7.28 . . . . . . . 5995 6 59 . 1 1 113 113 THR N N 15 80.88 6.56 . . . . . . . 5995 6 60 . 1 1 115 115 GLN N N 15 70.72 1.72 . . . . . . . 5995 6 61 . 1 1 116 116 LEU N N 15 82.67 3.48 . . . . . . . 5995 6 62 . 1 1 117 117 MET N N 15 73.03 5.03 . . . . . . . 5995 6 63 . 1 1 118 118 GLY N N 15 67.57 4.21 . . . . . . . 5995 6 64 . 1 1 121 121 GLY N N 15 70.52 6.09 . . . . . . . 5995 6 65 . 1 1 123 123 GLU N N 15 67.17 5.35 . . . . . . . 5995 6 66 . 1 1 125 125 ASP N N 15 68.84 2.91 . . . . . . . 5995 6 67 . 1 1 126 126 LEU N N 15 76.53 1.26 . . . . . . . 5995 6 68 . 1 1 127 127 SER N N 15 78.27 1.89 . . . . . . . 5995 6 69 . 1 1 129 129 ASP N N 15 77.14 3.35 . . . . . . . 5995 6 70 . 1 1 130 130 ILE N N 15 76.62 4.05 . . . . . . . 5995 6 71 . 1 1 131 131 LYS N N 15 75.25 5.01 . . . . . . . 5995 6 72 . 1 1 133 133 ARG N N 15 71.88 3.66 . . . . . . . 5995 6 73 . 1 1 136 136 GLN N N 15 76.33 2.86 . . . . . . . 5995 6 74 . 1 1 137 137 LEU N N 15 74.79 3.17 . . . . . . . 5995 6 75 . 1 1 138 138 CYS N N 15 70.59 1.96 . . . . . . . 5995 6 76 . 1 1 140 140 LYS N N 15 74.39 3.57 . . . . . . . 5995 6 77 . 1 1 141 141 HIS N N 15 77.54 3.89 . . . . . . . 5995 6 78 . 1 1 142 142 GLY N N 15 80.80 5.79 . . . . . . . 5995 6 79 . 1 1 144 144 LEU N N 15 77.79 3.19 . . . . . . . 5995 6 80 . 1 1 145 145 ARG N N 15 76.81 3.51 . . . . . . . 5995 6 81 . 1 1 148 148 ILE N N 15 74.28 2.52 . . . . . . . 5995 6 82 . 1 1 151 151 LEU N N 15 68.00 5.04 . . . . . . . 5995 6 83 . 1 1 153 153 ASN N N 15 79.52 5.27 . . . . . . . 5995 6 84 . 1 1 158 158 LEU N N 15 76.58 2.21 . . . . . . . 5995 6 stop_ save_ save_297_500_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 297_500_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Sample_condition_list_ID 8 _Heteronucl_T2_list.Sample_condition_list_label $297K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 7 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 93.19 7.28 . . . . . . . 5995 7 2 . 1 1 4 4 SER N N 15 86.77 4.27 . . . . . . . 5995 7 3 . 1 1 6 6 THR N N 15 82.18 14.2 . . . . . . . 5995 7 4 . 1 1 7 7 GLY N N 15 89.33 7.87 . . . . . . . 5995 7 5 . 1 1 11 11 ASN N N 15 88.16 7.28 . . . . . . . 5995 7 6 . 1 1 12 12 VAL N N 15 86.42 2.61 . . . . . . . 5995 7 7 . 1 1 13 13 GLU N N 15 73.51 1.16 . . . . . . . 5995 7 8 . 1 1 15 15 ILE N N 15 80.70 3.27 . . . . . . . 5995 7 9 . 1 1 16 16 ASN N N 15 68.57 1.93 . . . . . . . 5995 7 10 . 1 1 17 17 GLY N N 15 88.59 3.53 . . . . . . . 5995 7 11 . 1 1 21 21 THR N N 15 74.19 11.4 . . . . . . . 5995 7 12 . 1 1 22 22 ILE N N 15 78.33 3.64 . . . . . . . 5995 7 13 . 1 1 23 23 ILE N N 15 82.03 2.26 . . . . . . . 