data_53244 ####################### # Entry information # ####################### save_entry_information_1 _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information_1 _Entry.ID 53244 _Entry.Title ; 1H Chemical Shift Assignments of the HCV 5BSL3.2 apical stem loop element ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2025-06-25 _Entry.Accession_date 2025-06-25 _Entry.Last_release_date 2025-06-26 _Entry.Original_release_date 2025-06-26 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.14.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype solution _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID 1 _Entry.Generated_software_label $software_1 _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Ajit kumar . . . . 53244 2 Srinivas Penumutchu . . . . 53244 3 Love Panchariya . . . . 53244 4 Purba Daripa . . . . 53244 5 Arockiasamy Arulandu . . . . 53244 6 Mandar Deshmukh . . . . 53244 7 Souvik Maiti . . . . 53244 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 2 53244 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 71 53244 '15N chemical shifts' 7 53244 '1H chemical shifts' 184 53244 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2025-12-20 . original BMRB . 53244 stop_ save_ ############### # Citations # ############### save_citations_1 _Citation.Sf_category citations _Citation.Sf_framecode citations_1 _Citation.Entry_ID 53244 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID 41285614 _Citation.DOI . _Citation.Full_citation . _Citation.Title ; Loop of Fate: Structural and Mechanistic Insights into hnRNPA1 Binding to the Hepatitis C Virus RNA ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev RNA _Citation.Journal_name_full . _Citation.Journal_volume . _Citation.Journal_issue . _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first . _Citation.Page_last . _Citation.Year 2025 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Ajit Kumar A. . . . 53244 1 2 Srinivas Penumutchu S. . . . 53244 1 3 Love Panchariya L. . . . 53244 1 4 Priyanka Kumari P. . . . 53244 1 5 Shubham Thakur S. . . . 53244 1 6 Purba Daripa P. . . . 53244 1 7 Vandana Singh V. . . . 53244 1 8 Arockiasamy Arulandu A. . . . 53244 1 9 Souvik Maiti S. . . . 53244 1 10 Mandar Deshmukh M. V. . . 53244 1 11 Niyati Jain N. . . . 53244 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly_1 _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly_1 _Assembly.Entry_ID 53244 _Assembly.ID 1 _Assembly.Name '5BSL3.2 Apical stem loop' _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds no _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 '5BSL3.2 Apical stem loop' 1 $entity_1 . . yes native no no . . . 53244 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 53244 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name entity_1 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GGAGACAUAUAUCACAGCCU GUCUCC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states yes _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 26 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_biological_function.Biological_function _Entity_biological_function.Entry_ID _Entity_biological_function.Entity_ID 'HCV replication' 53244 1 stop_ loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . G . 