data_51773 ####################### # Entry information # ####################### save_entry_information_1 _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information_1 _Entry.ID 51773 _Entry.Title ; CTADC-H2AH2B complex ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2023-01-09 _Entry.Accession_date 2023-01-09 _Entry.Last_release_date 2023-01-10 _Entry.Original_release_date 2023-01-10 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.14.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype solution _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID 1 _Entry.Generated_software_label $software_1 _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Hideaki Ohtomo . . . . 51773 2 Junichi Kurita . . . 0000-0002-7369-3130 51773 3 Yoshifumi Nishimura . . . . 51773 stop_ loop_ _Entry_src.ID _Entry_src.Project_name _Entry_src.Organization_full_name _Entry_src.Organization_initials _Entry_src.Entry_ID 1 . 'Project laboratory' . 51773 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 3 51773 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '15N chemical shifts' 243 51773 '1H chemical shifts' 243 51773 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2023-07-07 2023-01-09 update BMRB 'update entry citation' 51773 1 . . 2023-06-30 2023-01-09 original author 'original release' 51773 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 51771 'CTADC region of NAP1' 51773 BMRB 51772 'CTADN region of NAP1' 51773 BMRB 51774 H2AH2B 51773 BMRB 51775 'R77EH2B hetero dimer' 51773 BMRB 51776 'CTADN-R77EH2B complex' 51773 BMRB 51777 'CTADN-H2AH2B complex' 51773 stop_ save_ ############### # Citations # ############### save_citations_1 _Citation.Sf_category citations _Citation.Sf_framecode citations_1 _Citation.Entry_ID 51773 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID 37380014 _Citation.DOI . _Citation.Full_citation . _Citation.Title ; Dynamic solution structures of whole human NAP1 dimer bound to one and two histone H2A-H2B heterodimers obtained by integrative methods ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'J. Mol. Biol.' _Citation.Journal_name_full 'Journal of molecular biology' _Citation.Journal_volume 435 _Citation.Journal_issue 15 _Citation.Journal_ASTM . _Citation.Journal_ISSN 1089-8638 _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 168189 _Citation.Page_last 168189 _Citation.Year 2023 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Hideaki Ohtomo . . . . 51773 1 2 Tsutomu Yamane . . . . 51773 1 3 Takashi Oda . . . . 51773 1 4 Noriyuki Kodera . . . . 51773 1 5 Junichi Kurita . . . . 51773 1 6 Yasuo Tsunaka . . . . 51773 1 7 Romain Amyot . . . . 51773 1 8 Mutsunori Ikeguchi . . . . 51773 1 9 Yoshifumi Nishimura . . . . 51773 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly_1 _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly_1 _Assembly.Entry_ID 51773 _Assembly.ID 1 _Assembly.Name 'CTADC-H2AH2B complex' _Assembly.BMRB_code . _Assembly.Number_of_components 3 _Assembly.Organic_ligands 0 _Assembly.Metal_ions 0 _Assembly.Non_standard_bonds no _Assembly.Ambiguous_conformational_states no _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange no _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 CTADC 1 $entity_1 . . yes native no no . . . 