data_53296 ####################### # Entry information # ####################### save_entry_information_1 _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information_1 _Entry.ID 53296 _Entry.Title ; 15N-Relaxation data for the N-terminal region (residues 1-132) of the human DEAD-box RNA helicase DDX3X ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2025-07-31 _Entry.Accession_date 2025-07-31 _Entry.Last_release_date 2025-07-31 _Entry.Original_release_date 2025-07-31 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.14.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype solution _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details ; This entry includes 15N R1/R2 relaxation rates, 1H-15N heteronuclear NOE values, and a set of 1H-15N relaxation rates (1H-15N longitudinal order, anti-phase 1H and 15N single-quantum coherences, and 1H-15N multiple quantum coherences). Uniformly 15N- or 2H, 15N-labeled samples were used. For the experiments using 2H,15N labeled proteins, datasets obtained with 3 different protein concentrations were deposited. All relaxation rates are represented in the laboratory frame. [Reference] An Exchange-Free Measure of 15 N Transverse Relaxation: An NMR Spectroscopy Application to the Study of a Folding Intermediate with Pervasive Chemical Exchange J. AM. CHEM. SOC. 2007, 129, 11468 - 11479 ; _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Yuki Toyama . . . 0000-0003-0457-678X 53296 2 Koh Takeuchi . . . 0000-0002-6227-4627 53296 3 Ichio Shimada . . . 0000-0001-5168-8894 53296 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID heteronucl_NOEs 4 53296 heteronucl_T1_relaxation 7 53296 heteronucl_T2_relaxation 13 53296 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID 'T1 relaxation values' 624 53296 'T2 relaxation values' 1164 53296 'heteronuclear NOE values' 354 53296 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2026-06-06 . original BMRB . 53296 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 52738 '1H, 15N, and 13C chemical shift assignments for the N-terminal region (residues 1-132) of the human DEAD-box RNA helicase DDX3X' 53296 stop_ save_ ############### # Citations # ############### save_citations_1 _Citation.Sf_category citations _Citation.Sf_framecode citations_1 _Citation.Entry_ID 53296 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID 42159288 _Citation.DOI . _Citation.Full_citation . _Citation.Title ; Phase Separation Driven by Dynamic Interactions in the N-Terminal Intrinsically Disordered Region of the DEAD-Box RNA Helicase DDX3X ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'J. Am. Chem. Soc.' _Citation.Journal_name_full 'Journal of the American Chemical Society' _Citation.Journal_volume 148 _Citation.Journal_issue 21 _Citation.Journal_ASTM . _Citation.Journal_ISSN 1520-5126 _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 21313 _Citation.Page_last 21331 _Citation.Year 2026 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Yuki Toyama Y. . . . 53296 1 2 Shinichiro Inakami S. . . . 53296 1 3 Masaharu Takarada M. . . . 53296 1 4 Kohki Okabe K. . . . 53296 1 5 Koh Takeuchi K. . . . 53296 1 6 Ichio Shimada I. . . . 53296 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly_1 _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly_1 _Assembly.Entry_ID 53296 _Assembly.ID 1 _Assembly.Name N-IDR _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds no _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 N-IDR 1 $entity_1 . . yes native no no . . . 53296 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 53296 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name entity_1 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; MSHVAVENALGLDQQFAGLD LNSSDNQSGGSTASKGRYIP PHLRNREATKGFYDKDSSGW SSSKDKDAYSSFGSRSDSRG KSSFFSDRGSGSRGRFDDRG RSDYDGIGSRGDRSGFGKFE RGGNSRWCDKSD ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 132 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'all free' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_db_link.Ordinal _Entity_db_link.Author_supplied _Entity_db_link.Database_code _Entity_db_link.Accession_code _Entity_db_link.Entry_mol_code _Entity_db_link.Entry_mol_name _Entity_db_link.Entry_experimental_method _Entity_db_link.Entry_structure_resolution _Entity_db_link.Entry_relation_type _Entity_db_link.Entry_details _Entity_db_link.Chimera_segment_ID _Entity_db_link.Seq_query_to_submitted_percent _Entity_db_link.Seq_subject_length _Entity_db_link.Seq_identity _Entity_db_link.Seq_positive _Entity_db_link.Seq_homology_expectation_val _Entity_db_link.Seq_align_begin _Entity_db_link.Seq_align_end _Entity_db_link.Seq_difference_details _Entity_db_link.Seq_alignment_details _Entity_db_link.Entry_ID _Entity_db_link.Entity_ID 1 yes UNP O00571 . 'ATP-dependent RNA helicase DDX3X' . . . . . . . . . . . . . . 53296 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . MET . 53296 1 2 . SER . 53296 1 3 . HIS . 53296 1 4 . VAL . 53296 1 5 . ALA . 53296 1 6 . VAL . 53296 1 7 . GLU . 53296 1 8 . ASN . 53296 1 9 . ALA . 53296 1 10 . LEU . 53296 1 11 . GLY . 53296 1 12 . LEU . 53296 1 13 . ASP . 53296 1 14 . GLN . 53296 1 15 . GLN . 53296 1 16 . PHE . 53296 1 17 . ALA . 53296 1 18 . GLY . 53296 1 19 . LEU . 53296 1 20 . ASP . 53296 1 21 . LEU . 53296 1 22 . ASN . 53296 1 23 . SER . 53296 1 24 . SER . 53296 1 25 . ASP . 53296 1 26 . ASN . 53296 1 27 . GLN . 53296 1 28 . SER . 53296 1 29 . GLY . 53296 1 30 . GLY . 53296 1 31 . SER . 53296 1 32 . THR . 53296 1 33 . ALA . 53296 1 34 . SER . 53296 1 35 . LYS . 53296 1 36 . GLY . 53296 1 37 . ARG . 53296 1 38 . TYR . 53296 1 39 . ILE . 53296 1 40 . PRO . 53296 1 41 . PRO . 53296 1 42 . HIS . 53296 1 43 . LEU . 53296 1 44 . ARG . 53296 1 45 . ASN . 53296 1 46 . ARG . 53296 1 47 . GLU . 53296 1 48 . ALA . 53296 1 49 . THR . 53296 1 50 . LYS . 53296 1 51 . GLY . 53296 1 52 . PHE . 53296 1 53 . TYR . 53296 1 54 . ASP . 53296 1 55 . LYS . 53296 1 56 . ASP . 53296 1 57 . SER . 53296 1 58 . SER . 53296 1 59 . GLY . 53296 1 60 . TRP . 53296 1 61 . SER . 53296 1 62 . SER . 53296 1 63 . SER . 53296 1 64 . LYS . 53296 1 65 . ASP . 53296 1 66 . LYS . 53296 1 67 . ASP . 53296 1 68 . ALA . 53296 1 69 . TYR . 53296 1 70 . SER . 53296 1 71 . SER . 53296 1 72 . PHE . 53296 1 73 . GLY . 53296 1 74 . SER . 53296 1 75 . ARG . 53296 1 76 . SER . 53296 1 77 . ASP . 53296 1 78 . SER . 53296 1 79 . ARG . 53296 1 80 . GLY . 53296 1 81 . LYS . 53296 1 82 . SER . 53296 1 83 . SER . 53296 1 84 . PHE . 53296 1 85 . PHE . 53296 1 86 . SER . 53296 1 87 . ASP . 53296 1 88 . ARG . 53296 1 89 . GLY . 53296 1 90 . SER . 53296 1 91 . GLY . 53296 1 92 . SER . 53296 1 93 . ARG . 53296 1 94 . GLY . 53296 1 95 . ARG . 53296 1 96 . PHE . 53296 1 97 . ASP . 53296 1 98 . ASP . 53296 1 99 . ARG . 53296 1 100 . GLY . 53296 1 101 . ARG . 53296 1 102 . SER . 53296 1 103 . ASP . 53296 1 104 . TYR . 53296 1 105 . ASP . 53296 1 106 . GLY . 53296 1 107 . ILE . 53296 1 108 . GLY . 53296 1 109 . SER . 53296 1 110 . ARG . 53296 1 111 . GLY . 53296 1 112 . ASP . 53296 1 113 . ARG . 53296 1 114 . SER . 53296 1 115 . GLY . 53296 1 116 . PHE . 53296 1 117 . GLY . 53296 1 118 . LYS . 53296 1 119 . PHE . 53296 1 120 . GLU . 53296 1 121 . ARG . 53296 1 122 . GLY . 53296 1 123 . GLY . 53296 1 124 . ASN . 53296 1 125 . SER . 53296 1 126 . ARG . 53296 1 127 . TRP . 53296 1 128 . CYS . 53296 1 129 . ASP . 53296 1 130 . LYS . 53296 1 131 . SER . 53296 1 132 . ASP . 53296 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . MET 1 1 53296 1 . SER 2 2 53296 1 . HIS 3 3 53296 1 . VAL 4 4 53296 1 . ALA 5 5 53296 1 . VAL 6 6 53296 1 . GLU 7 7 53296 1 . ASN 8 8 53296 1 . ALA 9 9 53296 1 . LEU 10 10 53296 1 . GLY 11 11 53296 1 . LEU 12 12 53296 1 . ASP 13 13 53296 1 . GLN 14 14 53296 1 . GLN 15 15 53296 1 . PHE 16 16 53296 1 . ALA 17 17 53296 1 . GLY 18 18 53296 1 . LEU 19 19 53296 1 . ASP 20 20 53296 1 . LEU 21 21 53296 1 . ASN 22 22 53296 1 . SER 23 23 53296 1 . SER 24 24 53296 1 . ASP 25 25 53296 1 . ASN 26 26 53296 1 . GLN 27 27 53296 1 . SER 28 28 53296 1 . GLY 29 29 53296 1 . GLY 30 30 53296 1 . SER 31 31 53296 1 . THR 32 32 53296 1 . ALA 33 33 53296 1 . SER 34 34 53296 1 . LYS 35 35 53296 1 . GLY 36 36 53296 1 . ARG 37 37 53296 1 . TYR 38 38 53296 1 . ILE 39 39 53296 1 . PRO 40 40 53296 1 . PRO 41 41 53296 1 . HIS 42 42 53296 1 . LEU 43 43 53296 1 . ARG 44 44 53296 1 . ASN 45 45 53296 1 . ARG 46 46 53296 1 . GLU 47 47 53296 1 . ALA 48 48 53296 1 . THR 49 49 53296 1 . LYS 50 50 53296 1 . GLY 51 51 53296 1 . PHE 52 52 53296 1 . TYR 53 53 53296 1 . ASP 54 54 53296 1 . LYS 55 55 53296 1 . ASP 56 56 53296 1 . SER 57 57 53296 1 . SER 58 58 53296 1 . GLY 59 59 53296 1 . TRP 60 60 53296 1 . SER 61 61 53296 1 . SER 62 62 53296 1 . SER 63 63 53296 1 . LYS 64 64 53296 1 . ASP 65 65 53296 1 . LYS 66 66 53296 1 . ASP 67 67 53296 1 . ALA 68 68 53296 1 . TYR 69 69 53296 1 . SER 70 70 53296 1 . SER 71 71 53296 1 . PHE 72 72 53296 1 . GLY 73 73 53296 1 . SER 74 74 53296 1 . ARG 75 75 53296 1 . SER 76 76 53296 1 . ASP 77 77 53296 1 . SER 78 78 53296 1 . ARG 79 79 53296 1 . GLY 80 80 53296 1 . LYS 81 81 53296 1 . SER 82 82 53296 1 . SER 83 83 53296 1 . PHE 84 84 53296 1 . PHE 85 85 53296 1 . SER 86 86 53296 1 . ASP 87 87 53296 1 . ARG 88 88 53296 1 . GLY 89 89 53296 1 . SER 90 90 53296 1 . GLY 91 91 53296 1 . SER 92 92 53296 1 . ARG 93 93 53296 1 . GLY 94 94 53296 1 . ARG 95 95 53296 1 . PHE 96 96 53296 1 . ASP 97 97 53296 1 . ASP 98 98 53296 1 . ARG 99 99 53296 1 . GLY 100 100 53296 1 . ARG 101 101 53296 1 . SER 102 102 53296 1 . ASP 103 103 53296 1 . TYR 104 104 53296 1 . ASP 105 105 53296 1 . GLY 106 106 53296 1 . ILE 107 107 53296 1 . GLY 108 108 53296 1 . SER 109 109 53296 1 . ARG 110 110 53296 1 . GLY 111 111 53296 1 . ASP 112 112 53296 1 . ARG 113 113 53296 1 . SER 114 114 53296 1 . GLY 115 115 53296 1 . PHE 116 116 53296 1 . GLY 117 117 53296 1 . LYS 118 118 53296 1 . PHE 119 119 53296 1 . GLU 120 120 53296 1 . ARG 121 121 53296 1 . GLY 122 122 53296 1 . GLY 123 123 53296 1 . ASN 124 124 53296 1 . SER 125 125 53296 1 . ARG 126 126 53296 1 . TRP 127 127 53296 1 . CYS 128 128 53296 1 . ASP 129 129 53296 1 . LYS 130 130 53296 1 . SER 131 131 53296 1 . ASP 132 132 53296 1 stop_ save_ #################### # Natural source # #################### save_natural_source_1 _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source_1 _Entity_natural_src_list.Entry_ID 53296 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 9606 organism . 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 53296 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source_1 _Entity_experimental_src_list.Entry_ID 53296 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli . . . plasmid . . pET-SUMO . . . 53296 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 53296 _Sample.ID 1 _Sample.Name 'u-15N N-IDR' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 1 _Sample.Solvent_system '95% H2O/5% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'potassium phosphate' 'natural abundance' . . . . . . 20 . . mM . . . . 53296 1 2 'potassium chloride' 'natural abundance' . . . . . . 200 . . mM . . . . 53296 1 3 EDTA 'natural abundance' . . . . . . 1 . . mM . . . . 53296 1 4 DTT 'natural abundance' . . . . . . 5 . . mM . . . . 53296 1 5 N-IDR '[U-99% 15N]' . . 1 $entity_1 . . 300 . . uM . . . . 53296 1 stop_ save_ save_sample_2 _Sample.Sf_category sample _Sample.Sf_framecode sample_2 _Sample.Entry_ID 53296 _Sample.ID 2 _Sample.Name 'u-2H,15N N-IDR 100 uM' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 3 _Sample.Solvent_system '95% H2O/5% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'potassium phosphate' 'natural abundance' . . . . . . 20 . . mM . . . . 53296 2 2 'potassium chloride' 'natural abundance' . . . . . . 200 . . mM . . . . 53296 2 3 EDTA 'natural abundance' . . . . . . 1 . . mM . . . . 53296 2 4 DTT 'natural abundance' . . . . . . 5 . . mM . . . . 53296 2 5 N-IDR '[U-2H; U-15N]' . . 1 $entity_1 . . 100 . . uM . . . . 53296 2 stop_ save_ save_sample_3 _Sample.Sf_category sample _Sample.Sf_framecode sample_3 _Sample.Entry_ID 53296 _Sample.ID 3 _Sample.Name 'u-2H,15N N-IDR 300 uM' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 3 _Sample.Solvent_system '95% H2O/5% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'potassium phosphate' 'natural abundance' . . . . . . 20 . . mM . . . . 53296 3 2 'potassium chloride' 'natural abundance' . . . . . . 200 . . mM . . . . 53296 3 3 EDTA 'natural abundance' . . . . . . 1 . . mM . . . . 53296 3 4 DTT 'natural abundance' . . . . . . 5 . . mM . . . . 53296 3 5 N-IDR '[U-2H; U-15N]' . . 1 $entity_1 . . 300 . . uM . . . . 53296 3 stop_ save_ save_sample_4 _Sample.Sf_category sample _Sample.Sf_framecode sample_4 _Sample.Entry_ID 53296 _Sample.ID 4 _Sample.Name 'u-2H,15N N-IDR 500 uM' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 3 _Sample.Solvent_system '95% H2O/5% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'potassium phosphate' 'natural abundance' . . . . . . 20 . . mM . . . . 53296 4 2 'potassium chloride' 'natural abundance' . . . . . . 200 . . mM . . . . 53296 4 3 EDTA 'natural abundance' . . . . . . 1 . . mM . . . . 53296 4 4 DTT 'natural abundance' . . . . . . 5 . . mM . . . . 53296 4 5 N-IDR '[U-2H; U-15N]' . . 1 $entity_1 . . 500 . . uM . . . . 53296 4 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 53296 _Sample_condition_list.ID 1 _Sample_condition_list.Name N-IDR _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID pH 6.0 . pH 53296 1 pressure 1 . atm 53296 1 temperature 283.15 . K 53296 1 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 53296 _Software.ID 1 _Software.Type . _Software.Name TOPSPIN _Software.Version 4.1.4 _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID collection . 53296 1 stop_ save_ save_software_2 _Software.Sf_category software _Software.Sf_framecode software_2 _Software.Entry_ID 53296 _Software.ID 2 _Software.Type . _Software.Name NMRPipe _Software.Version 11.1 _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID processing . 53296 2 stop_ save_ save_software_3 _Software.Sf_category software _Software.Sf_framecode software_3 _Software.Entry_ID 53296 _Software.ID 3 _Software.Type . _Software.Name NMRFAM-SPARKY _Software.Version 1.470 _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID 'data analysis' . 53296 3 stop_ save_ save_software_4 _Software.Sf_category software _Software.Sf_framecode software_4 _Software.Entry_ID 53296 _Software.ID 4 _Software.Type . _Software.Name peakipy _Software.Version 0.1.30 _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID 'data analysis' . 53296 4 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 53296 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name '1 GHz' _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model 'AVANCE NEO' _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 1000 save_ ############################# # NMR applied experiments # ############################# save_experiment_list_1 _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list_1 _Experiment_list.Entry_ID 53296 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NUS_flag _Experiment.Interleaved_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Details _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 'T1rho/R1rho relaxation' no no yes . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1rho relaxation measurement' 53296 1 2 'T1/R1 relaxation' no no yes . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1 relaxation measurement' 53296 1 3 '1H-15N heteronoe' no no yes . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '1H-15N heteronuclear NOE' 53296 1 4 'T1rho/R1rho relaxation HxNx' no no yes . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HxNx relaxation measurement' 53296 1 5 'T1rho/R1rho relaxation HxNz' no no yes . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HxNz relaxation measurement' 53296 1 6 'T1rho/R1rho relaxation HzNx' no no yes . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HzNx relaxation measurement' 53296 1 7 'T1/R1 relaxation HzNz' no no yes . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HzNz relaxation measurement' 53296 1 8 'T1rho/R1rho relaxation' no no yes . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1rho relaxation measurement' 53296 1 9 'T1/R1 relaxation' no no yes . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1 relaxation measurement' 53296 1 10 '1H-15N heteronoe' no no yes . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '1H-15N heteronuclear NOE' 53296 1 11 'T1rho/R1rho relaxation HxNx' no no yes . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HxNx relaxation measurement' 53296 1 12 'T1rho/R1rho relaxation HxNz' no no yes . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HxNz relaxation measurement' 53296 1 13 'T1rho/R1rho relaxation HzNx' no no yes . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HzNx relaxation measurement' 53296 1 14 'T1/R1 relaxation HzNz' no no yes . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HzNz relaxation measurement' 53296 1 15 'T1rho/R1rho relaxation' no no yes . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1rho relaxation measurement' 53296 1 16 'T1/R1 relaxation' no no yes . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1 relaxation measurement' 53296 1 17 '1H-15N heteronoe' no no yes . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '1H-15N heteronuclear NOE' 53296 1 18 'T1rho/R1rho relaxation HxNx' no no yes . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HxNx relaxation measurement' 53296 1 19 'T1rho/R1rho relaxation HxNz' no no yes . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HxNz relaxation measurement' 53296 1 20 'T1rho/R1rho relaxation HzNx' no no yes . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HzNx relaxation measurement' 53296 1 21 'T1/R1 relaxation HzNz' no no yes . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . 'HzNz relaxation measurement' 53296 1 22 'T1rho/R1rho relaxation' no no yes . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1rho relaxation measurement' 53296 1 23 'T1/R1 relaxation' no no yes . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '15N R1 relaxation measurement' 53296 1 24 '1H-15N heteronoe' no no yes . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '1H-15N heteronuclear NOE' 53296 1 stop_ save_ ############################## # Heteronuclear NOE values # ############################## save_heteronucl_NOEs_1 _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode heteronucl_NOEs_1 _Heteronucl_NOE_list.Entry_ID 53296 _Heteronucl_NOE_list.ID 1 _Heteronucl_NOE_list.Name 'hetNOE u-15N' _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_NOE_list.Spectrometer_frequency_1H 1000 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'peak integral' _Heteronucl_NOE_list.NOE_ref_val 1.0 _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 3 '1H-15N heteronoe' . . . 53296 1 stop_ loop_ _Heteronucl_NOE_software.Software_ID _Heteronucl_NOE_software.Software_label _Heteronucl_NOE_software.Method_ID _Heteronucl_NOE_software.Method_label _Heteronucl_NOE_software.Entry_ID _Heteronucl_NOE_software.Heteronucl_NOE_list_ID 1 $software_1 . . 53296 1 2 $software_2 . . 53296 1 3 $software_3 . . 53296 1 4 $software_4 . . 53296 1 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 HIS N N 15 . 1 1 3 3 HIS H H 1 0.161697816 0.007353522 . . . . . . . . . . 53296 1 2 . 1 1 5 5 ALA N N 15 . 1 1 5 5 ALA H H 1 0.410943446 0.008874103 . . . . . . . . . . 53296 1 3 . 1 1 7 7 GLU N N 15 . 1 1 7 7 GLU H H 1 0.457542211 0.008112289 . . . . . . . . . . 53296 1 4 . 1 1 8 8 ASN N N 15 . 1 1 8 8 ASN H H 1 0.424893664 0.007749578 . . . . . . . . . . 53296 1 5 . 1 1 9 9 ALA N N 15 . 1 1 9 9 ALA H H 1 0.487688676 0.008629719 . . . . . . . . . . 53296 1 6 . 1 1 11 11 GLY N N 15 . 1 1 11 11 GLY H H 1 0.542809116 0.01499445 . . . . . . . . . . 53296 1 7 . 1 1 13 13 ASP N N 15 . 1 1 13 13 ASP H H 1 0.565491095 0.009202438 . . . . . . . . . . 53296 1 8 . 1 1 17 17 ALA N N 15 . 1 1 17 17 ALA H H 1 0.583411438 0.009280829 . . . . . . . . . . 53296 1 9 . 1 1 18 18 GLY N N 15 . 1 1 18 18 GLY H H 1 0.497723667 0.010415489 . . . . . . . . . . 53296 1 10 . 1 1 20 20 ASP N N 15 . 1 1 20 20 ASP H H 1 0.482147054 0.009183411 . . . . . . . . . . 53296 1 11 . 1 1 21 21 LEU N N 15 . 1 1 21 21 LEU H H 1 0.566645182 0.011113407 . . . . . . . . . . 53296 1 12 . 1 1 22 22 ASN N N 15 . 1 1 22 22 ASN H H 1 0.465889997 0.008133546 . . . . . . . . . . 53296 1 13 . 1 1 23 23 SER N N 15 . 1 1 23 23 SER H H 1 0.547383343 0.009632465 . . . . . . . . . . 53296 1 14 . 1 1 24 24 SER N N 15 . 1 1 24 24 SER H H 1 0.514094845 0.007785718 . . . . . . . . . . 53296 1 15 . 1 1 25 25 ASP N N 15 . 1 1 25 25 ASP H H 1 0.542749333 0.012338655 . . . . . . . . . . 53296 1 16 . 1 1 26 26 ASN N N 15 . 1 1 26 26 ASN H H 1 0.501466896 0.008065281 . . . . . . . . . . 53296 1 17 . 1 1 27 27 GLN N N 15 . 1 1 27 27 GLN H H 1 0.500422055 0.009402099 . . . . . . . . . . 53296 1 18 . 1 1 29 29 GLY N N 15 . 1 1 29 29 GLY H H 1 0.490127079 0.008802144 . . . . . . . . . . 53296 1 19 . 1 1 30 30 GLY N N 15 . 1 1 30 30 GLY H H 1 0.555743158 0.014107746 . . . . . . . . . . 53296 1 20 . 1 1 31 31 SER N N 15 . 1 1 31 31 SER H H 1 0.423573074 0.006568896 . . . . . . . . . . 53296 1 21 . 1 1 33 33 ALA N N 15 . 1 1 33 33 ALA H H 1 0.550313916 0.008968013 . . . . . . . . . . 53296 1 22 . 1 1 34 34 SER N N 15 . 1 1 34 34 SER H H 1 0.493479259 0.008809185 . . . . . . . . . . 53296 1 23 . 1 1 35 35 LYS N N 15 . 1 1 35 35 LYS H H 1 0.458715612 0.010640558 . . . . . . . . . . 53296 1 24 . 1 1 37 37 ARG N N 15 . 1 1 37 37 ARG H H 1 0.599500454 0.016254446 . . . . . . . . . . 53296 1 25 . 1 1 38 38 TYR N N 15 . 1 1 38 38 TYR H H 1 0.556584915 0.011129289 . . . . . . . . . . 53296 1 26 . 1 1 39 39 ILE N N 15 . 1 1 39 39 ILE H H 1 0.61330146 0.012212665 . . . . . . . . . . 53296 1 27 . 1 1 42 42 HIS N N 15 . 1 1 42 42 HIS H H 1 0.573812547 0.029182441 . . . . . . . . . . 53296 1 28 . 1 1 43 43 LEU N N 15 . 1 1 43 43 LEU H H 1 0.641832358 0.016953066 . . . . . . . . . . 53296 1 29 . 1 1 45 45 ASN N N 15 . 1 1 45 45 ASN H H 1 0.566591656 0.011092499 . . . . . . . . . . 53296 1 30 . 1 1 47 47 GLU N N 15 . 1 1 47 47 GLU H H 1 0.520651947 0.011952883 . . . . . . . . . . 53296 1 31 . 1 1 48 48 ALA N N 15 . 1 1 48 48 ALA H H 1 0.61915382 0.034751992 . . . . . . . . . . 53296 1 32 . 1 1 49 49 THR N N 15 . 1 1 49 49 THR H H 1 0.592940606 0.014224584 . . . . . . . . . . 53296 1 33 . 1 1 50 50 LYS N N 15 . 1 1 50 50 LYS H H 1 0.561753037 0.013701094 . . . . . . . . . . 53296 1 34 . 1 1 51 51 GLY N N 15 . 1 1 51 51 GLY H H 1 0.552862218 0.016812388 . . . . . . . . . . 53296 1 35 . 1 1 54 54 ASP N N 15 . 1 1 54 54 ASP H H 1 0.734841537 0.02474623 . . . . . . . . . . 53296 1 36 . 1 1 57 57 SER N N 15 . 1 1 57 57 SER H H 1 0.584230798 0.012475965 . . . . . . . . . . 53296 1 37 . 1 1 58 58 SER N N 15 . 1 1 58 58 SER H H 1 0.516753831 0.00943135 . . . . . . . . . . 53296 1 38 . 1 1 59 59 GLY N N 15 . 1 1 59 59 GLY H H 1 0.585697081 0.012980129 . . . . . . . . . . 53296 1 39 . 1 1 61 61 SER N N 15 . 1 1 61 61 SER H H 1 0.66763771 0.011440694 . . . . . . . . . . 53296 1 40 . 1 1 62 62 SER N N 15 . 1 1 62 62 SER H H 1 0.590553792 0.012485842 . . . . . . . . . . 53296 1 41 . 1 1 63 63 SER N N 15 . 1 1 63 63 SER H H 1 0.630306791 0.012854305 . . . . . . . . . . 53296 1 42 . 1 1 64 64 LYS N N 15 . 1 1 64 64 LYS H H 1 0.700130855 0.01471068 . . . . . . . . . . 53296 1 43 . 1 1 66 66 LYS N N 15 . 1 1 66 66 LYS H H 1 0.644010192 0.017054522 . . . . . . . . . . 53296 1 44 . 1 1 68 68 ALA N N 15 . 1 1 68 68 ALA H H 1 0.602020487 0.010070907 . . . . . . . . . . 53296 1 45 . 1 1 69 69 TYR N N 15 . 1 1 69 69 TYR H H 1 0.695490742 0.011233643 . . . . . . . . . . 53296 1 46 . 1 1 70 70 SER N N 15 . 1 1 70 70 SER H H 1 0.712428877 0.013917227 . . . . . . . . . . 53296 1 47 . 1 1 71 71 SER N N 15 . 1 1 71 71 SER H H 1 0.655803781 0.011879062 . . . . . . . . . . 53296 1 48 . 1 1 73 73 GLY N N 15 . 1 1 73 73 GLY H H 1 0.640663321 0.013378922 . . . . . . . . . . 53296 1 49 . 1 1 74 74 SER N N 15 . 1 1 74 74 SER H H 1 0.696857346 0.018796249 . . . . . . . . . . 53296 1 50 . 1 1 78 78 SER N N 15 . 1 1 78 78 SER H H 1 0.557533029 0.013641317 . . . . . . . . . . 53296 1 51 . 1 1 82 82 SER N N 15 . 1 1 82 82 SER H H 1 0.544269134 0.016251765 . . . . . . . . . . 53296 1 52 . 1 1 83 83 SER N N 15 . 1 1 83 83 SER H H 1 0.622563378 0.012281334 . . . . . . . . . . 53296 1 53 . 1 1 85 85 PHE N N 15 . 1 1 85 85 PHE H H 1 0.718963006 0.027816759 . . . . . . . . . . 53296 1 54 . 1 1 86 86 SER N N 15 . 1 1 86 86 SER H H 1 0.628740048 0.011894539 . . . . . . . . . . 53296 1 55 . 1 1 88 88 ARG N N 15 . 1 1 88 88 ARG H H 1 0.594468365 0.012559769 . . . . . . . . . . 53296 1 56 . 1 1 89 89 GLY N N 15 . 1 1 89 89 GLY H H 1 0.566707217 0.010502986 . . . . . . . . . . 53296 1 57 . 1 1 91 91 GLY N N 15 . 1 1 91 91 GLY H H 1 0.557877674 0.008650827 . . . . . . . . . . 53296 1 58 . 1 1 92 92 SER N N 15 . 