53244 1 2 . G . 53244 1 3 . A . 53244 1 4 . G . 53244 1 5 . A . 53244 1 6 . C . 53244 1 7 . A . 53244 1 8 . U . 53244 1 9 . A . 53244 1 10 . U . 53244 1 11 . A . 53244 1 12 . U . 53244 1 13 . C . 53244 1 14 . A . 53244 1 15 . C . 53244 1 16 . A . 53244 1 17 . G . 53244 1 18 . C . 53244 1 19 . C . 53244 1 20 . U . 53244 1 21 . G . 53244 1 22 . U . 53244 1 23 . C . 53244 1 24 . U . 53244 1 25 . C . 53244 1 26 . C . 53244 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . G 1 1 53244 1 . G 2 2 53244 1 . A 3 3 53244 1 . G 4 4 53244 1 . A 5 5 53244 1 . C 6 6 53244 1 . A 7 7 53244 1 . U 8 8 53244 1 . A 9 9 53244 1 . U 10 10 53244 1 . A 11 11 53244 1 . U 12 12 53244 1 . C 13 13 53244 1 . A 14 14 53244 1 . C 15 15 53244 1 . A 16 16 53244 1 . G 17 17 53244 1 . C 18 18 53244 1 . C 19 19 53244 1 . U 20 20 53244 1 . G 21 21 53244 1 . U 22 22 53244 1 . C 23 23 53244 1 . U 24 24 53244 1 . C 25 25 53244 1 . C 26 26 53244 1 stop_ save_ #################### # Natural source # #################### save_natural_source_1 _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source_1 _Entity_natural_src_list.Entry_ID 53244 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 3052230 organism . 'Hepacivirus hominis' 'Hepatitis C Virus' . . Viruses . Hepacivirus hominis con1 . . . . . . . . . . . . 53244 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source_1 _Entity_experimental_src_list.Entry_ID 53244 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'enzymatic semisynthesis' . . . . . . . . . . . . . . . . 53244 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 53244 _Sample.ID 1 _Sample.Name '5BSL3.2 APICAL STEM LOOP' _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number 1 _Sample.Solvent_system '100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 '5BSL3.2 Apical stem loop' "[rRTPs (3',4',5',5''), and rYTPs (5,3',4',5',5'')]" . . 1 $entity_1 . . 200 . . uM . . . . 53244 1 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 53244 _Sample_condition_list.ID 1 _Sample_condition_list.Name '5BSL3.2 Apical stem loop' _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 5 . mM 53244 1 pH 6.5 . pH 53244 1 pressure 1 . atm 53244 1 temperature 303 . K 53244 1 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 53244 _Software.ID 1 _Software.Type . _Software.Name 'topspin4, NMRPipe/nmrdraw,NMRViewJ, XplorNIH 2.25' _Software.Version . _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID 'chemical shift assignment' . 53244 1 collection . 53244 1 'structure solution' . 53244 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 53244 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name 'Bruker Avance II 600' _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model 'Avance II' _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ ############################# # NMR applied experiments # ############################# save_experiment_list_1 _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list_1 _Experiment_list.Entry_ID 53244 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NUS_flag _Experiment.Interleaved_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Details _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-1H NOESY' no no no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '5mM k2hpo4 ph 6.5' 53244 1 2 TOCSY no no no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '5mM k2hpo4 ph 6.5' 53244 1 3 HMQC no no no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '5mM k2hpo4 ph 6.5' 53244 1 4 HSQC no no no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . '5mM k2hpo4 ph 6.5' 53244 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chem_shift_reference_1 _Chem_shift_reference.Entry_ID 53244 _Chem_shift_reference.ID 1 _Chem_shift_reference.Name 'Referenced relative to water signal (commonly in 1H)' _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 water protons . . . . ppm 4.7 na indirect 1 . . . . . 53244 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_1 _Assigned_chem_shift_list.Entry_ID 53244 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Name '2D 1H-1H NOESY' _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-1H NOESY' . . . 53244 1 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 53244 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 1 1 G H1' H 1 5.84 . . 1 . . . . . 1 G H1' . 53244 1 2 . 1 . 1 1 1 G H2' H 1 4.96 . . 1 . . . . . 1 G H2' . 53244 1 3 . 1 . 1 1 1 G H8 H 1 8.23 . . 1 . . . . . 1 G H8 . 53244 1 4 . 1 . 1 2 2 G H1' H 1 5.92 . . 1 . . . . . 2 G H1' . 53244 1 5 . 1 . 1 2 2 G H2' H 1 4.96 . . 1 . . . . . 2 G H2' . 53244 1 6 . 1 . 1 2 2 G H8 H 1 7.63 . . 1 . . . . . 2 G H8 . 53244 1 7 . 1 . 1 3 3 A H1' H 1 5.98 . . 1 . . . . . 3 A H1' . 53244 1 8 . 1 . 1 3 3 A H2' H 1 4.48 . . 1 . . . . . 3 A H2' . 53244 1 9 . 1 . 1 3 3 A H8 H 1 7.80 . . 1 . . . . . 3 A H8 . 53244 1 10 . 1 . 1 4 4 G H1' H 1 5.57 . . 1 . . . . . 4 G H1' . 53244 1 11 . 1 . 1 4 4 G H2' H 1 4.68 . . 1 . . . . . 4 G H2' . 53244 1 12 . 1 . 1 4 4 G H8 H 1 7.13 . . 1 . . . . . 4 G H8 . 53244 1 13 . 1 . 1 5 5 A H1' H 1 5.94 . . 1 . . . . . 5 A H1' . 53244 1 14 . 1 . 1 5 5 A H2' H 1 4.50 . . 1 . . . . . 5 A H2' . 53244 1 15 . 1 . 1 5 5 A H8 H 1 7.81 . . 1 . . . . . 5 A H8 . 53244 1 16 . 1 . 1 6 6 C H1' H 1 5.33 . . 1 . . . . . 6 C H1' . 53244 1 17 . 1 . 1 6 6 C H2' H 1 4.33 . . 1 . . . . . 6 C H2' . 53244 1 18 . 1 . 1 6 6 C H6 H 1 7.37 . . 1 . . . . . 6 C H6 . 53244 1 19 . 1 . 1 7 7 A H1' H 1 5.96 . . 1 . . . . . 7 A H1' . 53244 1 20 . 1 . 1 7 7 A H2' H 1 4.45 . . 1 . . . . . 7 A H2' . 53244 1 21 . 1 . 1 7 7 A H8 H 1 7.91 . . 1 . . . . . 7 A H8 . 53244 1 22 . 1 . 1 8 8 U H1' H 1 5.45 . . 1 . . . . . 8 U H1' . 53244 1 23 . 1 . 1 8 8 U H2' H 1 4.15 . . 1 . . . . . 8 U H2' . 53244 1 24 . 1 . 1 8 8 U H6 H 1 7.42 . . 1 . . . . . 8 U H6 . 53244 1 25 . 1 . 1 9 9 A H1' H 1 5.90 . . 1 . . . . . 9 A H1' . 53244 1 26 . 1 . 1 9 9 A H2' H 1 4.64 . . 1 . . . . . 9 A H2' . 53244 1 27 . 1 . 1 9 9 A H8 H 1 8.17 . . 1 . . . . . 9 A H8 . 53244 1 28 . 1 . 1 10 10 U H1' H 1 5.57 . . 1 . . . . . 10 U H1' . 53244 1 29 . 1 . 1 10 10 U H2' H 1 4.25 . . 1 . . . . . 10 U H2' . 53244 1 30 . 1 . 1 10 10 U H6 H 1 7.60 . . 1 . . . . . 10 U H6 . 53244 1 31 . 1 . 1 11 11 A H1' H 1 5.96 . . 