51773 1 2 H2A 2 $entity_2 . . yes native no no . . . 51773 1 3 H2B 3 $entity_3 . . yes native no no . . . 51773 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_entity_1 _Entity.Sf_category entity _Entity.Sf_framecode entity_1 _Entity.Entry_ID 51773 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name entity_1 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; LGSEEEGDEENDPDYDPKKD QNPAE ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 25 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method . _Entity.Parent_entity_ID 1 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 363 LEU . 51773 1 2 364 GLY . 51773 1 3 365 SER . 51773 1 4 366 GLU . 51773 1 5 367 GLU . 51773 1 6 368 GLU . 51773 1 7 369 GLY . 51773 1 8 370 ASP . 51773 1 9 371 GLU . 51773 1 10 372 GLU . 51773 1 11 373 ASN . 51773 1 12 374 ASP . 51773 1 13 375 PRO . 51773 1 14 376 ASP . 51773 1 15 377 TYR . 51773 1 16 378 ASP . 51773 1 17 379 PRO . 51773 1 18 380 LYS . 51773 1 19 381 LYS . 51773 1 20 382 ASP . 51773 1 21 383 GLN . 51773 1 22 384 ASN . 51773 1 23 385 PRO . 51773 1 24 386 ALA . 51773 1 25 387 GLU . 51773 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . LEU 1 1 51773 1 . GLY 2 2 51773 1 . SER 3 3 51773 1 . GLU 4 4 51773 1 . GLU 5 5 51773 1 . GLU 6 6 51773 1 . GLY 7 7 51773 1 . ASP 8 8 51773 1 . GLU 9 9 51773 1 . GLU 10 10 51773 1 . ASN 11 11 51773 1 . ASP 12 12 51773 1 . PRO 13 13 51773 1 . ASP 14 14 51773 1 . TYR 15 15 51773 1 . ASP 16 16 51773 1 . PRO 17 17 51773 1 . LYS 18 18 51773 1 . LYS 19 19 51773 1 . ASP 20 20 51773 1 . GLN 21 21 51773 1 . ASN 22 22 51773 1 . PRO 23 23 51773 1 . ALA 24 24 51773 1 . GLU 25 25 51773 1 stop_ save_ save_entity_2 _Entity.Sf_category entity _Entity.Sf_framecode entity_2 _Entity.Entry_ID 51773 _Entity.ID 2 _Entity.BMRB_code . _Entity.Name entity_2 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; AGPGMSGRGKQGGKARAKAK TRSSRAGLQFPVGRVHRLLR KGNYSERVGAGAPVYLAAVL EYLTAEILELAGNAARDNKK TRIIPRHLQLAIRNDEELNK LLGRVTIAQGGVLPNIQAVL LPKKTESHHKAKGK ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 134 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'all free' _Entity.Src_method . _Entity.Parent_entity_ID 2 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 -4 ALA . 51773 2 2 -3 GLY . 51773 2 3 -2 PRO . 51773 2 4 -1 GLY . 51773 2 5 0 MET . 51773 2 6 1 SER . 51773 2 7 2 GLY . 51773 2 8 3 ARG . 51773 2 9 4 GLY . 51773 2 10 5 LYS . 51773 2 11 6 GLN . 51773 2 12 7 GLY . 51773 2 13 8 GLY . 51773 2 14 9 LYS . 51773 2 15 10 ALA . 51773 2 16 11 ARG . 51773 2 17 12 ALA . 51773 2 18 13 LYS . 51773 2 19 14 ALA . 51773 2 20 15 LYS . 51773 2 21 16 THR . 51773 2 22 17 ARG . 51773 2 23 18 SER . 51773 2 24 19 SER . 51773 2 25 20 ARG . 51773 2 26 21 ALA . 51773 2 27 22 GLY . 51773 2 28 23 LEU . 51773 2 29 24 GLN . 51773 2 30 25 PHE . 51773 2 31 26 PRO . 51773 2 32 27 VAL . 51773 2 33 28 GLY . 51773 2 34 29 ARG . 51773 2 35 30 VAL . 51773 2 36 31 HIS . 51773 2 37 32 ARG . 51773 2 38 33 LEU . 51773 2 39 34 LEU . 51773 2 40 35 ARG . 51773 2 41 36 LYS . 51773 2 42 37 GLY . 51773 2 43 38 ASN . 51773 2 44 39 TYR . 51773 2 45 40 SER . 51773 2 46 41 GLU . 51773 2 47 42 ARG . 