1 1 92 92 SER H H 1 0.564545313 0.013601761 . . . . . . . . . . 53296 1 59 . 1 1 95 95 ARG N N 15 . 1 1 95 95 ARG H H 1 0.744339163 0.019953567 . . . . . . . . . . 53296 1 60 . 1 1 96 96 PHE N N 15 . 1 1 96 96 PHE H H 1 0.555838014 0.013041448 . . . . . . . . . . 53296 1 61 . 1 1 97 97 ASP N N 15 . 1 1 97 97 ASP H H 1 0.67418523 0.023458901 . . . . . . . . . . 53296 1 62 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.662560065 0.013388387 . . . . . . . . . . 53296 1 63 . 1 1 100 100 GLY N N 15 . 1 1 100 100 GLY H H 1 0.579579251 0.011849586 . . . . . . . . . . 53296 1 64 . 1 1 101 101 ARG N N 15 . 1 1 101 101 ARG H H 1 0.63677881 0.016023764 . . . . . . . . . . 53296 1 65 . 1 1 102 102 SER N N 15 . 1 1 102 102 SER H H 1 0.588836053 0.010409061 . . . . . . . . . . 53296 1 66 . 1 1 106 106 GLY N N 15 . 1 1 106 106 GLY H H 1 0.590189223 0.011462622 . . . . . . . . . . 53296 1 67 . 1 1 107 107 ILE N N 15 . 1 1 107 107 ILE H H 1 0.628784788 0.016107577 . . . . . . . . . . 53296 1 68 . 1 1 108 108 GLY N N 15 . 1 1 108 108 GLY H H 1 0.668623619 0.011421371 . . . . . . . . . . 53296 1 69 . 1 1 109 109 SER N N 15 . 1 1 109 109 SER H H 1 0.609711207 0.016389527 . . . . . . . . . . 53296 1 70 . 1 1 113 113 ARG N N 15 . 1 1 113 113 ARG H H 1 0.529220419 0.01082208 . . . . . . . . . . 53296 1 71 . 1 1 115 115 GLY N N 15 . 1 1 115 115 GLY H H 1 0.557329736 0.011216758 . . . . . . . . . . 53296 1 72 . 1 1 116 116 PHE N N 15 . 1 1 116 116 PHE H H 1 0.665894185 0.013128346 . . . . . . . . . . 53296 1 73 . 1 1 117 117 GLY N N 15 . 1 1 117 117 GLY H H 1 0.534338849 0.012004547 . . . . . . . . . . 53296 1 74 . 1 1 118 118 LYS N N 15 . 1 1 118 118 LYS H H 1 0.628101477 0.016819217 . . . . . . . . . . 53296 1 75 . 1 1 120 120 GLU N N 15 . 1 1 120 120 GLU H H 1 0.650466165 0.029539057 . . . . . . . . . . 53296 1 76 . 1 1 121 121 ARG N N 15 . 1 1 121 121 ARG H H 1 0.512249181 0.018471166 . . . . . . . . . . 53296 1 77 . 1 1 122 122 GLY N N 15 . 1 1 122 122 GLY H H 1 0.59092033 0.011626227 . . . . . . . . . . 53296 1 78 . 1 1 123 123 GLY N N 15 . 1 1 123 123 GLY H H 1 0.621584095 0.019807749 . . . . . . . . . . 53296 1 79 . 1 1 124 124 ASN N N 15 . 1 1 124 124 ASN H H 1 0.605621564 0.01066383 . . . . . . . . . . 53296 1 80 . 1 1 125 125 SER N N 15 . 1 1 125 125 SER H H 1 0.521031744 0.013244457 . . . . . . . . . . 53296 1 81 . 1 1 128 128 CYS N N 15 . 1 1 128 128 CYS H H 1 0.552648017 0.009858671 . . . . . . . . . . 53296 1 82 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.610242826 0.013613139 . . . . . . . . . . 53296 1 83 . 1 1 131 131 SER N N 15 . 1 1 131 131 SER H H 1 0.319590274 0.007267795 . . . . . . . . . . 53296 1 84 . 1 1 132 132 ASP N N 15 . 1 1 132 132 ASP H H 1 0.258112059 0.009713645 . . . . . . . . . . 53296 1 stop_ save_ save_heteronucl_NOEs_2 _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode heteronucl_NOEs_2 _Heteronucl_NOE_list.Entry_ID 53296 _Heteronucl_NOE_list.ID 2 _Heteronucl_NOE_list.Name 'hetNOE u-2H,15N 100 uM' _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_NOE_list.Spectrometer_frequency_1H 1000 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'peak integral' _Heteronucl_NOE_list.NOE_ref_val 1.0 _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 10 '1H-15N heteronoe' . . . 53296 2 stop_ loop_ _Heteronucl_NOE_software.Software_ID _Heteronucl_NOE_software.Software_label _Heteronucl_NOE_software.Method_ID _Heteronucl_NOE_software.Method_label _Heteronucl_NOE_software.Entry_ID _Heteronucl_NOE_software.Heteronucl_NOE_list_ID 1 $software_1 . . 53296 2 2 $software_2 . . 53296 2 3 $software_3 . . 53296 2 4 $software_4 . . 53296 2 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 HIS N N 15 . 1 1 3 3 HIS H H 1 0.139809973 0.011817934 . . . . . . . . . . 53296 2 2 . 1 1 5 5 ALA N N 15 . 1 1 5 5 ALA H H 1 0.419417399 0.013258378 . . . . . . . . . . 53296 2 3 . 1 1 7 7 GLU N N 15 . 1 1 7 7 GLU H H 1 0.471410101 0.012467726 . . . . . . . . . . 53296 2 4 . 1 1 8 8 ASN N N 15 . 1 1 8 8 ASN H H 1 0.459181143 0.01343548 . . . . . . . . . . 53296 2 5 . 1 1 9 9 ALA N N 15 . 1 1 9 9 ALA H H 1 0.487199385 0.018035711 . . . . . . . . . . 53296 2 6 . 1 1 11 11 GLY N N 15 . 1 1 11 11 GLY H H 1 0.56165227 0.014365637 . . . . . . . . . . 53296 2 7 . 1 1 12 12 LEU N N 15 . 1 1 12 12 LEU H H 1 0.517988658 0.024420995 . . . . . . . . . . 53296 2 8 . 1 1 13 13 ASP N N 15 . 1 1 13 13 ASP H H 1 0.491784171 0.013345819 . . . . . . . . . . 53296 2 9 . 1 1 17 17 ALA N N 15 . 1 1 17 17 ALA H H 1 0.670230033 0.013804103 . . . . . . . . . . 53296 2 10 . 1 1 18 18 GLY N N 15 . 1 1 18 18 GLY H H 1 0.44418272 0.013237408 . . . . . . . . . . 53296 2 11 . 1 1 20 20 ASP N N 15 . 1 1 20 20 ASP H H 1 0.533436386 0.015511653 . . . . . . . . . . 53296 2 12 . 1 1 21 21 LEU N N 15 . 1 1 21 21 LEU H H 1 0.505801267 0.014411951 . . . . . . . . . . 53296 2 13 . 1 1 22 22 ASN N N 15 . 1 1 22 22 ASN H H 1 0.537150164 0.013660232 . . . . . . . . . . 53296 2 14 . 1 1 23 23 SER N N 15 . 1 1 23 23 SER H H 1 0.591153284 0.018163373 . . . . . . . . . . 53296 2 15 . 1 1 24 24 SER N N 15 . 1 1 24 24 SER H H 1 0.557098836 0.014529953 . . . . . . . . . . 53296 2 16 . 1 1 25 25 ASP N N 15 . 1 1 25 25 ASP H H 1 0.60614087 0.015139504 . . . . . . . . . . 53296 2 17 . 1 1 26 26 ASN N N 15 . 1 1 26 26 ASN H H 1 0.564327642 0.013771599 . . . . . . . . . . 53296 2 18 . 1 1 27 27 GLN N N 15 . 1 1 27 27 GLN H H 1 0.486580595 0.014428556 . . . . . . . . . . 53296 2 19 . 1 1 29 29 GLY N N 15 . 1 1 29 29 GLY H H 1 0.396553707 0.011582632 . . . . . . . . . . 53296 2 20 . 1 1 30 30 GLY N N 15 . 1 1 30 30 GLY H H 1 0.495034456 0.014490807 . . . . . . . . . . 53296 2 21 . 1 1 31 31 SER N N 15 . 1 1 31 31 SER H H 1 0.409798974 0.013359814 . . . . . . . . . . 53296 2 22 . 1 1 32 32 THR N N 15 . 1 1 32 32 THR H H 1 0.547322863 0.01736585 . . . . . . . . . . 53296 2 23 . 1 1 33 33 ALA N N 15 . 1 1 33 33 ALA H H 1 0.577762559 0.014811665 . . . . . . . . . . 53296 2 24 . 1 1 34 34 SER N N 15 . 1 1 34 34 SER H H 1 0.544043609 0.012251006 . . . . . . . . . . 53296 2 25 . 1 1 35 35 LYS N N 15 . 1 1 35 35 LYS H H 1 0.492126071 0.016070651 . . . . . . . . . . 53296 2 26 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.445209112 0.014957445 . . . . . . . . . . 53296 2 27 . 1 1 37 37 ARG N N 15 . 1 1 37 37 ARG H H 1 0.604267344 0.019752702 . . . . . . . . . . 53296 2 28 . 1 1 38 38 TYR N N 15 . 1 1 38 38 TYR H H 1 0.607603203 0.011971819 . . . . . . . . . . 53296 2 29 . 1 1 39 39 ILE N N 15 . 1 1 39 39 ILE H H 1 0.610599247 0.013087671 . . . . . . . . . . 53296 2 30 . 1 1 43 43 LEU N N 15 . 1 1 43 43 LEU H H 1 0.59829577 0.021707259 . . . . . . . . . . 53296 2 31 . 1 1 45 45 ASN N N 15 . 1 1 45 45 ASN H H 1 0.571146867 0.014281394 . . . . . . . . . . 53296 2 32 . 1 1 47 47 GLU N N 15 . 1 1 47 47 GLU H H 1 0.590486289 0.020198317 . . . . . . . . . . 53296 2 33 . 1 1 48 48 ALA N N 15 . 1 1 48 48 ALA H H 1 0.672689449 0.018792699 . . . . . . . . . . 53296 2 34 . 1 1 49 49 THR N N 15 . 1 1 49 49 THR H H 1 0.564325508 0.014004008 . . . . . . . . . . 53296 2 35 . 1 1 50 50 LYS N N 15 . 1 1 50 50 LYS H H 1 0.577377404 0.017027645 . . . . . . . . . . 53296 2 36 . 1 1 51 51 GLY N N 15 . 1 1 51 51 GLY H H 1 0.63580146 0.018377355 . . . . . . . . . . 53296 2 37 . 1 1 52 52 PHE N N 15 . 1 1 52 52 PHE H H 1 0.624261895 0.019175512 . . . . . . . . . . 53296 2 38 . 1 1 54 54 ASP N N 15 . 1 1 54 54 ASP H H 1 0.657601638 0.016232798 . . . . . . . . . . 53296 2 39 . 1 1 57 57 SER N N 15 . 1 1 57 57 SER H H 1 0.647665073 0.01975106 . . . . . . . . . . 53296 2 40 . 1 1 58 58 SER N N 15 . 1 1 58 58 SER H H 1 0.573228608 0.015209603 . . . . . . . . . . 53296 2 41 . 1 1 59 59 GLY N N 15 . 1 1 59 59 GLY H H 1 0.631458133 0.01670884 . . . . . . . . . . 53296 2 42 . 1 1 61 61 SER N N 15 . 1 1 61 61 SER H H 1 0.721997425 0.017716799 . . . . . . . . . . 53296 2 43 . 1 1 62 62 SER N N 15 . 1 1 62 62 SER H H 1 0.690791535 0.019439003 . . . . . . . . . . 53296 2 44 . 1 1 63 63 SER N N 15 . 1 1 63 63 SER H H 1 0.680837531 0.019106972 . . . . . . . . . . 53296 2 45 . 1 1 64 64 LYS N N 15 . 1 1 64 64 LYS H H 1 0.655581717 0.016431743 . . . . . . . . . . 53296 2 46 . 1 1 66 66 LYS N N 15 . 1 1 66 66 LYS H H 1 0.690908187 0.033607086 . . . . . . . . . . 53296 2 47 . 1 1 68 68 ALA N N 15 . 1 1 68 68 ALA H H 1 0.575523174 0.015134234 . . . . . . . . . . 53296 2 48 . 1 1 69 69 TYR N N 15 . 1 1 69 69 TYR H H 1 0.812222846 0.018579086 . . . . . . . . . . 53296 2 49 . 1 1 70 70 SER N N 15 . 1 1 70 70 SER H H 1 0.655039043 0.01581805 . . . . . . . . . . 53296 2 50 . 1 1 71 71 SER N N 15 . 1 1 71 71 SER H H 1 0.669815801 0.018122719 . . . . . . . . . . 53296 2 51 . 1 1 73 73 GLY N N 15 . 1 1 73 73 GLY H H 1 0.607014273 0.015018489 . . . . . . . . . . 53296 2 52 . 1 1 74 74 SER N N 15 . 1 1 74 74 SER H H 1 0.605259258 0.017362173 . . . . . . . . . . 53296 2 53 . 1 1 78 78 SER N N 15 . 1 1 78 78 SER H H 1 0.547060035 0.015415661 . . . . . . . . . . 53296 2 54 . 1 1 82 82 SER N N 15 . 1 1 82 82 SER H H 1 0.476469393 0.014187272 . . . . . . . . . . 53296 2 55 . 1 1 83 83 SER N N 15 . 1 1 83 83 SER H H 1 0.650816976 0.018525409 . . . . . . . . . . 53296 2 56 . 1 1 85 85 PHE N N 15 . 1 1 85 85 PHE H H 1 0.673198035 0.021401172 . . . . . . . . . . 53296 2 57 . 1 1 86 86 SER N N 15 . 1 1 86 86 SER H H 1 0.654274902 0.014292926 . . . . . . . . . . 53296 2 58 . 1 1 88 88 ARG N N 15 . 1 1 88 88 ARG H H 1 0.686316255 0.015278765 . . . . . . . . . . 53296 2 59 . 1 1 89 89 GLY N N 15 . 1 1 89 89 GLY H H 1 0.572504648 0.013812257 . . . . . . . . . . 53296 2 60 . 1 1 90 90 SER N N 15 . 1 1 90 90 SER H H 1 0.564342696 0.020428362 . . . . . . . . . . 53296 2 61 . 1 1 91 91 GLY N N 15 . 1 1 91 91 GLY H H 1 0.516472662 0.010450059 . . . . . . . . . . 53296 2 62 . 1 1 92 92 SER N N 15 . 1 1 92 92 SER H H 1 0.638607834 0.018309494 . . . . . . . . . . 53296 2 63 . 1 1 94 94 GLY N N 15 . 1 1 94 94 GLY H H 1 0.62679809 0.017698244 . . . . . . . . . . 53296 2 64 . 1 1 95 95 ARG N N 15 . 1 1 95 95 ARG H H 1 0.713005696 0.021051001 . . . . . . . . . . 53296 2 65 . 1 1 96 96 PHE N N 15 . 1 1 96 96 PHE H H 1 0.652201197 0.019301284 . . . . . . . . . . 53296 2 66 . 1 1 97 97 ASP N N 15 . 1 1 97 97 ASP H H 1 0.696115224 0.034053665 . . . . . . . . . . 53296 2 67 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.672017136 0.015570772 . . . . . . . . . . 53296 2 68 . 1 1 100 100 GLY N N 15 . 1 1 100 100 GLY H H 1 0.567804003 0.015094274 . . . . . . . . . . 53296 2 69 . 1 1 101 101 ARG N N 15 . 1 1 101 101 ARG H H 1 0.649056978 0.020936782 . . . . . . . . . . 53296 2 70 . 1 1 102 102 SER N N 15 . 1 1 102 102 SER H H 1 0.638618818 0.014267079 . . . . . . . . . . 53296 2 71 . 1 1 104 104 TYR N N 15 . 1 1 104 104 TYR H H 1 0.631666534 0.026061449 . . . . . . . . . . 53296 2 72 . 1 1 106 106 GLY N N 15 . 1 1 106 106 GLY H H 1 0.654432429 0.020141712 . . . . . . . . . . 53296 2 73 . 1 1 107 107 ILE N N 15 . 1 1 107 107 ILE H H 1 0.659762266 0.022574071 . . . . . . . . . . 53296 2 74 . 1 1 108 108 GLY N N 15 . 1 1 108 108 GLY H H 1 0.592021477 0.0141121 . . . . . . . . . . 53296 2 75 . 1 1 109 109 SER N N 15 . 1 1 109 109 SER H H 1 0.621373579 0.016974844 . . . . . . . . . . 53296 2 76 . 1 1 113 113 ARG N N 15 . 1 1 113 113 ARG H H 1 0.568964968 0.017963882 . . . . . . . . . . 53296 2 77 . 1 1 115 115 GLY N N 15 . 1 1 115 115 GLY H H 1 0.650684579 0.0164308 . . . . . . . . . . 53296 2 78 . 1 1 116 116 PHE N N 15 . 1 1 116 116 PHE H H 1 0.662045086 0.017773941 . . . . . . . . . . 53296 2 79 . 1 1 117 117 GLY N N 15 . 1 1 117 117 GLY H H 1 0.562988809 0.014328396 . . . . . . . . . . 53296 2 80 . 1 1 118 118 LYS N N 15 . 1 1 118 118 LYS H H 1 0.719699477 0.023129913 . . . . . . . . . . 53296 2 81 . 1 1 120 120 GLU N N 15 . 1 1 120 120 GLU H H 1 0.646746253 0.02296086 . . . . . . . . . . 53296 2 82 . 1 1 121 121 ARG N N 15 . 1 1 121 121 ARG H H 1 0.540059312 0.015095288 . . . . . . . . . . 53296 2 83 . 1 1 122 122 GLY N N 15 . 1 1 122 122 GLY H H 1 0.549761311 0.014322122 . . . . . . . . . . 53296 2 84 . 1 1 123 123 GLY N N 15 . 1 1 123 123 GLY H H 1 0.604176581 0.017877826 . . . . . . . . . . 53296 2 85 . 1 1 124 124 ASN N N 15 . 1 1 124 124 ASN H H 1 0.56650552 0.015714911 . . . . . . . . . . 53296 2 86 . 1 1 125 125 SER N N 15 . 1 1 125 125 SER H H 1 0.615761498 0.016624758 . . . . . . . . . . 53296 2 87 . 1 1 128 128 CYS N N 15 . 1 1 128 128 CYS H H 1 0.596312241 0.014004833 . . . . . . . . . . 53296 2 88 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.72329178 0.018264229 . . . . . . . . . . 53296 2 89 . 1 1 131 131 SER N N 15 . 1 1 131 131 SER H H 1 0.327701999 0.012369708 . . . . . . . . . . 53296 2 90 . 1 1 132 132 ASP N N 15 . 1 1 132 132 ASP H H 1 0.208860544 0.009338528 . . . . . . . . . . 53296 2 stop_ save_ save_heteronucl_NOEs_3 _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode heteronucl_NOEs_3 _Heteronucl_NOE_list.Entry_ID 53296 _Heteronucl_NOE_list.ID 3 _Heteronucl_NOE_list.Name 'hetNOE u-2H,15N 300 uM' _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_NOE_list.Spectrometer_frequency_1H 1000 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'peak integral' _Heteronucl_NOE_list.NOE_ref_val 1.0 _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 17 '1H-15N heteronoe' . . . 53296 3 stop_ loop_ _Heteronucl_NOE_software.Software_ID _Heteronucl_NOE_software.Software_label _Heteronucl_NOE_software.Method_ID _Heteronucl_NOE_software.Method_label _Heteronucl_NOE_software.Entry_ID _Heteronucl_NOE_software.Heteronucl_NOE_list_ID 1 $software_1 . . 53296 3 2 $software_2 . . 53296 3 3 $software_3 . . 53296 3 4 $software_4 . . 53296 3 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 HIS N N 15 . 1 1 3 3 HIS H H 1 0.163732601 0.005709276 . . . . . . . . . . 53296 3 2 . 1 1 5 5 ALA N N 15 . 1 1 5 5 ALA H H 1 0.374505516 0.005904513 . . . . . . . . . . 53296 3 3 . 1 1 7 7 GLU N N 15 . 1 1 7 7 GLU H H 1 0.461950618 0.006036004 . . . . . . . . . . 53296 3 4 . 1 1 8 8 ASN N N 15 . 1 1 8 8 ASN H H 1 0.463299374 0.008779546 . . . . . . . . . . 53296 3 5 . 1 1 9 9 ALA N N 15 . 1 1 9 9 ALA H H 1 0.51519282 0.014709635 . . . . . . . . . . 53296 3 6 . 1 1 11 11 GLY N N 15 . 1 1 11 11 GLY H H 1 0.569160165 0.014249476 . . . . . . . . . . 53296 3 7 . 1 1 12 12 LEU N N 15 . 1 1 12 12 LEU H H 1 0.630306887 0.028953043 . . . . . . . . . . 53296 3 8 . 1 1 13 13 ASP N N 15 . 1 1 13 13 ASP H H 1 0.509324923 0.009199649 . . . . . . . . . . 53296 3 9 . 1 1 17 17 ALA N N 15 . 1 1 17 17 ALA H H 1 0.612780907 0.008046701 . . . . . . . . . . 53296 3 10 . 1 1 18 18 GLY N N 15 . 1 1 18 18 GLY H H 1 0.489253402 0.006562924 . . . . . . . . . . 53296 3 11 . 1 1 20 20 ASP N N 15 . 1 1 20 20 ASP H H 1 0.519170913 0.010198651 . . . . . . . . . . 53296 3 12 . 1 1 21 21 LEU N N 15 . 1 1 21 21 LEU H H 1 0.528095894 0.008594704 . . . . . . . . . . 53296 3 13 . 1 1 22 22 ASN N N 15 . 1 1 22 22 ASN H H 1 0.522462525 0.010196164 . . . . . . . . . . 53296 3 14 . 1 1 23 23 SER N N 15 . 1 1 23 23 SER H H 1 0.588815306 0.013859882 . . . . . . . . . . 53296 3 15 . 1 1 24 24 SER N N 15 . 1 1 24 24 SER H H 1 0.479294246 0.00896969 . . . . . . . . . . 53296 3 16 . 1 1 25 25 ASP N N 15 . 1 1 25 25 ASP H H 1 0.566213356 0.01259277 . . . . . . . . . . 53296 3 17 . 1 1 26 26 ASN N N 15 . 1 1 26 26 ASN H H 1 0.560598736 0.011257454 . . . . . . . . . . 53296 3 18 . 1 1 27 27 GLN N N 15 . 1 1 27 27 GLN H H 1 0.495697501 0.009550403 . . . . . . . . . . 53296 3 19 . 1 1 29 29 GLY N N 15 . 1 1 29 29 GLY H H 1 0.447599982 0.007252067 . . . . . . . . . . 53296 3 20 . 1 1 30 30 GLY N N 15 . 1 1 30 30 GLY H H 1 0.550864699 0.013828202 . . . . . . . . . . 53296 3 21 . 1 1 31 31 SER N N 15 . 1 1 31 31 SER H H 1 0.441347481 0.00870837 . . . . . . . . . . 53296 3 22 . 1 1 32 32 THR N N 15 . 1 1 32 32 THR H H 1 0.47029173 0.013189301 . . . . . . . . . . 53296 3 23 . 1 1 33 33 ALA N N 15 . 1 1 33 33 ALA H H 1 0.585363681 0.008151858 . . . . . . . . . . 53296 3 24 . 1 1 34 34 SER N N 15 . 1 1 34 34 SER H H 1 0.511971815 0.008151307 . . . . . . . . . . 53296 3 25 . 1 1 35 35 LYS N N 15 . 1 1 35 35 LYS H H 1 0.52476548 0.009101621 . . . . . . . . . . 53296 3 26 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.516059149 0.013962141 . . . . . . . . . . 53296 3 27 . 1 1 37 37 ARG N N 15 . 1 1 37 37 ARG H H 1 0.6726358 0.018262059 . . . . . . . . . . 53296 3 28 . 1 1 38 38 TYR N N 15 . 1 1 38 38 TYR H H 1 0.559772055 0.007319779 . . . . . . . . . . 53296 3 29 . 1 1 39 39 ILE N N 15 . 1 1 39 39 ILE H H 1 0.643960691 0.006635852 . . . . . . . . . . 53296 3 30 . 1 1 43 43 LEU N N 15 . 1 1 43 43 LEU H H 1 0.650294874 0.010772524 . . . . . . . . . . 53296 3 31 . 1 1 45 45 ASN N N 15 . 1 1 45 45 ASN H H 1 0.529776378 0.010389685 . . . . . . . . . . 53296 3 32 . 1 1 47 47 GLU N N 15 . 1 1 47 47 GLU H H 1 0.555874895 0.012480788 . . . . . . . . . . 53296 3 33 . 1 1 48 48 ALA N N 15 . 1 1 48 48 ALA H H 1 0.605325852 0.010378351 . . . . . . . . . . 53296 3 34 . 1 1 49 49 THR N N 15 . 1 1 49 49 THR H H 1 0.589896706 0.010064161 . . . . . . . . . . 53296 3 35 . 1 1 50 50 LYS N N 15 . 1 1 50 50 LYS H H 1 0.547990035 0.010195113 . . . . . . . . . . 53296 3 36 . 1 1 51 51 GLY N N 15 . 1 1 51 51 GLY H H 1 0.560416021 0.015118115 . . . . . . . . . . 53296 3 37 . 1 1 52 52 PHE N N 15 . 1 1 52 52 PHE H H 1 0.692508498 0.018240453 . . . . . . . . . . 53296 3 38 . 1 1 54 54 ASP N N 15 . 1 1 54 54 ASP H H 1 0.706653583 0.010199648 . . . . . . . . . . 53296 3 39 . 1 1 57 57 SER N N 15 . 1 1 57 57 SER H H 1 0.636147339 0.0161573 . . . . . . . . . . 53296 3 40 . 1 1 58 58 SER N N 15 . 1 1 58 58 SER H H 1 0.588804215 0.013078106 . . . . . . . . . . 53296 3 41 . 1 1 59 59 GLY N N 15 . 1 1 59 59 GLY H H 1 0.614882365 0.01108472 . . . . . . . . . . 53296 3 42 . 1 1 61 61 SER N N 15 . 1 1 61 61 SER H H 1 0.629162973 0.00973125 . . . . . . . . . . 53296 3 43 . 1 1 62 62 SER N N 15 . 1 1 62 62 SER H H 1 0.661343944 0.015072162 . . . . . . . . . . 53296 3 44 . 1 1 63 63 SER N N 15 . 1 1 63 63 SER H H 1 0.622000495 0.013777846 . . . . . . . . . . 53296 3 45 . 1 1 64 64 LYS N N 15 . 1 1 64 64 LYS H H 1 0.689691274 0.014269617 . . . . . . . . . . 53296 3 46 . 1 1 66 66 LYS N N 15 . 1 1 66 66 LYS H H 1 0.683374344 0.037039608 . . . . . . . . . . 53296 3 47 . 1 1 68 68 ALA N N 15 . 1 1 68 68 ALA H H 1 0.712833148 0.009174928 . . . . . . . . . . 53296 3 48 . 1 1 69 69 TYR N N 15 . 1 1 69 69 TYR H H 1 0.693284915 0.010901946 . . . . . . . . . . 53296 3 49 . 1 1 70 70 SER N N 15 . 1 1 70 70 SER H H 1 0.613408244 0.007636143 . . . . . . . . . . 53296 3 50 . 1 1 71 71 SER N N 15 . 1 1 71 71 SER H H 1 0.632258685 0.013464014 . . . . . . . . . . 53296 3 51 . 1 1 73 73 GLY N N 15 . 1 1 73 73 GLY H H 1 0.601219141 0.010335024 . . . . . . . . . . 53296 3 52 . 1 1 74 74 SER N N 15 . 1 1 74 74 SER H H 1 0.703728725 0.014967497 . . . . . . . . . . 53296 3 53 . 1 1 78 78 SER N N 15 . 1 1 78 78 SER H H 1 0.631537996 0.011099188 . . . . . . . . . . 53296 3 54 . 1 1 82 82 SER N N 15 . 1 1 82 82 SER H H 1 0.529067246 0.01453555 . . . . . . . . . . 53296 3 55 . 1 1 83 83 SER N N 15 . 1 1 83 83 SER H H 1 0.582350908 0.01150141 . . . . . . . . . . 53296 3 56 . 1 1 85 85 PHE N N 15 . 1 1 85 85 PHE H H 1 0.671904205 0.01950293 . . . . . . . . . . 53296 3 57 . 1 1 86 86 SER N N 15 . 1 1 86 86 SER H H 1 0.672346331 0.011837325 . . . . . . . . . . 53296 3 58 . 1 1 88 88 ARG N N 15 . 1 1 88 88 ARG H H 1 0.639144966 0.010681712 . . . . . . . . . . 53296 3 59 . 1 1 89 89 GLY N N 15 . 1 1 89 89 GLY H H 1 0.558404058 0.009964179 . . . . . . . . . . 53296 3 60 . 1 1 90 90 SER N N 15 . 1 1 90 90 SER H H 1 0.556622107 0.009252717 . . . . . . . . . . 53296 3 61 . 1 1 91 91 GLY N N 15 . 1 1 91 91 GLY H H 1 0.558975267 0.007092662 . . . . . . . . . . 53296 3 62 . 1 1 92 92 SER N N 15 . 1 1 92 92 SER H H 1 0.681352063 0.014805541 . . . . . . . . . . 53296 3 63 . 1 1 94 94 GLY N N 15 . 1 1 94 94 GLY H H 1 0.555157583 0.015110818 . . . . . . . . . . 53296 3 64 . 1 1 95 95 ARG N N 15 . 1 1 95 95 ARG H H 1 0.737959322 0.018474433 . . . . . . . . . . 53296 3 65 . 1 1 96 96 PHE N N 15 . 1 1 96 96 PHE H H 1 0.649696229 0.013432069 . . . . . . . . . . 53296 3 66 . 1 1 97 97 ASP N N 15 . 1 1 97 97 ASP H H 1 0.690759695 0.039994059 . . . . . . . . . . 53296 3 67 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.690863721 0.012064969 . . . . . . . . . . 53296 3 68 . 1 1 100 100 GLY N N 15 . 1 1 100 100 GLY H H 1 0.622823067 0.011681289 . . . . . . . . . . 53296 3 69 . 1 1 101 101 ARG N N 15 . 1 1 101 101 ARG H H 1 0.722658439 0.020042 . . . . . . . . . . 53296 3 70 . 1 1 102 102 SER N N 15 . 1 1 102 102 SER H H 1 0.563287279 0.007422981 . . . . . . . . . . 53296 3 71 . 1 1 104 104 TYR N N 15 . 1 1 104 104 TYR H H 1 0.643927723 0.019198899 . . . . . . . . . . 53296 3 72 . 1 1 106 106 GLY N N 15 . 1 1 106 106 GLY H H 1 0.663564677 0.011348173 . . . . . . . . . . 53296 3 73 . 1 1 107 107 ILE N N 15 . 1 1 107 107 ILE H H 1 0.705516507 0.019147695 . . . . . . . . . . 53296 3 74 . 1 1 108 108 GLY N N 15 . 1 1 108 108 GLY H H 1 0.636361106 0.011171392 . . . . . . . . . . 53296 3 75 . 1 1 109 109 SER N N 15 . 1 1 109 109 SER H H 1 0.660392723 0.015870316 . . . . . . . . . . 53296 3 76 . 1 1 113 113 ARG N N 15 . 1 1 113 113 ARG H H 1 0.55384252 0.012311784 . . . . . . . . . . 53296 3 77 . 1 1 115 115 GLY N N 15 . 1 1 115 115 GLY H H 1 0.587549306 0.009748669 . . . . . . . . . . 53296 3 78 . 1 1 116 116 PHE N N 15 . 1 1 116 116 PHE H H 1 0.736268831 0.017111694 . . . . . . . . . . 53296 3 79 . 1 1 117 117 GLY N N 15 . 1 1 117 117 GLY H H 1 0.56881174 0.009489537 . . . . . . . . . . 53296 3 80 . 1 1 118 118 LYS N N 15 . 1 1 118 118 LYS H H 1 0.736678842 0.019453862 . . . . . . . . . . 53296 3 81 . 1 1 120 120 GLU N N 15 . 1 1 120 120 GLU H H 1 0.663221002 0.019315807 . . . . . . . . . . 53296 3 82 . 1 1 121 121 ARG N N 15 . 1 1 121 121 ARG H H 1 0.55981867 0.012485412 . . . . . . . . . . 53296 3 83 . 1 1 122 122 GLY N N 15 . 1 1 122 122 GLY H H 1 0.538532537 0.007167019 . . . . . . . . . . 53296 3 84 . 1 1 123 123 GLY N N 15 . 1 1 123 123 GLY H H 1 0.674611567 0.01950772 . . . . . . . . . . 53296 3 85 . 1 1 124 124 ASN N N 15 . 1 1 124 124 ASN H H 1 0.569329415 0.010194112 . . . . . . . . . . 53296 3 86 . 1 1 125 125 SER N N 15 . 1 1 125 125 SER H H 1 0.556120821 0.010536433 . . . . . . . . . . 53296 3 87 . 1 1 128 128 CYS N N 15 . 1 1 128 128 CYS H H 1 0.602815749 0.006884707 . . . . . . . . . . 53296 3 88 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.647019377 0.013720737 . . . . . . . . . . 53296 3 89 . 1 1 131 131 SER N N 15 . 1 1 131 131 SER H H 1 0.366235112 0.008447142 . . . . . . . . . . 53296 3 90 . 1 1 132 132 ASP N N 15 . 1 1 132 132 ASP H H 1 0.20867292 0.004710883 . . . . . . . . . . 53296 3 stop_ save_ save_heteronucl_NOEs_4 _Heteronucl_NOE_list.Sf_category heteronucl_NOEs _Heteronucl_NOE_list.Sf_framecode heteronucl_NOEs_4 _Heteronucl_NOE_list.Entry_ID 53296 _Heteronucl_NOE_list.ID 4 _Heteronucl_NOE_list.Name 'hetNOE u-2H,15N 500 uM' _Heteronucl_NOE_list.Sample_condition_list_ID 1 _Heteronucl_NOE_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_NOE_list.Spectrometer_frequency_1H 1000 _Heteronucl_NOE_list.Heteronuclear_NOE_val_type 'peak integral' _Heteronucl_NOE_list.NOE_ref_val 1.0 _Heteronucl_NOE_list.NOE_ref_description . _Heteronucl_NOE_list.Details . _Heteronucl_NOE_list.Text_data_format . _Heteronucl_NOE_list.Text_data . loop_ _Heteronucl_NOE_experiment.Experiment_ID _Heteronucl_NOE_experiment.Experiment_name _Heteronucl_NOE_experiment.Sample_ID _Heteronucl_NOE_experiment.Sample_label _Heteronucl_NOE_experiment.Sample_state _Heteronucl_NOE_experiment.Entry_ID _Heteronucl_NOE_experiment.Heteronucl_NOE_list_ID 24 '1H-15N heteronoe' . . . 53296 4 stop_ loop_ _Heteronucl_NOE_software.Software_ID _Heteronucl_NOE_software.Software_label _Heteronucl_NOE_software.Method_ID _Heteronucl_NOE_software.Method_label _Heteronucl_NOE_software.Entry_ID _Heteronucl_NOE_software.Heteronucl_NOE_list_ID 1 $software_1 . . 53296 4 2 $software_2 . . 53296 4 3 $software_3 . . 53296 4 4 $software_4 . . 53296 4 stop_ loop_ _Heteronucl_NOE.ID _Heteronucl_NOE.Assembly_atom_ID_1 _Heteronucl_NOE.Entity_assembly_ID_1 _Heteronucl_NOE.Entity_ID_1 _Heteronucl_NOE.Comp_index_ID_1 _Heteronucl_NOE.Seq_ID_1 _Heteronucl_NOE.Comp_ID_1 _Heteronucl_NOE.Atom_ID_1 _Heteronucl_NOE.Atom_type_1 _Heteronucl_NOE.Atom_isotope_number_1 _Heteronucl_NOE.Assembly_atom_ID_2 _Heteronucl_NOE.Entity_assembly_ID_2 _Heteronucl_NOE.Entity_ID_2 _Heteronucl_NOE.Comp_index_ID_2 _Heteronucl_NOE.Seq_ID_2 _Heteronucl_NOE.Comp_ID_2 _Heteronucl_NOE.Atom_ID_2 _Heteronucl_NOE.Atom_type_2 _Heteronucl_NOE.Atom_isotope_number_2 _Heteronucl_NOE.Val _Heteronucl_NOE.Val_err _Heteronucl_NOE.Resonance_ID_1 _Heteronucl_NOE.Resonance_ID_2 _Heteronucl_NOE.Auth_entity_assembly_ID_1 _Heteronucl_NOE.Auth_seq_ID_1 _Heteronucl_NOE.Auth_comp_ID_1 _Heteronucl_NOE.Auth_atom_ID_1 _Heteronucl_NOE.Auth_entity_assembly_ID_2 _Heteronucl_NOE.Auth_seq_ID_2 _Heteronucl_NOE.Auth_comp_ID_2 _Heteronucl_NOE.Auth_atom_ID_2 _Heteronucl_NOE.Entry_ID _Heteronucl_NOE.Heteronucl_NOE_list_ID 1 . 