1 . . . . . 11 A H1' . 53244 1 32 . 1 . 1 11 11 A H2' H 1 4.68 . . 1 . . . . . 11 A H2' . 53244 1 33 . 1 . 1 11 11 A H8 H 1 8.27 . . 1 . . . . . 11 A H8 . 53244 1 34 . 1 . 1 12 12 U H1' H 1 5.56 . . 1 . . . . . 12 U H1' . 53244 1 35 . 1 . 1 12 12 U H2' H 1 4.32 . . 1 . . . . . 12 U H2' . 53244 1 36 . 1 . 1 12 12 U H6 H 1 7.67 . . 1 . . . . . 12 U H6 . 53244 1 37 . 1 . 1 13 13 C H1' H 1 5.56 . . 1 . . . . . 13 C H1' . 53244 1 38 . 1 . 1 13 13 C H2' H 1 4.68 . . 1 . . . . . 13 C H2' . 53244 1 39 . 1 . 1 13 13 C H6 H 1 7.53 . . 1 . . . . . 13 C H6 . 53244 1 40 . 1 . 1 14 14 A H1' H 1 5.84 . . 1 . . . . . 14 A H1' . 53244 1 41 . 1 . 1 14 14 A H2' H 1 4.29 . . 1 . . . . . 14 A H2' . 53244 1 42 . 1 . 1 14 14 A H8 H 1 8.24 . . 1 . . . . . 14 A H8 . 53244 1 43 . 1 . 1 15 15 C H1' H 1 5.74 . . 1 . . . . . 15 C H1' . 53244 1 44 . 1 . 1 15 15 C H2' H 1 4.31 . . 1 . . . . . 15 C H2' . 53244 1 45 . 1 . 1 15 15 C H6 H 1 7.73 . . 1 . . . . . 15 C H6 . 53244 1 46 . 1 . 1 16 16 A H1' H 1 5.84 . . 1 . . . . . 16 A H1' . 53244 1 47 . 1 . 1 16 16 A H2' H 1 4.66 . . 1 . . . . . 16 A H2' . 53244 1 48 . 1 . 1 16 16 A H8 H 1 8.12 . . 1 . . . . . 16 A H8 . 53244 1 49 . 1 . 1 17 17 G H1' H 1 5.68 . . 1 . . . . . 17 G H1' . 53244 1 50 . 1 . 1 17 17 G H2' H 1 4.37 . . 1 . . . . . 17 G H2' . 53244 1 51 . 1 . 1 17 17 G H8 H 1 7.69 . . 1 . . . . . 17 G H8 . 53244 1 52 . 1 . 1 18 18 C H1' H 1 5.81 . . 1 . . . . . 18 C H1' . 53244 1 53 . 1 . 1 18 18 C H2' H 1 4.32 . . 1 . . . . . 18 C H2' . 53244 1 54 . 1 . 1 18 18 C H6 H 1 7.83 . . 1 . . . . . 18 C H6 . 53244 1 55 . 1 . 1 19 19 C H1' H 1 5.55 . . 1 . . . . . 19 C H1' . 53244 1 56 . 1 . 1 19 19 C H2' H 1 4.59 . . 1 . . . . . 19 C H2' . 53244 1 57 . 1 . 1 19 19 C H6 H 1 7.70 . . 1 . . . . . 19 C H6 . 53244 1 58 . 1 . 1 20 20 U H1' H 1 5.64 . . 1 . . . . . 20 U H1' . 53244 1 59 . 1 . 1 20 20 U H2' H 1 4.63 . . 1 . . . . . 20 U H2' . 53244 1 60 . 1 . 1 20 20 U H6 H 1 7.92 . . 1 . . . . . 20 U H6 . 53244 1 61 . 1 . 1 21 21 G H1' H 1 5.88 . . 1 . . . . . 21 G H1' . 53244 1 62 . 1 . 1 21 21 G H2' H 1 4.55 . . 1 . . . . . 21 G H2' . 53244 1 63 . 1 . 1 21 21 G H8 H 1 7.90 . . 1 . . . . . 21 G H8 . 53244 1 64 . 1 . 1 22 22 U H1' H 1 5.58 . . 1 . . . . . 22 U H1' . 53244 1 65 . 1 . 1 22 22 U H2' H 1 4.48 . . 1 . . . . . 22 U H2' . 53244 1 66 . 1 . 1 22 22 U H6 H 1 7.92 . . 1 . . . . . 22 U H6 . 53244 1 67 . 1 . 1 23 23 C H1' H 1 5.61 . . 1 . . . . . 23 C H1' . 53244 1 68 . 1 . 1 23 23 C H2' H 1 4.32 . . 1 . . . . . 23 C H2' . 53244 1 69 . 1 . 1 23 23 C H6 H 1 7.95 . . 1 . . . . . 23 C H6 . 53244 1 70 . 1 . 1 24 24 U H1' H 1 5.51 . . 1 . . . . . 24 U H1' . 53244 1 71 . 1 . 1 24 24 U H2' H 1 4.34 . . 1 . . . . . 24 U H2' . 53244 1 72 . 1 . 1 24 24 U H6 H 1 7.97 . . 1 . . . . . 24 U H6 . 53244 1 73 . 1 . 1 25 25 C H1' H 1 5.56 . . 1 . . . . . 25 C H1' . 53244 1 74 . 1 . 1 25 25 C H2' H 1 4.20 . . 1 . . . . . 25 C H2' . 53244 1 75 . 1 . 1 25 25 C H6 H 1 7.93 . . 1 . . . . . 25 C H6 . 53244 1 76 . 1 . 1 26 26 C H1' H 1 5.70 . . 1 . . . . . 26 C H1' . 53244 1 77 . 1 . 1 26 26 C H2' H 1 3.97 . . 1 . . . . . 26 C H2' . 53244 1 78 . 1 . 1 26 26 C H6 H 1 7.68 . . 1 . . . . . 26 C H6 . 