5995 7 14 . 1 1 26 26 SER N N 15 46.23 3.27 . . . . . . . 5995 7 15 . 1 1 27 27 ASP N N 15 91.43 4.28 . . . . . . . 5995 7 16 . 1 1 30 30 GLU N N 15 86.02 4.16 . . . . . . . 5995 7 17 . 1 1 31 31 LYS N N 15 78.73 3.52 . . . . . . . 5995 7 18 . 1 1 32 32 ILE N N 15 86.61 6.07 . . . . . . . 5995 7 19 . 1 1 33 33 GLU N N 15 85.28 3.29 . . . . . . . 5995 7 20 . 1 1 36 36 GLY N N 15 89.27 2.81 . . . . . . . 5995 7 21 . 1 1 37 37 ASN N N 15 84.40 4.39 . . . . . . . 5995 7 22 . 1 1 39 39 ARG N N 15 77.37 4.22 . . . . . . . 5995 7 23 . 1 1 40 40 LEU N N 15 56.19 3.42 . . . . . . . 5995 7 24 . 1 1 42 42 LEU N N 15 61.16 3.36 . . . . . . . 5995 7 25 . 1 1 47 47 VAL N N 15 87.86 3.43 . . . . . . . 5995 7 26 . 1 1 48 48 LEU N N 15 88.31 2.12 . . . . . . . 5995 7 27 . 1 1 51 51 SER N N 15 94.27 4.52 . . . . . . . 5995 7 28 . 1 1 52 52 LEU N N 15 83.87 3.67 . . . . . . . 5995 7 29 . 1 1 54 54 LEU N N 15 85.01 3.61 . . . . . . . 5995 7 30 . 1 1 57 57 HIS N N 15 75.36 6.40 . . . . . . . 5995 7 31 . 1 1 60 60 ARG N N 15 89.19 7.16 . . . . . . . 5995 7 32 . 1 1 64 64 CYS N N 15 85.71 3.54 . . . . . . . 5995 7 33 . 1 1 65 65 SER N N 15 92.98 4.00 . . . . . . . 5995 7 34 . 1 1 66 66 GLU N N 15 85.04 3.09 . . . . . . . 5995 7 35 . 1 1 67 67 LEU N N 15 81.31 2.86 . . . . . . . 5995 7 36 . 1 1 68 68 SER N N 15 83.20 3.23 . . . . . . . 5995 7 37 . 1 1 69 69 MET N N 15 82.86 3.64 . . . . . . . 5995 7 38 . 1 1 71 71 ALA N N 15 86.32 5.61 . . . . . . . 5995 7 39 . 1 1 72 72 ASP N N 15 77.63 3.99 . . . . . . . 5995 7 40 . 1 1 74 74 THR N N 15 93.57 4.04 . . . . . . . 5995 7 41 . 1 1 77 77 ALA N N 15 91.76 3.23 . . . . . . . 5995 7 42 . 1 1 79 79 GLU N N 15 80.89 3.85 . . . . . . . 5995 7 43 . 1 1 80 80 TYR N N 15 92.51 12.7 . . . . . . . 5995 7 44 . 1 1 81 81 SER N N 15 85.04 3.38 . . . . . . . 5995 7 45 . 1 1 86 86 GLY N N 15 82.29 3.39 . . . . . . . 5995 7 46 . 1 1 88 88 ASN N N 15 84.34 2.17 . . . . . . . 5995 7 47 . 1 1 89 89 THR N N 15 79.14 4.43 . . . . . . . 5995 7 48 . 1 1 91 91 THR N N 15 51.85 3.59 . . . . . . . 5995 7 49 . 1 1 92 92 ILE N N 15 74.87 4.47 . . . . . . . 5995 7 50 . 1 1 94 94 LYS N N 15 81.8 3.72 . . . . . . . 5995 7 51 . 1 1 95 95 THR N N 15 78.90 4.02 . . . . . . . 5995 7 52 . 1 1 96 96 ASP N N 15 73.01 0.14 . . . . . . . 5995 7 53 . 1 1 97 97 TYR N N 15 88.02 2.45 . . . . . . . 5995 7 54 . 1 1 100 100 PHE N N 15 63.84 3.49 . . . . . . . 5995 7 55 . 1 1 101 101 LEU N N 15 79.79 4.69 . . . . . . . 5995 7 56 . 1 1 102 102 MET N N 15 82.12 2.68 . . . . . . . 5995 7 57 . 1 1 103 103 ALA N N 15 77.07 1.02 . . . . . . . 5995 7 58 . 1 1 104 104 HIS N N 15 84.96 4.98 . . . . . . . 