1 1 3 3 HIS N N 15 . 1 1 3 3 HIS H H 1 0.20958855 0.005076386 . . . . . . . . . . 53296 4 2 . 1 1 5 5 ALA N N 15 . 1 1 5 5 ALA H H 1 0.396195781 0.005448318 . . . . . . . . . . 53296 4 3 . 1 1 7 7 GLU N N 15 . 1 1 7 7 GLU H H 1 0.466137838 0.005557589 . . . . . . . . . . 53296 4 4 . 1 1 8 8 ASN N N 15 . 1 1 8 8 ASN H H 1 0.484149503 0.0084949 . . . . . . . . . . 53296 4 5 . 1 1 9 9 ALA N N 15 . 1 1 9 9 ALA H H 1 0.528647606 0.013837154 . . . . . . . . . . 53296 4 6 . 1 1 11 11 GLY N N 15 . 1 1 11 11 GLY H H 1 0.552462466 0.011141946 . . . . . . . . . . 53296 4 7 . 1 1 12 12 LEU N N 15 . 1 1 12 12 LEU H H 1 0.6598053 0.031526713 . . . . . . . . . . 53296 4 8 . 1 1 13 13 ASP N N 15 . 1 1 13 13 ASP H H 1 0.533425001 0.009049706 . . . . . . . . . . 53296 4 9 . 1 1 17 17 ALA N N 15 . 1 1 17 17 ALA H H 1 0.600375295 0.007713327 . . . . . . . . . . 53296 4 10 . 1 1 18 18 GLY N N 15 . 1 1 18 18 GLY H H 1 0.532802817 0.008628517 . . . . . . . . . . 53296 4 11 . 1 1 20 20 ASP N N 15 . 1 1 20 20 ASP H H 1 0.526211361 0.009058376 . . . . . . . . . . 53296 4 12 . 1 1 21 21 LEU N N 15 . 1 1 21 21 LEU H H 1 0.568161773 0.010471171 . . . . . . . . . . 53296 4 13 . 1 1 22 22 ASN N N 15 . 1 1 22 22 ASN H H 1 0.514391386 0.00846829 . . . . . . . . . . 53296 4 14 . 1 1 23 23 SER N N 15 . 1 1 23 23 SER H H 1 0.556365589 0.010937365 . . . . . . . . . . 53296 4 15 . 1 1 24 24 SER N N 15 . 1 1 24 24 SER H H 1 0.511697206 0.008725064 . . . . . . . . . . 53296 4 16 . 1 1 25 25 ASP N N 15 . 1 1 25 25 ASP H H 1 0.588777365 0.011214274 . . . . . . . . . . 53296 4 17 . 1 1 26 26 ASN N N 15 . 1 1 26 26 ASN H H 1 0.532442528 0.009373635 . . . . . . . . . . 53296 4 18 . 1 1 27 27 GLN N N 15 . 1 1 27 27 GLN H H 1 0.508069115 0.009245853 . . . . . . . . . . 53296 4 19 . 1 1 29 29 GLY N N 15 . 1 1 29 29 GLY H H 1 0.449189064 0.007002933 . . . . . . . . . . 53296 4 20 . 1 1 30 30 GLY N N 15 . 1 1 30 30 GLY H H 1 0.52491064 0.010709912 . . . . . . . . . . 53296 4 21 . 1 1 31 31 SER N N 15 . 1 1 31 31 SER H H 1 0.430823396 0.006905082 . . . . . . . . . . 53296 4 22 . 1 1 32 32 THR N N 15 . 1 1 32 32 THR H H 1 0.477119316 0.008187899 . . . . . . . . . . 53296 4 23 . 1 1 33 33 ALA N N 15 . 1 1 33 33 ALA H H 1 0.531266581 0.007906852 . . . . . . . . . . 53296 4 24 . 1 1 34 34 SER N N 15 . 1 1 34 34 SER H H 1 0.523503288 0.007726546 . . . . . . . . . . 53296 4 25 . 1 1 35 35 LYS N N 15 . 1 1 35 35 LYS H H 1 0.490009956 0.009676685 . . . . . . . . . . 53296 4 26 . 1 1 36 36 GLY N N 15 . 1 1 36 36 GLY H H 1 0.517318649 0.011336655 . . . . . . . . . . 53296 4 27 . 1 1 37 37 ARG N N 15 . 1 1 37 37 ARG H H 1 0.628206349 0.015911819 . . . . . . . . . . 53296 4 28 . 1 1 38 38 TYR N N 15 . 1 1 38 38 TYR H H 1 0.583578286 0.009096635 . . . . . . . . . . 53296 4 29 . 1 1 39 39 ILE N N 15 . 1 1 39 39 ILE H H 1 0.603792276 0.007226117 . . . . . . . . . . 53296 4 30 . 1 1 43 43 LEU N N 15 . 1 1 43 43 LEU H H 1 0.667546151 0.010936807 . . . . . . . . . . 53296 4 31 . 1 1 45 45 ASN N N 15 . 1 1 45 45 ASN H H 1 0.568656465 0.009973607 . . . . . . . . . . 53296 4 32 . 1 1 47 47 GLU N N 15 . 1 1 47 47 GLU H H 1 0.601588044 0.012167527 . . . . . . . . . . 53296 4 33 . 1 1 48 48 ALA N N 15 . 1 1 48 48 ALA H H 1 0.61249048 0.012511892 . . . . . . . . . . 53296 4 34 . 1 1 49 49 THR N N 15 . 1 1 49 49 THR H H 1 0.580839008 0.00761346 . . . . . . . . . . 53296 4 35 . 1 1 50 50 LYS N N 15 . 1 1 50 50 LYS H H 1 0.594331547 0.012462991 . . . . . . . . . . 53296 4 36 . 1 1 51 51 GLY N N 15 . 1 1 51 51 GLY H H 1 0.526368825 0.011777282 . . . . . . . . . . 53296 4 37 . 1 1 52 52 PHE N N 15 . 1 1 52 52 PHE H H 1 0.639511951 0.015605821 . . . . . . . . . . 53296 4 38 . 1 1 54 54 ASP N N 15 . 1 1 54 54 ASP H H 1 0.697564036 0.011125925 . . . . . . . . . . 53296 4 39 . 1 1 57 57 SER N N 15 . 1 1 57 57 SER H H 1 0.618819224 0.013723615 . . . . . . . . . . 53296 4 40 . 1 1 58 58 SER N N 15 . 1 1 58 58 SER H H 1 0.560141811 0.011460585 . . . . . . . . . . 53296 4 41 . 1 1 59 59 GLY N N 15 . 1 1 59 59 GLY H H 1 0.635896294 0.010009556 . . . . . . . . . . 53296 4 42 . 1 1 61 61 SER N N 15 . 1 1 61 61 SER H H 1 0.653064835 0.012248956 . . . . . . . . . . 53296 4 43 . 1 1 62 62 SER N N 15 . 1 1 62 62 SER H H 1 0.645037304 0.011589936 . . . . . . . . . . 53296 4 44 . 1 1 63 63 SER N N 15 . 1 1 63 63 SER H H 1 0.627772524 0.010745478 . . . . . . . . . . 53296 4 45 . 1 1 64 64 LYS N N 15 . 1 1 64 64 LYS H H 1 0.661499305 0.014593935 . . . . . . . . . . 53296 4 46 . 1 1 66 66 LYS N N 15 . 1 1 66 66 LYS H H 1 0.655836436 0.03821595 . . . . . . . . . . 53296 4 47 . 1 1 68 68 ALA N N 15 . 1 1 68 68 ALA H H 1 0.66888677 0.009942481 . . . . . . . . . . 53296 4 48 . 1 1 69 69 TYR N N 15 . 1 1 69 69 TYR H H 1 0.734248431 0.010945934 . . . . . . . . . . 53296 4 49 . 1 1 70 70 SER N N 15 . 1 1 70 70 SER H H 1 0.643340037 0.00905939 . . . . . . . . . . 53296 4 50 . 1 1 71 71 SER N N 15 . 1 1 71 71 SER H H 1 0.680543749 0.010898229 . . . . . . . . . . 53296 4 51 . 1 1 73 73 GLY N N 15 . 1 1 73 73 GLY H H 1 0.59326079 0.008793106 . . . . . . . . . . 53296 4 52 . 1 1 74 74 SER N N 15 . 1 1 74 74 SER H H 1 0.687925609 0.012860585 . . . . . . . . . . 53296 4 53 . 1 1 78 78 SER N N 15 . 1 1 78 78 SER H H 1 0.586358127 0.012218745 . . . . . . . . . . 53296 4 54 . 1 1 82 82 SER N N 15 . 1 1 82 82 SER H H 1 0.512439624 0.01196603 . . . . . . . . . . 53296 4 55 . 1 1 83 83 SER N N 15 . 1 1 83 83 SER H H 1 0.585190521 0.009368493 . . . . . . . . . . 53296 4 56 . 1 1 85 85 PHE N N 15 . 1 1 85 85 PHE H H 1 0.696250418 0.019704807 . . . . . . . . . . 53296 4 57 . 1 1 86 86 SER N N 15 . 1 1 86 86 SER H H 1 0.655575718 0.008410962 . . . . . . . . . . 53296 4 58 . 1 1 88 88 ARG N N 15 . 1 1 88 88 ARG H H 1 0.627606422 0.011136345 . . . . . . . . . . 53296 4 59 . 1 1 89 89 GLY N N 15 . 1 1 89 89 GLY H H 1 0.562749731 0.0099479 . . . . . . . . . . 53296 4 60 . 1 1 90 90 SER N N 15 . 1 1 90 90 SER H H 1 0.631615246 0.022011649 . . . . . . . . . . 53296 4 61 . 1 1 91 91 GLY N N 15 . 1 1 91 91 GLY H H 1 0.516802067 0.005562777 . . . . . . . . . . 53296 4 62 . 1 1 92 92 SER N N 15 . 1 1 92 92 SER H H 1 0.652011908 0.013207687 . . . . . . . . . . 53296 4 63 . 1 1 94 94 GLY N N 15 . 1 1 94 94 GLY H H 1 0.541895345 0.011648994 . . . . . . . . . . 53296 4 64 . 1 1 95 95 ARG N N 15 . 1 1 95 95 ARG H H 1 0.689286347 0.016550426 . . . . . . . . . . 53296 4 65 . 1 1 96 96 PHE N N 15 . 1 1 96 96 PHE H H 1 0.631289202 0.012765971 . . . . . . . . . . 53296 4 66 . 1 1 97 97 ASP N N 15 . 1 1 97 97 ASP H H 1 0.660432802 0.041457217 . . . . . . . . . . 53296 4 67 . 1 1 98 98 ASP N N 15 . 1 1 98 98 ASP H H 1 0.730820393 0.012624538 . . . . . . . . . . 53296 4 68 . 1 1 100 100 GLY N N 15 . 1 1 100 100 GLY H H 1 0.64760376 0.011788669 . . . . . . . . . . 53296 4 69 . 1 1 101 101 ARG N N 15 . 1 1 101 101 ARG H H 1 0.730245134 0.018670042 . . . . . . . . . . 53296 4 70 . 1 1 102 102 SER N N 15 . 1 1 102 102 SER H H 1 0.59756454 0.009538566 . . . . . . . . . . 53296 4 71 . 1 1 104 104 TYR N N 15 . 1 1 104 104 TYR H H 1 0.684423739 0.019187411 . . . . . . . . . . 53296 4 72 . 1 1 106 106 GLY N N 15 . 1 1 106 106 GLY H H 1 0.691390884 0.010735337 . . . . . . . . . . 53296 4 73 . 1 1 107 107 ILE N N 15 . 1 1 107 107 ILE H H 1 0.671769538 0.016839444 . . . . . . . . . . 53296 4 74 . 1 1 108 108 GLY N N 15 . 1 1 108 108 GLY H H 1 0.607807843 0.008937834 . . . . . . . . . . 53296 4 75 . 1 1 109 109 SER N N 15 . 1 1 109 109 SER H H 1 0.652238646 0.014395461 . . . . . . . . . . 53296 4 76 . 1 1 113 113 ARG N N 15 . 1 1 113 113 ARG H H 1 0.514772361 0.010612037 . . . . . . . . . . 53296 4 77 . 1 1 115 115 GLY N N 15 . 1 1 115 115 GLY H H 1 0.620704979 0.009290933 . . . . . . . . . . 53296 4 78 . 1 1 116 116 PHE N N 15 . 1 1 116 116 PHE H H 1 0.719941967 0.014526894 . . . . . . . . . . 53296 4 79 . 1 1 117 117 GLY N N 15 . 1 1 117 117 GLY H H 1 0.558614661 0.009167573 . . . . . . . . . . 53296 4 80 . 1 1 118 118 LYS N N 15 . 1 1 118 118 LYS H H 1 0.692037069 0.017596465 . . . . . . . . . . 53296 4 81 . 1 1 120 120 GLU N N 15 . 1 1 120 120 GLU H H 1 0.698352394 0.023060222 . . . . . . . . . . 53296 4 82 . 1 1 121 121 ARG N N 15 . 1 1 121 121 ARG H H 1 0.593467862 0.010775262 . . . . . . . . . . 53296 4 83 . 1 1 122 122 GLY N N 15 . 1 1 122 122 GLY H H 1 0.545303911 0.008497591 . . . . . . . . . . 53296 4 84 . 1 1 123 123 GLY N N 15 . 1 1 123 123 GLY H H 1 0.613256695 0.014053651 . . . . . . . . . . 53296 4 85 . 1 1 124 124 ASN N N 15 . 1 1 124 124 ASN H H 1 0.542593113 0.00819804 . . . . . . . . . . 53296 4 86 . 1 1 125 125 SER N N 15 . 1 1 125 125 SER H H 1 0.594599528 0.013097499 . . . . . . . . . . 53296 4 87 . 1 1 128 128 CYS N N 15 . 1 1 128 128 CYS H H 1 0.615438383 0.007442792 . . . . . . . . . . 53296 4 88 . 1 1 129 129 ASP N N 15 . 1 1 129 129 ASP H H 1 0.653768918 0.014696033 . . . . . . . . . . 53296 4 89 . 1 1 131 131 SER N N 15 . 1 1 131 131 SER H H 1 0.351189629 0.007668852 . . . . . . . . . . 53296 4 90 . 1 1 132 132 ASP N N 15 . 1 1 132 132 ASP H H 1 0.243471047 0.005992187 . . . . . . . . . . 53296 4 stop_ save_ ######################################## # Heteronuclear T1 relaxation values # ######################################## save_heteronucl_T1_relaxation_1 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_1 _Heteronucl_T1_list.Entry_ID 53296 _Heteronucl_T1_list.ID 1 _Heteronucl_T1_list.Name '15N R1 u-15N' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 1000 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 2 'T1/R1 relaxation' . . . 53296 1 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 53296 1 2 $software_2 . . 53296 1 3 $software_3 . . 53296 1 4 $software_4 . . 53296 1 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 HIS N N 15 1.370390767 0.022730004 . . . . . 53296 1 2 . 1 1 5 5 ALA N N 15 1.555615318 0.007032958 . . . . . 53296 1 3 . 1 1 7 7 GLU N N 15 1.581372108 0.010189758 . . . . . 53296 1 4 . 1 1 8 8 ASN N N 15 1.509813486 0.006863933 . . . . . 53296 1 5 . 1 1 9 9 ALA N N 15 1.452883323 0.0241703 . . . . . 53296 1 6 . 1 1 11 11 GLY N N 15 1.508874984 0.015926602 . . . . . 53296 1 7 . 1 1 13 13 ASP N N 15 1.516570658 0.00875992 . . . . . 53296 1 8 . 1 1 17 17 ALA N N 15 1.46035139 0.009380272 . . . . . 53296 1 9 . 1 1 18 18 GLY N N 15 1.409588573 0.015915608 . . . . . 53296 1 10 . 1 1 20 20 ASP N N 15 1.431398189 0.026139639 . . . . . 53296 1 11 . 1 1 21 21 LEU N N 15 1.414853246 0.015052508 . . . . . 53296 1 12 . 1 1 22 22 ASN N N 15 1.473299342 0.014310449 . . . . . 53296 1 13 . 1 1 23 23 SER N N 15 1.425493718 0.018104949 . . . . . 53296 1 14 . 1 1 24 24 SER N N 15 1.509939658 0.010974306 . . . . . 53296 1 15 . 1 1 25 25 ASP N N 15 1.532904603 0.013274279 . . . . . 53296 1 16 . 1 1 26 26 ASN N N 15 1.496248167 0.01419167 . . . . . 53296 1 17 . 1 1 27 27 GLN N N 15 1.504364639 0.009455201 . . . . . 53296 1 18 . 1 1 29 29 GLY N N 15 1.497084738 0.013840148 . . . . . 53296 1 19 . 1 1 30 30 GLY N N 15 1.485198827 0.016075829 . . . . . 53296 1 20 . 1 1 31 31 SER N N 15 1.428225663 0.021421917 . . . . . 53296 1 21 . 1 1 33 33 ALA N N 15 1.512791213 0.01305192 . . . . . 53296 1 22 . 1 1 34 34 SER N N 15 1.421025339 0.005117806 . . . . . 53296 1 23 . 1 1 35 35 LYS N N 15 1.426206691 0.015907136 . . . . . 53296 1 24 . 1 1 37 37 ARG N N 15 1.37621837 0.010203312 . . . . . 53296 1 25 . 1 1 38 38 TYR N N 15 1.249569345 0.017094967 . . . . . 53296 1 26 . 1 1 39 39 ILE N N 15 1.251501511 0.026736748 . . . . . 53296 1 27 . 1 1 42 42 HIS N N 15 1.226682515 0.071582657 . . . . . 53296 1 28 . 1 1 43 43 LEU N N 15 1.242596877 0.047232298 . . . . . 53296 1 29 . 1 1 45 45 ASN N N 15 1.241508275 0.033047911 . . . . . 53296 1 30 . 1 1 47 47 GLU N N 15 1.287327506 0.011069889 . . . . . 53296 1 31 . 1 1 48 48 ALA N N 15 1.298818756 0.019752764 . . . . . 53296 1 32 . 1 1 49 49 THR N N 15 1.2439586 0.027995835 . . . . . 53296 1 33 . 1 1 50 50 LYS N N 15 1.32685621 0.017036939 . . . . . 53296 1 34 . 1 1 51 51 GLY N N 15 1.311772075 0.034184378 . . . . . 53296 1 35 . 1 1 54 54 ASP N N 15 1.322993927 0.01885569 . . . . . 53296 1 36 . 1 1 57 57 SER N N 15 1.278178658 0.015742316 . . . . . 53296 1 37 . 1 1 58 58 SER N N 15 1.326641998 0.01014436 . . . . . 53296 1 38 . 1 1 59 59 GLY N N 15 1.349423693 0.024359124 . . . . . 53296 1 39 . 1 1 61 61 SER N N 15 1.289780188 0.02766551 . . . . . 53296 1 40 . 1 1 62 62 SER N N 15 1.285925622 0.027983324 . . . . . 53296 1 41 . 1 1 63 63 SER N N 15 1.347699699 0.026023225 . . . . . 53296 1 42 . 1 1 64 64 LYS N N 15 1.338315007 0.018945748 . . . . . 53296 1 43 . 1 1 66 66 LYS N N 15 1.275590793 0.016599952 . . . . . 53296 1 44 . 1 1 68 68 ALA N N 15 1.308095955 0.017642498 . . . . . 53296 1 45 . 1 1 69 69 TYR N N 15 1.301809846 0.016662304 . . . . . 53296 1 46 . 1 1 70 70 SER N N 15 1.305530863 0.01622099 . . . . . 53296 1 47 . 1 1 71 71 SER N N 15 1.367902989 0.026720765 . . . . . 53296 1 48 . 1 1 73 73 GLY N N 15 1.331918404 0.030027089 . . . . . 53296 1 49 . 1 1 74 74 SER N N 15 1.323863323 0.019113172 . . . . . 53296 1 50 . 1 1 78 78 SER N N 15 1.361125292 0.019935801 . . . . . 53296 1 51 . 1 1 82 82 SER N N 15 1.306088266 0.00851427 . . . . . 53296 1 52 . 1 1 83 83 SER N N 15 1.30942328 0.02717883 . . . . . 53296 1 53 . 1 1 85 85 PHE N N 15 1.309445605 0.015289915 . . . . . 53296 1 54 . 1 1 86 86 SER N N 15 1.286394206 0.024461329 . . . . . 53296 1 55 . 1 1 88 88 ARG N N 15 1.292105663 0.011146337 . . . . . 53296 1 56 . 1 1 89 89 GLY N N 15 1.388935504 0.014002974 . . . . . 53296 1 57 . 1 1 91 91 GLY N N 15 1.414051966 0.016376621 . . . . . 53296 1 58 . 1 1 92 92 SER N N 15 1.333078527 0.012754036 . . . . . 53296 1 59 . 1 1 95 95 ARG N N 15 1.302085649 0.014608702 . . . . . 53296 1 60 . 1 1 96 96 PHE N N 15 1.259699588 0.010992371 . . . . . 53296 1 61 . 1 1 97 97 ASP N N 15 1.311705233 0.021353321 . . . . . 53296 1 62 . 1 1 98 98 ASP N N 15 1.226812539 0.028260256 . . . . . 53296 1 63 . 1 1 100 100 GLY N N 15 1.238518767 0.017711302 . . . . . 53296 1 64 . 1 1 101 101 ARG N N 15 1.271080756 0.014080532 . . . . . 53296 1 65 . 1 1 102 102 SER N N 15 1.246903505 0.023092165 . . . . . 53296 1 66 . 1 1 106 106 GLY N N 15 1.27031342 0.023882339 . . . . . 53296 1 67 . 1 1 107 107 ILE N N 15 1.279683665 0.022625288 . . . . . 53296 1 68 . 1 1 108 108 GLY N N 15 1.309445443 0.025186464 . . . . . 53296 1 69 . 1 1 109 109 SER N N 15 1.348595098 0.009582426 . . . . . 53296 1 70 . 1 1 113 113 ARG N N 15 1.334470467 0.019211114 . . . . . 53296 1 71 . 1 1 115 115 GLY N N 15 1.357655237 0.017091669 . . . . . 53296 1 72 . 1 1 116 116 PHE N N 15 1.359174407 0.008302923 . . . . . 53296 1 73 . 1 1 117 117 GLY N N 15 1.402659215 0.025250492 . . . . . 53296 1 74 . 1 1 118 118 LYS N N 15 1.353704961 0.006350586 . . . . . 53296 1 75 . 1 1 120 120 GLU N N 15 1.329788633 0.012720372 . . . . . 53296 1 76 . 1 1 121 121 ARG N N 15 1.431599328 0.039603575 . . . . . 53296 1 77 . 1 1 122 122 GLY N N 15 1.417352666 0.012854891 . . . . . 53296 1 78 . 1 1 123 123 GLY N N 15 1.452053293 0.018304134 . . . . . 53296 1 79 . 1 1 124 124 ASN N N 15 1.431671952 0.011447514 . . . . . 53296 1 80 . 1 1 125 125 SER N N 15 1.396344077 0.013434393 . . . . . 53296 1 81 . 1 1 128 128 CYS N N 15 1.445645827 0.014530145 . . . . . 53296 1 82 . 1 1 129 129 ASP N N 15 1.486830626 0.02479316 . . . . . 53296 1 83 . 1 1 131 131 SER N N 15 1.438421791 0.012079791 . . . . . 53296 1 84 . 1 1 132 132 ASP N N 15 1.299823202 0.013306374 . . . . . 53296 1 stop_ save_ save_heteronucl_T1_relaxation_2 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_2 _Heteronucl_T1_list.Entry_ID 53296 _Heteronucl_T1_list.ID 2 _Heteronucl_T1_list.Name '15N R1 u-2H,15N 100 uM' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 1000 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 9 'T1/R1 relaxation' . . . 53296 2 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 53296 2 2 $software_2 . . 53296 2 3 $software_3 . . 53296 2 4 $software_4 . . 53296 2 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 HIS N N 15 1.270889893 0.057676861 . . . . . 53296 2 2 . 1 1 5 5 ALA N N 15 1.484770942 0.027484928 . . . . . 53296 2 3 . 1 1 7 7 GLU N N 15 1.554802039 0.041263709 . . . . . 53296 2 4 . 1 1 8 8 ASN N N 15 1.512861377 0.007724755 . . . . . 53296 2 5 . 1 1 9 9 ALA N N 15 1.469873322 0.049230963 . . . . . 53296 2 6 . 1 1 11 11 GLY N N 15 1.519056791 0.017859616 . . . . . 53296 2 7 . 1 1 12 12 LEU N N 15 1.432962013 0.036504265 . . . . . 53296 2 8 . 1 1 13 13 ASP N N 15 1.491005498 0.028844761 . . . . . 53296 2 9 . 1 1 17 17 ALA N N 15 1.48859874 0.050252628 . . . . . 53296 2 10 . 1 1 18 18 GLY N N 15 1.308287802 0.025201513 . . . . . 53296 2 11 . 1 1 20 20 ASP N N 15 1.434236896 0.038790227 . . . . . 53296 2 12 . 1 1 21 21 LEU N N 15 1.384789772 0.031386648 . . . . . 53296 2 13 . 1 1 22 22 ASN N N 15 1.464412995 0.016851729 . . . . . 53296 2 14 . 1 1 23 23 SER N N 15 1.47834633 0.029791443 . . . . . 53296 2 15 . 1 1 24 24 SER N N 15 1.52084737 0.024791149 . . . . . 53296 2 16 . 1 1 25 25 ASP N N 15 1.540628231 0.014157963 . . . . . 53296 2 17 . 1 1 26 26 ASN N N 15 1.493402994 0.032458076 . . . . . 53296 2 18 . 1 1 27 27 GLN N N 15 1.521514043 0.019783415 . . . . . 53296 2 19 . 1 1 29 29 GLY N N 15 1.526705377 0.024953029 . . . . . 53296 2 20 . 1 1 30 30 GLY N N 15 1.472757328 0.01485112 . . . . . 53296 2 21 . 1 1 31 31 SER N N 15 1.367591823 0.035752007 . . . . . 53296 2 22 . 1 1 32 32 THR N N 15 1.509656611 0.021498312 . . . . . 53296 2 23 . 1 1 33 33 ALA N N 15 1.516420589 0.042863602 . . . . . 53296 2 24 . 1 1 34 34 SER N N 15 1.355722589 0.011300293 . . . . . 53296 2 25 . 1 1 35 35 LYS N N 15 1.465458689 0.018225862 . . . . . 53296 2 26 . 1 1 36 36 GLY N N 15 1.419717686 0.035286733 . . . . . 53296 2 27 . 1 1 37 37 ARG N N 15 1.317611339 0.043812129 . . . . . 53296 2 28 . 1 1 38 38 TYR N N 15 1.275987011 0.043677845 . . . . . 53296 2 29 . 1 1 39 39 ILE N N 15 1.253251157 0.039677058 . . . . . 53296 2 30 . 1 1 43 43 LEU N N 15 1.254684523 0.047843819 . . . . . 53296 2 31 . 1 1 45 45 ASN N N 15 1.253586935 0.017460499 . . . . . 53296 2 32 . 1 1 47 47 GLU N N 15 1.284063385 0.042382387 . . . . . 53296 2 33 . 1 1 48 48 ALA N N 15 1.293911225 0.04198605 . . . . . 53296 2 34 . 1 1 49 49 THR N N 15 1.283380058 0.050174226 . . . . . 53296 2 35 . 1 1 50 50 LYS N N 15 1.272633705 0.027661138 . . . . . 53296 2 36 . 1 1 51 51 GLY N N 15 1.268443361 0.019303677 . . . . . 53296 2 37 . 1 1 52 52 PHE N N 15 1.35223836 0.029240251 . . . . . 53296 2 38 . 1 1 54 54 ASP N N 15 1.342077512 0.030277342 . . . . . 53296 2 39 . 1 1 57 57 SER N N 15 1.324479653 0.027574594 . . . . . 53296 2 40 . 1 1 58 58 SER N N 15 1.288060511 0.029234989 . . . . . 53296 2 41 . 1 1 59 59 GLY N N 15 1.365668698 0.022354498 . . . . . 53296 2 42 . 1 1 61 61 SER N N 15 1.362700465 0.053008477 . . . . . 53296 2 43 . 1 1 62 62 SER N N 15 1.27600916 0.045166882 . . . . . 53296 2 44 . 1 1 63 63 SER N N 15 1.344531829 0.015643858 . . . . . 53296 2 45 . 1 1 64 64 LYS N N 15 1.295469885 0.022413961 . . . . . 53296 2 46 . 1 1 66 66 LYS N N 15 1.24398582 0.00960211 . . . . . 53296 2 47 . 1 1 68 68 ALA N N 15 1.330507708 0.051901067 . . . . . 53296 2 48 . 1 1 69 69 TYR N N 15 1.308212168 0.027826771 . . . . . 53296 2 49 . 1 1 70 70 SER N N 15 1.326102923 0.043058806 . . . . . 53296 2 50 . 1 1 71 71 SER N N 15 1.326470546 0.032084977 . . . . . 53296 2 51 . 1 1 73 73 GLY N N 15 1.341111245 0.033197378 . . . . . 53296 2 52 . 1 1 74 74 SER N N 15 1.296793598 0.045794898 . . . . . 53296 2 53 . 1 1 78 78 SER N N 15 1.323592141 0.025486094 . . . . . 53296 2 54 . 1 1 82 82 SER N N 15 1.303385891 0.018475484 . . . . . 53296 2 55 . 1 1 83 83 SER N N 15 1.385592474 0.038007734 . . . . . 53296 2 56 . 1 1 85 85 PHE N N 15 1.310457176 0.022312311 . . . . . 53296 2 57 . 1 1 86 86 SER N N 15 1.253041377 0.025384852 . . . . . 53296 2 58 . 1 1 88 88 ARG N N 15 1.382529731 0.03819908 . . . . . 53296 2 59 . 1 1 89 89 GLY N N 15 1.396431946 0.025503558 . . . . . 53296 2 60 . 1 1 90 90 SER N N 15 1.27450427 0.034670625 . . . . . 53296 2 61 . 1 1 91 91 GLY N N 15 1.407009795 0.033541756 . . . . . 53296 2 62 . 1 1 92 92 SER N N 15 1.396473704 0.029773587 . . . . . 53296 2 63 . 1 1 94 94 GLY N N 15 1.345278723 0.013232229 . . . . . 53296 2 64 . 1 1 95 95 ARG N N 15 1.317841539 0.030702626 . . . . . 53296 2 65 . 1 1 96 96 PHE N N 15 1.299350212 0.028240573 . . . . . 53296 2 66 . 1 1 97 97 ASP N N 15 1.333984346 0.041445994 . . . . . 53296 2 67 . 1 1 98 98 ASP N N 15 1.264108173 0.026105118 . . . . . 53296 2 68 . 1 1 100 100 GLY N N 15 1.316908322 0.011502712 . . . . . 53296 2 69 . 1 1 101 101 ARG N N 15 1.282630712 0.038468313 . . . . . 53296 2 70 . 1 1 102 102 SER N N 15 1.257711551 0.022799717 . . . . . 53296 2 71 . 1 1 104 104 TYR N N 15 1.255862317 0.035233402 . . . . . 53296 2 72 . 1 1 106 106 GLY N N 15 1.342748882 0.039120248 . . . . . 53296 2 73 . 1 1 107 107 ILE N N 15 1.30453405 0.011435018 . . . . . 53296 2 74 . 1 1 108 108 GLY N N 15 1.351425883 0.029229351 . . . . . 53296 2 75 . 1 1 109 109 SER N N 15 1.337787365 0.045743536 . . . . . 53296 2 76 . 1 1 113 113 ARG N N 15 1.339783596 0.020810922 . . . . . 53296 2 77 . 1 1 115 115 GLY N N 15 1.451001409 0.054031378 . . . . . 53296 2 78 . 1 1 116 116 PHE N N 15 1.408331649 0.015591518 . . . . . 53296 2 79 . 1 1 117 117 GLY N N 15 1.364584011 0.016354174 . . . . . 53296 2 80 . 1 1 118 118 LYS N N 15 1.372699554 0.015500275 . . . . . 53296 2 81 . 1 1 120 120 GLU N N 15 1.426150178 0.030013838 . . . . . 53296 2 82 . 1 1 121 121 ARG N N 15 1.41802956 0.017831493 . . . . . 53296 2 83 . 1 1 122 122 GLY N N 15 1.432311847 0.035418382 . . . . . 53296 2 84 . 1 1 123 123 GLY N N 15 1.445338968 0.031727859 . . . . . 53296 2 85 . 1 1 124 124 ASN N N 15 1.462430944 0.010052325 . . . . . 53296 2 86 . 1 1 125 125 SER N N 15 1.397440411 0.016459709 . . . . . 53296 2 87 . 1 1 128 128 CYS N N 15 1.499242016 0.018593833 . . . . . 53296 2 88 . 1 1 129 129 ASP N N 15 1.550813539 0.03225387 . . . . . 53296 2 89 . 1 1 131 131 SER N N 15 1.455302011 0.032433322 . . . . . 53296 2 90 . 1 1 132 132 ASP N N 15 1.229035241 0.027070403 . . . . . 53296 2 stop_ save_ save_heteronucl_T1_relaxation_3 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_3 _Heteronucl_T1_list.Entry_ID 53296 _Heteronucl_T1_list.ID 3 _Heteronucl_T1_list.Name 'HzNz u-2H,15N 100 uM' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 1000 _Heteronucl_T1_list.T1_coherence_type HzNz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 7 'T1/R1 relaxation HzNz' . . . 53296 3 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 53296 3 2 $software_2 . . 53296 3 3 $software_3 . . 53296 3 4 $software_4 . . 53296 3 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 HIS N N 15 16.97680146 0.570957275 . . . . . 53296 3 2 . 1 1 5 5 ALA N N 15 2.442466391 0.348253226 . . . . . 53296 3 3 . 1 1 7 7 GLU N N 15 2.179652873 0.192901357 . . . . . 53296 3 4 . 1 1 8 8 ASN N N 15 2.249940856 0.154626428 . . . . . 53296 3 5 . 1 1 9 9 ALA N N 15 1.965240348 0.204680211 . . . . . 53296 3 6 . 1 1 11 11 GLY N N 15 2.18092982 0.404308644 . . . . . 53296 3 7 . 1 1 12 12 LEU N N 15 2.018124756 0.235968897 . . . . . 53296 3 8 . 1 1 13 13 ASP N N 15 2.21100885 0.158726724 . . . . . 53296 3 9 . 1 1 17 17 ALA N N 15 2.188667295 0.17397453 . . . . . 53296 3 10 . 1 1 18 18 GLY N N 15 2.389066578 0.284514031 . . . . . 53296 3 11 . 1 1 20 20 ASP N N 15 2.095417536 0.20313423 . . . . . 53296 3 12 . 1 1 21 21 LEU N N 15 2.343991646 0.19287643 . . . . . 53296 3 13 . 1 1 22 22 ASN N N 15 2.549525744 0.32440098 . . . . . 53296 3 14 . 1 1 23 23 SER N N 15 3.496340958 0.221696575 . . . . . 53296 3 15 . 1 1 24 24 SER N N 15 3.735684073 0.285093544 . . . . . 53296 3 16 . 1 1 25 25 ASP N N 15 2.769647393 0.194382768 . . . . . 53296 3 17 . 1 1 26 26 ASN N N 15 2.935854913 0.26611774 . . . . . 53296 3 18 . 1 1 27 27 GLN N N 15 3.336039809 0.155652918 . . . . . 53296 3 19 . 1 1 29 29 GLY N N 15 3.308281461 0.232632828 . . . . . 53296 3 20 . 1 1 30 30 GLY N N 15 2.819170527 0.343621038 . . . . . 53296 3 21 . 1 1 31 31 SER N N 15 4.544143428 0.468179183 . . . . . 53296 3 22 . 1 1 32 32 THR N N 15 4.434162246 0.305147418 . . . . . 53296 3 23 . 1 1 33 33 ALA N N 15 3.375909075 0.396046309 . . . . . 53296 3 24 . 1 1 34 34 SER N N 15 3.501684592 0.17210799 . . . . . 53296 3 25 . 1 1 35 35 LYS N N 15 3.083350989 0.295148717 . . . . . 53296 3 26 . 1 1 36 36 GLY N N 15 3.664888646 0.260979103 . . . . . 53296 3 27 . 1 1 37 37 ARG N N 15 2.856757443 0.327238908 . . . . . 53296 3 28 . 1 1 38 38 TYR N N 15 1.947179134 0.227261889 . . . . . 53296 3 29 . 1 1 39 39 ILE N N 15 1.458511451 0.346434747 . . . . . 53296 3 30 . 1 1 43 43 LEU N N 15 3.199702441 0.987309344 . . . . . 53296 3 31 . 1 1 45 45 ASN N N 15 4.20126303 0.368285805 . . . . . 53296 3 32 . 1 1 47 47 GLU N N 15 2.56892199 0.277290509 . . . . . 53296 3 33 . 1 1 48 48 ALA N N 15 2.656762978 0.361268844 . . . . . 53296 3 34 . 1 1 49 49 THR N N 15 3.128161085 0.278537289 . . . . . 53296 3 35 . 1 1 50 50 LYS N N 15 3.252481179 0.255078006 . . . . . 53296 3 36 . 