53244 1 stop_ save_ save_assigned_chemical_shifts_2 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_2 _Assigned_chem_shift_list.Entry_ID 53244 _Assigned_chem_shift_list.ID 2 _Assigned_chem_shift_list.Name 'TOCSY,HMQC, HSQC' _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 2 TOCSY . . . 53244 2 3 HMQC . . . 53244 2 4 HSQC . . . 53244 2 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 53244 2 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 1 1 G H1 H 1 12.78 . . 1 . . . . . 1 G H1 . 53244 2 2 . 1 . 1 1 1 G H1' H 1 5.84 . . 1 . . . . . 1 G H1' . 53244 2 3 . 1 . 1 1 1 G H2' H 1 4.96 . . 1 . . . . . 1 G H2' . 53244 2 4 . 1 . 1 1 1 G H8 H 1 8.23 . . 1 . . . . . 1 G H8 . 53244 2 5 . 1 . 1 1 1 G C1' C 13 93.07 . . 1 . . . . . 1 G C1' . 53244 2 6 . 1 . 1 1 1 G C8 C 13 140.05 . . 1 . . . . . 1 G C8 . 53244 2 7 . 1 . 1 1 1 G N1 N 15 147.71 . . 1 . . . . . 1 G N1 . 53244 2 8 . 1 . 1 2 2 G H1 H 1 12.63 . . 1 . . . . . 2 G H1 . 53244 2 9 . 1 . 1 2 2 G H1' H 1 5.92 . . 1 . . . . . 2 G H1' . 53244 2 10 . 1 . 1 2 2 G H2' H 1 4.97 . . 1 . . . . . 2 G H2' . 53244 2 11 . 1 . 1 2 2 G H8 H 1 7.63 . . 1 . . . . . 2 G H8 . 53244 2 12 . 1 . 1 2 2 G C1' C 13 93.11 . . 1 . . . . . 2 G C1' . 53244 2 13 . 1 . 1 2 2 G C8 C 13 137.29 . . 1 . . . . . 2 G C8 . 53244 2 14 . 1 . 1 2 2 G N1 N 15 146.95 . . 1 . . . . . 2 G N1 . 53244 2 15 . 1 . 1 3 3 A H1' H 1 5.98 . . 1 . . . . . 3 A H1' . 53244 2 16 . 1 . 1 3 3 A H2 H 1 7.45 . . 1 . . . . . 3 A H2 . 53244 2 17 . 1 . 1 3 3 A H2' H 1 4.48 . . 1 . . . . . 3 A H2' . 53244 2 18 . 1 . 1 3 3 A H8 H 1 7.80 . . 1 . . . . . 3 A H8 . 53244 2 19 . 1 . 1 3 3 A C1' C 13 93.07 . . 1 . . . . . 3 A C1' . 53244 2 20 . 1 . 1 3 3 A C2 C 13 153.67 . . 1 . . . . . 3 A C2 . 53244 2 21 . 1 . 1 3 3 A C8 C 13 139.43 . . 1 . . . . . 3 A C8 . 53244 2 22 . 1 . 1 4 4 G H1 H 1 12.57 . . 1 . . . . . 4 G H1 . 53244 2 23 . 1 . 1 4 4 G H1' H 1 5.57 . . 1 . . . . . 4 G H1' . 53244 2 24 . 1 . 1 4 4 G H2' H 1 4.68 . . 1 . . . . . 4 G H2' . 53244 2 25 . 1 . 1 4 4 G H8 H 1 7.13 . . 1 . . . . . 4 G H8 . 53244 2 26 . 1 . 1 4 4 G C1' C 13 92.83 . . 1 . . . . . 4 G C1' . 53244 2 27 . 1 . 1 4 4 G C8 C 13 136.03 . . 1 . . . . . 4 G C8 . 53244 2 28 . 1 . 1 4 4 G N1 N 15 146.84 . . 1 . . . . . 4 G N1 . 53244 2 29 . 1 . 1 5 5 A H1' H 1 5.94 . . 1 . . . . . 5 A H1' . 53244 2 30 . 1 . 1 5 5 A H2 H 1 7.77 . . 1 . . . . . 5 A H2 . 53244 2 31 . 1 . 1 5 5 A H2' H 1 4.50 . . 1 . . . . . 5 A H2' . 53244 2 32 . 1 . 1 5 5 A H8 H 1 7.81 . . 1 . . . . . 5 A H8 . 53244 2 33 . 1 . 1 5 5 A C1' C 13 92.87 . . 1 . . . . . 5 A C1' . 53244 2 34 . 1 . 1 5 5 A C2 C 13 153.80 . . 1 . . . . . 5 A C2 . 53244 2 35 . 1 . 1 5 5 A C8 C 13 139.46 . . 1 . . . . . 5 A C8 . 53244 2 36 . 1 . 1 6 6 C H1' H 1 5.33 . . 1 . . . . . 6 C H1' . 53244 2 37 . 1 . 1 6 6 C H2' H 1 4.33 . . 1 . . . . . 6 C H2' . 53244 2 38 . 1 . 1 6 6 C H5 H 1 5.19 . . 1 . . . . . 6 C H5 . 53244 2 39 . 1 . 1 6 6 C H6 H 1 7.38 . . 1 . . . . . 6 C H6 . 53244 2 40 . 1 . 1 6 6 C C1' C 13 93.68 . . 1 . . . . . 6 C C1' . 53244 2 41 . 1 . 1 6 6 C C5 C 13 93.37 . . 1 . . . . . 6 C C5 . 53244 2 42 . 1 . 1 6 6 C C6 C 13 138.83 . . 1 . . . . . 6 C C6 . 53244 2 43 . 1 . 1 7 7 A H1' H 1 5.96 . . 1 . . . . . 