5995 7 59 . 1 1 105 105 LEU N N 15 73.10 3.60 . . . . . . . 5995 7 60 . 1 1 107 107 ASN N N 15 79.76 3.60 . . . . . . . 5995 7 61 . 1 1 108 108 GLU N N 15 58.54 3.06 . . . . . . . 5995 7 62 . 1 1 111 111 GLY N N 15 95.31 9.55 . . . . . . . 5995 7 63 . 1 1 113 113 THR N N 15 79.45 2.82 . . . . . . . 5995 7 64 . 1 1 115 115 GLN N N 15 84.27 3.30 . . . . . . . 5995 7 65 . 1 1 116 116 LEU N N 15 81.96 2.50 . . . . . . . 5995 7 66 . 1 1 117 117 MET N N 15 81.22 4.00 . . . . . . . 5995 7 67 . 1 1 118 118 GLY N N 15 83.06 3.15 . . . . . . . 5995 7 68 . 1 1 121 121 GLY N N 15 84.43 3.20 . . . . . . . 5995 7 69 . 1 1 123 123 GLU N N 15 81.97 4.29 . . . . . . . 5995 7 70 . 1 1 125 125 ASP N N 15 79.18 2.61 . . . . . . . 5995 7 71 . 1 1 126 126 LEU N N 15 85.89 3.32 . . . . . . . 5995 7 72 . 1 1 127 127 SER N N 15 91.48 3.58 . . . . . . . 5995 7 73 . 1 1 129 129 ASP N N 15 80.70 3.70 . . . . . . . 5995 7 74 . 1 1 130 130 ILE N N 15 84.37 3.44 . . . . . . . 5995 7 75 . 1 1 131 131 LYS N N 15 81.83 2.51 . . . . . . . 5995 7 76 . 1 1 133 133 ARG N N 15 84.14 2.90 . . . . . . . 5995 7 77 . 1 1 136 136 GLN N N 15 85.23 2.61 . . . . . . . 5995 7 78 . 1 1 137 137 LEU N N 15 85.25 3.09 . . . . . . . 5995 7 79 . 1 1 138 138 CYS N N 15 81.29 3.32 . . . . . . . 5995 7 80 . 1 1 140 140 LYS N N 15 83.43 2.87 . . . . . . . 5995 7 81 . 1 1 141 141 HIS N N 15 85.66 3.25 . . . . . . . 5995 7 82 . 1 1 142 142 GLY N N 15 90.41 2.92 . . . . . . . 5995 7 83 . 1 1 144 144 LEU N N 15 91.81 3.99 . . . . . . . 5995 7 84 . 1 1 145 145 ARG N N 15 88.81 2.57 . . . . . . . 5995 7 85 . 1 1 148 148 ILE N N 15 88.66 3.50 . . . . . . . 5995 7 86 . 1 1 151 151 LEU N N 15 81.23 6.13 . . . . . . . 5995 7 87 . 1 1 152 152 SER N N 15 84.18 3.20 . . . . . . . 5995 7 88 . 1 1 153 153 ASN N N 15 95.67 4.25 . . . . . . . 5995 7 89 . 1 1 155 155 ASN N N 15 72.05 1.46 . . . . . . . 5995 7 stop_ save_ save_302_500_free_t2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode 302_500_free_t2 _Heteronucl_T2_list.Entry_ID 5995 _Heteronucl_T2_list.ID 8 _Heteronucl_T2_list.Sample_condition_list_ID 9 _Heteronucl_T2_list.Sample_condition_list_label $302K _Heteronucl_T2_list.Temp_calibration_method . _Heteronucl_T2_list.Temp_control_method . _Heteronucl_T2_list.Spectrometer_frequency_1H 500 _Heteronucl_T2_list.T2_coherence_type Nx _Heteronucl_T2_list.T2_val_units ms _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 '15N T2' 1 $sample_1 . 5995 8 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 ALA N N 15 99.22 4.66 . . . . . . . 5995 8 2 . 1 1 4 4 SER N N 15 98.25 6.56 . . . . . . . 5995 8 3 . 