1 1 51 51 GLY N N 15 2.95007826 0.497349808 . . . . . 53296 3 37 . 1 1 52 52 PHE N N 15 2.944111788 0.467911704 . . . . . 53296 3 38 . 1 1 54 54 ASP N N 15 2.971477844 0.32032832 . . . . . 53296 3 39 . 1 1 57 57 SER N N 15 3.755340806 0.39987376 . . . . . 53296 3 40 . 1 1 58 58 SER N N 15 4.291334279 0.277154371 . . . . . 53296 3 41 . 1 1 59 59 GLY N N 15 3.564729349 0.46484416 . . . . . 53296 3 42 . 1 1 61 61 SER N N 15 3.815448774 0.433267902 . . . . . 53296 3 43 . 1 1 62 62 SER N N 15 4.212167705 0.10679249 . . . . . 53296 3 44 . 1 1 63 63 SER N N 15 4.914553917 0.405978513 . . . . . 53296 3 45 . 1 1 64 64 LYS N N 15 3.337007894 0.129940425 . . . . . 53296 3 46 . 1 1 66 66 LYS N N 15 2.872143791 0.346202543 . . . . . 53296 3 47 . 1 1 68 68 ALA N N 15 2.574585368 0.478619796 . . . . . 53296 3 48 . 1 1 69 69 TYR N N 15 3.202839123 0.209885894 . . . . . 53296 3 49 . 1 1 70 70 SER N N 15 3.265616193 0.267789335 . . . . . 53296 3 50 . 1 1 71 71 SER N N 15 4.773056893 0.370800215 . . . . . 53296 3 51 . 1 1 73 73 GLY N N 15 3.159542483 0.17729423 . . . . . 53296 3 52 . 1 1 74 74 SER N N 15 4.063554885 0.29525047 . . . . . 53296 3 53 . 1 1 78 78 SER N N 15 4.452207755 0.209082152 . . . . . 53296 3 54 . 1 1 82 82 SER N N 15 4.202380404 0.250559089 . . . . . 53296 3 55 . 1 1 83 83 SER N N 15 5.642013286 0.406581972 . . . . . 53296 3 56 . 1 1 85 85 PHE N N 15 3.133915281 0.23896418 . . . . . 53296 3 57 . 1 1 86 86 SER N N 15 3.181386522 0.243732396 . . . . . 53296 3 58 . 1 1 88 88 ARG N N 15 3.539437379 0.421175922 . . . . . 53296 3 59 . 1 1 89 89 GLY N N 15 3.788699758 0.247832772 . . . . . 53296 3 60 . 1 1 90 90 SER N N 15 4.472755281 0.190423738 . . . . . 53296 3 61 . 1 1 91 91 GLY N N 15 3.904834578 0.227067319 . . . . . 53296 3 62 . 1 1 92 92 SER N N 15 4.380401139 0.298326818 . . . . . 53296 3 63 . 1 1 94 94 GLY N N 15 3.852041295 0.281074236 . . . . . 53296 3 64 . 1 1 95 95 ARG N N 15 2.695882453 0.256484871 . . . . . 53296 3 65 . 1 1 96 96 PHE N N 15 2.920480375 0.195233448 . . . . . 53296 3 66 . 1 1 97 97 ASP N N 15 2.508371746 0.360041769 . . . . . 53296 3 67 . 1 1 98 98 ASP N N 15 2.74008999 0.286045698 . . . . . 53296 3 68 . 1 1 100 100 GLY N N 15 3.116474626 0.549207229 . . . . . 53296 3 69 . 1 1 101 101 ARG N N 15 2.721419658 0.381765312 . . . . . 53296 3 70 . 1 1 102 102 SER N N 15 3.702323692 0.389677232 . . . . . 53296 3 71 . 1 1 104 104 TYR N N 15 2.635930899 0.359845444 . . . . . 53296 3 72 . 1 1 106 106 GLY N N 15 2.164540985 0.683378353 . . . . . 53296 3 73 . 1 1 107 107 ILE N N 15 2.976420997 0.44708623 . . . . . 53296 3 74 . 1 1 108 108 GLY N N 15 2.583686199 0.190403176 . . . . . 53296 3 75 . 1 1 109 109 SER N N 15 3.567718372 0.256691192 . . . . . 53296 3 76 . 1 1 113 113 ARG N N 15 3.276471919 0.297219783 . . . . . 53296 3 77 . 1 1 115 115 GLY N N 15 3.926301517 0.326215266 . . . . . 53296 3 78 . 1 1 116 116 PHE N N 15 2.311983045 0.282123564 . . . . . 53296 3 79 . 1 1 117 117 GLY N N 15 3.015813416 0.314070913 . . . . . 53296 3 80 . 1 1 118 118 LYS N N 15 3.142929416 0.406714135 . . . . . 53296 3 81 . 1 1 120 120 GLU N N 15 2.865157986 0.199175602 . . . . . 53296 3 82 . 1 1 121 121 ARG N N 15 2.800661896 0.354393237 . . . . . 53296 3 83 . 1 1 122 122 GLY N N 15 3.26626771 0.312258839 . . . . . 53296 3 84 . 1 1 123 123 GLY N N 15 3.333463044 0.549897826 . . . . . 53296 3 85 . 1 1 124 124 ASN N N 15 4.308829427 0.396764066 . . . . . 53296 3 86 . 1 1 125 125 SER N N 15 4.23543315 0.372737897 . . . . . 53296 3 87 . 1 1 128 128 CYS N N 15 2.814627246 0.156183123 . . . . . 53296 3 88 . 1 1 129 129 ASP N N 15 2.554329558 0.351561304 . . . . . 53296 3 89 . 1 1 131 131 SER N N 15 2.641186708 0.289583956 . . . . . 53296 3 90 . 1 1 132 132 ASP N N 15 1.483445716 0.321405591 . . . . . 53296 3 stop_ save_ save_heteronucl_T1_relaxation_4 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_4 _Heteronucl_T1_list.Entry_ID 53296 _Heteronucl_T1_list.ID 4 _Heteronucl_T1_list.Name '15N R1 u-2H,15N 300 uM' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 1000 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 16 'T1/R1 relaxation' . . . 53296 4 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 53296 4 2 $software_2 . . 53296 4 3 $software_3 . . 53296 4 4 $software_4 . . 53296 4 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 HIS N N 15 1.321546947 0.020433307 . . . . . 53296 4 2 . 1 1 5 5 ALA N N 15 1.493239544 0.019822109 . . . . . 53296 4 3 . 1 1 7 7 GLU N N 15 1.502159806 0.01860477 . . . . . 53296 4 4 . 1 1 8 8 ASN N N 15 1.480314431 0.011882141 . . . . . 53296 4 5 . 1 1 9 9 ALA N N 15 1.42405763 0.013502066 . . . . . 53296 4 6 . 1 1 11 11 GLY N N 15 1.466669753 0.025343096 . . . . . 53296 4 7 . 1 1 12 12 LEU N N 15 1.463931521 0.018242623 . . . . . 53296 4 8 . 1 1 13 13 ASP N N 15 1.451877548 0.015293443 . . . . . 53296 4 9 . 1 1 17 17 ALA N N 15 1.441972116 0.018191885 . . . . . 53296 4 10 . 1 1 18 18 GLY N N 15 1.361566904 0.024389803 . . . . . 53296 4 11 . 1 1 20 20 ASP N N 15 1.408933945 0.019118594 . . . . . 53296 4 12 . 1 1 21 21 LEU N N 15 1.414055798 0.011637089 . . . . . 53296 4 13 . 1 1 22 22 ASN N N 15 1.470680664 0.010139154 . . . . . 53296 4 14 . 1 1 23 23 SER N N 15 1.407603364 0.018734505 . . . . . 53296 4 15 . 1 1 24 24 SER N N 15 1.480380925 0.01011732 . . . . . 53296 4 16 . 1 1 25 25 ASP N N 15 1.502985439 0.015178619 . . . . . 53296 4 17 . 1 1 26 26 ASN N N 15 1.456170498 0.022871909 . . . . . 53296 4 18 . 1 1 27 27 GLN N N 15 1.488593947 0.007792171 . . . . . 53296 4 19 . 1 1 29 29 GLY N N 15 1.462992729 0.033573472 . . . . . 53296 4 20 . 1 1 30 30 GLY N N 15 1.46584868 0.010416189 . . . . . 53296 4 21 . 1 1 31 31 SER N N 15 1.428967108 0.005910206 . . . . . 53296 4 22 . 1 1 32 32 THR N N 15 1.463901386 0.008896314 . . . . . 53296 4 23 . 1 1 33 33 ALA N N 15 1.509397671 0.014936221 . . . . . 53296 4 24 . 1 1 34 34 SER N N 15 1.387399423 0.034259771 . . . . . 53296 4 25 . 1 1 35 35 LYS N N 15 1.428729812 0.014534391 . . . . . 53296 4 26 . 1 1 36 36 GLY N N 15 1.389665322 0.014770339 . . . . . 53296 4 27 . 1 1 37 37 ARG N N 15 1.318512622 0.021926864 . . . . . 53296 4 28 . 1 1 38 38 TYR N N 15 1.230524798 0.020614416 . . . . . 53296 4 29 . 1 1 39 39 ILE N N 15 1.259782881 0.02279483 . . . . . 53296 4 30 . 1 1 43 43 LEU N N 15 1.215608007 0.035806981 . . . . . 53296 4 31 . 1 1 45 45 ASN N N 15 1.253455882 0.014234341 . . . . . 53296 4 32 . 1 1 47 47 GLU N N 15 1.28643773 0.015488161 . . . . . 53296 4 33 . 1 1 48 48 ALA N N 15 1.27536047 0.015768891 . . . . . 53296 4 34 . 1 1 49 49 THR N N 15 1.250692849 0.016068662 . . . . . 53296 4 35 . 1 1 50 50 LYS N N 15 1.267902208 0.011685402 . . . . . 53296 4 36 . 1 1 51 51 GLY N N 15 1.275582559 0.004262409 . . . . . 53296 4 37 . 1 1 52 52 PHE N N 15 1.273659735 0.014634204 . . . . . 53296 4 38 . 1 1 54 54 ASP N N 15 1.288344312 0.018222777 . . . . . 53296 4 39 . 1 1 57 57 SER N N 15 1.243325417 0.014346871 . . . . . 53296 4 40 . 1 1 58 58 SER N N 15 1.326461643 0.030208611 . . . . . 53296 4 41 . 1 1 59 59 GLY N N 15 1.297234148 0.009327535 . . . . . 53296 4 42 . 1 1 61 61 SER N N 15 1.268489019 0.014677286 . . . . . 53296 4 43 . 1 1 62 62 SER N N 15 1.289399307 0.018279177 . . . . . 53296 4 44 . 1 1 63 63 SER N N 15 1.286399099 0.024370039 . . . . . 53296 4 45 . 1 1 64 64 LYS N N 15 1.305170688 0.007714993 . . . . . 53296 4 46 . 1 1 66 66 LYS N N 15 1.243915672 0.029568854 . . . . . 53296 4 47 . 1 1 68 68 ALA N N 15 1.241728387 0.00482931 . . . . . 53296 4 48 . 1 1 69 69 TYR N N 15 1.263615279 0.015209294 . . . . . 53296 4 49 . 1 1 70 70 SER N N 15 1.280963797 0.015879291 . . . . . 53296 4 50 . 1 1 71 71 SER N N 15 1.291420252 0.017558097 . . . . . 53296 4 51 . 1 1 73 73 GLY N N 15 1.316159269 0.014481308 . . . . . 53296 4 52 . 1 1 74 74 SER N N 15 1.34785512 0.015768192 . . . . . 53296 4 53 . 1 1 78 78 SER N N 15 1.317246911 0.01414918 . . . . . 53296 4 54 . 1 1 82 82 SER N N 15 1.301391095 0.010989517 . . . . . 53296 4 55 . 1 1 83 83 SER N N 15 1.315324992 0.020309468 . . . . . 53296 4 56 . 1 1 85 85 PHE N N 15 1.2746473 0.02529242 . . . . . 53296 4 57 . 1 1 86 86 SER N N 15 1.265290892 0.011270687 . . . . . 53296 4 58 . 1 1 88 88 ARG N N 15 1.274925173 0.026192916 . . . . . 53296 4 59 . 1 1 89 89 GLY N N 15 1.361373764 0.015000995 . . . . . 53296 4 60 . 1 1 90 90 SER N N 15 1.313400715 0.00993852 . . . . . 53296 4 61 . 1 1 91 91 GLY N N 15 1.357304876 0.016439239 . . . . . 53296 4 62 . 1 1 92 92 SER N N 15 1.356101585 0.019086538 . . . . . 53296 4 63 . 1 1 94 94 GLY N N 15 1.288174218 0.017537406 . . . . . 53296 4 64 . 1 1 95 95 ARG N N 15 1.232325409 0.012971778 . . . . . 53296 4 65 . 1 1 96 96 PHE N N 15 1.242263169 0.005116854 . . . . . 53296 4 66 . 1 1 97 97 ASP N N 15 1.213396926 0.008611549 . . . . . 53296 4 67 . 1 1 98 98 ASP N N 15 1.202151128 0.014585128 . . . . . 53296 4 68 . 1 1 100 100 GLY N N 15 1.23603692 0.012145255 . . . . . 53296 4 69 . 1 1 101 101 ARG N N 15 1.199278273 0.01637325 . . . . . 53296 4 70 . 1 1 102 102 SER N N 15 1.225803743 0.015006366 . . . . . 53296 4 71 . 1 1 104 104 TYR N N 15 1.193841563 0.021041066 . . . . . 53296 4 72 . 1 1 106 106 GLY N N 15 1.326344596 0.038918914 . . . . . 53296 4 73 . 1 1 107 107 ILE N N 15 1.281671377 0.008599596 . . . . . 53296 4 74 . 1 1 108 108 GLY N N 15 1.307885751 0.020734426 . . . . . 53296 4 75 . 1 1 109 109 SER N N 15 1.263710188 0.020229076 . . . . . 53296 4 76 . 1 1 113 113 ARG N N 15 1.287891775 0.003670668 . . . . . 53296 4 77 . 1 1 115 115 GLY N N 15 1.341816649 0.028676658 . . . . . 53296 4 78 . 1 1 116 116 PHE N N 15 1.362984488 0.01706216 . . . . . 53296 4 79 . 1 1 117 117 GLY N N 15 1.301511099 0.026824536 . . . . . 53296 4 80 . 1 1 118 118 LYS N N 15 1.35105096 0.027327185 . . . . . 53296 4 81 . 1 1 120 120 GLU N N 15 1.347135856 0.009295862 . . . . . 53296 4 82 . 1 1 121 121 ARG N N 15 1.367078732 0.009826516 . . . . . 53296 4 83 . 1 1 122 122 GLY N N 15 1.366710627 0.014533624 . . . . . 53296 4 84 . 1 1 123 123 GLY N N 15 1.417093251 0.017052859 . . . . . 53296 4 85 . 1 1 124 124 ASN N N 15 1.422140951 0.015898992 . . . . . 53296 4 86 . 1 1 125 125 SER N N 15 1.414446663 0.025986567 . . . . . 53296 4 87 . 1 1 128 128 CYS N N 15 1.475659998 0.0153245 . . . . . 53296 4 88 . 1 1 129 129 ASP N N 15 1.470926818 0.01630061 . . . . . 53296 4 89 . 1 1 131 131 SER N N 15 1.428856289 0.009694789 . . . . . 53296 4 90 . 1 1 132 132 ASP N N 15 1.245500746 0.009537967 . . . . . 53296 4 stop_ save_ save_heteronucl_T1_relaxation_5 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_5 _Heteronucl_T1_list.Entry_ID 53296 _Heteronucl_T1_list.ID 5 _Heteronucl_T1_list.Name 'HzNz u-2H,15N 300 uM' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 1000 _Heteronucl_T1_list.T1_coherence_type HzNz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 14 'T1/R1 relaxation HzNz' . . . 53296 5 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 53296 5 2 $software_2 . . 53296 5 3 $software_3 . . 53296 5 4 $software_4 . . 53296 5 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 HIS N N 15 16.86208413 0.217095219 . . . . . 53296 5 2 . 1 1 5 5 ALA N N 15 2.107288591 0.207233253 . . . . . 53296 5 3 . 1 1 7 7 GLU N N 15 1.928400661 0.111489834 . . . . . 53296 5 4 . 1 1 8 8 ASN N N 15 2.572701278 0.175204322 . . . . . 53296 5 5 . 1 1 9 9 ALA N N 15 2.506775576 0.1251554 1 . 1 1 . 53296 5 6 . 1 1 11 11 GLY N N 15 2.029093319 0.175353165 . . . . . 53296 5 7 . 1 1 12 12 LEU N N 15 2.180463871 0.233860882 . . . . . 53296 5 8 . 1 1 13 13 ASP N N 15 2.394500603 0.174258212 . . . . . 53296 5 9 . 1 1 17 17 ALA N N 15 2.496567734 0.210750622 . . . . . 53296 5 10 . 1 1 18 18 GLY N N 15 2.393110288 0.221500107 . . . . . 53296 5 11 . 1 1 20 20 ASP N N 15 2.081531173 0.089228434 . . . . . 53296 5 12 . 1 1 21 21 LEU N N 15 2.358809988 0.068050806 . . . . . 53296 5 13 . 1 1 22 22 ASN N N 15 2.876567127 0.1163001 1 . 1 1 . 53296 5 14 . 1 1 23 23 SER N N 15 3.361581342 0.303292611 . . . . . 53296 5 15 . 1 1 24 24 SER N N 15 3.727852479 0.141579148 . . . . . 53296 5 16 . 1 1 25 25 ASP N N 15 3.012231582 0.092183822 . . . . . 53296 5 17 . 1 1 26 26 ASN N N 15 3.006693887 0.238207834 . . . . . 53296 5 18 . 1 1 27 27 GLN N N 15 3.206198469 0.21339156 . . . . . 53296 5 19 . 1 1 29 29 GLY N N 15 3.229270548 0.345946717 . . . . . 53296 5 20 . 1 1 30 30 GLY N N 15 3.046575188 0.177518033 . . . . . 53296 5 21 . 1 1 31 31 SER N N 15 4.542955469 0.148199991 . . . . . 53296 5 22 . 1 1 32 32 THR N N 15 4.718214746 0.261964319 . . . . . 53296 5 23 . 1 1 33 33 ALA N N 15 3.103900212 0.210114589 . . . . . 53296 5 24 . 1 1 34 34 SER N N 15 3.793457504 0.214068049 . . . . . 53296 5 25 . 1 1 35 35 LYS N N 15 3.393058475 0.287147626 . . . . . 53296 5 26 . 1 1 36 36 GLY N N 15 3.128797522 0.306932576 . . . . . 53296 5 27 . 1 1 37 37 ARG N N 15 2.468216719 0.343737716 . . . . . 53296 5 28 . 1 1 38 38 TYR N N 15 2.156098665 0.100619584 . . . . . 53296 5 29 . 1 1 39 39 ILE N N 15 1.684513525 0.188865406 . . . . . 53296 5 30 . 1 1 43 43 LEU N N 15 3.622991072 0.560783023 . . . . . 53296 5 31 . 1 1 45 45 ASN N N 15 3.862610163 0.140177913 . . . . . 53296 5 32 . 1 1 47 47 GLU N N 15 2.721560229 0.191487847 . . . . . 53296 5 33 . 1 1 48 48 ALA N N 15 2.645832084 0.236878289 . . . . . 53296 5 34 . 1 1 49 49 THR N N 15 3.137837839 0.144764184 . . . . . 53296 5 35 . 1 1 50 50 LYS N N 15 2.773711578 0.262847691 . . . . . 53296 5 36 . 1 1 51 51 GLY N N 15 3.086751943 0.222922574 . . . . . 53296 5 37 . 1 1 52 52 PHE N N 15 2.854749791 0.301916644 . . . . . 53296 5 38 . 1 1 54 54 ASP N N 15 2.806262103 0.205199311 . . . . . 53296 5 39 . 1 1 57 57 SER N N 15 4.155150331 0.301326565 . . . . . 53296 5 40 . 1 1 58 58 SER N N 15 4.485712069 0.294412312 . . . . . 53296 5 41 . 1 1 59 59 GLY N N 15 4.210725674 0.231476537 . . . . . 53296 5 42 . 1 1 61 61 SER N N 15 3.813515995 0.114236828 . . . . . 53296 5 43 . 1 1 62 62 SER N N 15 4.625446129 0.115255891 . . . . . 53296 5 44 . 1 1 63 63 SER N N 15 5.700971955 0.280448331 . . . . . 53296 5 45 . 1 1 64 64 LYS N N 15 3.591966158 0.174975493 . . . . . 53296 5 46 . 1 1 66 66 LYS N N 15 2.528325933 0.45152076 . . . . . 53296 5 47 . 1 1 68 68 ALA N N 15 2.940529871 0.163752916 . . . . . 53296 5 48 . 1 1 69 69 TYR N N 15 2.749919139 0.139358808 . . . . . 53296 5 49 . 1 1 70 70 SER N N 15 3.466390148 0.321971711 . . . . . 53296 5 50 . 1 1 71 71 SER N N 15 5.055889618 0.148763233 . . . . . 53296 5 51 . 1 1 73 73 GLY N N 15 3.330155171 0.275816149 . . . . . 53296 5 52 . 1 1 74 74 SER N N 15 4.111765492 0.18066861 . . . . . 53296 5 53 . 1 1 78 78 SER N N 15 4.163585553 0.186167342 . . . . . 53296 5 54 . 1 1 82 82 SER N N 15 4.417138697 0.238721061 . . . . . 53296 5 55 . 1 1 83 83 SER N N 15 5.167994935 0.22725274 . . . . . 53296 5 56 . 1 1 85 85 PHE N N 15 3.020836058 0.060180265 . . . . . 53296 5 57 . 1 1 86 86 SER N N 15 3.406169485 0.231028514 . . . . . 53296 5 58 . 1 1 88 88 ARG N N 15 2.952324034 0.409551761 . . . . . 53296 5 59 . 1 1 89 89 GLY N N 15 3.578336907 0.331920058 . . . . . 53296 5 60 . 1 1 90 90 SER N N 15 4.685277649 0.268629002 . . . . . 53296 5 61 . 1 1 91 91 GLY N N 15 4.474551791 0.117759117 . . . . . 53296 5 62 . 1 1 92 92 SER N N 15 4.401400403 0.210453259 . . . . . 53296 5 63 . 1 1 94 94 GLY N N 15 3.268657165 0.369859875 . . . . . 53296 5 64 . 1 1 95 95 ARG N N 15 2.701621799 0.14885064 . . . . . 53296 5 65 . 1 1 96 96 PHE N N 15 3.042270882 0.203262768 . . . . . 53296 5 66 . 1 1 97 97 ASP N N 15 3.056037043 0.148121616 . . . . . 53296 5 67 . 1 1 98 98 ASP N N 15 2.749573764 0.16011568 . . . . . 53296 5 68 . 1 1 100 100 GLY N N 15 3.316478235 0.280129891 . . . . . 53296 5 69 . 1 1 101 101 ARG N N 15 2.574171522 0.284583548 . . . . . 53296 5 70 . 1 1 102 102 SER N N 15 4.033623496 0.081837416 . . . . . 53296 5 71 . 1 1 104 104 TYR N N 15 2.703586327 0.254247179 . . . . . 53296 5 72 . 1 1 106 106 GLY N N 15 2.607737778 0.561555739 . . . . . 53296 5 73 . 1 1 107 107 ILE N N 15 2.361221626 0.312854145 . . . . . 53296 5 74 . 1 1 108 108 GLY N N 15 2.814656604 0.156078261 . . . . . 53296 5 75 . 1 1 109 109 SER N N 15 3.707540763 0.242678611 . . . . . 53296 5 76 . 1 1 113 113 ARG N N 15 3.231310491 0.216666992 . . . . . 53296 5 77 . 1 1 115 115 GLY N N 15 3.681919458 0.132771393 . . . . . 53296 5 78 . 1 1 116 116 PHE N N 15 2.945493919 0.159648163 . . . . . 53296 5 79 . 1 1 117 117 GLY N N 15 3.710639436 0.3811932 1 . 1 1 . 53296 5 80 . 1 1 118 118 LYS N N 15 2.609921393 0.092157409 . . . . . 53296 5 81 . 1 1 120 120 GLU N N 15 2.613259674 0.145838863 . . . . . 53296 5 82 . 1 1 121 121 ARG N N 15 2.844795484 0.183800984 . . . . . 53296 5 83 . 1 1 122 122 GLY N N 15 3.714878869 0.23260969 . . . . . 53296 5 84 . 1 1 123 123 GLY N N 15 3.055976531 0.245148108 . . . . . 53296 5 85 . 1 1 124 124 ASN N N 15 4.642806614 0.215942644 . . . . . 53296 5 86 . 1 1 125 125 SER N N 15 4.289202511 0.218881985 . . . . . 53296 5 87 . 1 1 128 128 CYS N N 15 2.798102086 0.22922374 . . . . . 53296 5 88 . 1 1 129 129 ASP N N 15 2.853043542 0.15981468 . . . . . 53296 5 89 . 1 1 131 131 SER N N 15 2.696289769 0.12597822 . . . . . 53296 5 90 . 1 1 132 132 ASP N N 15 1.475844194 0.179502637 . . . . . 53296 5 stop_ save_ save_heteronucl_T1_relaxation_6 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_6 _Heteronucl_T1_list.Entry_ID 53296 _Heteronucl_T1_list.ID 6 _Heteronucl_T1_list.Name '15N R1 u-2H,15N 500 uM' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 1000 _Heteronucl_T1_list.T1_coherence_type Nz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 23 'T1/R1 relaxation' . . . 53296 6 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 53296 6 2 $software_2 . . 53296 6 3 $software_3 . . 53296 6 4 $software_4 . . 53296 6 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 HIS N N 15 1.316448943 0.024071858 . . . . . 53296 6 2 . 1 1 5 5 ALA N N 15 1.488823227 0.015750228 . . . . . 53296 6 3 . 1 1 7 7 GLU N N 15 1.522358662 0.012067613 . . . . . 53296 6 4 . 1 1 8 8 ASN N N 15 1.473142854 0.010062429 . . . . . 53296 6 5 . 1 1 9 9 ALA N N 15 1.445323511 0.007300528 . . . . . 53296 6 6 . 1 1 11 11 GLY N N 15 1.437423414 0.010847446 . . . . . 53296 6 7 . 1 1 12 12 LEU N N 15 1.461342144 0.010903137 . . . . . 53296 6 8 . 1 1 13 13 ASP N N 15 1.46321804 0.016368763 . . . . . 53296 6 9 . 1 1 17 17 ALA N N 15 1.412598486 0.004876529 . . . . . 53296 6 10 . 1 1 18 18 GLY N N 15 1.323036591 0.016433465 . . . . . 53296 6 11 . 1 1 20 20 ASP N N 15 1.380732637 0.00903231 . . . . . 53296 6 12 . 1 1 21 21 LEU N N 15 1.383308788 0.00568507 . . . . . 53296 6 13 . 1 1 22 22 ASN N N 15 1.42707685 0.010409194 . . . . . 53296 6 14 . 1 1 23 23 SER N N 15 1.396960197 0.017556057 . . . . . 53296 6 15 . 1 1 24 24 SER N N 15 1.494678593 0.005586913 . . . . . 53296 6 16 . 1 1 25 25 ASP N N 15 1.525257977 0.006557524 . . . . . 53296 6 17 . 1 1 26 26 ASN N N 15 1.487712819 0.011696489 . . . . . 53296 6 18 . 1 1 27 27 GLN N N 15 1.468968811 0.009199096 . . . . . 53296 6 19 . 1 1 29 29 GLY N N 15 1.470693397 0.013337443 . . . . . 53296 6 20 . 1 1 30 30 GLY N N 15 1.430455247 0.008971129 . . . . . 53296 6 21 . 1 1 31 31 SER N N 15 1.413120699 0.006112351 . . . . . 53296 6 22 . 1 1 32 32 THR N N 15 1.447209754 0.010278809 . . . . . 53296 6 23 . 1 1 33 33 ALA N N 15 1.503158541 0.010053863 . . . . . 53296 6 24 . 1 1 34 34 SER N N 15 1.35543786 0.011412085 . . . . . 53296 6 25 . 1 1 35 35 LYS N N 15 1.382990503 0.007105467 . . . . . 53296 6 26 . 1 1 36 36 GLY N N 15 1.357889138 0.007000567 . . . . . 53296 6 27 . 1 1 37 37 ARG N N 15 1.30976454 0.020526643 . . . . . 53296 6 28 . 1 1 38 38 TYR N N 15 1.230148584 0.005730106 . . . . . 53296 6 29 . 1 1 39 39 ILE N N 15 1.209634673 0.012343869 . . . . . 53296 6 30 . 1 1 43 43 LEU N N 15 1.233361699 0.012744168 . . . . . 53296 6 31 . 1 1 45 45 ASN N N 15 1.182485457 0.011150864 . . . . . 53296 6 32 . 1 1 47 47 GLU N N 15 1.251935599 0.014087505 . . . . . 53296 6 33 . 1 1 48 48 ALA N N 15 1.229237921 0.01660188 . . . . . 53296 6 34 . 1 1 49 49 THR N N 15 1.189524728 0.0135351 1 . 1 1 . 53296 6 35 . 1 1 50 50 LYS N N 15 1.257210256 0.008117666 . . . . . 53296 6 36 . 1 1 51 51 GLY N N 15 1.253951278 0.009372753 . . . . . 53296 6 37 . 1 1 52 52 PHE N N 15 1.250883335 0.010511435 . . . . . 53296 6 38 . 1 1 54 54 ASP N N 15 1.251584542 0.014082101 . . . . . 53296 6 39 . 1 1 57 57 SER N N 15 1.223591118 0.018958555 . . . . . 53296 6 40 . 1 1 58 58 SER N N 15 1.295102058 0.024790744 . . . . . 53296 6 41 . 1 1 59 59 GLY N N 15 1.317288069 0.019893481 . . . . . 53296 6 42 . 1 1 61 61 SER N N 15 1.248447041 0.014045784 . . . . . 53296 6 43 . 1 1 62 62 SER N N 15 1.242073752 0.011806818 . . . . . 53296 6 44 . 1 1 63 63 SER N N 15 1.315538286 0.010544858 . . . . . 53296 6 45 . 1 1 64 64 LYS N N 15 1.29535992 0.014730426 . . . . . 53296 6 46 . 1 1 66 66 LYS N N 15 1.190086132 0.018774859 . . . . . 53296 6 47 . 1 1 68 68 ALA N N 15 1.232739078 0.012508245 . . . . . 53296 6 48 . 1 1 69 69 TYR N N 15 1.208232018 0.005407089 . . . . . 53296 6 49 . 1 1 70 70 SER N N 15 1.264438637 0.015574259 . . . . . 53296 6 50 . 1 1 71 71 SER N N 15 1.317663372 0.00906813 . . . . . 53296 6 51 . 1 1 73 73 GLY N N 15 1.288788118 0.011538814 . . . . . 53296 6 52 . 1 1 74 74 SER N N 15 1.279795082 0.015185451 . . . . . 53296 6 53 . 1 1 78 78 SER N N 15 1.291544135 0.011520541 . . . . . 53296 6 54 . 1 1 82 82 SER N N 15 1.270269895 0.008853879 . . . . . 53296 6 55 . 1 1 83 83 SER N N 15 1.296177565 0.008701987 . . . . . 53296 6 56 . 1 1 85 85 PHE N N 15 1.222286124 0.011400955 . . . . . 53296 6 57 . 1 1 86 86 SER N N 15 1.253767367 0.007467764 . . . . . 53296 6 58 . 1 1 88 88 ARG N N 15 1.272472349 0.011648616 . . . . . 53296 6 59 . 1 1 89 89 GLY N N 15 1.300062535 0.013852303 . . . . . 53296 6 60 . 1 1 90 90 SER N N 15 1.285973112 0.004992795 . . . . . 53296 6 61 . 1 1 91 91 GLY N N 15 1.347318798 0.016224326 . . . . . 53296 6 62 . 1 1 92 92 SER N N 15 1.314232894 0.020644915 . . . . . 53296 6 63 . 1 1 94 94 GLY N N 15 1.303927504 0.012888004 . . . . . 53296 6 64 . 1 1 95 95 ARG N N 15 1.243659878 0.007285307 . . . . . 53296 6 65 . 1 1 96 96 PHE N N 15 1.213136265 0.012408791 . . . . . 53296 6 66 . 1 1 97 97 ASP N N 15 1.197000583 0.027234164 . . . . . 53296 6 67 . 1 1 98 98 ASP N N 15 1.17395752 0.009086232 . . . . . 53296 6 68 . 1 1 100 100 GLY N N 15 1.210284355 0.006656832 . . . . . 53296 6 69 . 1 1 101 101 ARG N N 15 1.245875912 0.011733643 . . . . . 53296 6 70 . 1 1 102 102 SER N N 15 1.207630283 0.015154795 . . . . . 53296 6 71 . 1 1 104 104 TYR N N 15 1.202112621 0.009613352 . . . . . 53296 6 72 . 1 1 106 106 GLY N N 15 1.233238075 0.017659967 . . . . . 53296 6 73 . 1 1 107 107 ILE N N 15 1.237873416 0.014588714 . . . . . 53296 6 74 . 1 1 108 108 GLY N N 15 1.270064846 0.008046949 . . . . . 53296 6 75 . 1 1 109 109 SER N N 15 1.265658807 0.01570393 . . . . . 53296 6 76 . 1 1 113 113 ARG N N 15 1.280784994 0.006302667 . . . . . 53296 6 77 . 1 1 115 115 GLY N N 15 1.314009886 0.029731146 . . . . . 53296 6 78 . 1 1 116 116 PHE N N 15 1.295949922 0.008555537 . . . . . 53296 6 79 . 1 1 117 117 GLY N N 15 1.329092162 0.017086677 . . . . . 53296 6 80 . 1 1 118 118 LYS N N 15 1.302970319 0.014111429 . . . . . 53296 6 81 . 1 1 120 120 GLU N N 15 1.316258068 0.011297825 . . . . . 53296 6 82 . 1 1 121 121 ARG N N 15 1.351306822 0.020568925 . . . . . 53296 6 83 . 1 1 122 122 GLY N N 15 1.376735247 0.008192411 . . . . . 53296 6 84 . 1 1 123 123 GLY N N 15 1.381993357 0.014185197 . . . . . 53296 6 85 . 1 1 124 124 ASN N N 15 1.371125436 0.01577598 . . . . . 53296 6 86 . 1 1 125 125 SER N N 15 1.369982259 0.008888851 . . . . . 53296 6 87 . 1 1 128 128 CYS N N 15 1.39186345 0.010112655 . . . . . 53296 6 88 . 1 1 129 129 ASP N N 15 1.4599968 0.007942934 . . . . . 53296 6 89 . 1 1 131 131 SER N N 15 1.384719997 0.015035759 . . . . . 53296 6 90 . 1 1 132 132 ASP N N 15 1.254942932 0.008905783 . . . . . 53296 6 stop_ save_ save_heteronucl_T1_relaxation_7 _Heteronucl_T1_list.Sf_category heteronucl_T1_relaxation _Heteronucl_T1_list.Sf_framecode heteronucl_T1_relaxation_7 _Heteronucl_T1_list.Entry_ID 53296 _Heteronucl_T1_list.ID 7 _Heteronucl_T1_list.Name 'HzNz u-2H,15N 500 uM' _Heteronucl_T1_list.Sample_condition_list_ID 1 _Heteronucl_T1_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T1_list.Spectrometer_frequency_1H 1000 _Heteronucl_T1_list.T1_coherence_type HzNz _Heteronucl_T1_list.T1_val_units s-1 _Heteronucl_T1_list.Details . _Heteronucl_T1_list.Text_data_format . _Heteronucl_T1_list.Text_data . loop_ _Heteronucl_T1_experiment.Experiment_ID _Heteronucl_T1_experiment.Experiment_name _Heteronucl_T1_experiment.Sample_ID _Heteronucl_T1_experiment.Sample_label _Heteronucl_T1_experiment.Sample_state _Heteronucl_T1_experiment.Entry_ID _Heteronucl_T1_experiment.Heteronucl_T1_list_ID 21 'T1/R1 relaxation HzNz' . . . 53296 7 stop_ loop_ _Heteronucl_T1_software.Software_ID _Heteronucl_T1_software.Software_label _Heteronucl_T1_software.Method_ID _Heteronucl_T1_software.Method_label _Heteronucl_T1_software.Entry_ID _Heteronucl_T1_software.Heteronucl_T1_list_ID 1 $software_1 . . 