7 A H1' . 53244 2 44 . 1 . 1 7 7 A H2 H 1 7.39 . . 1 . . . . . 7 A H2 . 53244 2 45 . 1 . 1 7 7 A H2' H 1 4.45 . . 1 . . . . . 7 A H2' . 53244 2 46 . 1 . 1 7 7 A H8 H 1 7.91 . . 1 . . . . . 7 A H8 . 53244 2 47 . 1 . 1 7 7 A C1' C 13 90.96 . . 1 . . . . . 7 A C1' . 53244 2 48 . 1 . 1 7 7 A C2 C 13 153.68 . . 1 . . . . . 7 A C2 . 53244 2 49 . 1 . 1 7 7 A C8 C 13 139.83 . . 1 . . . . . 7 A C8 . 53244 2 50 . 1 . 1 8 8 U H1' H 1 5.45 . . 1 . . . . . 8 U H1' . 53244 2 51 . 1 . 1 8 8 U H2' H 1 4.15 . . 1 . . . . . 8 U H2' . 53244 2 52 . 1 . 1 8 8 U H5 H 1 5.21 . . 1 . . . . . 8 U H5 . 53244 2 53 . 1 . 1 8 8 U H6 H 1 7.42 . . 1 . . . . . 8 U H6 . 53244 2 54 . 1 . 1 8 8 U C1' C 13 92.19 . . 1 . . . . . 8 U C1' . 53244 2 55 . 1 . 1 8 8 U C5 C 13 104.13 . . 1 . . . . . 8 U C5 . 53244 2 56 . 1 . 1 8 8 U C6 C 13 141.50 . . 1 . . . . . 8 U C6 . 53244 2 57 . 1 . 1 9 9 A H1' H 1 5.90 . . 1 . . . . . 9 A H1' . 53244 2 58 . 1 . 1 9 9 A H2 H 1 7.92 . . 1 . . . . . 9 A H2 . 53244 2 59 . 1 . 1 9 9 A H2' H 1 4.64 . . 1 . . . . . 9 A H2' . 53244 2 60 . 1 . 1 9 9 A H8 H 1 8.17 . . 1 . . . . . 9 A H8 . 53244 2 61 . 1 . 1 9 9 A C1' C 13 91.32 . . 1 . . . . . 9 A C1' . 53244 2 62 . 1 . 1 9 9 A C2 C 13 154.81 . . 1 . . . . . 9 A C2 . 53244 2 63 . 1 . 1 9 9 A C8 C 13 141.63 . . 1 . . . . . 9 A C8 . 53244 2 64 . 1 . 1 10 10 U H1' H 1 5.58 . . 1 . . . . . 10 U H1' . 53244 2 65 . 1 . 1 10 10 U H2' H 1 4.25 . . 1 . . . . . 10 U H2' . 53244 2 66 . 1 . 1 10 10 U H5 H 1 5.52 . . 1 . . . . . 10 U H5 . 53244 2 67 . 1 . 1 10 10 U H6 H 1 7.59 . . 1 . . . . . 10 U H6 . 53244 2 68 . 1 . 1 10 10 U C1' C 13 93.00 . . 1 . . . . . 10 U C1' . 53244 2 69 . 1 . 1 10 10 U C5 C 13 104.98 . . 1 . . . . . 10 U C5 . 53244 2 70 . 1 . 1 10 10 U C6 C 13 142.45 . . 1 . . . . . 10 U C6 . 53244 2 71 . 1 . 1 11 11 A H1' H 1 5.96 . . 1 . . . . . 11 A H1' . 53244 2 72 . 1 . 1 11 11 A H2 H 1 7.90 . . 1 . . . . . 11 A H2 . 53244 2 73 . 1 . 1 11 11 A H2' H 1 4.68 . . 1 . . . . . 11 A H2' . 53244 2 74 . 1 . 1 11 11 A H8 H 1 8.27 . . 1 . . . . . 11 A H8 . 53244 2 75 . 1 . 1 11 11 A C1' C 13 92.84 . . 1 . . . . . 11 A C1' . 53244 2 76 . 1 . 1 11 11 A C2 C 13 154.31 . . 1 . . . . . 11 A C2 . 53244 2 77 . 1 . 1 11 11 A C8 C 13 141.95 . . 1 . . . . . 11 A C8 . 53244 2 78 . 1 . 1 12 12 U H1' H 1 5.56 . . 1 . . . . . 12 U H1' . 53244 2 79 . 1 . 1 12 12 U H2' H 1 4.32 . . 1 . . . . . 12 U H2' . 53244 2 80 . 1 . 1 12 12 U H5 H 1 5.48 . . 1 . . . . . 12 U H5 . 53244 2 81 . 1 . 1 12 12 U H6 H 1 7.68 . . 1 . . . . . 12 U H6 . 53244 2 82 . 1 . 1 12 12 U C1' C 13 93.88 . . 1 . . . . . 12 U C1' . 53244 2 83 . 1 . 1 12 12 U C5 C 13 104.96 . . 1 . . . . . 12 U C5 . 53244 2 84 . 1 . 1 12 12 U C6 C 13 142.86 . . 1 . . . . . 12 U C6 . 53244 2 85 . 1 . 1 13 13 C H1' H 1 5.92 . . 1 . . . . . 13 C H1' . 53244 2 86 . 1 . 1 13 13 C H2' H 1 4.68 . . 1 . . . . . 13 C H2' . 53244 2 87 . 1 . 1 13 13 C H5 H 1 5.50 . . 1 . . . . . 13 C H5 . 53244 2 88 . 1 . 1 13 13 C H6 H 1 7.53 . . 1 . . . . . 13 C H6 . 53244 2 89 . 1 . 1 13 13 C C5 C 13 97.96 . . 1 . . . . . 13 C C5 . 53244 2 90 . 1 . 1 13 13 C C6 C 13 141.64 . . 1 . . . . . 13 C C6 . 53244 2 91 . 1 . 1 14 14 A H1' H 1 5.84 . . 1 . . . . . 14 A H1' . 