1 1 11 11 ASN N N 15 113.9 6.57 . . . . . . . 5995 8 4 . 1 1 12 12 VAL N N 15 94.84 4.84 . . . . . . . 5995 8 5 . 1 1 13 13 GLU N N 15 87.49 3.30 . . . . . . . 5995 8 6 . 1 1 16 16 ASN N N 15 84.76 3.29 . . . . . . . 5995 8 7 . 1 1 17 17 GLY N N 15 97.23 5.73 . . . . . . . 5995 8 8 . 1 1 19 19 TRP N N 15 75.38 2.94 . . . . . . . 5995 8 9 . 1 1 20 20 HIS N N 15 39.95 3.54 . . . . . . . 5995 8 10 . 1 1 21 21 THR N N 15 94.59 16.1 . . . . . . . 5995 8 11 . 1 1 22 22 ILE N N 15 102.1 4.64 . . . . . . . 5995 8 12 . 1 1 23 23 ILE N N 15 95.19 3.84 . . . . . . . 5995 8 13 . 1 1 26 26 SER N N 15 63.30 4.09 . . . . . . . 5995 8 14 . 1 1 27 27 ASP N N 15 98.38 5.91 . . . . . . . 5995 8 15 . 1 1 30 30 GLU N N 15 93.08 5.08 . . . . . . . 5995 8 16 . 1 1 31 31 LYS N N 15 88.20 3.80 . . . . . . . 5995 8 17 . 1 1 32 32 ILE N N 15 97.11 4.56 . . . . . . . 5995 8 18 . 1 1 33 33 GLU N N 15 99.13 4.53 . . . . . . . 5995 8 19 . 1 1 35 35 ASN N N 15 93.73 5.12 . . . . . . . 5995 8 20 . 1 1 36 36 GLY N N 15 100.1 5.26 . . . . . . . 5995 8 21 . 1 1 37 37 ASN N N 15 93.25 4.81 . . . . . . . 5995 8 22 . 1 1 39 39 ARG N N 15 89.86 4.81 . . . . . . . 5995 8 23 . 1 1 40 40 LEU N N 15 90.77 3.81 . . . . . . . 5995 8 24 . 1 1 41 41 PHE N N 15 68.31 1.70 . . . . . . . 5995 8 25 . 1 1 42 42 LEU N N 15 83.30 3.29 . . . . . . . 5995 8 26 . 1 1 48 48 LEU N N 15 96.35 2.87 . . . . . . . 5995 8 27 . 1 1 51 51 SER N N 15 104.1 5.53 . . . . . . . 5995 8 28 . 1 1 52 52 LEU N N 15 92.98 7.92 . . . . . . . 5995 8 29 . 1 1 54 54 LEU N N 15 95.67 3.06 . . . . . . . 5995 8 30 . 1 1 57 57 HIS N N 15 85.97 4.52 . . . . . . . 5995 8 31 . 1 1 58 58 THR N N 15 69.40 0.57 . . . . . . . 5995 8 32 . 1 1 60 60 ARG N N 15 96.82 4.96 . . . . . . . 5995 8 33 . 1 1 64 64 CYS N N 15 97.37 3.80 . . . . . . . 5995 8 34 . 1 1 65 65 SER N N 15 105.3 5.72 . . . . . . . 5995 8 35 . 1 1 66 66 GLU N N 15 81.65 6.12 . . . . . . . 5995 8 36 . 1 1 68 68 SER N N 15 102.9 3.17 . . . . . . . 5995 8 37 . 1 1 69 69 MET N N 15 92.22 3.99 . . . . . . . 5995 8 38 . 1 1 70 70 VAL N N 15 92.52 1.96 . . . . . . . 5995 8 39 . 1 1 71 71 ALA N N 15 98.89 5.42 . . . . . . . 5995 8 40 . 1 1 72 72 ASP N N 15 83.21 5.88 . . . . . . . 5995 8 41 . 1 1 74 74 THR N N 15 109.1 2.42 . . . . . . . 5995 8 42 . 1 1 76 76 LYS N N 15 94.66 4.24 . . . . . . . 5995 8 43 . 1 1 77 77 ALA N N 15 107.5 4.05 . . . . . . . 5995 8 44 . 1 1 79 79 GLU N N 15 92.63 3.86 . . . . . . . 5995 8 45 . 1 1 81 81 SER N N 15 93.29 3.34 . . . . . . . 5995 8 46 . 1 1 86 86 GLY N N 15 96.79 3.13 . . . . . . . 5995 8 47 . 1 1 88 88 ASN N N 15 96.31 4.17 . . . . . . . 5995 8 48 . 