53296 7 2 $software_2 . . 53296 7 3 $software_3 . . 53296 7 4 $software_4 . . 53296 7 stop_ loop_ _T1.ID _T1.Assembly_atom_ID _T1.Entity_assembly_ID _T1.Entity_ID _T1.Comp_index_ID _T1.Seq_ID _T1.Comp_ID _T1.Atom_ID _T1.Atom_type _T1.Atom_isotope_number _T1.Val _T1.Val_err _T1.Resonance_ID _T1.Auth_entity_assembly_ID _T1.Auth_seq_ID _T1.Auth_comp_ID _T1.Auth_atom_ID _T1.Entry_ID _T1.Heteronucl_T1_list_ID 1 . 1 1 3 3 HIS N N 15 17.0966 0.125606981 . . . . . 53296 7 2 . 1 1 5 5 ALA N N 15 2.218851445 0.177311542 . . . . . 53296 7 3 . 1 1 7 7 GLU N N 15 2.127545059 0.109336688 . . . . . 53296 7 4 . 1 1 8 8 ASN N N 15 2.674233732 0.048709607 . . . . . 53296 7 5 . 1 1 9 9 ALA N N 15 2.612325192 0.098271076 . . . . . 53296 7 6 . 1 1 11 11 GLY N N 15 2.194433058 0.185929178 . . . . . 53296 7 7 . 1 1 12 12 LEU N N 15 2.352757151 0.127369976 . . . . . 53296 7 8 . 1 1 13 13 ASP N N 15 2.40467903 0.158215561 . . . . . 53296 7 9 . 1 1 17 17 ALA N N 15 2.499046514 0.084390443 . . . . . 53296 7 10 . 1 1 18 18 GLY N N 15 2.390435358 0.137539627 . . . . . 53296 7 11 . 1 1 20 20 ASP N N 15 2.372263643 0.093781662 . . . . . 53296 7 12 . 1 1 21 21 LEU N N 15 2.446080241 0.131014402 . . . . . 53296 7 13 . 1 1 22 22 ASN N N 15 2.821353007 0.097658966 . . . . . 53296 7 14 . 1 1 23 23 SER N N 15 3.297979966 0.159282891 . . . . . 53296 7 15 . 1 1 24 24 SER N N 15 3.92512408 0.073036681 . . . . . 53296 7 16 . 1 1 25 25 ASP N N 15 2.970075504 0.182540582 . . . . . 53296 7 17 . 1 1 26 26 ASN N N 15 3.205204212 0.131263468 . . . . . 53296 7 18 . 1 1 27 27 GLN N N 15 3.198962664 0.093455731 . . . . . 53296 7 19 . 1 1 29 29 GLY N N 15 3.820711312 0.193275375 . . . . . 53296 7 20 . 1 1 30 30 GLY N N 15 3.135977061 0.208565981 . . . . . 53296 7 21 . 1 1 31 31 SER N N 15 4.478460548 0.138012471 . . . . . 53296 7 22 . 1 1 32 32 THR N N 15 4.849718294 0.225180687 . . . . . 53296 7 23 . 1 1 33 33 ALA N N 15 3.23688507 0.053979974 . . . . . 53296 7 24 . 1 1 34 34 SER N N 15 3.698918446 0.134901911 . . . . . 53296 7 25 . 1 1 35 35 LYS N N 15 3.337415885 0.123039664 . . . . . 53296 7 26 . 1 1 36 36 GLY N N 15 3.136841327 0.200810678 . . . . . 53296 7 27 . 1 1 37 37 ARG N N 15 2.338755259 0.306547578 . . . . . 53296 7 28 . 1 1 38 38 TYR N N 15 2.551779113 0.209557018 . . . . . 53296 7 29 . 1 1 39 39 ILE N N 15 1.691686517 0.105569998 . . . . . 53296 7 30 . 1 1 43 43 LEU N N 15 3.467567558 0.413461767 . . . . . 53296 7 31 . 1 1 45 45 ASN N N 15 4.012165008 0.147462262 . . . . . 53296 7 32 . 1 1 47 47 GLU N N 15 2.650893369 0.107129856 . . . . . 53296 7 33 . 1 1 48 48 ALA N N 15 2.726773975 0.271826679 . . . . . 53296 7 34 . 1 1 49 49 THR N N 15 3.334851457 0.070576443 . . . . . 53296 7 35 . 1 1 50 50 LYS N N 15 3.108459815 0.164303204 . . . . . 53296 7 36 . 1 1 51 51 GLY N N 15 3.383104043 0.300631388 . . . . . 53296 7 37 . 1 1 52 52 PHE N N 15 2.93823625 0.129762625 . . . . . 53296 7 38 . 1 1 54 54 ASP N N 15 3.026635958 0.218045167 . . . . . 53296 7 39 . 1 1 57 57 SER N N 15 4.210472653 0.218262355 . . . . . 53296 7 40 . 1 1 58 58 SER N N 15 4.658323073 0.197034656 . . . . . 53296 7 41 . 1 1 59 59 GLY N N 15 4.164564453 0.181038463 . . . . . 53296 7 42 . 1 1 61 61 SER N N 15 3.975118857 0.165121295 . . . . . 53296 7 43 . 1 1 62 62 SER N N 15 4.7409858 0.185849751 . . . . . 53296 7 44 . 1 1 63 63 SER N N 15 5.739032546 0.136549023 . . . . . 53296 7 45 . 1 1 64 64 LYS N N 15 3.741324315 0.126621298 . . . . . 53296 7 46 . 1 1 66 66 LYS N N 15 2.478758526 0.225230774 . . . . . 53296 7 47 . 1 1 68 68 ALA N N 15 3.054920654 0.133066341 . . . . . 53296 7 48 . 1 1 69 69 TYR N N 15 3.018505814 0.184963889 . . . . . 53296 7 49 . 1 1 70 70 SER N N 15 3.645858847 0.084735702 . . . . . 53296 7 50 . 1 1 71 71 SER N N 15 5.492288396 0.159060029 . . . . . 53296 7 51 . 1 1 73 73 GLY N N 15 3.493440021 0.20625837 . . . . . 53296 7 52 . 1 1 74 74 SER N N 15 3.955626798 0.129255433 . . . . . 53296 7 53 . 1 1 78 78 SER N N 15 4.562411229 0.151573803 . . . . . 53296 7 54 . 1 1 82 82 SER N N 15 4.412990141 0.20247568 . . . . . 53296 7 55 . 1 1 83 83 SER N N 15 5.414946689 0.188320112 . . . . . 53296 7 56 . 1 1 85 85 PHE N N 15 3.421962947 0.19959345 . . . . . 53296 7 57 . 1 1 86 86 SER N N 15 3.761020647 0.140333329 . . . . . 53296 7 58 . 1 1 88 88 ARG N N 15 3.354079019 0.184782019 . . . . . 53296 7 59 . 1 1 89 89 GLY N N 15 3.465403129 0.185207668 . . . . . 53296 7 60 . 1 1 90 90 SER N N 15 4.822227571 0.265873553 . . . . . 53296 7 61 . 1 1 91 91 GLY N N 15 4.566494984 0.114058391 . . . . . 53296 7 62 . 1 1 92 92 SER N N 15 4.707277985 0.215665352 . . . . . 53296 7 63 . 1 1 94 94 GLY N N 15 3.460419429 0.167110882 . . . . . 53296 7 64 . 1 1 95 95 ARG N N 15 2.941578342 0.193871602 . . . . . 53296 7 65 . 1 1 96 96 PHE N N 15 2.993943705 0.178881337 . . . . . 53296 7 66 . 1 1 97 97 ASP N N 15 3.428542735 0.295676201 . . . . . 53296 7 67 . 1 1 98 98 ASP N N 15 2.931761346 0.111986045 . . . . . 53296 7 68 . 1 1 100 100 GLY N N 15 3.373280981 0.362300525 . . . . . 53296 7 69 . 1 1 101 101 ARG N N 15 2.8906759 0.158867166 . . . . . 53296 7 70 . 1 1 102 102 SER N N 15 4.149519336 0.13390049 . . . . . 53296 7 71 . 1 1 104 104 TYR N N 15 2.691149926 0.166861826 . . . . . 53296 7 72 . 1 1 106 106 GLY N N 15 3.036730368 0.385102501 . . . . . 53296 7 73 . 1 1 107 107 ILE N N 15 2.566025597 0.110959678 . . . . . 53296 7 74 . 1 1 108 108 GLY N N 15 3.154058836 0.181139821 . . . . . 53296 7 75 . 1 1 109 109 SER N N 15 3.898690246 0.276032799 . . . . . 53296 7 76 . 1 1 113 113 ARG N N 15 3.506621673 0.133175907 . . . . . 53296 7 77 . 1 1 115 115 GLY N N 15 4.03385048 0.222004791 . . . . . 53296 7 78 . 1 1 116 116 PHE N N 15 3.100856 0.145154076 . . . . . 53296 7 79 . 1 1 117 117 GLY N N 15 3.179673598 0.348708287 . . . . . 53296 7 80 . 1 1 118 118 LYS N N 15 2.779743255 0.17011514 . . . . . 53296 7 81 . 1 1 120 120 GLU N N 15 2.892965342 0.098225241 . . . . . 53296 7 82 . 1 1 121 121 ARG N N 15 3.018296184 0.190023356 . . . . . 53296 7 83 . 1 1 122 122 GLY N N 15 3.471926163 0.210839919 . . . . . 53296 7 84 . 1 1 123 123 GLY N N 15 3.224234776 0.195709092 . . . . . 53296 7 85 . 1 1 124 124 ASN N N 15 4.736932909 0.321758841 . . . . . 53296 7 86 . 1 1 125 125 SER N N 15 4.785357792 0.20324745 . . . . . 53296 7 87 . 1 1 128 128 CYS N N 15 2.838600463 0.117212855 . . . . . 53296 7 88 . 1 1 129 129 ASP N N 15 2.959861284 0.183277889 . . . . . 53296 7 89 . 1 1 131 131 SER N N 15 2.73453841 0.080979951 . . . . . 53296 7 90 . 1 1 132 132 ASP N N 15 1.714670999 0.088017106 . . . . . 53296 7 stop_ save_ ######################################## # Heteronuclear T2 relaxation values # ######################################## save_heteronucl_T2_relaxation_1 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_1 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 1 _Heteronucl_T2_list.Name '15N R2 u-15N' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type N(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 1 'T1rho/R1rho relaxation' . . . 53296 1 2 'T1/R1 relaxation' . . . 53296 1 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 1 2 $software_2 . . 53296 1 3 $software_3 . . 53296 1 4 $software_4 . . 53296 1 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 3.342096124 0.161820857 . . . . . . . 53296 1 2 . 1 1 5 5 ALA N N 15 4.61390927 0.072362088 . . . . . . . 53296 1 3 . 1 1 7 7 GLU N N 15 5.525876044 0.092759656 . . . . . . . 53296 1 4 . 1 1 8 8 ASN N N 15 4.872058665 0.097237374 . . . . . . . 53296 1 5 . 1 1 9 9 ALA N N 15 5.277526056 0.096619903 . . . . . . . 53296 1 6 . 1 1 11 11 GLY N N 15 4.99230671 0.183996251 . . . . . . . 53296 1 7 . 1 1 13 13 ASP N N 15 6.18515511 0.181405627 . . . . . . . 53296 1 8 . 1 1 17 17 ALA N N 15 6.947548486 0.12911407 . . . . . . . 53296 1 9 . 1 1 18 18 GLY N N 15 5.841552851 0.138240317 . . . . . . . 53296 1 10 . 1 1 20 20 ASP N N 15 6.292659166 0.172278307 . . . . . . . 53296 1 11 . 1 1 21 21 LEU N N 15 6.500328298 0.098519732 . . . . . . . 53296 1 12 . 1 1 22 22 ASN N N 15 6.265211354 0.177446024 . . . . . . . 53296 1 13 . 1 1 23 23 SER N N 15 5.635353663 0.191395844 . . . . . . . 53296 1 14 . 1 1 24 24 SER N N 15 5.624299675 0.132017251 . . . . . . . 53296 1 15 . 1 1 25 25 ASP N N 15 5.952017489 0.12342981 . . . . . . . 53296 1 16 . 1 1 26 26 ASN N N 15 5.34066211 0.266080044 . . . . . . . 53296 1 17 . 1 1 27 27 GLN N N 15 4.976493608 0.108794403 . . . . . . . 53296 1 18 . 1 1 29 29 GLY N N 15 4.519257299 0.128276049 . . . . . . . 53296 1 19 . 1 1 30 30 GLY N N 15 4.149724885 0.132361257 . . . . . . . 53296 1 20 . 1 1 31 31 SER N N 15 4.525938526 0.118968259 . . . . . . . 53296 1 21 . 1 1 33 33 ALA N N 15 5.760499281 0.177115987 . . . . . . . 53296 1 22 . 1 1 34 34 SER N N 15 5.593150021 0.116316624 . . . . . . . 53296 1 23 . 1 1 35 35 LYS N N 15 6.640830632 0.226435975 . . . . . . . 53296 1 24 . 1 1 37 37 ARG N N 15 7.385245997 0.37568458 . . . . . . . 53296 1 25 . 1 1 38 38 TYR N N 15 11.21494466 0.25144041 . . . . . . . 53296 1 26 . 1 1 39 39 ILE N N 15 12.21200362 0.554319488 . . . . . . . 53296 1 27 . 1 1 42 42 HIS N N 15 16.80680683 0.349279095 . . . . . . . 53296 1 28 . 1 1 43 43 LEU N N 15 15.24555439 0.144467459 . . . . . . . 53296 1 29 . 1 1 45 45 ASN N N 15 11.6098685 0.076996645 . . . . . . . 53296 1 30 . 1 1 47 47 GLU N N 15 10.8736021 0.221738537 . . . . . . . 53296 1 31 . 1 1 48 48 ALA N N 15 10.40427949 0.104845974 . . . . . . . 53296 1 32 . 1 1 49 49 THR N N 15 9.908784103 0.265573548 . . . . . . . 53296 1 33 . 1 1 50 50 LYS N N 15 10.88880922 0.215308625 . . . . . . . 53296 1 34 . 1 1 51 51 GLY N N 15 9.277250244 0.273530062 . . . . . . . 53296 1 35 . 1 1 54 54 ASP N N 15 12.85422389 0.259177109 . . . . . . . 53296 1 36 . 1 1 57 57 SER N N 15 10.48920264 0.245097773 . . . . . . . 53296 1 37 . 1 1 58 58 SER N N 15 9.957766008 0.191151076 . . . . . . . 53296 1 38 . 1 1 59 59 GLY N N 15 10.37838527 0.253280073 . . . . . . . 53296 1 39 . 1 1 61 61 SER N N 15 11.09867305 0.387021979 . . . . . . . 53296 1 40 . 1 1 62 62 SER N N 15 10.25351937 0.252770996 . . . . . . . 53296 1 41 . 1 1 63 63 SER N N 15 10.03375665 0.200034191 . . . . . . . 53296 1 42 . 1 1 64 64 LYS N N 15 10.85728719 0.209975667 . . . . . . . 53296 1 43 . 1 1 66 66 LYS N N 15 10.67797809 0.179146739 . . . . . . . 53296 1 44 . 1 1 68 68 ALA N N 15 11.428472 0.172718674 . . . . . . . 53296 1 45 . 1 1 69 69 TYR N N 15 11.6135875 0.293560012 . . . . . . . 53296 1 46 . 1 1 70 70 SER N N 15 10.71064242 0.302925161 . . . . . . . 53296 1 47 . 1 1 71 71 SER N N 15 10.21537598 0.14518282 . . . . . . . 53296 1 48 . 1 1 73 73 GLY N N 15 9.295634271 0.282575998 . . . . . . . 53296 1 49 . 1 1 74 74 SER N N 15 8.906393711 0.060844933 . . . . . . . 53296 1 50 . 1 1 78 78 SER N N 15 9.205009165 0.121738453 . . . . . . . 53296 1 51 . 1 1 82 82 SER N N 15 9.253596864 0.15781758 . . . . . . . 53296 1 52 . 1 1 83 83 SER N N 15 9.71768561 0.290247829 . . . . . . . 53296 1 53 . 1 1 85 85 PHE N N 15 12.42202794 0.319990974 . . . . . . . 53296 1 54 . 1 1 86 86 SER N N 15 10.59379228 0.120794442 . . . . . . . 53296 1 55 . 1 1 88 88 ARG N N 15 10.28267739 0.209518166 . . . . . . . 53296 1 56 . 1 1 89 89 GLY N N 15 9.151989784 0.285825597 . . . . . . . 53296 1 57 . 1 1 91 91 GLY N N 15 7.990131439 0.199809488 . . . . . . . 53296 1 58 . 1 1 92 92 SER N N 15 9.062903646 0.213213803 . . . . . . . 53296 1 59 . 1 1 95 95 ARG N N 15 11.07837016 0.24147692 . . . . . . . 53296 1 60 . 1 1 96 96 PHE N N 15 11.82389336 0.397178283 . . . . . . . 53296 1 61 . 1 1 97 97 ASP N N 15 12.24313768 0.345274066 . . . . . . . 53296 1 62 . 1 1 98 98 ASP N N 15 11.92186475 0.284283875 . . . . . . . 53296 1 63 . 1 1 100 100 GLY N N 15 11.43996356 0.2579223 1 . 1 1 . . . 53296 1 64 . 1 1 101 101 ARG N N 15 10.65319085 0.45187308 . . . . . . . 53296 1 65 . 1 1 102 102 SER N N 15 10.78158015 0.171342722 . . . . . . . 53296 1 66 . 1 1 106 106 GLY N N 15 10.42705794 0.758511717 . . . . . . . 53296 1 67 . 1 1 107 107 ILE N N 15 11.21070861 0.12825599 . . . . . . . 53296 1 68 . 1 1 108 108 GLY N N 15 10.25520664 0.251711794 . . . . . . . 53296 1 69 . 1 1 109 109 SER N N 15 9.000479563 0.159724985 . . . . . . . 53296 1 70 . 1 1 113 113 ARG N N 15 9.316657096 0.390106021 . . . . . . . 53296 1 71 . 1 1 115 115 GLY N N 15 9.051710006 0.327013172 . . . . . . . 53296 1 72 . 1 1 116 116 PHE N N 15 9.976318281 0.108934467 . . . . . . . 53296 1 73 . 1 1 117 117 GLY N N 15 8.982539691 0.171038505 . . . . . . . 53296 1 74 . 1 1 118 118 LYS N N 15 9.523789735 0.238231239 . . . . . . . 53296 1 75 . 1 1 120 120 GLU N N 15 9.809341514 0.317244371 . . . . . . . 53296 1 76 . 1 1 121 121 ARG N N 15 9.064215842 0.176656438 . . . . . . . 53296 1 77 . 1 1 122 122 GLY N N 15 8.515925107 0.362191087 . . . . . . . 53296 1 78 . 1 1 123 123 GLY N N 15 7.015441135 0.125386546 . . . . . . . 53296 1 79 . 1 1 124 124 ASN N N 15 7.499699026 0.191716 1 . 1 1 . . . 53296 1 80 . 1 1 125 125 SER N N 15 7.916468829 0.072704841 . . . . . . . 53296 1 81 . 1 1 128 128 CYS N N 15 9.282852573 0.228421572 . . . . . . . 53296 1 82 . 1 1 129 129 ASP N N 15 7.114261337 0.122720274 . . . . . . . 53296 1 83 . 1 1 131 131 SER N N 15 4.414708533 0.118729443 . . . . . . . 53296 1 84 . 1 1 132 132 ASP N N 15 3.19827929 0.133631305 . . . . . . . 53296 1 stop_ save_ save_heteronucl_T2_relaxation_2 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_2 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 2 _Heteronucl_T2_list.Name '15N R2 u-2H,15N 100 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type N(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 8 'T1rho/R1rho relaxation' . . . 53296 2 9 'T1/R1 relaxation' . . . 53296 2 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 2 2 $software_2 . . 53296 2 3 $software_3 . . 53296 2 4 $software_4 . . 53296 2 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 3.145391244 0.444589791 . . . . . . . 53296 2 2 . 1 1 5 5 ALA N N 15 4.557841404 0.220577018 . . . . . . . 53296 2 3 . 1 1 7 7 GLU N N 15 5.000702648 0.267970022 . . . . . . . 53296 2 4 . 1 1 8 8 ASN N N 15 4.752011605 0.195375603 . . . . . . . 53296 2 5 . 1 1 9 9 ALA N N 15 4.91954928 0.525711076 . . . . . . . 53296 2 6 . 1 1 11 11 GLY N N 15 3.912239378 0.377946882 . . . . . . . 53296 2 7 . 1 1 12 12 LEU N N 15 5.162659686 0.131683102 . . . . . . . 53296 2 8 . 1 1 13 13 ASP N N 15 5.647645231 0.224946492 . . . . . . . 53296 2 9 . 1 1 17 17 ALA N N 15 5.426267269 0.177664967 . . . . . . . 53296 2 10 . 1 1 18 18 GLY N N 15 4.685137149 0.40603367 . . . . . . . 53296 2 11 . 1 1 20 20 ASP N N 15 5.747308119 0.291844254 . . . . . . . 53296 2 12 . 1 1 21 21 LEU N N 15 5.711244001 0.142159664 . . . . . . . 53296 2 13 . 1 1 22 22 ASN N N 15 5.579801267 0.260696187 . . . . . . . 53296 2 14 . 1 1 23 23 SER N N 15 5.14578395 0.254053982 . . . . . . . 53296 2 15 . 1 1 24 24 SER N N 15 5.057393922 0.245201316 . . . . . . . 53296 2 16 . 1 1 25 25 ASP N N 15 4.932503415 0.205823204 . . . . . . . 53296 2 17 . 1 1 26 26 ASN N N 15 4.831993195 0.187368399 . . . . . . . 53296 2 18 . 1 1 27 27 GLN N N 15 4.840032892 0.200148648 . . . . . . . 53296 2 19 . 1 1 29 29 GLY N N 15 3.926814557 0.428117137 . . . . . . . 53296 2 20 . 1 1 30 30 GLY N N 15 3.747478545 0.246824891 . . . . . . . 53296 2 21 . 1 1 31 31 SER N N 15 3.86149296 0.087377978 . . . . . . . 53296 2 22 . 1 1 32 32 THR N N 15 4.559089246 0.233983096 . . . . . . . 53296 2 23 . 1 1 33 33 ALA N N 15 5.540590857 0.229145834 . . . . . . . 53296 2 24 . 1 1 34 34 SER N N 15 5.061171153 0.190066857 . . . . . . . 53296 2 25 . 1 1 35 35 LYS N N 15 5.468868729 0.202807094 . . . . . . . 53296 2 26 . 1 1 36 36 GLY N N 15 6.173727357 0.413467442 . . . . . . . 53296 2 27 . 1 1 37 37 ARG N N 15 6.667449092 0.352391358 . . . . . . . 53296 2 28 . 1 1 38 38 TYR N N 15 9.168533716 0.327964163 . . . . . . . 53296 2 29 . 1 1 39 39 ILE N N 15 10.76772234 0.487617071 . . . . . . . 53296 2 30 . 1 1 43 43 LEU N N 15 13.87863017 0.509328128 . . . . . . . 53296 2 31 . 1 1 45 45 ASN N N 15 10.13060377 0.524443005 . . . . . . . 53296 2 32 . 1 1 47 47 GLU N N 15 9.186510368 0.232261851 . . . . . . . 53296 2 33 . 1 1 48 48 ALA N N 15 9.102468271 0.374935741 . . . . . . . 53296 2 34 . 1 1 49 49 THR N N 15 8.13040606 0.172093652 . . . . . . . 53296 2 35 . 1 1 50 50 LYS N N 15 8.985371433 0.125115161 . . . . . . . 53296 2 36 . 1 1 51 51 GLY N N 15 7.649393258 0.290072509 . . . . . . . 53296 2 37 . 1 1 52 52 PHE N N 15 8.98572679 0.30476626 . . . . . . . 53296 2 38 . 1 1 54 54 ASP N N 15 10.60142635 0.580916811 . . . . . . . 53296 2 39 . 1 1 57 57 SER N N 15 7.945932946 0.456989881 . . . . . . . 53296 2 40 . 1 1 58 58 SER N N 15 8.358899738 0.350676864 . . . . . . . 53296 2 41 . 1 1 59 59 GLY N N 15 8.633359862 0.425876253 . . . . . . . 53296 2 42 . 1 1 61 61 SER N N 15 9.191003678 0.492696399 . . . . . . . 53296 2 43 . 1 1 62 62 SER N N 15 8.455181668 0.466392956 . . . . . . . 53296 2 44 . 1 1 63 63 SER N N 15 8.595578774 0.112604401 . . . . . . . 53296 2 45 . 1 1 64 64 LYS N N 15 8.727171741 0.416629204 . . . . . . . 53296 2 46 . 1 1 66 66 LYS N N 15 8.55560761 0.276881263 . . . . . . . 53296 2 47 . 1 1 68 68 ALA N N 15 8.713335804 0.664947512 . . . . . . . 53296 2 48 . 1 1 69 69 TYR N N 15 9.159208479 0.555698929 . . . . . . . 53296 2 49 . 1 1 70 70 SER N N 15 8.818665529 0.273863571 . . . . . . . 53296 2 50 . 1 1 71 71 SER N N 15 8.027477622 0.350250961 . . . . . . . 53296 2 51 . 1 1 73 73 GLY N N 15 7.330333172 0.293706576 . . . . . . . 53296 2 52 . 1 1 74 74 SER N N 15 7.33590388 0.229244547 . . . . . . . 53296 2 53 . 1 1 78 78 SER N N 15 7.979232737 0.075133825 . . . . . . . 53296 2 54 . 1 1 82 82 SER N N 15 6.567701131 0.272346184 . . . . . . . 53296 2 55 . 1 1 83 83 SER N N 15 7.476875415 0.296107628 . . . . . . . 53296 2 56 . 1 1 85 85 PHE N N 15 9.337805248 0.26522726 . . . . . . . 53296 2 57 . 1 1 86 86 SER N N 15 8.399061646 0.106530908 . . . . . . . 53296 2 58 . 1 1 88 88 ARG N N 15 8.379471832 0.27668193 . . . . . . . 53296 2 59 . 1 1 89 89 GLY N N 15 7.294442212 0.334059392 . . . . . . . 53296 2 60 . 1 1 90 90 SER N N 15 6.973526969 0.360585009 . . . . . . . 53296 2 61 . 1 1 91 91 GLY N N 15 6.294791119 0.330625276 . . . . . . . 53296 2 62 . 1 1 92 92 SER N N 15 7.203705766 0.210429642 . . . . . . . 53296 2 63 . 1 1 94 94 GLY N N 15 8.597765057 0.383459518 . . . . . . . 53296 2 64 . 1 1 95 95 ARG N N 15 8.536074783 0.297584362 . . . . . . . 53296 2 65 . 1 1 96 96 PHE N N 15 9.566853612 0.342657625 . . . . . . . 53296 2 66 . 1 1 97 97 ASP N N 15 9.87586681 0.29944148 . . . . . . . 53296 2 67 . 1 1 98 98 ASP N N 15 10.59441604 0.588582598 . . . . . . . 53296 2 68 . 1 1 100 100 GLY N N 15 9.190572225 0.262205875 . . . . . . . 53296 2 69 . 1 1 101 101 ARG N N 15 9.354527832 0.363474439 . . . . . . . 53296 2 70 . 1 1 102 102 SER N N 15 8.766326611 0.248502539 . . . . . . . 53296 2 71 . 1 1 104 104 TYR N N 15 8.765437726 0.281407217 . . . . . . . 53296 2 72 . 1 1 106 106 GLY N N 15 7.520620935 0.59039238 . . . . . . . 53296 2 73 . 1 1 107 107 ILE N N 15 8.725330991 0.311966489 . . . . . . . 53296 2 74 . 1 1 108 108 GLY N N 15 8.200305497 0.604777022 . . . . . . . 53296 2 75 . 1 1 109 109 SER N N 15 7.490903911 0.599937287 . . . . . . . 53296 2 76 . 1 1 113 113 ARG N N 15 7.515223443 0.290191471 . . . . . . . 53296 2 77 . 1 1 115 115 GLY N N 15 7.42881033 0.541477364 . . . . . . . 53296 2 78 . 1 1 116 116 PHE N N 15 7.978024653 0.360509819 . . . . . . . 53296 2 79 . 1 1 117 117 GLY N N 15 6.777192127 0.286745602 . . . . . . . 53296 2 80 . 1 1 118 118 LYS N N 15 7.550913122 0.234912839 . . . . . . . 53296 2 81 . 1 1 120 120 GLU N N 15 8.337204316 0.252331549 . . . . . . . 53296 2 82 . 1 1 121 121 ARG N N 15 7.747152751 0.434737503 . . . . . . . 53296 2 83 . 1 1 122 122 GLY N N 15 6.217109792 0.507453623 . . . . . . . 53296 2 84 . 1 1 123 123 GLY N N 15 5.582631727 0.436587412 . . . . . . . 53296 2 85 . 1 1 124 124 ASN N N 15 5.50118904 0.302602977 . . . . . . . 53296 2 86 . 1 1 125 125 SER N N 15 6.15606044 0.285681166 . . . . . . . 53296 2 87 . 1 1 128 128 CYS N N 15 7.487270704 0.344360572 . . . . . . . 53296 2 88 . 1 1 129 129 ASP N N 15 6.691926707 0.25966174 . . . . . . . 53296 2 89 . 1 1 131 131 SER N N 15 3.415850719 0.204222857 . . . . . . . 53296 2 90 . 1 1 132 132 ASP N N 15 2.945665846 0.23303917 . . . . . . . 53296 2 stop_ save_ save_heteronucl_T2_relaxation_3 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_3 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 3 _Heteronucl_T2_list.Name 'HxNx u-2H,15N 100 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HxNx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 4 'T1rho/R1rho relaxation HxNx' . . . 53296 3 5 'T1rho/R1rho relaxation HxNz' . . . 53296 3 6 'T1rho/R1rho relaxation HzNx' . . . 53296 3 7 'T1/R1 relaxation HzNz' . . . 53296 3 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 3 2 $software_2 . . 53296 3 3 $software_3 . . 53296 3 4 $software_4 . . 53296 3 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 18.62847499 0.570957275 . . . . . . . 53296 3 2 . 1 1 5 5 ALA N N 15 4.96932899 0.348253226 . . . . . . . 53296 3 3 . 1 1 7 7 GLU N N 15 5.94821999 0.192901357 . . . . . . . 53296 3 4 . 1 1 8 8 ASN N N 15 6.056685655 0.154626428 . . . . . . . 53296 3 5 . 1 1 9 9 ALA N N 15 5.893446529 0.204680211 . . . . . . . 53296 3 6 . 1 1 11 11 GLY N N 15 5.917363891 0.404308644 . . . . . . . 53296 3 7 . 1 1 12 12 LEU N N 15 6.237795434 0.235968897 . . . . . . . 53296 3 8 . 1 1 13 13 ASP N N 15 6.737444787 0.158726724 . . . . . . . 53296 3 9 . 1 1 17 17 ALA N N 15 7.305293621 0.17397453 . . . . . . . 53296 3 10 . 1 1 18 18 GLY N N 15 7.304894742 0.284514031 . . . . . . . 53296 3 11 . 1 1 20 20 ASP N N 15 6.709212391 0.20313423 . . . . . . . 53296 3 12 . 1 1 21 21 LEU N N 15 6.973233193 0.19287643 . . . . . . . 53296 3 13 . 1 1 22 22 ASN N N 15 7.470308037 0.32440098 . . . . . . . 53296 3 14 . 1 1 23 23 SER N N 15 7.279353185 0.221696575 . . . . . . . 53296 3 15 . 1 1 24 24 SER N N 15 7.598557945 0.285093544 . . . . . . . 53296 3 16 . 1 1 25 25 ASP N N 15 6.774927456 0.194382768 . . . . . . . 53296 3 17 . 1 1 26 26 ASN N N 15 6.881544435 0.26611774 . . . . . . . 53296 3 18 . 1 1 27 27 GLN N N 15 6.836926383 0.155652918 . . . . . . . 53296 3 19 . 1 1 29 29 GLY N N 15 6.43561294 0.232632828 . . . . . . . 53296 3 20 . 1 1 30 30 GLY N N 15 5.18665925 0.343621038 . . . . . . . 53296 3 21 . 1 1 31 31 SER N N 15 7.564919448 0.468179183 . . . . . . . 53296 3 22 . 1 1 32 32 THR N N 15 8.167319782 0.305147418 . . . . . . . 53296 3 23 . 1 1 33 33 ALA N N 15 6.75972534 0.396046309 . . . . . . . 53296 3 24 . 1 1 34 34 SER N N 15 6.980036203 0.17210799 . . . . . . . 53296 3 25 . 1 1 35 35 LYS N N 15 7.731849818 0.295148717 . . . . . . . 53296 3 26 . 1 1 36 36 GLY N N 15 6.563814496 0.260979103 . . . . . . . 53296 3 27 . 1 1 37 37 ARG N N 15 8.512205372 0.327238908 . . . . . . . 53296 3 28 . 1 1 38 38 TYR N N 15 9.810995334 0.227261889 . . . . . . . 53296 3 29 . 1 1 39 39 ILE N N 15 10.04584009 0.346434747 . . . . . . . 53296 3 30 . 1 1 43 43 LEU N N 15 27.72429031 0.987309344 . . . . . . . 53296 3 31 . 1 1 45 45 ASN N N 15 13.52966138 0.368285805 . . . . . . . 53296 3 32 . 1 1 47 47 GLU N N 15 10.73566441 0.277290509 . . . . . . . 53296 3 33 . 1 1 48 48 ALA N N 15 11.38916162 0.361268844 . . . . . . . 53296 3 34 . 1 1 49 49 THR N N 15 11.04836149 0.278537289 . . . . . . . 53296 3 35 . 1 1 50 50 LYS N N 15 11.53554386 0.255078006 . . . . . . . 53296 3 36 . 1 1 51 51 GLY N N 15 11.60389194 0.497349808 . . . . . . . 53296 3 37 . 1 1 52 52 PHE N N 15 10.47618673 0.467911704 . . . . . . . 53296 3 38 . 1 1 54 54 ASP N N 15 12.53767127 0.32032832 . . . . . . . 53296 3 39 . 1 1 57 57 SER N N 15 13.17559114 0.39987376 . . . . . . . 53296 3 40 . 1 1 58 58 SER N N 15 13.01648385 0.277154371 . . . . . . . 53296 3 41 . 1 1 59 59 GLY N N 15 13.43495428 0.46484416 . . . . . . . 53296 3 42 . 1 1 61 61 SER N N 15 15.85726689 0.433267902 . . . . . . . 53296 3 43 . 1 1 62 62 SER N N 15 13.03515801 0.10679249 . . . . . . . 53296 3 44 . 1 1 63 63 SER N N 15 15.4425766 0.405978513 . . . . . . . 53296 3 45 . 1 1 64 64 LYS N N 15 12.81714073 0.129940425 . . . . . . . 53296 3 46 . 1 1 66 66 LYS N N 15 11.42076212 0.346202543 . . . . . . . 53296 3 47 . 1 1 68 68 ALA N N 15 11.25663804 0.478619796 . . . . . . . 53296 3 48 . 1 1 69 69 TYR N N 15 11.11362268 0.209885894 . . . . . . . 53296 3 49 . 1 1 70 70 SER N N 15 11.36928683 0.267789335 . . . . . . . 53296 3 50 . 1 1 71 71 SER N N 15 13.41546316 0.370800215 . . . . . . . 53296 3 51 . 1 1 73 73 GLY N N 15 9.947825517 0.17729423 . . . . . . . 53296 3 52 . 1 1 74 74 SER N N 15 10.42839776 0.29525047 . . . . . . . 53296 3 53 . 1 1 78 78 SER N N 15 11.56684049 0.209082152 . . . . . . . 53296 3 54 . 1 1 82 82 SER N N 15 10.82118654 0.250559089 . . . . . . . 53296 3 55 . 1 1 83 83 SER N N 15 12.77776276 0.406581972 . . . . . . . 53296 3 56 . 1 1 85 85 PHE N N 15 12.13948069 0.23896418 . . . . . . . 53296 3 57 . 1 1 86 86 SER N N 15 11.0245535 0.243732396 . . . . . . . 53296 3 58 . 