53244 2 92 . 1 . 1 14 14 A H2 H 1 8.03 . . 1 . . . . . 14 A H2 . 53244 2 93 . 1 . 1 14 14 A H2' H 1 4.29 . . 1 . . . . . 14 A H2' . 53244 2 94 . 1 . 1 14 14 A H8 H 1 8.24 . . 1 . . . . . 14 A H8 . 53244 2 95 . 1 . 1 14 14 A C1' C 13 91.68 . . 1 . . . . . 14 A C1' . 53244 2 96 . 1 . 1 14 14 A C2 C 13 155.02 . . 1 . . . . . 14 A C2 . 53244 2 97 . 1 . 1 14 14 A C8 C 13 141.59 . . 1 . . . . . 14 A C8 . 53244 2 98 . 1 . 1 15 15 C H1' H 1 5.75 . . 1 . . . . . 15 C H1' . 53244 2 99 . 1 . 1 15 15 C H2' H 1 4.31 . . 1 . . . . . 15 C H2' . 53244 2 100 . 1 . 1 15 15 C H5 H 1 5.84 . . 1 . . . . . 15 C H5 . 53244 2 101 . 1 . 1 15 15 C H6 H 1 7.74 . . 1 . . . . . 15 C H6 . 53244 2 102 . 1 . 1 15 15 C C1' C 13 91.11 . . 1 . . . . . 15 C C1' . 53244 2 103 . 1 . 1 15 15 C C5 C 13 98.54 . . 1 . . . . . 15 C C5 . 53244 2 104 . 1 . 1 15 15 C C6 C 13 143.01 . . 1 . . . . . 15 C C6 . 53244 2 105 . 1 . 1 16 16 A H1' H 1 5.84 . . 1 . . . . . 16 A H1' . 53244 2 106 . 1 . 1 16 16 A H2 H 1 7.97 . . 1 . . . . . 16 A H2 . 53244 2 107 . 1 . 1 16 16 A H2' H 1 4.66 . . 1 . . . . . 16 A H2' . 53244 2 108 . 1 . 1 16 16 A H8 H 1 8.12 . . 1 . . . . . 16 A H8 . 53244 2 109 . 1 . 1 16 16 A C1' C 13 91.81 . . 1 . . . . . 16 A C1' . 53244 2 110 . 1 . 1 16 16 A C2 C 13 154.98 . . 1 . . . . . 16 A C2 . 53244 2 111 . 1 . 1 16 16 A C8 C 13 141.19 . . 1 . . . . . 16 A C8 . 53244 2 112 . 1 . 1 17 17 G H1' H 1 5.50 . . 1 . . . . . 17 G H1' . 53244 2 113 . 1 . 1 17 17 G H2' H 1 4.58 . . 1 . . . . . 17 G H2' . 53244 2 114 . 1 . 1 17 17 G H8 H 1 7.70 . . 1 . . . . . 17 G H8 . 53244 2 115 . 1 . 1 17 17 G C1' C 13 91.33 . . 1 . . . . . 17 G C1' . 53244 2 116 . 1 . 1 17 17 G C8 C 13 138.53 . . 1 . . . . . 17 G C8 . 53244 2 117 . 1 . 1 18 18 C H1' H 1 5.68 . . 1 . . . . . 18 C H1' . 53244 2 118 . 1 . 1 18 18 C H2' H 1 4.35 . . 1 . . . . . 18 C H2' . 53244 2 119 . 1 . 1 18 18 C H5 H 1 5.59 . . 1 . . . . . 18 C H5 . 53244 2 120 . 1 . 1 18 18 C H6 H 1 7.70 . . 1 . . . . . 18 C H6 . 53244 2 121 . 1 . 1 18 18 C C1' C 13 92.52 . . 1 . . . . . 18 C C1' . 53244 2 122 . 1 . 1 18 18 C C5 C 13 98.02 . . 1 . . . . . 18 C C5 . 53244 2 123 . 1 . 1 18 18 C C6 C 13 141.58 . . 1 . . . . . 18 C C6 . 53244 2 124 . 1 . 1 19 19 C H1' H 1 5.81 . . 1 . . . . . 19 C H1' . 53244 2 125 . 1 . 1 19 19 C H2' H 1 4.39 . . 1 . . . . . 19 C H2' . 53244 2 126 . 1 . 1 19 19 C H5 H 1 5.80 . . 1 . . . . . 19 C H5 . 53244 2 127 . 1 . 1 19 19 C H6 H 1 7.83 . . 1 . . . . . 19 C H6 . 53244 2 128 . 1 . 1 19 19 C C5 C 13 98.44 . . 1 . . . . . 19 C C5 . 53244 2 129 . 1 . 1 19 19 C C6 C 13 141.67 . . 1 . . . . . 19 C C6 . 53244 2 130 . 1 . 1 20 20 U H1' H 1 5.65 . . 1 . . . . . 20 U H1' . 53244 2 131 . 1 . 1 20 20 U H2' H 1 4.54 . . 1 . . . . . 20 U H2' . 53244 2 132 . 1 . 1 20 20 U H3 H 1 13.87 . . 1 . . . . . 20 U H3 . 53244 2 133 . 1 . 1 20 20 U H5 H 1 5.75 . . 1 . . . . . 20 U H5 . 53244 2 134 . 1 . 1 20 20 U H6 H 1 7.90 . . 1 . . . . . 20 U H6 . 53244 2 135 . 1 . 1 20 20 U C1' C 13 91.56 . . 1 . . . . . 20 U C1' . 53244 2 136 . 1 . 1 20 20 U C5 C 13 104.88 . . 1 . . . . . 20 U C5 . 53244 2 137 . 1 . 1 20 20 U C6 C 13 142.40 . . 1 . . . . . 20 U C6 . 53244 2 138 . 1 . 1 20 20 U N3 N 15 162.76 . . 