1 1 89 89 THR N N 15 88.67 7.81 . . . . . . . 5995 8 49 . 1 1 92 92 ILE N N 15 90.63 4.19 . . . . . . . 5995 8 50 . 1 1 94 94 LYS N N 15 90.82 5.24 . . . . . . . 5995 8 51 . 1 1 96 96 ASP N N 15 83.50 4.37 . . . . . . . 5995 8 52 . 1 1 97 97 TYR N N 15 84.17 3.84 . . . . . . . 5995 8 53 . 1 1 99 99 ASN N N 15 92.83 4.12 . . . . . . . 5995 8 54 . 1 1 100 100 PHE N N 15 86.41 3.60 . . . . . . . 5995 8 55 . 1 1 101 101 LEU N N 15 90.11 3.36 . . . . . . . 5995 8 56 . 1 1 102 102 MET N N 15 86.60 3.33 . . . . . . . 5995 8 57 . 1 1 103 103 ALA N N 15 91.66 5.11 . . . . . . . 5995 8 58 . 1 1 104 104 HIS N N 15 92.65 4.40 . . . . . . . 5995 8 59 . 1 1 105 105 LEU N N 15 86.39 4.86 . . . . . . . 5995 8 60 . 1 1 106 106 ILE N N 15 86.41 5.56 . . . . . . . 5995 8 61 . 1 1 107 107 ASN N N 15 93.88 3.66 . . . . . . . 5995 8 62 . 1 1 111 111 GLY N N 15 108.5 5.44 . . . . . . . 5995 8 63 . 1 1 113 113 THR N N 15 85.82 5.15 . . . . . . . 5995 8 64 . 1 1 115 115 GLN N N 15 98.81 3.37 . . . . . . . 5995 8 65 . 1 1 116 116 LEU N N 15 96.10 4.08 . . . . . . . 5995 8 66 . 1 1 117 117 MET N N 15 91.06 4.29 . . . . . . . 5995 8 67 . 1 1 118 118 GLY N N 15 89.67 4.57 . . . . . . . 5995 8 68 . 1 1 120 120 TYR N N 15 84.10 4.16 . . . . . . . 5995 8 69 . 1 1 121 121 GLY N N 15 89.84 4.74 . . . . . . . 5995 8 70 . 1 1 123 123 GLU N N 15 90.11 6.08 . . . . . . . 5995 8 71 . 1 1 125 125 ASP N N 15 90.82 3.43 . . . . . . . 5995 8 72 . 1 1 126 126 LEU N N 15 99.89 5.74 . . . . . . . 5995 8 73 . 1 1 127 127 SER N N 15 102.1 5.86 . . . . . . . 5995 8 74 . 1 1 128 128 SER N N 15 63.67 3.74 . . . . . . . 5995 8 75 . 1 1 129 129 ASP N N 15 94.23 3.68 . . . . . . . 5995 8 76 . 1 1 130 130 ILE N N 15 93.91 4.74 . . . . . . . 5995 8 77 . 1 1 131 131 LYS N N 15 92.03 3.46 . . . . . . . 5995 8 78 . 1 1 133 133 ARG N N 15 90.89 3.24 . . . . . . . 5995 8 79 . 1 1 136 136 GLN N N 15 92.52 3.14 . . . . . . . 5995 8 80 . 1 1 137 137 LEU N N 15 92.99 4.60 . . . . . . . 5995 8 81 . 1 1 138 138 CYS N N 15 80.34 4.08 . . . . . . . 5995 8 82 . 1 1 140 140 LYS N N 15 93.13 3.41 . . . . . . . 5995 8 83 . 1 1 141 141 HIS N N 15 95.70 4.79 . . . . . . . 5995 8 84 . 1 1 142 142 GLY N N 15 96.09 3.93 . . . . . . . 5995 8 85 . 1 1 143 143 ILE N N 15 65.56 3.72 . . . . . . . 5995 8 86 . 1 1 144 144 LEU N N 15 103.0 4.37 . . . . . . . 5995 8 87 . 1 1 145 145 ARG N N 15 100.1 4.74 . . . . . . . 5995 8 88 . 1 1 148 148 ILE N N 15 97.43 3.66 . . . . . . . 5995 8 89 . 1 1 151 151 LEU N N 15 91.11 6.10 . . . . . . . 5995 8 90 . 1 1 153 153 ASN N N 15 100.6 5.02 . . . . . . . 5995 8 91 . 1 1 157 157 CYS N N 15 91.73 4.33 . . . . . . . 5995 8 stop_ save_