1 1 88 88 ARG N N 15 11.56116416 0.421175922 . . . . . . . 53296 3 59 . 1 1 89 89 GLY N N 15 10.52419694 0.247832772 . . . . . . . 53296 3 60 . 1 1 90 90 SER N N 15 11.63671813 0.190423738 . . . . . . . 53296 3 61 . 1 1 91 91 GLY N N 15 9.790176702 0.227067319 . . . . . . . 53296 3 62 . 1 1 92 92 SER N N 15 9.936682245 0.298326818 . . . . . . . 53296 3 63 . 1 1 94 94 GLY N N 15 11.32944758 0.281074236 . . . . . . . 53296 3 64 . 1 1 95 95 ARG N N 15 11.25211553 0.256484871 . . . . . . . 53296 3 65 . 1 1 96 96 PHE N N 15 11.84215715 0.195233448 . . . . . . . 53296 3 66 . 1 1 97 97 ASP N N 15 12.50664354 0.360041769 . . . . . . . 53296 3 67 . 1 1 98 98 ASP N N 15 12.23689328 0.286045698 . . . . . . . 53296 3 68 . 1 1 100 100 GLY N N 15 11.72022828 0.549207229 . . . . . . . 53296 3 69 . 1 1 101 101 ARG N N 15 11.97223247 0.381765312 . . . . . . . 53296 3 70 . 1 1 102 102 SER N N 15 12.39880797 0.389677232 . . . . . . . 53296 3 71 . 1 1 104 104 TYR N N 15 12.20625559 0.359845444 . . . . . . . 53296 3 72 . 1 1 106 106 GLY N N 15 19.04361258 0.683378353 . . . . . . . 53296 3 73 . 1 1 107 107 ILE N N 15 10.5114269 0.44708623 . . . . . . . 53296 3 74 . 1 1 108 108 GLY N N 15 11.96283893 0.190403176 . . . . . . . 53296 3 75 . 1 1 109 109 SER N N 15 11.52573249 0.256691192 . . . . . . . 53296 3 76 . 1 1 113 113 ARG N N 15 10.95570225 0.297219783 . . . . . . . 53296 3 77 . 1 1 115 115 GLY N N 15 10.67893992 0.326215266 . . . . . . . 53296 3 78 . 1 1 116 116 PHE N N 15 9.746930087 0.282123564 . . . . . . . 53296 3 79 . 1 1 117 117 GLY N N 15 9.948616459 0.314070913 . . . . . . . 53296 3 80 . 1 1 118 118 LYS N N 15 9.625037393 0.406714135 . . . . . . . 53296 3 81 . 1 1 120 120 GLU N N 15 10.12375034 0.199175602 . . . . . . . 53296 3 82 . 1 1 121 121 ARG N N 15 9.387743116 0.354393237 . . . . . . . 53296 3 83 . 1 1 122 122 GLY N N 15 9.357567442 0.312258839 . . . . . . . 53296 3 84 . 1 1 123 123 GLY N N 15 8.382982624 0.549897826 . . . . . . . 53296 3 85 . 1 1 124 124 ASN N N 15 9.546737215 0.396764066 . . . . . . . 53296 3 86 . 1 1 125 125 SER N N 15 9.693921113 0.372737897 . . . . . . . 53296 3 87 . 1 1 128 128 CYS N N 15 10.13546911 0.156183123 . . . . . . . 53296 3 88 . 1 1 129 129 ASP N N 15 8.387875085 0.351561304 . . . . . . . 53296 3 89 . 1 1 131 131 SER N N 15 5.307718882 0.289583956 . . . . . . . 53296 3 90 . 1 1 132 132 ASP N N 15 2.819971594 0.321405591 . . . . . . . 53296 3 stop_ save_ save_heteronucl_T2_relaxation_4 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_4 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 4 _Heteronucl_T2_list.Name 'HxNz u-2H,15N 100 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HxNz _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 4 'T1rho/R1rho relaxation HxNx' . . . 53296 4 5 'T1rho/R1rho relaxation HxNz' . . . 53296 4 6 'T1rho/R1rho relaxation HzNx' . . . 53296 4 7 'T1/R1 relaxation HzNz' . . . 53296 4 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 4 2 $software_2 . . 53296 4 3 $software_3 . . 53296 4 4 $software_4 . . 53296 4 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS H H 1 18.26757489 0.233540768 . . . . . . . 53296 4 2 . 1 1 5 5 ALA H H 1 3.998256637 0.240782111 . . . . . . . 53296 4 3 . 1 1 7 7 GLU H H 1 4.795036331 0.183143144 . . . . . . . 53296 4 4 . 1 1 8 8 ASN H H 1 5.664356711 0.145771719 . . . . . . . 53296 4 5 . 1 1 9 9 ALA H H 1 5.778637346 0.29654457 . . . . . . . 53296 4 6 . 1 1 11 11 GLY H H 1 5.672298746 0.475556864 . . . . . . . 53296 4 7 . 1 1 12 12 LEU H H 1 5.864861816 0.275464421 . . . . . . . 53296 4 8 . 1 1 13 13 ASP H H 1 6.001584658 0.225860539 . . . . . . . 53296 4 9 . 1 1 17 17 ALA H H 1 6.522957461 0.258116025 . . . . . . . 53296 4 10 . 1 1 18 18 GLY H H 1 6.810629627 0.293514684 . . . . . . . 53296 4 11 . 1 1 20 20 ASP H H 1 5.718481004 0.098471048 . . . . . . . 53296 4 12 . 1 1 21 21 LEU H H 1 6.184844043 0.256641652 . . . . . . . 53296 4 13 . 1 1 22 22 ASN H H 1 6.663992273 0.244166335 . . . . . . . 53296 4 14 . 1 1 23 23 SER H H 1 7.13464666 0.306394642 . . . . . . . 53296 4 15 . 1 1 24 24 SER H H 1 7.188190028 0.234956644 . . . . . . . 53296 4 16 . 1 1 25 25 ASP H H 1 6.561957644 0.148079987 . . . . . . . 53296 4 17 . 1 1 26 26 ASN H H 1 6.295192833 0.277375741 . . . . . . . 53296 4 18 . 1 1 27 27 GLN H H 1 6.173577648 0.22515506 . . . . . . . 53296 4 19 . 1 1 29 29 GLY H H 1 6.159729469 0.44379056 . . . . . . . 53296 4 20 . 1 1 30 30 GLY H H 1 5.395554123 0.168015003 . . . . . . . 53296 4 21 . 1 1 31 31 SER H H 1 6.797944978 0.092960811 . . . . . . . 53296 4 22 . 1 1 32 32 THR H H 1 7.217679178 0.256776801 . . . . . . . 53296 4 23 . 1 1 33 33 ALA H H 1 6.469989785 0.341684307 . . . . . . . 53296 4 24 . 1 1 34 34 SER H H 1 7.389989655 0.195136435 . . . . . . . 53296 4 25 . 1 1 35 35 LYS H H 1 7.337891061 0.186286921 . . . . . . . 53296 4 26 . 1 1 36 36 GLY H H 1 7.301266639 0.200596795 . . . . . . . 53296 4 27 . 1 1 37 37 ARG H H 1 8.093773024 0.504368494 . . . . . . . 53296 4 28 . 1 1 38 38 TYR H H 1 8.434033926 0.423787177 . . . . . . . 53296 4 29 . 1 1 39 39 ILE H H 1 8.687034713 0.35274643 . . . . . . . 53296 4 30 . 1 1 43 43 LEU H H 1 25.6429029 0.629060935 . . . . . . . 53296 4 31 . 1 1 45 45 ASN H H 1 12.36981303 0.355362806 . . . . . . . 53296 4 32 . 1 1 47 47 GLU H H 1 9.743208993 0.175249089 . . . . . . . 53296 4 33 . 1 1 48 48 ALA H H 1 9.705817052 0.279065298 . . . . . . . 53296 4 34 . 1 1 49 49 THR H H 1 9.838894163 0.37170872 . . . . . . . 53296 4 35 . 1 1 50 50 LYS H H 1 10.32538991 0.291849074 . . . . . . . 53296 4 36 . 1 1 51 51 GLY H H 1 10.26026934 0.234740268 . . . . . . . 53296 4 37 . 1 1 52 52 PHE H H 1 9.433733921 0.431341264 . . . . . . . 53296 4 38 . 1 1 54 54 ASP H H 1 11.14410745 0.314966089 . . . . . . . 53296 4 39 . 1 1 57 57 SER H H 1 12.36440401 0.385954002 . . . . . . . 53296 4 40 . 1 1 58 58 SER H H 1 11.96026461 0.357207372 . . . . . . . 53296 4 41 . 1 1 59 59 GLY H H 1 12.19859059 0.246295195 . . . . . . . 53296 4 42 . 1 1 61 61 SER H H 1 14.37233415 0.237217576 . . . . . . . 53296 4 43 . 1 1 62 62 SER H H 1 12.32529933 0.378580418 . . . . . . . 53296 4 44 . 1 1 63 63 SER H H 1 13.9087013 0.320534666 . . . . . . . 53296 4 45 . 1 1 64 64 LYS H H 1 11.98792598 0.088370459 . . . . . . . 53296 4 46 . 1 1 66 66 LYS H H 1 9.889706494 0.32626766 . . . . . . . 53296 4 47 . 1 1 68 68 ALA H H 1 10.18113405 0.213310688 . . . . . . . 53296 4 48 . 1 1 69 69 TYR H H 1 9.94101108 0.259135573 . . . . . . . 53296 4 49 . 1 1 70 70 SER H H 1 10.64376203 0.067792686 . . . . . . . 53296 4 50 . 1 1 71 71 SER H H 1 12.14005633 0.114601527 . . . . . . . 53296 4 51 . 1 1 73 73 GLY H H 1 8.962390336 0.185082336 . . . . . . . 53296 4 52 . 1 1 74 74 SER H H 1 9.494374071 0.253004016 . . . . . . . 53296 4 53 . 1 1 78 78 SER H H 1 10.0536296 0.31931793 . . . . . . . 53296 4 54 . 1 1 82 82 SER H H 1 10.14407291 0.106908386 . . . . . . . 53296 4 55 . 1 1 83 83 SER H H 1 11.76807929 0.179935535 . . . . . . . 53296 4 56 . 1 1 85 85 PHE H H 1 9.906390975 0.247744299 . . . . . . . 53296 4 57 . 1 1 86 86 SER H H 1 10.2331395 0.252920845 . . . . . . . 53296 4 58 . 1 1 88 88 ARG H H 1 9.98473686 0.336495711 . . . . . . . 53296 4 59 . 1 1 89 89 GLY H H 1 8.839085409 0.176873034 . . . . . . . 53296 4 60 . 1 1 90 90 SER H H 1 11.00411908 0.242978721 . . . . . . . 53296 4 61 . 1 1 91 91 GLY H H 1 9.528543431 0.086390416 . . . . . . . 53296 4 62 . 1 1 92 92 SER H H 1 9.334101768 0.303036534 . . . . . . . 53296 4 63 . 1 1 94 94 GLY H H 1 10.66388607 0.246769454 . . . . . . . 53296 4 64 . 1 1 95 95 ARG H H 1 9.910909873 0.26342896 . . . . . . . 53296 4 65 . 1 1 96 96 PHE H H 1 10.68964746 0.287216958 . . . . . . . 53296 4 66 . 1 1 97 97 ASP H H 1 11.13740282 0.268034048 . . . . . . . 53296 4 67 . 1 1 98 98 ASP H H 1 10.51727058 0.432325759 . . . . . . . 53296 4 68 . 1 1 100 100 GLY H H 1 11.19653384 0.647910434 . . . . . . . 53296 4 69 . 1 1 101 101 ARG H H 1 11.41097164 0.611591342 . . . . . . . 53296 4 70 . 1 1 102 102 SER H H 1 11.3375372 0.171251229 . . . . . . . 53296 4 71 . 1 1 104 104 TYR H H 1 11.39116848 0.315693392 . . . . . . . 53296 4 72 . 1 1 106 106 GLY H H 1 19.77732405 0.512389247 . . . . . . . 53296 4 73 . 1 1 107 107 ILE H H 1 9.690130571 0.321119091 . . . . . . . 53296 4 74 . 1 1 108 108 GLY H H 1 10.54562449 0.169515702 . . . . . . . 53296 4 75 . 1 1 109 109 SER H H 1 10.56170851 0.298604289 . . . . . . . 53296 4 76 . 1 1 113 113 ARG H H 1 9.484925415 0.295928352 . . . . . . . 53296 4 77 . 1 1 115 115 GLY H H 1 10.17872139 0.275030448 . . . . . . . 53296 4 78 . 1 1 116 116 PHE H H 1 8.777897048 0.20569486 . . . . . . . 53296 4 79 . 1 1 117 117 GLY H H 1 8.939326062 0.422845093 . . . . . . . 53296 4 80 . 1 1 118 118 LYS H H 1 9.040542968 0.378835817 . . . . . . . 53296 4 81 . 1 1 120 120 GLU H H 1 9.210548862 0.169294137 . . . . . . . 53296 4 82 . 1 1 121 121 ARG H H 1 8.951361191 0.340584447 . . . . . . . 53296 4 83 . 1 1 122 122 GLY H H 1 7.931764083 0.250195098 . . . . . . . 53296 4 84 . 1 1 123 123 GLY H H 1 7.672108972 0.382859146 . . . . . . . 53296 4 85 . 1 1 124 124 ASN H H 1 9.247937525 0.413400598 . . . . . . . 53296 4 86 . 1 1 125 125 SER H H 1 9.479514072 0.250476762 . . . . . . . 53296 4 87 . 1 1 128 128 CYS H H 1 8.637861674 0.211912071 . . . . . . . 53296 4 88 . 1 1 129 129 ASP H H 1 7.187540872 0.171309429 . . . . . . . 53296 4 89 . 1 1 131 131 SER H H 1 4.510029466 0.210829135 . . . . . . . 53296 4 90 . 1 1 132 132 ASP H H 1 2.901791475 0.252986112 . . . . . . . 53296 4 stop_ save_ save_heteronucl_T2_relaxation_5 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_5 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 5 _Heteronucl_T2_list.Name 'HzNx u-2H,15N 100 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HzNx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 4 'T1rho/R1rho relaxation HxNx' . . . 53296 5 5 'T1rho/R1rho relaxation HxNz' . . . 53296 5 6 'T1rho/R1rho relaxation HzNx' . . . 53296 5 7 'T1/R1 relaxation HzNz' . . . 53296 5 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 5 2 $software_2 . . 53296 5 3 $software_3 . . 53296 5 4 $software_4 . . 53296 5 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 18.59776853 0.324576143 . . . . . . . 53296 5 2 . 1 1 5 5 ALA N N 15 4.1836543 0.260804192 . . . . . . . 53296 5 3 . 1 1 7 7 GLU N N 15 4.900606713 0.263064844 . . . . . . . 53296 5 4 . 1 1 8 8 ASN N N 15 5.634898797 0.270169915 . . . . . . . 53296 5 5 . 1 1 9 9 ALA N N 15 5.490582882 0.230890484 . . . . . . . 53296 5 6 . 1 1 11 11 GLY N N 15 5.271310466 0.347976788 . . . . . . . 53296 5 7 . 1 1 12 12 LEU N N 15 6.302574207 0.162752831 . . . . . . . 53296 5 8 . 1 1 13 13 ASP N N 15 6.457239172 0.378920893 . . . . . . . 53296 5 9 . 1 1 17 17 ALA N N 15 7.134513675 0.246050139 . . . . . . . 53296 5 10 . 1 1 18 18 GLY N N 15 5.343941709 0.277825051 . . . . . . . 53296 5 11 . 1 1 20 20 ASP N N 15 5.975357137 0.157823449 . . . . . . . 53296 5 12 . 1 1 21 21 LEU N N 15 6.391723162 0.188798536 . . . . . . . 53296 5 13 . 1 1 22 22 ASN N N 15 6.510298124 0.222441773 . . . . . . . 53296 5 14 . 1 1 23 23 SER N N 15 6.900242861 0.229476368 . . . . . . . 53296 5 15 . 1 1 24 24 SER N N 15 7.187618686 0.311281051 . . . . . . . 53296 5 16 . 1 1 25 25 ASP N N 15 6.829359707 0.252488275 . . . . . . . 53296 5 17 . 1 1 26 26 ASN N N 15 6.101260267 0.270438172 . . . . . . . 53296 5 18 . 1 1 27 27 GLN N N 15 6.17986331 0.229865815 . . . . . . . 53296 5 19 . 1 1 29 29 GLY N N 15 5.934969999 0.354352538 . . . . . . . 53296 5 20 . 1 1 30 30 GLY N N 15 4.953247697 0.27316234 . . . . . . . 53296 5 21 . 1 1 31 31 SER N N 15 7.282964389 0.187264884 . . . . . . . 53296 5 22 . 1 1 32 32 THR N N 15 7.698673697 0.079652685 . . . . . . . 53296 5 23 . 1 1 33 33 ALA N N 15 7.062884511 0.25938495 . . . . . . . 53296 5 24 . 1 1 34 34 SER N N 15 7.189322129 0.282304212 . . . . . . . 53296 5 25 . 1 1 35 35 LYS N N 15 8.095951485 0.333848752 . . . . . . . 53296 5 26 . 1 1 36 36 GLY N N 15 6.943042017 0.498869154 . . . . . . . 53296 5 27 . 1 1 37 37 ARG N N 15 8.52118083 0.638986445 . . . . . . . 53296 5 28 . 1 1 38 38 TYR N N 15 9.727203298 0.312799988 . . . . . . . 53296 5 29 . 1 1 39 39 ILE N N 15 10.44535498 0.66756301 . . . . . . . 53296 5 30 . 1 1 43 43 LEU N N 15 15.94329441 0.256610043 . . . . . . . 53296 5 31 . 1 1 45 45 ASN N N 15 12.36452731 0.301069163 . . . . . . . 53296 5 32 . 1 1 47 47 GLU N N 15 10.53608046 0.354754652 . . . . . . . 53296 5 33 . 1 1 48 48 ALA N N 15 10.04532838 0.189972032 . . . . . . . 53296 5 34 . 1 1 49 49 THR N N 15 9.955774521 0.206593663 . . . . . . . 53296 5 35 . 1 1 50 50 LYS N N 15 9.717577082 0.197368321 . . . . . . . 53296 5 36 . 1 1 51 51 GLY N N 15 9.081847886 0.313039608 . . . . . . . 53296 5 37 . 1 1 52 52 PHE N N 15 10.16184153 0.215512569 . . . . . . . 53296 5 38 . 1 1 54 54 ASP N N 15 11.51257751 0.474135075 . . . . . . . 53296 5 39 . 1 1 57 57 SER N N 15 11.20453291 0.298046952 . . . . . . . 53296 5 40 . 1 1 58 58 SER N N 15 11.97202639 0.380848794 . . . . . . . 53296 5 41 . 1 1 59 59 GLY N N 15 10.89895275 0.353396702 . . . . . . . 53296 5 42 . 1 1 61 61 SER N N 15 11.39737004 0.20690327 . . . . . . . 53296 5 43 . 1 1 62 62 SER N N 15 11.85047728 0.25777276 . . . . . . . 53296 5 44 . 1 1 63 63 SER N N 15 13.31005403 0.414425698 . . . . . . . 53296 5 45 . 1 1 64 64 LYS N N 15 10.38804117 0.339743328 . . . . . . . 53296 5 46 . 1 1 66 66 LYS N N 15 10.23468133 0.277717335 . . . . . . . 53296 5 47 . 1 1 68 68 ALA N N 15 10.48319522 0.332371674 . . . . . . . 53296 5 48 . 1 1 69 69 TYR N N 15 10.14862294 0.236332499 . . . . . . . 53296 5 49 . 1 1 70 70 SER N N 15 10.08811349 0.306753654 . . . . . . . 53296 5 50 . 1 1 71 71 SER N N 15 11.47740689 0.221850885 . . . . . . . 53296 5 51 . 1 1 73 73 GLY N N 15 9.11548903 0.221741192 . . . . . . . 53296 5 52 . 1 1 74 74 SER N N 15 9.495021512 0.231561313 . . . . . . . 53296 5 53 . 1 1 78 78 SER N N 15 10.34441908 0.204747208 . . . . . . . 53296 5 54 . 1 1 82 82 SER N N 15 10.12581119 0.348119201 . . . . . . . 53296 5 55 . 1 1 83 83 SER N N 15 11.54686752 0.300952707 . . . . . . . 53296 5 56 . 1 1 85 85 PHE N N 15 10.63601197 0.205019875 . . . . . . . 53296 5 57 . 1 1 86 86 SER N N 15 9.973332203 0.461765326 . . . . . . . 53296 5 58 . 1 1 88 88 ARG N N 15 10.57498922 0.399994642 . . . . . . . 53296 5 59 . 1 1 89 89 GLY N N 15 9.22287256 0.47277746 . . . . . . . 53296 5 60 . 1 1 90 90 SER N N 15 11.11082495 0.362750535 . . . . . . . 53296 5 61 . 1 1 91 91 GLY N N 15 9.178124414 0.265943756 . . . . . . . 53296 5 62 . 1 1 92 92 SER N N 15 9.815467884 0.293990058 . . . . . . . 53296 5 63 . 1 1 94 94 GLY N N 15 8.839756863 0.271901881 . . . . . . . 53296 5 64 . 1 1 95 95 ARG N N 15 10.1655374 0.190913095 . . . . . . . 53296 5 65 . 1 1 96 96 PHE N N 15 11.23939754 0.202970867 . . . . . . . 53296 5 66 . 1 1 97 97 ASP N N 15 10.920901 0.255508387 . . . . . . . 53296 5 67 . 1 1 98 98 ASP N N 15 11.09356043 0.588643008 . . . . . . . 53296 5 68 . 1 1 100 100 GLY N N 15 10.67705899 0.344800306 . . . . . . . 53296 5 69 . 1 1 101 101 ARG N N 15 11.62909939 0.320239385 . . . . . . . 53296 5 70 . 1 1 102 102 SER N N 15 10.82160683 0.25850984 . . . . . . . 53296 5 71 . 1 1 104 104 TYR N N 15 10.94562973 0.366001153 . . . . . . . 53296 5 72 . 1 1 106 106 GLY N N 15 7.820792429 0.814264702 . . . . . . . 53296 5 73 . 1 1 107 107 ILE N N 15 10.11523232 0.457079103 . . . . . . . 53296 5 74 . 1 1 108 108 GLY N N 15 9.811131456 0.327833478 . . . . . . . 53296 5 75 . 1 1 109 109 SER N N 15 9.822653 0.473970123 . . . . . . . 53296 5 76 . 1 1 113 113 ARG N N 15 10.0199201 0.267891656 . . . . . . . 53296 5 77 . 1 1 115 115 GLY N N 15 9.622442369 0.49392065 . . . . . . . 53296 5 78 . 1 1 116 116 PHE N N 15 9.192394942 0.279174317 . . . . . . . 53296 5 79 . 1 1 117 117 GLY N N 15 7.916828798 0.428815445 . . . . . . . 53296 5 80 . 1 1 118 118 LYS N N 15 8.798456186 0.575852295 . . . . . . . 53296 5 81 . 1 1 120 120 GLU N N 15 8.476701024 0.327869828 . . . . . . . 53296 5 82 . 1 1 121 121 ARG N N 15 8.40035517 0.467704467 . . . . . . . 53296 5 83 . 1 1 122 122 GLY N N 15 7.961779339 0.62511783 . . . . . . . 53296 5 84 . 1 1 123 123 GLY N N 15 6.824098489 0.370661684 . . . . . . . 53296 5 85 . 1 1 124 124 ASN N N 15 8.220017676 0.658044507 . . . . . . . 53296 5 86 . 1 1 125 125 SER N N 15 9.722818746 0.282716024 . . . . . . . 53296 5 87 . 1 1 128 128 CYS N N 15 8.645891595 0.323915245 . . . . . . . 53296 5 88 . 1 1 129 129 ASP N N 15 7.024560614 0.176067802 . . . . . . . 53296 5 89 . 1 1 131 131 SER N N 15 5.048126876 0.16017218 . . . . . . . 53296 5 90 . 1 1 132 132 ASP N N 15 2.680869152 0.263082722 . . . . . . . 53296 5 stop_ save_ save_heteronucl_T2_relaxation_6 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_6 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 6 _Heteronucl_T2_list.Name '15N R2 u-2H,15N 300 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type N(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 15 'T1rho/R1rho relaxation' . . . 53296 6 16 'T1/R1 relaxation' . . . 53296 6 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 6 2 $software_2 . . 53296 6 3 $software_3 . . 53296 6 4 $software_4 . . 53296 6 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 2.894000759 0.151998724 . . . . . . . 53296 6 2 . 1 1 5 5 ALA N N 15 4.222389562 0.250917793 . . . . . . . 53296 6 3 . 1 1 7 7 GLU N N 15 4.717735943 0.132537783 . . . . . . . 53296 6 4 . 1 1 8 8 ASN N N 15 4.333701176 0.070061724 . . . . . . . 53296 6 5 . 1 1 9 9 ALA N N 15 4.958746433 0.15199934 . . . . . . . 53296 6 6 . 1 1 11 11 GLY N N 15 4.986709917 0.273912829 . . . . . . . 53296 6 7 . 1 1 12 12 LEU N N 15 5.733642627 0.244486303 . . . . . . . 53296 6 8 . 1 1 13 13 ASP N N 15 5.608573409 0.161989987 . . . . . . . 53296 6 9 . 1 1 17 17 ALA N N 15 6.347938005 0.203588471 . . . . . . . 53296 6 10 . 1 1 18 18 GLY N N 15 4.804874331 0.42623106 . . . . . . . 53296 6 11 . 1 1 20 20 ASP N N 15 5.671539431 0.156734545 . . . . . . . 53296 6 12 . 1 1 21 21 LEU N N 15 6.202787218 0.219534143 . . . . . . . 53296 6 13 . 1 1 22 22 ASN N N 15 5.988815101 0.153514448 . . . . . . . 53296 6 14 . 1 1 23 23 SER N N 15 5.056595751 0.315728953 . . . . . . . 53296 6 15 . 1 1 24 24 SER N N 15 5.352105122 0.11151644 . . . . . . . 53296 6 16 . 1 1 25 25 ASP N N 15 5.353367911 0.116926871 . . . . . . . 53296 6 17 . 1 1 26 26 ASN N N 15 4.669831813 0.19073098 . . . . . . . 53296 6 18 . 1 1 27 27 GLN N N 15 4.965086483 0.205234203 . . . . . . . 53296 6 19 . 1 1 29 29 GLY N N 15 4.231094204 0.137490108 . . . . . . . 53296 6 20 . 1 1 30 30 GLY N N 15 3.800729216 0.105908476 . . . . . . . 53296 6 21 . 1 1 31 31 SER N N 15 4.047255874 0.146357526 . . . . . . . 53296 6 22 . 1 1 32 32 THR N N 15 4.672069529 0.091551155 . . . . . . . 53296 6 23 . 1 1 33 33 ALA N N 15 5.368285333 0.144530963 . . . . . . . 53296 6 24 . 1 1 34 34 SER N N 15 5.214845723 0.176020543 . . . . . . . 53296 6 25 . 1 1 35 35 LYS N N 15 6.1176741 0.2820789 1 . 1 1 . . . 53296 6 26 . 1 1 36 36 GLY N N 15 5.425931069 0.352113304 . . . . . . . 53296 6 27 . 1 1 37 37 ARG N N 15 7.872079256 0.366414671 . . . . . . . 53296 6 28 . 1 1 38 38 TYR N N 15 9.819109182 0.128060379 . . . . . . . 53296 6 29 . 1 1 39 39 ILE N N 15 12.02343251 0.314150673 . . . . . . . 53296 6 30 . 1 1 43 43 LEU N N 15 14.17712592 0.115785284 . . . . . . . 53296 6 31 . 1 1 45 45 ASN N N 15 10.67045899 0.261562993 . . . . . . . 53296 6 32 . 1 1 47 47 GLU N N 15 10.42501308 0.177561432 . . . . . . . 53296 6 33 . 1 1 48 48 ALA N N 15 9.557065537 0.304005047 . . . . . . . 53296 6 34 . 1 1 49 49 THR N N 15 9.429238378 0.395104953 . . . . . . . 53296 6 35 . 1 1 50 50 LYS N N 15 9.493213679 0.142868006 . . . . . . . 53296 6 36 . 1 1 51 51 GLY N N 15 8.978363857 0.169894616 . . . . . . . 53296 6 37 . 1 1 52 52 PHE N N 15 10.1322861 0.253421594 . . . . . . . 53296 6 38 . 1 1 54 54 ASP N N 15 11.4719339 0.121714632 . . . . . . . 53296 6 39 . 1 1 57 57 SER N N 15 9.314930629 0.324308502 . . . . . . . 53296 6 40 . 1 1 58 58 SER N N 15 9.041431761 0.339668204 . . . . . . . 53296 6 41 . 1 1 59 59 GLY N N 15 9.206558604 0.433093858 . . . . . . . 53296 6 42 . 1 1 61 61 SER N N 15 10.28934327 0.143723716 . . . . . . . 53296 6 43 . 1 1 62 62 SER N N 15 9.693355783 0.1665269 1 . 1 1 . . . 53296 6 44 . 1 1 63 63 SER N N 15 9.612043255 0.180437749 . . . . . . . 53296 6 45 . 1 1 64 64 LYS N N 15 9.78719351 0.341683087 . . . . . . . 53296 6 46 . 1 1 66 66 LYS N N 15 9.796983688 0.339566585 . . . . . . . 53296 6 47 . 1 1 68 68 ALA N N 15 10.24969405 0.218033651 . . . . . . . 53296 6 48 . 1 1 69 69 TYR N N 15 10.22739647 0.200617755 . . . . . . . 53296 6 49 . 1 1 70 70 SER N N 15 9.82395436 0.200572883 . . . . . . . 53296 6 50 . 1 1 71 71 SER N N 15 9.594751079 0.211716798 . . . . . . . 53296 6 51 . 1 1 73 73 GLY N N 15 8.509481777 0.256993906 . . . . . . . 53296 6 52 . 1 1 74 74 SER N N 15 8.203742433 0.224156825 . . . . . . . 53296 6 53 . 1 1 78 78 SER N N 15 8.358673628 0.120442979 . . . . . . . 53296 6 54 . 1 1 82 82 SER N N 15 7.83569018 0.098437698 . . . . . . . 53296 6 55 . 1 1 83 83 SER N N 15 8.735054936 0.27393231 . . . . . . . 53296 6 56 . 1 1 85 85 PHE N N 15 10.34080513 0.110987325 . . . . . . . 53296 6 57 . 1 1 86 86 SER N N 15 9.503971896 0.228530383 . . . . . . . 53296 6 58 . 1 1 88 88 ARG N N 15 10.05101158 0.271291138 . . . . . . . 53296 6 59 . 1 1 89 89 GLY N N 15 7.879049628 0.182185809 . . . . . . . 53296 6 60 . 1 1 90 90 SER N N 15 8.441099291 0.162113103 . . . . . . . 53296 6 61 . 1 1 91 91 GLY N N 15 7.5717393 0.136630719 . . . . . . . 53296 6 62 . 1 1 92 92 SER N N 15 7.642770013 0.28112496 . . . . . . . 53296 6 63 . 1 1 94 94 GLY N N 15 9.316239298 0.333960161 . . . . . . . 53296 6 64 . 1 1 95 95 ARG N N 15 10.38002923 0.349092515 . . . . . . . 53296 6 65 . 1 1 96 96 PHE N N 15 10.80348008 0.152299732 . . . . . . . 53296 6 66 . 1 1 97 97 ASP N N 15 11.59117585 0.225275973 . . . . . . . 53296 6 67 . 1 1 98 98 ASP N N 15 11.62453606 0.31724193 . . . . . . . 53296 6 68 . 1 1 100 100 GLY N N 15 10.65558977 0.487030825 . . . . . . . 53296 6 69 . 1 1 101 101 ARG N N 15 11.24476808 0.310261361 . . . . . . . 53296 6 70 . 1 1 102 102 SER N N 15 10.14058218 0.160774895 . . . . . . . 53296 6 71 . 1 1 104 104 TYR N N 15 10.71482151 0.145711328 . . . . . . . 53296 6 72 . 1 1 106 106 GLY N N 15 8.653523362 0.272530946 . . . . . . . 53296 6 73 . 1 1 107 107 ILE N N 15 10.49544628 0.306441408 . . . . . . . 53296 6 74 . 1 1 108 108 GLY N N 15 9.694014943 0.265920964 . . . . . . . 53296 6 75 . 1 1 109 109 SER N N 15 8.723345958 0.253569928 . . . . . . . 53296 6 76 . 1 1 113 113 ARG N N 15 9.425807763 0.253982235 . . . . . . . 53296 6 77 . 1 1 115 115 GLY N N 15 8.623327216 0.192772968 . . . . . . . 53296 6 78 . 1 1 116 116 PHE N N 15 8.976743423 0.070720897 . . . . . . . 53296 6 79 . 1 1 117 117 GLY N N 15 8.56639446 0.315286936 . . . . . . . 53296 6 80 . 1 1 118 118 LYS N N 15 9.201292449 0.241521028 . . . . . . . 53296 6 81 . 1 1 120 120 GLU N N 15 9.241444776 0.170856315 . . . . . . . 53296 6 82 . 1 1 121 121 ARG N N 15 8.475664488 0.308015912 . . . . . . . 53296 6 83 . 1 1 122 122 GLY N N 15 7.355004794 0.438731665 . . . . . . . 53296 6 84 . 1 1 123 123 GLY N N 15 5.975531002 0.283324383 . . . . . . . 53296 6 85 . 1 1 124 124 ASN N N 15 6.996660547 0.093107915 . . . . . . . 53296 6 86 . 1 1 125 125 SER N N 15 7.746858657 0.226230421 . . . . . . . 53296 6 87 . 1 1 128 128 CYS N N 15 8.337088989 0.074800893 . . . . . . . 53296 6 88 . 1 1 129 129 ASP N N 15 6.800505048 0.281210362 . . . . . . . 53296 6 89 . 1 1 131 131 SER N N 15 3.928657746 0.094450969 . . . . . . . 53296 6 90 . 1 1 132 132 ASP N N 15 3.087490986 0.253398475 . . . . . . . 53296 6 stop_ save_ save_heteronucl_T2_relaxation_7 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_7 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 7 _Heteronucl_T2_list.Name 'HxNx u-2H,15N 300 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HxNx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 11 'T1rho/R1rho relaxation HxNx' . . . 53296 7 12 'T1rho/R1rho relaxation HxNz' . . . 53296 7 13 'T1rho/R1rho relaxation HzNx' . . . 53296 7 14 'T1/R1 relaxation HzNz' . . . 53296 7 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 7 2 $software_2 . . 53296 7 3 $software_3 . . 53296 7 4 $software_4 . . 53296 7 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 19.42020082 0.217095219 . . . . . . . 53296 7 2 . 1 1 5 5 ALA N N 15 5.178391325 0.207233253 . . . . . . . 53296 7 3 . 1 1 7 7 GLU N N 15 5.856250152 0.111489834 . . . . . . . 53296 7 4 . 1 1 8 8 ASN N N 15 6.870391204 0.175204322 . . . . . . . 53296 7 5 . 1 1 9 9 ALA N N 15 6.17337456 0.1251554 . . . . . . . 53296 7 6 . 1 1 11 11 GLY N N 15 6.591651075 0.175353165 . . . . . . . 53296 7 7 . 1 1 12 12 LEU N N 15 6.895627945 0.233860882 . . . . . . . 53296 7 8 . 1 1 13 13 ASP N N 15 7.132723417 0.174258212 . . . . . . . 53296 7 9 . 1 1 17 17 ALA N N 15 7.660916749 0.210750622 . . . . . . . 53296 7 10 . 1 1 18 18 GLY N N 15 7.744953431 0.221500107 . . . . . . . 53296 7 11 . 1 1 20 20 ASP N N 15 7.172636806 0.089228434 . . . . . . . 