1 . . . . . 20 U N3 . 53244 2 139 . 1 . 1 21 21 G H1 H 1 14.40 . . 1 . . . . . 21 G H1 . 53244 2 140 . 1 . 1 21 21 G H1' H 1 5.88 . . 1 . . . . . 21 G H1' . 53244 2 141 . 1 . 1 21 21 G H2' H 1 4.63 . . 1 . . . . . 21 G H2' . 53244 2 142 . 1 . 1 21 21 G H8 H 1 7.90 . . 1 . . . . . 21 G H8 . 53244 2 143 . 1 . 1 21 21 G C1' C 13 93.12 . . 1 . . . . . 21 G C1' . 53244 2 144 . 1 . 1 21 21 G C8 C 13 137.39 . . 1 . . . . . 21 G C8 . 53244 2 145 . 1 . 1 21 21 G N1 N 15 146.92 . . 1 . . . . . 21 G N1 . 53244 2 146 . 1 . 1 22 22 U H1' H 1 5.57 . . 1 . . . . . 22 U H1' . 53244 2 147 . 1 . 1 22 22 U H2' H 1 4.48 . . 1 . . . . . 22 U H2' . 53244 2 148 . 1 . 1 22 22 U H3 H 1 13.91 . . 1 . . . . . 22 U H3 . 53244 2 149 . 1 . 1 22 22 U H5 H 1 5.15 . . 1 . . . . . 22 U H5 . 53244 2 150 . 1 . 1 22 22 U H6 H 1 7.90 . . 1 . . . . . 22 U H6 . 53244 2 151 . 1 . 1 22 22 U C1' C 13 93.79 . . 1 . . . . . 22 U C1' . 53244 2 152 . 1 . 1 22 22 U C5 C 13 102.71 . . 1 . . . . . 22 U C5 . 53244 2 153 . 1 . 1 22 22 U C6 C 13 142.34 . . 1 . . . . . 22 U C6 . 53244 2 154 . 1 . 1 22 22 U N3 N 15 162.19 . . 1 . . . . . 22 U N3 . 53244 2 155 . 1 . 1 23 23 C H1' H 1 5.59 . . 1 . . . . . 23 C H1' . 53244 2 156 . 1 . 1 23 23 C H2' H 1 4.50 . . 1 . . . . . 23 C H2' . 53244 2 157 . 1 . 1 23 23 C H5 H 1 5.69 . . 1 . . . . . 23 C H5 . 53244 2 158 . 1 . 1 23 23 C H6 H 1 7.94 . . 1 . . . . . 23 C H6 . 53244 2 159 . 1 . 1 23 23 C C1' C 13 93.88 . . 1 . . . . . 23 C C1' . 53244 2 160 . 1 . 1 23 23 C C5 C 13 96.70 . . 1 . . . . . 23 C C5 . 53244 2 161 . 1 . 1 23 23 C C6 C 13 141.48 . . 1 . . . . . 23 C C6 . 53244 2 162 . 1 . 1 24 24 U H1' H 1 5.51 . . 1 . . . . . 24 U H1' . 53244 2 163 . 1 . 1 24 24 U H2' H 1 4.33 . . 1 . . . . . 24 U H2' . 53244 2 164 . 1 . 1 24 24 U H3 H 1 14.27 . . 1 . . . . . 24 U H3 . 53244 2 165 . 1 . 1 24 24 U H5 H 1 5.43 . . 1 . . . . . 24 U H5 . 53244 2 166 . 1 . 1 24 24 U H6 H 1 7.97 . . 1 . . . . . 24 U H6 . 53244 2 167 . 1 . 1 24 24 U C1' C 13 91.56 . . 1 . . . . . 24 U C1' . 53244 2 168 . 1 . 1 24 24 U C5 C 13 103.50 . . 1 . . . . . 24 U C5 . 53244 2 169 . 1 . 1 24 24 U C6 C 13 142.25 . . 1 . . . . . 24 U C6 . 53244 2 170 . 1 . 1 24 24 U N3 N 15 162.40 . . 1 . . . . . 24 U N3 . 53244 2 171 . 1 . 1 25 25 C H1' H 1 5.56 . . 1 . . . . . 25 C H1' . 53244 2 172 . 1 . 1 25 25 C H2' H 1 4.20 . . 1 . . . . . 25 C H2' . 53244 2 173 . 1 . 1 25 25 C H5 H 1 5.68 . . 1 . . . . . 25 C H5 . 53244 2 174 . 1 . 1 25 25 C H6 H 1 7.94 . . 1 . . . . . 25 C H6 . 53244 2 175 . 1 . 1 25 25 C C1' C 13 92.59 . . 1 . . . . . 25 C C1' . 53244 2 176 . 1 . 1 25 25 C C5 C 13 97.99 . . 1 . . . . . 25 C C5 . 53244 2 177 . 1 . 1 25 25 C C6 C 13 141.47 . . 1 . . . . . 25 C C6 . 53244 2 178 . 1 . 1 26 26 C H1' H 1 5.70 . . 1 . . . . . 26 C H1' . 53244 2 179 . 1 . 1 26 26 C H2' H 1 3.97 . . 1 . . . . . 26 C H2' . 53244 2 180 . 1 . 1 26 26 C H5 H 1 5.60 . . 1 . . . . . 26 C H5 . 53244 2 181 . 1 . 1 26 26 C H6 H 1 7.67 . . 1 . . . . . 26 C H6 . 53244 2 182 . 1 . 1 26 26 C C1' C 13 90.98 . . 1 . . . . . 26 C C1' . 53244 2 183 . 1 . 1 26 26 C C5 C 13 98.01 . . 1 . . . . . 26 C C5 . 53244 2 184 . 1 . 1 26 26 C C6 C 13 141.54 . . 1 . . . . . 26 C C6 . 53244 2 stop_ save_