53296 7 12 . 1 1 21 21 LEU N N 15 7.455066718 0.068050806 . . . . . . . 53296 7 13 . 1 1 22 22 ASN N N 15 7.686951388 0.1163001 . . . . . . . 53296 7 14 . 1 1 23 23 SER N N 15 8.735584994 0.303292611 . . . . . . . 53296 7 15 . 1 1 24 24 SER N N 15 8.150479561 0.141579148 . . . . . . . 53296 7 16 . 1 1 25 25 ASP N N 15 7.174530933 0.092183822 . . . . . . . 53296 7 17 . 1 1 26 26 ASN N N 15 7.254221603 0.238207834 . . . . . . . 53296 7 18 . 1 1 27 27 GLN N N 15 7.307443969 0.21339156 . . . . . . . 53296 7 19 . 1 1 29 29 GLY N N 15 6.651572809 0.345946717 . . . . . . . 53296 7 20 . 1 1 30 30 GLY N N 15 5.547877587 0.177518033 . . . . . . . 53296 7 21 . 1 1 31 31 SER N N 15 7.858834721 0.148199991 . . . . . . . 53296 7 22 . 1 1 32 32 THR N N 15 8.762663959 0.261964319 . . . . . . . 53296 7 23 . 1 1 33 33 ALA N N 15 7.698060069 0.210114589 . . . . . . . 53296 7 24 . 1 1 34 34 SER N N 15 8.004605463 0.214068049 . . . . . . . 53296 7 25 . 1 1 35 35 LYS N N 15 8.758939928 0.287147626 . . . . . . . 53296 7 26 . 1 1 36 36 GLY N N 15 7.407609576 0.306932576 . . . . . . . 53296 7 27 . 1 1 37 37 ARG N N 15 9.185578078 0.343737716 . . . . . . . 53296 7 28 . 1 1 38 38 TYR N N 15 11.01162992 0.100619584 . . . . . . . 53296 7 29 . 1 1 39 39 ILE N N 15 11.12179157 0.188865406 . . . . . . . 53296 7 30 . 1 1 43 43 LEU N N 15 31.35689036 0.560783023 . . . . . . . 53296 7 31 . 1 1 45 45 ASN N N 15 14.85366881 0.140177913 . . . . . . . 53296 7 32 . 1 1 47 47 GLU N N 15 11.9880402 0.191487847 . . . . . . . 53296 7 33 . 1 1 48 48 ALA N N 15 12.01933083 0.236878289 . . . . . . . 53296 7 34 . 1 1 49 49 THR N N 15 12.53123673 0.144764184 . . . . . . . 53296 7 35 . 1 1 50 50 LYS N N 15 12.92407057 0.262847691 . . . . . . . 53296 7 36 . 1 1 51 51 GLY N N 15 12.45088785 0.222922574 . . . . . . . 53296 7 37 . 1 1 52 52 PHE N N 15 12.52570663 0.301916644 . . . . . . . 53296 7 38 . 1 1 54 54 ASP N N 15 14.62948034 0.205199311 . . . . . . . 53296 7 39 . 1 1 57 57 SER N N 15 14.80586737 0.301326565 . . . . . . . 53296 7 40 . 1 1 58 58 SER N N 15 14.79170422 0.294412312 . . . . . . . 53296 7 41 . 1 1 59 59 GLY N N 15 14.47520569 0.231476537 . . . . . . . 53296 7 42 . 1 1 61 61 SER N N 15 16.35021311 0.114236828 . . . . . . . 53296 7 43 . 1 1 62 62 SER N N 15 14.5687125 0.115255891 . . . . . . . 53296 7 44 . 1 1 63 63 SER N N 15 16.00539821 0.280448331 . . . . . . . 53296 7 45 . 1 1 64 64 LYS N N 15 13.82501651 0.174975493 . . . . . . . 53296 7 46 . 1 1 66 66 LYS N N 15 12.76866264 0.45152076 . . . . . . . 53296 7 47 . 1 1 68 68 ALA N N 15 12.76913551 0.163752916 . . . . . . . 53296 7 48 . 1 1 69 69 TYR N N 15 12.64172247 0.139358808 . . . . . . . 53296 7 49 . 1 1 70 70 SER N N 15 13.00622623 0.321971711 . . . . . . . 53296 7 50 . 1 1 71 71 SER N N 15 15.10890785 0.148763233 . . . . . . . 53296 7 51 . 1 1 73 73 GLY N N 15 11.36436017 0.275816149 . . . . . . . 53296 7 52 . 1 1 74 74 SER N N 15 11.3891349 0.18066861 . . . . . . . 53296 7 53 . 1 1 78 78 SER N N 15 12.5482948 0.186167342 . . . . . . . 53296 7 54 . 1 1 82 82 SER N N 15 11.82505924 0.238721061 . . . . . . . 53296 7 55 . 1 1 83 83 SER N N 15 14.39713805 0.22725274 . . . . . . . 53296 7 56 . 1 1 85 85 PHE N N 15 13.66761001 0.060180265 . . . . . . . 53296 7 57 . 1 1 86 86 SER N N 15 12.92485404 0.231028514 . . . . . . . 53296 7 58 . 1 1 88 88 ARG N N 15 12.77773962 0.409551761 . . . . . . . 53296 7 59 . 1 1 89 89 GLY N N 15 11.68917553 0.331920058 . . . . . . . 53296 7 60 . 1 1 90 90 SER N N 15 12.86264014 0.268629002 . . . . . . . 53296 7 61 . 1 1 91 91 GLY N N 15 11.40488209 0.117759117 . . . . . . . 53296 7 62 . 1 1 92 92 SER N N 15 11.18921406 0.210453259 . . . . . . . 53296 7 63 . 1 1 94 94 GLY N N 15 12.8714445 0.369859875 . . . . . . . 53296 7 64 . 1 1 95 95 ARG N N 15 12.41814327 0.14885064 . . . . . . . 53296 7 65 . 1 1 96 96 PHE N N 15 14.13770004 0.203262768 . . . . . . . 53296 7 66 . 1 1 97 97 ASP N N 15 15.02395782 0.148121616 . . . . . . . 53296 7 67 . 1 1 98 98 ASP N N 15 13.88917112 0.16011568 . . . . . . . 53296 7 68 . 1 1 100 100 GLY N N 15 13.04449065 0.280129891 . . . . . . . 53296 7 69 . 1 1 101 101 ARG N N 15 13.85692348 0.284583548 . . . . . . . 53296 7 70 . 1 1 102 102 SER N N 15 14.23068772 0.081837416 . . . . . . . 53296 7 71 . 1 1 104 104 TYR N N 15 14.16150607 0.254247179 . . . . . . . 53296 7 72 . 1 1 106 106 GLY N N 15 23.8758919 0.561555739 . . . . . . . 53296 7 73 . 1 1 107 107 ILE N N 15 12.25286385 0.312854145 . . . . . . . 53296 7 74 . 1 1 108 108 GLY N N 15 13.03374781 0.156078261 . . . . . . . 53296 7 75 . 1 1 109 109 SER N N 15 13.40103992 0.242678611 . . . . . . . 53296 7 76 . 1 1 113 113 ARG N N 15 12.32487994 0.216666992 . . . . . . . 53296 7 77 . 1 1 115 115 GLY N N 15 12.23929012 0.132771393 . . . . . . . 53296 7 78 . 1 1 116 116 PHE N N 15 11.46546032 0.159648163 . . . . . . . 53296 7 79 . 1 1 117 117 GLY N N 15 10.98050509 0.3811932 . . . . . . . 53296 7 80 . 1 1 118 118 LYS N N 15 11.13592776 0.092157409 . . . . . . . 53296 7 81 . 1 1 120 120 GLU N N 15 11.62593277 0.145838863 . . . . . . . 53296 7 82 . 1 1 121 121 ARG N N 15 11.20356798 0.183800984 . . . . . . . 53296 7 83 . 1 1 122 122 GLY N N 15 10.32757641 0.23260969 . . . . . . . 53296 7 84 . 1 1 123 123 GLY N N 15 9.397700943 0.245148108 . . . . . . . 53296 7 85 . 1 1 124 124 ASN N N 15 10.64366432 0.215942644 . . . . . . . 53296 7 86 . 1 1 125 125 SER N N 15 10.98760533 0.218881985 . . . . . . . 53296 7 87 . 1 1 128 128 CYS N N 15 12.13172534 0.22922374 . . . . . . . 53296 7 88 . 1 1 129 129 ASP N N 15 9.387986914 0.15981468 . . . . . . . 53296 7 89 . 1 1 131 131 SER N N 15 5.844791789 0.12597822 . . . . . . . 53296 7 90 . 1 1 132 132 ASP N N 15 3.126799529 0.179502637 . . . . . . . 53296 7 stop_ save_ save_heteronucl_T2_relaxation_8 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_8 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 8 _Heteronucl_T2_list.Name 'HxNz u-2H,15N 300 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HxNz _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 11 'T1rho/R1rho relaxation HxNx' . . . 53296 8 12 'T1rho/R1rho relaxation HxNz' . . . 53296 8 13 'T1rho/R1rho relaxation HzNx' . . . 53296 8 14 'T1/R1 relaxation HzNz' . . . 53296 8 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 8 2 $software_2 . . 53296 8 3 $software_3 . . 53296 8 4 $software_4 . . 53296 8 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS H H 1 18.93983517 0.217280101 . . . . . . . 53296 8 2 . 1 1 5 5 ALA H H 1 4.289336008 0.136959347 . . . . . . . 53296 8 3 . 1 1 7 7 GLU H H 1 5.189457683 0.122604802 . . . . . . . 53296 8 4 . 1 1 8 8 ASN H H 1 5.874994474 0.101690279 . . . . . . . 53296 8 5 . 1 1 9 9 ALA H H 1 6.101565229 0.167621218 . . . . . . . 53296 8 6 . 1 1 11 11 GLY H H 1 6.1561707 0.120399991 . . . . . . . 53296 8 7 . 1 1 12 12 LEU H H 1 6.509148156 0.181373399 . . . . . . . 53296 8 8 . 1 1 13 13 ASP H H 1 6.35452994 0.111534212 . . . . . . . 53296 8 9 . 1 1 17 17 ALA H H 1 7.304290024 0.058401394 . . . . . . . 53296 8 10 . 1 1 18 18 GLY H H 1 7.741484058 0.049869642 . . . . . . . 53296 8 11 . 1 1 20 20 ASP H H 1 5.917381107 0.204573897 . . . . . . . 53296 8 12 . 1 1 21 21 LEU H H 1 6.644506767 0.196178211 . . . . . . . 53296 8 13 . 1 1 22 22 ASN H H 1 6.987979969 0.210974679 . . . . . . . 53296 8 14 . 1 1 23 23 SER H H 1 7.186004557 0.410512175 . . . . . . . 53296 8 15 . 1 1 24 24 SER H H 1 7.877372231 0.179957393 . . . . . . . 53296 8 16 . 1 1 25 25 ASP H H 1 6.359831263 0.272284828 . . . . . . . 53296 8 17 . 1 1 26 26 ASN H H 1 6.750755705 0.185665334 . . . . . . . 53296 8 18 . 1 1 27 27 GLN H H 1 6.806855379 0.21783766 . . . . . . . 53296 8 19 . 1 1 29 29 GLY H H 1 6.422021019 0.324583801 . . . . . . . 53296 8 20 . 1 1 30 30 GLY H H 1 5.894877834 0.055230366 . . . . . . . 53296 8 21 . 1 1 31 31 SER H H 1 7.198076681 0.20734014 . . . . . . . 53296 8 22 . 1 1 32 32 THR H H 1 7.877951932 0.325580544 . . . . . . . 53296 8 23 . 1 1 33 33 ALA H H 1 6.803127041 0.211653277 . . . . . . . 53296 8 24 . 1 1 34 34 SER H H 1 7.605861152 0.192479558 . . . . . . . 53296 8 25 . 1 1 35 35 LYS H H 1 7.959442394 0.176172203 . . . . . . . 53296 8 26 . 1 1 36 36 GLY H H 1 7.333853213 0.213630014 . . . . . . . 53296 8 27 . 1 1 37 37 ARG H H 1 8.813376516 0.366614267 . . . . . . . 53296 8 28 . 1 1 38 38 TYR H H 1 9.630396855 0.252659791 . . . . . . . 53296 8 29 . 1 1 39 39 ILE H H 1 9.844960193 0.163292213 . . . . . . . 53296 8 30 . 1 1 43 43 LEU H H 1 27.27479652 0.431167084 . . . . . . . 53296 8 31 . 1 1 45 45 ASN H H 1 13.31960291 0.214436209 . . . . . . . 53296 8 32 . 1 1 47 47 GLU H H 1 10.58344823 0.166053472 . . . . . . . 53296 8 33 . 1 1 48 48 ALA H H 1 10.64496415 0.223914988 . . . . . . . 53296 8 34 . 1 1 49 49 THR H H 1 11.27881212 0.302196474 . . . . . . . 53296 8 35 . 1 1 50 50 LYS H H 1 11.34778454 0.301061985 . . . . . . . 53296 8 36 . 1 1 51 51 GLY H H 1 11.92060442 0.215934267 . . . . . . . 53296 8 37 . 1 1 52 52 PHE H H 1 11.19206881 0.358074569 . . . . . . . 53296 8 38 . 1 1 54 54 ASP H H 1 12.61979582 0.214817894 . . . . . . . 53296 8 39 . 1 1 57 57 SER H H 1 13.56201502 0.287277854 . . . . . . . 53296 8 40 . 1 1 58 58 SER H H 1 14.16375334 0.228696642 . . . . . . . 53296 8 41 . 1 1 59 59 GLY H H 1 13.49619364 0.238260515 . . . . . . . 53296 8 42 . 1 1 61 61 SER H H 1 15.93611751 0.214588939 . . . . . . . 53296 8 43 . 1 1 62 62 SER H H 1 13.36538124 0.250461767 . . . . . . . 53296 8 44 . 1 1 63 63 SER H H 1 14.91369115 0.422949841 . . . . . . . 53296 8 45 . 1 1 64 64 LYS H H 1 12.67176136 0.231540257 . . . . . . . 53296 8 46 . 1 1 66 66 LYS H H 1 11.58502535 0.450044905 . . . . . . . 53296 8 47 . 1 1 68 68 ALA H H 1 12.15743738 0.153742104 . . . . . . . 53296 8 48 . 1 1 69 69 TYR H H 1 11.31302644 0.241706892 . . . . . . . 53296 8 49 . 1 1 70 70 SER H H 1 12.02721911 0.113590726 . . . . . . . 53296 8 50 . 1 1 71 71 SER H H 1 13.23477779 0.195421377 . . . . . . . 53296 8 51 . 1 1 73 73 GLY H H 1 10.86105263 0.195965785 . . . . . . . 53296 8 52 . 1 1 74 74 SER H H 1 10.64955535 0.187949009 . . . . . . . 53296 8 53 . 1 1 78 78 SER H H 1 11.48910949 0.238434796 . . . . . . . 53296 8 54 . 1 1 82 82 SER H H 1 11.16083846 0.271064822 . . . . . . . 53296 8 55 . 1 1 83 83 SER H H 1 13.6006911 0.32506377 . . . . . . . 53296 8 56 . 1 1 85 85 PHE H H 1 12.11152606 0.227032953 . . . . . . . 53296 8 57 . 1 1 86 86 SER H H 1 11.8680066 0.229033462 . . . . . . . 53296 8 58 . 1 1 88 88 ARG H H 1 11.76480683 0.327908745 . . . . . . . 53296 8 59 . 1 1 89 89 GLY H H 1 10.29417043 0.299534955 . . . . . . . 53296 8 60 . 1 1 90 90 SER H H 1 11.73191641 0.280349263 . . . . . . . 53296 8 61 . 1 1 91 91 GLY H H 1 10.81358409 0.140702266 . . . . . . . 53296 8 62 . 1 1 92 92 SER H H 1 10.32523901 0.337381317 . . . . . . . 53296 8 63 . 1 1 94 94 GLY H H 1 11.51699039 0.090524715 . . . . . . . 53296 8 64 . 1 1 95 95 ARG H H 1 11.47136813 0.239474245 . . . . . . . 53296 8 65 . 1 1 96 96 PHE H H 1 12.01017459 0.144159806 . . . . . . . 53296 8 66 . 1 1 97 97 ASP H H 1 12.72624719 0.326846495 . . . . . . . 53296 8 67 . 1 1 98 98 ASP H H 1 12.4515894 0.266327199 . . . . . . . 53296 8 68 . 1 1 100 100 GLY H H 1 12.80533963 0.301453524 . . . . . . . 53296 8 69 . 1 1 101 101 ARG H H 1 12.9302313 0.449636789 . . . . . . . 53296 8 70 . 1 1 102 102 SER H H 1 12.75711562 0.174464916 . . . . . . . 53296 8 71 . 1 1 104 104 TYR H H 1 12.57632408 0.440108122 . . . . . . . 53296 8 72 . 1 1 106 106 GLY H H 1 22.09432632 0.346283953 . . . . . . . 53296 8 73 . 1 1 107 107 ILE H H 1 10.76328808 0.31538938 . . . . . . . 53296 8 74 . 1 1 108 108 GLY H H 1 12.11063175 0.262119524 . . . . . . . 53296 8 75 . 1 1 109 109 SER H H 1 12.09052039 0.272923464 . . . . . . . 53296 8 76 . 1 1 113 113 ARG H H 1 11.35408438 0.241026276 . . . . . . . 53296 8 77 . 1 1 115 115 GLY H H 1 11.8172535 0.165742328 . . . . . . . 53296 8 78 . 1 1 116 116 PHE H H 1 10.45778226 0.147001445 . . . . . . . 53296 8 79 . 1 1 117 117 GLY H H 1 10.7946477 0.296915874 . . . . . . . 53296 8 80 . 1 1 118 118 LYS H H 1 10.4832204 0.358062547 . . . . . . . 53296 8 81 . 1 1 120 120 GLU H H 1 10.57826745 0.141710127 . . . . . . . 53296 8 82 . 1 1 121 121 ARG H H 1 9.652043043 0.204797483 . . . . . . . 53296 8 83 . 1 1 122 122 GLY H H 1 9.581857557 0.244470355 . . . . . . . 53296 8 84 . 1 1 123 123 GLY H H 1 8.619762742 0.249686685 . . . . . . . 53296 8 85 . 1 1 124 124 ASN H H 1 10.24735685 0.204013085 . . . . . . . 53296 8 86 . 1 1 125 125 SER H H 1 10.51230283 0.289959448 . . . . . . . 53296 8 87 . 1 1 128 128 CYS H H 1 10.31980758 0.152557004 . . . . . . . 53296 8 88 . 1 1 129 129 ASP H H 1 8.660077969 0.151063831 . . . . . . . 53296 8 89 . 1 1 131 131 SER H H 1 5.38876559 0.220488888 . . . . . . . 53296 8 90 . 1 1 132 132 ASP H H 1 2.896853642 0.16768629 . . . . . . . 53296 8 stop_ save_ save_heteronucl_T2_relaxation_9 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_9 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 9 _Heteronucl_T2_list.Name 'HzNx u-2H,15N 300 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HzNx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 11 'T1rho/R1rho relaxation HxNx' . . . 53296 9 12 'T1rho/R1rho relaxation HxNz' . . . 53296 9 13 'T1rho/R1rho relaxation HzNx' . . . 53296 9 14 'T1/R1 relaxation HzNz' . . . 53296 9 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 9 2 $software_2 . . 53296 9 3 $software_3 . . 53296 9 4 $software_4 . . 53296 9 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 19.05614011 0.138528498 . . . . . . . 53296 9 2 . 1 1 5 5 ALA N N 15 4.802029771 0.195178468 . . . . . . . 53296 9 3 . 1 1 7 7 GLU N N 15 5.531272378 0.093814128 . . . . . . . 53296 9 4 . 1 1 8 8 ASN N N 15 5.781479377 0.094910494 . . . . . . . 53296 9 5 . 1 1 9 9 ALA N N 15 5.639202705 0.165299747 . . . . . . . 53296 9 6 . 1 1 11 11 GLY N N 15 5.374260655 0.233445238 . . . . . . . 53296 9 7 . 1 1 12 12 LEU N N 15 6.736298543 0.224622653 . . . . . . . 53296 9 8 . 1 1 13 13 ASP N N 15 6.737503856 0.221463612 . . . . . . . 53296 9 9 . 1 1 17 17 ALA N N 15 7.360717798 0.083252295 . . . . . . . 53296 9 10 . 1 1 18 18 GLY N N 15 6.062548845 0.231099034 . . . . . . . 53296 9 11 . 1 1 20 20 ASP N N 15 6.567562196 0.157385711 . . . . . . . 53296 9 12 . 1 1 21 21 LEU N N 15 6.831269219 0.054288855 . . . . . . . 53296 9 13 . 1 1 22 22 ASN N N 15 7.175797709 0.060647571 . . . . . . . 53296 9 14 . 1 1 23 23 SER N N 15 7.616384461 0.23896976 . . . . . . . 53296 9 15 . 1 1 24 24 SER N N 15 7.853395347 0.091857456 . . . . . . . 53296 9 16 . 1 1 25 25 ASP N N 15 7.086619588 0.140660295 . . . . . . . 53296 9 17 . 1 1 26 26 ASN N N 15 6.759380609 0.120106027 . . . . . . . 53296 9 18 . 1 1 27 27 GLN N N 15 6.72734143 0.093640335 . . . . . . . 53296 9 19 . 1 1 29 29 GLY N N 15 6.351653873 0.145596523 . . . . . . . 53296 9 20 . 1 1 30 30 GLY N N 15 4.958223284 0.141397096 . . . . . . . 53296 9 21 . 1 1 31 31 SER N N 15 7.448758863 0.199586144 . . . . . . . 53296 9 22 . 1 1 32 32 THR N N 15 8.335949004 0.140426901 . . . . . . . 53296 9 23 . 1 1 33 33 ALA N N 15 7.524663799 0.142230485 . . . . . . . 53296 9 24 . 1 1 34 34 SER N N 15 7.631742923 0.177569966 . . . . . . . 53296 9 25 . 1 1 35 35 LYS N N 15 8.322698351 0.181190525 . . . . . . . 53296 9 26 . 1 1 36 36 GLY N N 15 7.24605859 0.326603295 . . . . . . . 53296 9 27 . 1 1 37 37 ARG N N 15 9.253883542 0.153619633 . . . . . . . 53296 9 28 . 1 1 38 38 TYR N N 15 11.13181607 0.261001857 . . . . . . . 53296 9 29 . 1 1 39 39 ILE N N 15 12.43008948 0.174836566 . . . . . . . 53296 9 30 . 1 1 43 43 LEU N N 15 17.97170492 0.309342588 . . . . . . . 53296 9 31 . 1 1 45 45 ASN N N 15 13.55635586 0.316101799 . . . . . . . 53296 9 32 . 1 1 47 47 GLU N N 15 11.94695471 0.119125095 . . . . . . . 53296 9 33 . 1 1 48 48 ALA N N 15 11.33966978 0.145255896 . . . . . . . 53296 9 34 . 1 1 49 49 THR N N 15 11.09750866 0.319893209 . . . . . . . 53296 9 35 . 1 1 50 50 LYS N N 15 11.71539453 0.180492063 . . . . . . . 53296 9 36 . 1 1 51 51 GLY N N 15 10.48836512 0.220376744 . . . . . . . 53296 9 37 . 1 1 52 52 PHE N N 15 11.58080511 0.160394888 . . . . . . . 53296 9 38 . 1 1 54 54 ASP N N 15 12.76405682 0.190376168 . . . . . . . 53296 9 39 . 1 1 57 57 SER N N 15 12.48710256 0.237062413 . . . . . . . 53296 9 40 . 1 1 58 58 SER N N 15 13.68896221 0.117663498 . . . . . . . 53296 9 41 . 1 1 59 59 GLY N N 15 11.44134247 0.327169609 . . . . . . . 53296 9 42 . 1 1 61 61 SER N N 15 12.47297312 0.205374079 . . . . . . . 53296 9 43 . 1 1 62 62 SER N N 15 13.31461124 0.199551083 . . . . . . . 53296 9 44 . 1 1 63 63 SER N N 15 14.37883899 0.138071014 . . . . . . . 53296 9 45 . 1 1 64 64 LYS N N 15 12.33980267 0.153216902 . . . . . . . 53296 9 46 . 1 1 66 66 LYS N N 15 11.7266704 0.247809546 . . . . . . . 53296 9 47 . 1 1 68 68 ALA N N 15 12.05388431 0.077224406 . . . . . . . 53296 9 48 . 1 1 69 69 TYR N N 15 12.13558252 0.092341247 . . . . . . . 53296 9 49 . 1 1 70 70 SER N N 15 12.18361124 0.174137652 . . . . . . . 53296 9 50 . 1 1 71 71 SER N N 15 13.26551419 0.049987106 . . . . . . . 53296 9 51 . 1 1 73 73 GLY N N 15 10.28535398 0.172071326 . . . . . . . 53296 9 52 . 1 1 74 74 SER N N 15 10.95909042 0.168522585 . . . . . . . 53296 9 53 . 1 1 78 78 SER N N 15 11.37223944 0.09895992 . . . . . . . 53296 9 54 . 1 1 82 82 SER N N 15 11.5861962 0.145491474 . . . . . . . 53296 9 55 . 1 1 83 83 SER N N 15 13.13462265 0.215119636 . . . . . . . 53296 9 56 . 1 1 85 85 PHE N N 15 12.66347224 0.100809698 . . . . . . . 53296 9 57 . 1 1 86 86 SER N N 15 12.21467467 0.192584371 . . . . . . . 53296 9 58 . 1 1 88 88 ARG N N 15 11.59402183 0.153601286 . . . . . . . 53296 9 59 . 1 1 89 89 GLY N N 15 10.06280582 0.258803731 . . . . . . . 53296 9 60 . 1 1 90 90 SER N N 15 12.02004647 0.218985542 . . . . . . . 53296 9 61 . 1 1 91 91 GLY N N 15 10.49471534 0.111497292 . . . . . . . 53296 9 62 . 1 1 92 92 SER N N 15 11.16880632 0.155849054 . . . . . . . 53296 9 63 . 1 1 94 94 GLY N N 15 10.53530442 0.282519681 . . . . . . . 53296 9 64 . 1 1 95 95 ARG N N 15 11.91384233 0.276731024 . . . . . . . 53296 9 65 . 1 1 96 96 PHE N N 15 12.91286535 0.178285056 . . . . . . . 53296 9 66 . 1 1 97 97 ASP N N 15 13.04484773 0.086844906 . . . . . . . 53296 9 67 . 1 1 98 98 ASP N N 15 12.95892543 0.1384318 1 . 1 1 . . . 53296 9 68 . 1 1 100 100 GLY N N 15 11.98639261 0.399758278 . . . . . . . 53296 9 69 . 1 1 101 101 ARG N N 15 12.61979786 0.30033012 . . . . . . . 53296 9 70 . 1 1 102 102 SER N N 15 12.71568845 0.155862024 . . . . . . . 53296 9 71 . 1 1 104 104 TYR N N 15 12.81550687 0.292296931 . . . . . . . 53296 9 72 . 1 1 106 106 GLY N N 15 10.98367201 0.344843273 . . . . . . . 53296 9 73 . 1 1 107 107 ILE N N 15 11.934553 0.155795485 . . . . . . . 53296 9 74 . 1 1 108 108 GLY N N 15 11.27425799 0.189308226 . . . . . . . 53296 9 75 . 1 1 109 109 SER N N 15 11.26992711 0.178916742 . . . . . . . 53296 9 76 . 1 1 113 113 ARG N N 15 11.31015398 0.110134287 . . . . . . . 53296 9 77 . 1 1 115 115 GLY N N 15 11.09816957 0.149752719 . . . . . . . 53296 9 78 . 1 1 116 116 PHE N N 15 10.55275835 0.134293312 . . . . . . . 53296 9 79 . 1 1 117 117 GLY N N 15 9.555663044 0.178175738 . . . . . . . 53296 9 80 . 1 1 118 118 LYS N N 15 10.66517559 0.227593852 . . . . . . . 53296 9 81 . 1 1 120 120 GLU N N 15 10.41150099 0.153243947 . . . . . . . 53296 9 82 . 1 1 121 121 ARG N N 15 10.00242007 0.066948539 . . . . . . . 53296 9 83 . 1 1 122 122 GLY N N 15 8.855144648 0.244445433 . . . . . . . 53296 9 84 . 1 1 123 123 GLY N N 15 8.191540971 0.178669646 . . . . . . . 53296 9 85 . 1 1 124 124 ASN N N 15 9.876076875 0.292258572 . . . . . . . 53296 9 86 . 1 1 125 125 SER N N 15 10.1476392 0.104844409 . . . . . . . 53296 9 87 . 1 1 128 128 CYS N N 15 9.414373879 0.193197494 . . . . . . . 53296 9 88 . 1 1 129 129 ASP N N 15 8.136823696 0.142061283 . . . . . . . 53296 9 89 . 1 1 131 131 SER N N 15 5.397597105 0.158464083 . . . . . . . 53296 9 90 . 1 1 132 132 ASP N N 15 3.395916304 0.269658305 . . . . . . . 53296 9 stop_ save_ save_heteronucl_T2_relaxation_10 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_10 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 10 _Heteronucl_T2_list.Name '15N R2 u-2H,15N 500 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type N(+,-) _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 22 'T1rho/R1rho relaxation' . . . 53296 10 23 'T1/R1 relaxation' . . . 53296 10 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 10 2 $software_2 . . 53296 10 3 $software_3 . . 53296 10 4 $software_4 . . 53296 10 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 3.356067199 0.13334419 . . . . . . . 53296 10 2 . 1 1 5 5 ALA N N 15 4.768039407 0.260070584 . . . . . . . 53296 10 3 . 1 1 7 7 GLU N N 15 5.177604875 0.124124736 . . . . . . . 53296 10 4 . 1 1 8 8 ASN N N 15 5.026997294 0.06178636 . . . . . . . 53296 10 5 . 1 1 9 9 ALA N N 15 5.342880245 0.109368463 . . . . . . . 53296 10 6 . 1 1 11 11 GLY N N 15 5.384058368 0.221421937 . . . . . . . 53296 10 7 . 1 1 12 12 LEU N N 15 6.36068497 0.068314035 . . . . . . . 53296 10 8 . 1 1 13 13 ASP N N 15 6.34135589 0.12256517 . . . . . . . 53296 10 9 . 1 1 17 17 ALA N N 15 7.060812731 0.236533481 . . . . . . . 53296 10 10 . 1 1 18 18 GLY N N 15 5.518285764 0.194634923 . . . . . . . 53296 10 11 . 1 1 20 20 ASP N N 15 6.503126326 0.175429056 . . . . . . . 53296 10 12 . 1 1 21 21 LEU N N 15 6.632125558 0.087232277 . . . . . . . 53296 10 13 . 1 1 22 22 ASN N N 15 6.257423078 0.122584407 . . . . . . . 53296 10 14 . 1 1 23 23 SER N N 15 5.560834816 0.162756156 . . . . . . . 53296 10 15 . 1 1 24 24 SER N N 15 5.96103128 0.178797967 . . . . . . . 53296 10 16 . 1 1 25 25 ASP N N 15 5.838749328 0.08061197 . . . . . . . 53296 10 17 . 1 1 26 26 ASN N N 15 5.117622019 0.072131573 . . . . . . . 53296 10 18 . 1 1 27 27 GLN N N 15 5.247923886 0.169903564 . . . . . . . 53296 10 19 . 1 1 29 29 GLY N N 15 4.352512822 0.150430881 . . . . . . . 53296 10 20 . 1 1 30 30 GLY N N 15 4.325969201 0.082954825 . . . . . . . 53296 10 21 . 1 1 31 31 SER N N 15 4.417279194 0.175869668 . . . . . . . 53296 10 22 . 1 1 32 32 THR N N 15 4.820041467 0.172416548 . . . . . . . 53296 10 23 . 1 1 33 33 ALA N N 15 5.880855317 0.147891597 . . . . . . . 53296 10 24 . 1 1 34 34 SER N N 15 5.822925007 0.082536971 . . . . . . . 53296 10 25 . 1 1 35 35 LYS N N 15 6.632466377 0.216123166 . . . . . . . 53296 10 26 . 1 1 36 36 GLY N N 15 6.506194822 0.334525389 . . . . . . . 53296 10 27 . 1 1 37 37 ARG N N 15 8.525898787 0.224573246 . . . . . . . 53296 10 28 . 1 1 38 38 TYR N N 15 11.30461018 0.267912311 . . . . . . . 53296 10 29 . 1 1 39 39 ILE N N 15 12.86714631 0.142961408 . . . . . . . 53296 10 30 . 1 1 43 43 LEU N N 15 16.30167957 0.522209809 . . . . . . . 53296 10 31 . 1 1 45 45 ASN N N 15 11.92066805 0.110406194 . . . . . . . 53296 10 32 . 1 1 47 47 GLU N N 15 11.18089635 0.155100636 . . . . . . . 53296 10 33 . 1 1 48 48 ALA N N 15 10.69609362 0.121476944 . . . . . . . 53296 10 34 . 1 1 49 49 THR N N 15 10.05148342 0.252682252 . . . . . . . 53296 10 35 . 1 1 50 50 LYS N N 15 10.56817621 0.205950979 . . . . . . . 53296 10 36 . 1 1 51 51 GLY N N 15 9.962633774 0.110856354 . . . . . . . 53296 10 37 . 1 1 52 52 PHE N N 15 11.28169166 0.209771722 . . . . . . . 53296 10 38 . 1 1 54 54 ASP N N 15 12.38122171 0.129329782 . . . . . . . 53296 10 39 . 1 1 57 57 SER N N 15 10.38326832 0.159836622 . . . . . . . 53296 10 40 . 1 1 58 58 SER N N 15 10.36933279 0.15501391 . . . . . . . 53296 10 41 . 1 1 59 59 GLY N N 15 10.35485459 0.276967713 . . . . . . . 53296 10 42 . 1 1 61 61 SER N N 15 11.37961338 0.066711384 . . . . . . . 53296 10 43 . 1 1 62 62 SER N N 15 10.56292662 0.149384501 . . . . . . . 53296 10 44 . 1 1 63 63 SER N N 15 10.6325139 0.164614069 . . . . . . . 53296 10 45 . 1 1 64 64 LYS N N 15 11.13850729 0.204971721 . . . . . . . 53296 10 46 . 1 1 66 66 LYS N N 15 10.90510973 0.175357169 . . . . . . . 53296 10 47 . 1 1 68 68 ALA N N 15 11.36456581 0.142388111 . . . . . . . 53296 10 48 . 1 1 69 69 TYR N N 15 11.26889059 0.09915064 . . . . . . . 53296 10 49 . 1 1 70 70 SER N N 15 11.21271249 0.077483859 . . . . . . . 53296 10 50 . 1 1 71 71 SER N N 15 10.26192634 0.143846404 . . . . . . . 53296 10 51 . 1 1 73 73 GLY N N 15 9.440070564 0.123467089 . . . . . . . 53296 10 52 . 1 1 74 74 SER N N 15 8.987052262 0.177599804 . . . . . . . 53296 10 53 . 1 1 78 78 SER N N 15 9.060483403 0.129736769 . . . . . . . 53296 10 54 . 1 1 82 82 SER N N 15 9.211175132 0.174146044 . . . . . . . 53296 10 55 . 1 1 83 83 SER N N 15 10.16743471 0.147309512 . . . . . . . 53296 10 56 . 1 1 85 85 PHE N N 15 12.55439295 0.216489378 . . . . . . . 53296 10 57 . 1 1 86 86 SER N N 15 10.83499761 0.155707218 . . . . . . . 53296 10 58 . 1 1 88 88 ARG N N 15 10.69386072 0.186067101 . . . . . . . 53296 10 59 . 1 1 89 89 GLY N N 15 9.494125583 0.202001399 . . . . . . . 53296 10 60 . 1 1 90 90 SER N N 15 9.563702141 0.111150773 . . . . . . . 53296 10 61 . 1 1 91 91 GLY N N 15 8.148467881 0.071089512 . . . . . . . 53296 10 62 . 1 1 92 92 SER N N 15 8.596209033 0.084133912 . . . . . . . 53296 10 63 . 1 1 94 94 GLY N N 15 11.02995554 0.134300185 . . . . . . . 53296 10 64 . 1 1 95 95 ARG N N 15 11.72638186 0.138005577 . . . . . . . 53296 10 65 . 1 1 96 96 PHE N N 15 12.88579958 0.110994877 . . . . . . . 53296 10 66 . 1 1 97 97 ASP N N 15 13.10938966 0.150992241 . . . . . . . 53296 10 67 . 1 1 98 98 ASP N N 15 13.06829004 0.121257154 . . . . . . . 53296 10 68 . 1 1 100 100 GLY N N 15 12.19298196 0.268278209 . . . . . . . 53296 10 69 . 1 1 101 101 ARG N N 15 12.38090107 0.1552943 1 . 1 1 . . . 53296 10 70 . 1 1 102 102 SER N N 15 11.88121516 0.058117017 . . . . . . . 53296 10 71 . 1 1 104 104 TYR N N 15 12.66043482 0.164332169 . . . . . . . 53296 10 72 . 1 1 106 106 GLY N N 15 10.60002851 0.415550339 . . . . . . . 53296 10 73 . 1 1 107 107 ILE N N 15 11.68776594 0.223679297 . . . . . . . 53296 10 74 . 1 1 108 108 GLY N N 15 11.01921787 0.103277631 . . . . . . . 53296 10 75 . 1 1 109 109 SER N N 15 10.44406012 0.055298999 . . . . . . . 53296 10 76 . 1 1 113 113 ARG N N 15 10.72301348 0.260798853 . . . . . . . 53296 10 77 . 1 1 115 115 GLY N N 15 9.869057157 0.266699834 . . . . . . . 53296 10 78 . 1 1 116 116 PHE N N 15 10.27773019 0.104085433 . . . . . . . 53296 10 79 . 1 1 117 117 GLY N N 15 9.092895786 0.156421784 . . . . . . . 53296 10 80 . 1 1 118 118 LYS N N 15 10.30956905 0.259398685 . . . . . . . 53296 10 81 . 1 1 120 120 GLU N N 15 10.26768085 0.147386162 . . . . . . . 53296 10 82 . 1 1 121 121 ARG N N 15 9.913465855 0.143127474 . . . . . . . 53296 10 83 . 1 1 122 122 GLY N N 15 8.346540207 0.1980543 1 . 1 1 . . . 53296 10 84 . 1 1 123 123 GLY N N 15 7.824769473 0.166167031 . . . . . . . 53296 10 85 . 1 1 124 124 ASN N N 15 7.430480035 0.176407811 . . . . . . . 53296 10 86 . 1 1 125 125 SER N N 15 8.587800099 0.134198877 . . . . . . . 53296 10 87 . 1 1 128 128 CYS N N 15 9.722746252 0.17881586 . . . . . . . 53296 10 88 . 1 1 129 129 ASP N N 15 7.538719731 0.148397512 . . . . . . . 53296 10 89 . 1 1 131 131 SER N N 15 4.563331655 0.158455833 . . . . . . . 53296 10 90 . 1 1 132 132 ASP N N 15 3.590307097 0.120956565 . . . . . . . 53296 10 stop_ save_ save_heteronucl_T2_relaxation_11 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_11 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 11 _Heteronucl_T2_list.Name 'HxNx u-2H,15N 500 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HxNx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 18 'T1rho/R1rho relaxation HxNx' . . . 53296 11 19 'T1rho/R1rho relaxation HxNz' . . . 53296 11 20 'T1rho/R1rho relaxation HzNx' . . . 53296 11 21 'T1/R1 relaxation HzNz' . . . 53296 11 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 11 2 $software_2 . . 53296 11 3 $software_3 . . 53296 11 4 $software_4 . . 53296 11 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 19.87440778 0.125606981 . . . . . . . 53296 11 2 . 1 1 5 5 ALA N N 15 5.546520198 0.177311542 . . . . . . . 53296 11 3 . 1 1 7 7 GLU N N 15 6.512377856 0.109336688 . . . . . . . 53296 11 4 . 1 1 8 8 ASN N N 15 7.115836846 0.048709607 . . . . . . . 53296 11 5 . 1 1 9 9 ALA N N 15 7.165849887 0.098271076 . . . . . . . 53296 11 6 . 1 1 11 11 GLY N N 15 6.872967663 0.185929178 . . . . . . . 53296 11 7 . 1 1 12 12 LEU N N 15 7.698193725 0.127369976 . . . . . . . 53296 11 8 . 1 1 13 13 ASP N N 15 7.684187064 0.158215561 . . . . . . . 53296 11 9 . 1 1 17 17 ALA N N 15 8.480814695 0.084390443 . . . . . . . 53296 11 10 . 1 1 18 18 GLY N N 15 7.974880403 0.137539627 . . . . . . . 53296 11 11 . 1 1 20 20 ASP N N 15 7.647521719 0.093781662 . . . . . . . 53296 11 12 . 1 1 21 21 LEU N N 15 7.917494762 0.131014402 . . . . . . . 53296 11 13 . 1 1 22 22 ASN N N 15 8.366502306 0.097658966 . . . . . . . 53296 11 14 . 1 1 23 23 SER N N 15 8.543887101 0.159282891 . . . . . . . 53296 11 15 . 1 1 24 24 SER N N 15 8.816357102 0.073036681 . . . . . . . 53296 11 16 . 1 1 25 25 ASP N N 15 7.79955015 0.182540582 . . . . . . . 53296 11 17 . 1 1 26 26 ASN N N 15 7.416547936 0.131263468 . . . . . . . 53296 11 18 . 1 1 27 27 GLN N N 15 7.498076143 0.093455731 . . . . . . . 53296 11 19 . 1 1 29 29 GLY N N 15 6.935291974 0.193275375 . . . . . . . 53296 11 20 . 1 1 30 30 GLY N N 15 5.82252933 0.208565981 . . . . . . . 53296 11 21 . 1 1 31 31 SER N N 15 7.981187303 0.138012471 . . . . . . . 53296 11 22 . 1 1 32 32 THR N N 15 9.454379803 0.225180687 . . . . . . . 53296 11 23 . 1 1 33 33 ALA N N 15 8.065964687 0.053979974 . . . . . . . 53296 11 24 . 1 1 34 34 SER N N 15 8.419198243 0.134901911 . . . . . . . 53296 11 25 . 1 1 35 35 LYS N N 15 9.168340284 0.123039664 . . . . . . . 53296 11 26 . 1 1 36 36 GLY N N 15 8.596234879 0.200810678 . . . . . . . 53296 11 27 . 1 1 37 37 ARG N N 15 10.1032371 0.306547578 . . . . . . . 53296 11 28 . 1 1 38 38 TYR N N 15 12.30431781 0.209557018 . . . . . . . 53296 11 29 . 1 1 39 39 ILE N N 15 12.19504117 0.105569998 . . . . . . . 53296 11 30 . 1 1 43 43 LEU N N 15 33.112665 0.413461767 . . . . . . . 53296 11 31 . 1 1 45 45 ASN N N 15 16.46119969 0.147462262 . . . . . . . 53296 11 32 . 1 1 47 47 GLU N N 15 13.49187981 0.107129856 . . . . . . . 53296 11 33 . 1 1 48 48 ALA N N 15 13.27129099 0.271826679 . . . . . . . 53296 11 34 . 1 1 49 49 THR N N 15 13.59736359 0.070576443 . . . . . . . 53296 11 35 . 1 1 50 50 LYS N N 15 14.14479243 0.164303204 . . . . . . . 53296 11 36 . 1 1 51 51 GLY N N 15 13.60624145 0.300631388 . . . . . . . 53296 11 37 . 1 1 52 52 PHE N N 15 13.38826324 0.129762625 . . . . . . . 53296 11 38 . 1 1 54 54 ASP N N 15 15.9573177 0.218045167 . . . . . . . 53296 11 39 . 1 1 57 57 SER N N 15 15.72898575 0.218262355 . . . . . . . 53296 11 40 . 1 1 58 58 SER N N 15 16.49571536 0.197034656 . . . . . . . 53296 11 41 . 1 1 59 59 GLY N N 15 16.09560842 0.181038463 . . . . . . . 53296 11 42 . 1 1 61 61 SER N N 15 18.31861628 0.165121295 . . . . . . . 53296 11 43 . 1 1 62 62 SER N N 15 15.88712759 0.185849751 . . . . . . . 53296 11 44 . 1 1 63 63 SER N N 15 17.7202247 0.136549023 . . . . . . . 53296 11 45 . 1 1 64 64 LYS N N 15 15.23514159 0.126621298 . . . . . . . 53296 11 46 . 1 1 66 66 LYS N N 15 13.95740618 0.225230774 . . . . . . . 53296 11 47 . 1 1 68 68 ALA N N 15 13.92794761 0.133066341 . . . . . . . 53296 11 48 . 1 1 69 69 TYR N N 15 14.12024992 0.184963889 . . . . . . . 53296 11 49 . 1 1 70 70 SER N N 15 14.27042281 0.084735702 . . . . . . . 53296 11 50 . 1 1 71 71 SER N N 15 16.32741245 0.159060029 . . . . . . . 53296 11 51 . 1 1 73 73 GLY N N 15 12.46042156 0.20625837 . . . . . . . 53296 11 52 . 1 1 74 74 SER N N 15 12.92220864 0.129255433 . . . . . . . 53296 11 53 . 1 1 78 78 SER N N 15 13.81920393 0.151573803 . . . . . . . 53296 11 54 . 1 1 82 82 SER N N 15 13.11444382 0.20247568 . . . . . . . 53296 11 55 . 1 1 83 83 SER N N 15 15.48376114 0.188320112 . . . . . . . 53296 11 56 . 1 1 85 85 PHE N N 15 15.7746476 0.19959345 . . . . . . . 53296 11 57 . 1 1 86 86 SER N N 15 14.37814606 0.140333329 . . . . . . . 53296 11 58 . 1 1 88 88 ARG N N 15 14.39043253 0.184782019 . . . . . . . 53296 11 59 . 1 1 89 89 GLY N N 15 12.34537775 0.185207668 . . . . . . . 53296 11 60 . 1 1 90 90 SER N N 15 13.89148884 0.265873553 . . . . . . . 53296 11 61 . 1 1 91 91 GLY N N 15 12.82927148 0.114058391 . . . . . . . 53296 11 62 . 1 1 92 92 SER N N 15 12.80898406 0.215665352 . . . . . . . 53296 11 63 . 1 1 94 94 GLY N N 15 14.82784402 0.167110882 . . . . . . . 53296 11 64 . 1 1 95 95 ARG N N 15 14.46914889 0.193871602 . . . . . . . 53296 11 65 . 1 1 96 96 PHE N N 15 16.11785644 0.178881337 . . . . . . . 53296 11 66 . 1 1 97 97 ASP N N 15 16.98485649 0.295676201 . . . . . . . 53296 11 67 . 1 1 98 98 ASP N N 15 16.00794746 0.111986045 . . . . . . . 53296 11 68 . 1 1 100 100 GLY N N 15 15.91329986 0.362300525 . . . . . . . 53296 11 69 . 1 1 101 101 ARG N N 15 15.83986969 0.158867166 . . . . . . . 53296 11 70 . 1 1 102 102 SER N N 15 15.85952406 0.13390049 . . . . . . . 53296 11 71 . 1 1 104 104 TYR N N 15 16.18855519 0.166861826 . . . . . . . 53296 11 72 . 1 1 106 106 GLY N N 15 23.89561415 0.385102501 . . . . . . . 53296 11 73 . 1 1 107 107 ILE N N 15 13.8357247 0.110959678 . . . . . . . 53296 11 74 . 1 1 108 108 GLY N N 15 15.14981008 0.181139821 . . . . . . . 53296 11 75 . 1 1 109 109 SER N N 15 14.80589493 0.276032799 . . . . . . . 53296 11 76 . 1 1 113 113 ARG N N 15 13.93628192 0.133175907 . . . . . . . 53296 11 77 . 1 1 115 115 GLY N N 15 13.38471838 0.222004791 . . . . . . . 53296 11 78 . 1 1 116 116 PHE N N 15 12.8135065 0.145154076 . . . . . . . 53296 11 79 . 1 1 117 117 GLY N N 15 12.76935101 0.348708287 . . . . . . . 53296 11 80 . 1 1 118 118 LYS N N 15 12.17234483 0.17011514 . . . . . . . 53296 11 81 . 1 1 120 120 GLU N N 15 13.24145667 0.098225241 . . . . . . . 53296 11 82 . 1 1 121 121 ARG N N 15 12.51368806 0.190023356 . . . . . . . 53296 11 83 . 1 1 122 122 GLY N N 15 11.45143863 0.210839919 . . . . . . . 53296 11 84 . 1 1 123 123 GLY N N 15 9.89565445 0.195709092 . . . . . . . 53296 11 85 . 1 1 124 124 ASN N N 15 11.75420832 0.321758841 . . . . . . . 53296 11 86 . 1 1 125 125 SER N N 15 12.80330037 0.20324745 . . . . . . . 53296 11 87 . 1 1 128 128 CYS N N 15 13.43040209 0.117212855 . . . . . . . 53296 11 88 . 1 1 129 129 ASP N N 15 10.2272871 0.183277889 . . . . . . . 53296 11 89 . 1 1 131 131 SER N N 15 6.491022178 0.080979951 . . . . . . . 53296 11 90 . 1 1 132 132 ASP N N 15 3.540968304 0.088017106 . . . . . . . 53296 11 stop_ save_ save_heteronucl_T2_relaxation_12 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_12 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 12 _Heteronucl_T2_list.Name 'HxNz u-2H,15N 500 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HxNz _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 18 'T1rho/R1rho relaxation HxNx' . . . 53296 12 19 'T1rho/R1rho relaxation HxNz' . . . 53296 12 20 'T1rho/R1rho relaxation HzNx' . . . 53296 12 21 'T1/R1 relaxation HzNz' . . . 53296 12 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 12 2 $software_2 . . 53296 12 3 $software_3 . . 53296 12 4 $software_4 . . 53296 12 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS H H 1 19.21089092 0.156207511 . . . . . . . 53296 12 2 . 1 1 5 5 ALA H H 1 4.750158928 0.102075946 . . . . . . . 53296 12 3 . 1 1 7 7 GLU H H 1 5.373896976 0.068994899 . . . . . . . 53296 12 4 . 1 1 8 8 ASN H H 1 6.236372234 0.096510989 . . . . . . . 53296 12 5 . 1 1 9 9 ALA H H 1 6.184128052 0.046091475 . . . . . . . 53296 12 6 . 1 1 11 11 GLY H H 1 6.601949053 0.204036896 . . . . . . . 53296 12 7 . 1 1 12 12 LEU H H 1 6.956333267 0.079909971 . . . . . . . 53296 12 8 . 1 1 13 13 ASP H H 1 6.758305852 0.094164032 . . . . . . . 53296 12 9 . 1 1 17 17 ALA H H 1 7.625432934 0.135083387 . . . . . . . 53296 12 10 . 1 1 18 18 GLY H H 1 8.233830287 0.099831442 . . . . . . . 53296 12 11 . 1 1 20 20 ASP H H 1 6.607998099 0.121546451 . . . . . . . 53296 12 12 . 1 1 21 21 LEU H H 1 7.0115226 0.091208653 . . . . . . . 53296 12 13 . 1 1 22 22 ASN H H 1 7.517971813 0.068650064 . . . . . . . 53296 12 14 . 1 1 23 23 SER H H 1 7.861135728 0.181304557 . . . . . . . 53296 12 15 . 1 1 24 24 SER H H 1 7.907597463 0.140895085 . . . . . . . 53296 12 16 . 1 1 25 25 ASP H H 1 7.046109257 0.16780189 . . . . . . . 53296 12 17 . 1 1 26 26 ASN H H 1 6.943599234 0.097380063 . . . . . . . 53296 12 18 . 1 1 27 27 GLN H H 1 6.8210263 0.112040435 . . . . . . . 53296 12 19 . 1 1 29 29 GLY H H 1 6.710418312 0.261685317 . . . . . . . 53296 12 20 . 1 1 30 30 GLY H H 1 5.907139348 0.057909428 . . . . . . . 53296 12 21 . 1 1 31 31 SER H H 1 7.387892878 0.098761473 . . . . . . . 53296 12 22 . 1 1 32 32 THR H H 1 8.719867051 0.089793874 . . . . . . . 53296 12 23 . 1 1 33 33 ALA H H 1 7.418599335 0.119758717 . . . . . . . 53296 12 24 . 1 1 34 34 SER H H 1 8.051903674 0.132006935 . . . . . . . 53296 12 25 . 1 1 35 35 LYS H H 1 8.793414307 0.206666289 . . . . . . . 53296 12 26 . 1 1 36 36 GLY H H 1 8.32229654 0.123252791 . . . . . . . 53296 12 27 . 1 1 37 37 ARG H H 1 9.473744363 0.139898465 . . . . . . . 53296 12 28 . 1 1 38 38 TYR H H 1 10.6156402 0.133334046 . . . . . . . 53296 12 29 . 1 1 39 39 ILE H H 1 10.95076301 0.077974845 . . . . . . . 53296 12 30 . 1 1 43 43 LEU H H 1 29.59469705 0.352879899 . . . . . . . 53296 12 31 . 1 1 45 45 ASN H H 1 14.45003765 0.143034176 . . . . . . . 53296 12 32 . 1 1 47 47 GLU H H 1 11.94496171 0.100470783 . . . . . . . 53296 12 33 . 1 1 48 48 ALA H H 1 11.87444579 0.14856205 . . . . . . . 53296 12 34 . 1 1 49 49 THR H H 1 12.08178568 0.058632124 . . . . . . . 53296 12 35 . 1 1 50 50 LYS H H 1 12.73321181 0.144447936 . . . . . . . 53296 12 36 . 1 1 51 51 GLY H H 1 12.35411022 0.179719042 . . . . . . . 53296 12 37 . 1 1 52 52 PHE H H 1 12.19700863 0.098078466 . . . . . . . 53296 12 38 . 1 1 54 54 ASP H H 1 13.68095607 0.156495446 . . . . . . . 53296 12 39 . 1 1 57 57 SER H H 1 14.39783944 0.149287784 . . . . . . . 53296 12 40 . 1 1 58 58 SER H H 1 14.51648265 0.288671764 . . . . . . . 53296 12 41 . 1 1 59 59 GLY H H 1 15.08516395 0.203460168 . . . . . . . 53296 12 42 . 1 1 61 61 SER H H 1 16.54223183 0.07495697 . . . . . . . 53296 12 43 . 1 1 62 62 SER H H 1 14.84659209 0.129739325 . . . . . . . 53296 12 44 . 1 1 63 63 SER H H 1 16.21434522 0.164311055 . . . . . . . 53296 12 45 . 1 1 64 64 LYS H H 1 13.88656078 0.1221469 1 . 1 1 . . . 53296 12 46 . 1 1 66 66 LYS H H 1 12.91434652 0.225509405 . . . . . . . 53296 12 47 . 1 1 68 68 ALA H H 1 12.74149953 0.075302978 . . . . . . . 53296 12 48 . 1 1 69 69 TYR H H 1 12.68579325 0.125760506 . . . . . . . 53296 12 49 . 1 1 70 70 SER H H 1 13.31948612 0.130067346 . . . . . . . 53296 12 50 . 1 1 71 71 SER H H 1 14.76365894 0.127232554 . . . . . . . 53296 12 51 . 1 1 73 73 GLY H H 1 11.64525441 0.124177915 . . . . . . . 53296 12 52 . 1 1 74 74 SER H H 1 11.80862703 0.072383726 . . . . . . . 53296 12 53 . 1 1 78 78 SER H H 1 12.61848441 0.1439922 1 . 1 1 . . . 53296 12 54 . 1 1 82 82 SER H H 1 12.20124733 0.162574858 . . . . . . . 53296 12 55 . 1 1 83 83 SER H H 1 14.31496638 0.057681946 . . . . . . . 53296 12 56 . 1 1 85 85 PHE H H 1 13.60449911 0.042044715 . . . . . . . 53296 12 57 . 1 1 86 86 SER H H 1 13.22848481 0.113992787 . . . . . . . 53296 12 58 . 1 1 88 88 ARG H H 1 12.98430709 0.125240624 . . . . . . . 53296 12 59 . 1 1 89 89 GLY H H 1 11.84842377 0.173110789 . . . . . . . 53296 12 60 . 1 1 90 90 SER H H 1 12.31034242 0.12524519 . . . . . . . 53296 12 61 . 1 1 91 91 GLY H H 1 11.78647551 0.123623229 . . . . . . . 53296 12 62 . 1 1 92 92 SER H H 1 11.46771429 0.076854799 . . . . . . . 53296 12 63 . 1 1 94 94 GLY H H 1 13.41419256 0.126175581 . . . . . . . 53296 12 64 . 1 1 95 95 ARG H H 1 13.02657639 0.09515868 . . . . . . . 53296 12 65 . 1 1 96 96 PHE H H 1 14.01485089 0.102748563 . . . . . . . 53296 12 66 . 1 1 97 97 ASP H H 1 14.92415413 0.221441901 . . . . . . . 53296 12 67 . 1 1 98 98 ASP H H 1 14.01910935 0.138120982 . . . . . . . 53296 12 68 . 1 1 100 100 GLY H H 1 15.12655966 0.203610308 . . . . . . . 53296 12 69 . 1 1 101 101 ARG H H 1 14.35157932 0.184215832 . . . . . . . 53296 12 70 . 1 1 102 102 SER H H 1 14.51656926 0.149455175 . . . . . . . 53296 12 71 . 1 1 104 104 TYR H H 1 14.90836792 0.119780554 . . . . . . . 53296 12 72 . 1 1 106 106 GLY H H 1 23.71972619 0.246073233 . . . . . . . 53296 12 73 . 1 1 107 107 ILE H H 1 12.3607567 0.156440709 . . . . . . . 53296 12 74 . 1 1 108 108 GLY H H 1 13.35089181 0.093656864 . . . . . . . 53296 12 75 . 1 1 109 109 SER H H 1 13.62935874 0.103562732 . . . . . . . 53296 12 76 . 1 1 113 113 ARG H H 1 12.75356116 0.193958286 . . . . . . . 53296 12 77 . 1 1 115 115 GLY H H 1 12.80421558 0.102572247 . . . . . . . 53296 12 78 . 1 1 116 116 PHE H H 1 11.55040573 0.177111131 . . . . . . . 53296 12 79 . 1 1 117 117 GLY H H 1 11.902836 0.374829447 . . . . . . . 53296 12 80 . 1 1 118 118 LYS H H 1 11.75839148 0.153214041 . . . . . . . 53296 12 81 . 1 1 120 120 GLU H H 1 11.94573214 0.056263529 . . . . . . . 53296 12 82 . 1 1 121 121 ARG H H 1 11.28248061 0.122154545 . . . . . . . 53296 12 83 . 1 1 122 122 GLY H H 1 10.92832522 0.184815727 . . . . . . . 53296 12 84 . 1 1 123 123 GLY H H 1 10.07639057 0.096903222 . . . . . . . 53296 12 85 . 1 1 124 124 ASN H H 1 11.31423779 0.093905707 . . . . . . . 53296 12 86 . 1 1 125 125 SER H H 1 11.21827664 0.110685057 . . . . . . . 53296 12 87 . 1 1 128 128 CYS H H 1 11.46580616 0.117239754 . . . . . . . 53296 12 88 . 1 1 129 129 ASP H H 1 9.591123686 0.135410843 . . . . . . . 53296 12 89 . 1 1 131 131 SER H H 1 5.81752445 0.101592239 . . . . . . . 53296 12 90 . 1 1 132 132 ASP H H 1 3.245193003 0.037149351 . . . . . . . 53296 12 stop_ save_ save_heteronucl_T2_relaxation_13 _Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation _Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_13 _Heteronucl_T2_list.Entry_ID 53296 _Heteronucl_T2_list.ID 13 _Heteronucl_T2_list.Name 'HzNx u-2H,15N 500 uM' _Heteronucl_T2_list.Sample_condition_list_ID 1 _Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1 _Heteronucl_T2_list.Temp_calibration_method methanol _Heteronucl_T2_list.Temp_control_method 'temperature compensation block' _Heteronucl_T2_list.Spectrometer_frequency_1H 1000 _Heteronucl_T2_list.T2_coherence_type HzNx _Heteronucl_T2_list.T2_val_units s-1 _Heteronucl_T2_list.Rex_units . _Heteronucl_T2_list.Details . _Heteronucl_T2_list.Text_data_format . _Heteronucl_T2_list.Text_data . loop_ _Heteronucl_T2_experiment.Experiment_ID _Heteronucl_T2_experiment.Experiment_name _Heteronucl_T2_experiment.Sample_ID _Heteronucl_T2_experiment.Sample_label _Heteronucl_T2_experiment.Sample_state _Heteronucl_T2_experiment.Entry_ID _Heteronucl_T2_experiment.Heteronucl_T2_list_ID 18 'T1rho/R1rho relaxation HxNx' . . . 53296 13 19 'T1rho/R1rho relaxation HxNz' . . . 53296 13 20 'T1rho/R1rho relaxation HzNx' . . . 53296 13 21 'T1/R1 relaxation HzNz' . . . 53296 13 stop_ loop_ _Heteronucl_T2_software.Software_ID _Heteronucl_T2_software.Software_label _Heteronucl_T2_software.Method_ID _Heteronucl_T2_software.Method_label _Heteronucl_T2_software.Entry_ID _Heteronucl_T2_software.Heteronucl_T2_list_ID 1 $software_1 . . 53296 13 2 $software_2 . . 53296 13 3 $software_3 . . 53296 13 4 $software_4 . . 53296 13 stop_ loop_ _T2.ID _T2.Assembly_atom_ID _T2.Entity_assembly_ID _T2.Entity_ID _T2.Comp_index_ID _T2.Seq_ID _T2.Comp_ID _T2.Atom_ID _T2.Atom_type _T2.Atom_isotope_number _T2.T2_val _T2.T2_val_err _T2.Rex_val _T2.Rex_err _T2.Resonance_ID _T2.Auth_entity_assembly_ID _T2.Auth_seq_ID _T2.Auth_comp_ID _T2.Auth_atom_ID _T2.Entry_ID _T2.Heteronucl_T2_list_ID 1 . 1 1 3 3 HIS N N 15 19.7824126 0.192722526 . . . . . . . 53296 13 2 . 1 1 5 5 ALA N N 15 5.099784452 0.090545404 . . . . . . . 53296 13 3 . 1 1 7 7 GLU N N 15 5.969681911 0.065901905 . . . . . . . 53296 13 4 . 1 1 8 8 ASN N N 15 6.401478964 0.143099646 . . . . . . . 53296 13 5 . 1 1 9 9 ALA N N 15 6.675201662 0.071991367 . . . . . . . 53296 13 6 . 1 1 11 11 GLY N N 15 5.643002055 0.167568937 . . . . . . . 53296 13 7 . 1 1 12 12 LEU N N 15 7.387506987 0.114008394 . . . . . . . 53296 13 8 . 1 1 13 13 ASP N N 15 7.520066213 0.116624721 . . . . . . . 53296 13 9 . 1 1 17 17 ALA N N 15 8.077010497 0.124406413 . . . . . . . 53296 13 10 . 1 1 18 18 GLY N N 15 6.120016966 0.076970725 . . . . . . . 53296 13 11 . 1 1 20 20 ASP N N 15 7.321346481 0.07950853 . . . . . . . 53296 13 12 . 1 1 21 21 LEU N N 15 7.386173249 0.187447352 . . . . . . . 53296 13 13 . 1 1 22 22 ASN N N 15 7.851188343 0.117415478 . . . . . . . 53296 13 14 . 1 1 23 23 SER N N 15 7.847027017 0.09123445 . . . . . . . 53296 13 15 . 1 1 24 24 SER N N 15 8.213780731 0.110593412 . . . . . . . 53296 13 16 . 1 1 25 25 ASP N N 15 7.604302452 0.196112688 . . . . . . . 53296 13 17 . 1 1 26 26 ASN N N 15 6.903184146 0.0779407 1 . 1 1 . . . 53296 13 18 . 1 1 27 27 GLN N N 15 6.975035779 0.123430971 . . . . . . . 53296 13 19 . 1 1 29 29 GLY N N 15 6.520591201 0.163101044 . . . . . . . 53296 13 20 . 1 1 30 30 GLY N N 15 5.589547752 0.119030511 . . . . . . . 53296 13 21 . 1 1 31 31 SER N N 15 7.833771967 0.106875001 . . . . . . . 53296 13 22 . 1 1 32 32 THR N N 15 8.776469185 0.201232926 . . . . . . . 53296 13 23 . 1 1 33 33 ALA N N 15 7.915847309 0.115409878 . . . . . . . 53296 13 24 . 1 1 34 34 SER N N 15 8.033693341 0.135942439 . . . . . . . 53296 13 25 . 1 1 35 35 LYS N N 15 8.659172254 0.127918838 . . . . . . . 53296 13 26 . 1 1 36 36 GLY N N 15 8.149788237 0.189955095 . . . . . . . 53296 13 27 . 1 1 37 37 ARG N N 15 10.18616658 0.211343611 . . . . . . . 53296 13 28 . 1 1 38 38 TYR N N 15 12.49409598 0.130858839 . . . . . . . 53296 13 29 . 1 1 39 39 ILE N N 15 13.34031092 0.113448601 . . . . . . . 53296 13 30 . 1 1 43 43 LEU N N 15 19.12411218 0.186411065 . . . . . . . 53296 13 31 . 1 1 45 45 ASN N N 15 15.03528009 0.225328235 . . . . . . . 53296 13 32 . 1 1 47 47 GLU N N 15 12.81493957 0.113086664 . . . . . . . 53296 13 33 . 1 1 48 48 ALA N N 15 12.46261666 0.159825097 . . . . . . . 53296 13 34 . 1 1 49 49 THR N N 15 12.15579122 0.06988183 . . . . . . . 53296 13 35 . 1 1 50 50 LYS N N 15 13.03221873 0.276502876 . . . . . . . 53296 13 36 . 1 1 51 51 GLY N N 15 11.57841457 0.132442841 . . . . . . . 53296 13 37 . 1 1 52 52 PHE N N 15 13.05876683 0.175568693 . . . . . . . 53296 13 38 . 1 1 54 54 ASP N N 15 14.49545445 0.167152688 . . . . . . . 53296 13 39 . 1 1 57 57 SER N N 15 13.80641014 0.16402885 . . . . . . . 53296 13 40 . 1 1 58 58 SER N N 15 14.71808957 0.276891511 . . . . . . . 53296 13 41 . 1 1 59 59 GLY N N 15 13.51916482 0.17762556 . . . . . . . 53296 13 42 . 1 1 61 61 SER N N 15 14.38046958 0.1647805 1 . 1 1 . . . 53296 13 43 . 1 1 62 62 SER N N 15 14.57279425 0.117902046 . . . . . . . 53296 13 44 . 1 1 63 63 SER N N 15 15.86397958 0.108426223 . . . . . . . 53296 13 45 . 1 1 64 64 LYS N N 15 13.80193755 0.099437342 . . . . . . . 53296 13 46 . 1 1 66 66 LYS N N 15 12.25386148 0.247202771 . . . . . . . 53296 13 47 . 1 1 68 68 ALA N N 15 13.26122261 0.136155291 . . . . . . . 53296 13 48 . 1 1 69 69 TYR N N 15 13.30321891 0.102672946 . . . . . . . 53296 13 49 . 1 1 70 70 SER N N 15 13.80800368 0.175399887 . . . . . . . 53296 13 50 . 1 1 71 71 SER N N 15 15.10612379 0.098702779 . . . . . . . 53296 13 51 . 1 1 73 73 GLY N N 15 11.4191616 0.172434004 . . . . . . . 53296 13 52 . 1 1 74 74 SER N N 15 12.25318717 0.127898006 . . . . . . . 53296 13 53 . 1 1 78 78 SER N N 15 12.65940782 0.136463099 . . . . . . . 53296 13 54 . 1 1 82 82 SER N N 15 12.8768987 0.158181293 . . . . . . . 53296 13 55 . 1 1 83 83 SER N N 15 14.39839588 0.139112805 . . . . . . . 53296 13 56 . 1 1 85 85 PHE N N 15 14.72227454 0.151967112 . . . . . . . 53296 13 57 . 1 1 86 86 SER N N 15 13.56374844 0.11683458 . . . . . . . 53296 13 58 . 1 1 88 88 ARG N N 15 12.97590167 0.089428869 . . . . . . . 53296 13 59 . 1 1 89 89 GLY N N 15 11.38836072 0.215552474 . . . . . . . 53296 13 60 . 1 1 90 90 SER N N 15 13.27274841 0.215139574 . . . . . . . 53296 13 61 . 1 1 91 91 GLY N N 15 11.76433002 0.130968983 . . . . . . . 53296 13 62 . 1 1 92 92 SER N N 15 12.46914899 0.139321324 . . . . . . . 53296 13 63 . 1 1 94 94 GLY N N 15 12.56176401 0.207842056 . . . . . . . 53296 13 64 . 1 1 95 95 ARG N N 15 13.28050922 0.251904614 . . . . . . . 53296 13 65 . 1 1 96 96 PHE N N 15 14.96758133 0.173383389 . . . . . . . 53296 13 66 . 1 1 97 97 ASP N N 15 15.19793119 0.12263963 . . . . . . . 53296 13 67 . 1 1 98 98 ASP N N 15 14.62003781 0.196626767 . . . . . . . 53296 13 68 . 1 1 100 100 GLY N N 15 14.02056964 0.308005939 . . . . . . . 53296 13 69 . 1 1 101 101 ARG N N 15 14.1920074 0.177263721 . . . . . . . 53296 13 70 . 1 1 102 102 SER N N 15 15.0196559 0.142811975 . . . . . . . 53296 13 71 . 1 1 104 104 TYR N N 15 14.46932571 0.169641067 . . . . . . . 53296 13 72 . 1 1 106 106 GLY N N 15 11.89012302 0.183380316 . . . . . . . 53296 13 73 . 1 1 107 107 ILE N N 15 13.27753595 0.151210933 . . . . . . . 53296 13 74 . 1 1 108 108 GLY N N 15 12.64472578 0.15170906 . . . . . . . 53296 13 75 . 1 1 109 109 SER N N 15 13.08001761 0.130248051 . . . . . . . 53296 13 76 . 1 1 113 113 ARG N N 15 12.82344358 0.145573635 . . . . . . . 53296 13 77 . 1 1 115 115 GLY N N 15 12.3213184 0.074228129 . . . . . . . 53296 13 78 . 1 1 116 116 PHE N N 15 12.42652461 0.204004644 . . . . . . . 53296 13 79 . 1 1 117 117 GLY N N 15 11.34216172 0.242574178 . . . . . . . 53296 13 80 . 1 1 118 118 LYS N N 15 12.15390832 0.200769813 . . . . . . . 53296 13 81 . 1 1 120 120 GLU N N 15 12.0090395 0.157551267 . . . . . . . 53296 13 82 . 1 1 121 121 ARG N N 15 11.80751869 0.207433422 . . . . . . . 53296 13 83 . 1 1 122 122 GLY N N 15 10.31727536 0.112452483 . . . . . . . 53296 13 84 . 1 1 123 123 GLY N N 15 9.197328487 0.254189377 . . . . . . . 53296 13 85 . 1 1 124 124 ASN N N 15 11.08240097 0.382062935 . . . . . . . 53296 13 86 . 1 1 125 125 SER N N 15 11.68707093 0.187026333 . . . . . . . 53296 13 87 . 1 1 128 128 CYS N N 15 11.67381583 0.13891164 . . . . . . . 53296 13 88 . 1 1 129 129 ASP N N 15 9.304899841 0.167579809 . . . . . . . 53296 13 89 . 1 1 131 131 SER N N 15 5.941215387 0.084712992 . . . . . . . 53296 13 90 . 1 1 132 132 ASP N N 15 3.62637373 0.117751543 . . . . . . . 53296 13 stop_ save_