51773 2 48 43 VAL . 51773 2 49 44 GLY . 51773 2 50 45 ALA . 51773 2 51 46 GLY . 51773 2 52 47 ALA . 51773 2 53 48 PRO . 51773 2 54 49 VAL . 51773 2 55 50 TYR . 51773 2 56 51 LEU . 51773 2 57 52 ALA . 51773 2 58 53 ALA . 51773 2 59 54 VAL . 51773 2 60 55 LEU . 51773 2 61 56 GLU . 51773 2 62 57 TYR . 51773 2 63 58 LEU . 51773 2 64 59 THR . 51773 2 65 60 ALA . 51773 2 66 61 GLU . 51773 2 67 62 ILE . 51773 2 68 63 LEU . 51773 2 69 64 GLU . 51773 2 70 65 LEU . 51773 2 71 66 ALA . 51773 2 72 67 GLY . 51773 2 73 68 ASN . 51773 2 74 69 ALA . 51773 2 75 70 ALA . 51773 2 76 71 ARG . 51773 2 77 72 ASP . 51773 2 78 73 ASN . 51773 2 79 74 LYS . 51773 2 80 75 LYS . 51773 2 81 76 THR . 51773 2 82 77 ARG . 51773 2 83 78 ILE . 51773 2 84 79 ILE . 51773 2 85 80 PRO . 51773 2 86 81 ARG . 51773 2 87 82 HIS . 51773 2 88 83 LEU . 51773 2 89 84 GLN . 51773 2 90 85 LEU . 51773 2 91 86 ALA . 51773 2 92 87 ILE . 51773 2 93 88 ARG . 51773 2 94 89 ASN . 51773 2 95 90 ASP . 51773 2 96 91 GLU . 51773 2 97 92 GLU . 51773 2 98 93 LEU . 51773 2 99 94 ASN . 51773 2 100 95 LYS . 51773 2 101 96 LEU . 51773 2 102 97 LEU . 51773 2 103 98 GLY . 51773 2 104 99 ARG . 51773 2 105 100 VAL . 51773 2 106 101 THR . 51773 2 107 102 ILE . 51773 2 108 103 ALA . 51773 2 109 104 GLN . 51773 2 110 105 GLY . 51773 2 111 106 GLY . 51773 2 112 107 VAL . 51773 2 113 108 LEU . 51773 2 114 109 PRO . 51773 2 115 110 ASN . 51773 2 116 111 ILE . 51773 2 117 112 GLN . 51773 2 118 113 ALA . 51773 2 119 114 VAL . 51773 2 120 115 LEU . 51773 2 121 116 LEU . 51773 2 122 117 PRO . 51773 2 123 118 LYS . 51773 2 124 119 LYS . 51773 2 125 120 THR . 51773 2 126 121 GLU . 51773 2 127 122 SER . 51773 2 128 123 HIS . 51773 2 129 124 HIS . 51773 2 130 125 LYS . 51773 2 131 126 ALA . 51773 2 132 127 LYS . 51773 2 133 128 GLY . 51773 2 134 129 LYS . 51773 2 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . ALA 1 1 51773 2 . GLY 2 2 51773 2 . PRO 3 3 51773 2 . GLY 4 4 51773 2 . MET 5 5 51773 2 . SER 6 6 51773 2 . GLY 7 7 51773 2 . ARG 8 8 51773 2 . GLY 9 9 51773 2 . LYS 10 10 51773 2 . GLN 11 11 51773 2 . GLY 12 12 51773 2 . GLY 13 13 51773 2 . LYS 14 14 51773 2 . ALA 15 15 51773 2 . ARG 16 16 51773 2 . ALA 17 17 51773 2 . LYS 18 18 51773 2 . ALA 19 19 51773 2 . LYS 20 20 51773 2 . THR 21 21 51773 2 . ARG 22 22 51773 2 . SER 23 23 51773 2 . SER 24 24 51773 2 . ARG 25 25 51773 2 . ALA 26 26 51773 2 . GLY 27 27 51773 2 . LEU 28 28 51773 2 . GLN 29 29 51773 2 . PHE 30 30 51773 2 . PRO 31 31 51773 2 . VAL 32 32 51773 2 . GLY 33 33 51773 2 . ARG 34 34 51773 2 . VAL 35 35 51773 2 . HIS 36 36 51773 2 . ARG 37 37 51773 2 . LEU 38 38 51773 2 . LEU 39 39 51773 2 . ARG 40 40 51773 2 . LYS 41 41 51773 2 . GLY 42 42 51773 2 . ASN 43 43 51773 2 . TYR 44 44 51773 2 . SER 45 45 51773 2 . GLU 46 46 51773 2 . ARG 47 47 51773 2 . VAL 48 48 51773 2 . GLY 49 49 51773 2 . ALA 50 50 51773 2 . GLY 51 51 51773 2 . ALA 52 52 51773 2 . PRO 53 53 51773 2 . VAL 54 54 51773 2 . TYR 55 55 51773 2 . LEU 56 56 51773 2 . ALA 57 57 51773 2 . ALA 58 58 51773 2 . VAL 59 59 51773 2 . LEU 60 60 51773 2 . GLU 61 61 51773 2 . TYR 62 62 51773 2 . LEU 63 63 51773 2 . THR 64 64 51773 2 . ALA 65 65 51773 2 . GLU 66 66 51773 2 . ILE 67 67 51773 2 . LEU 68 68 51773 2 . GLU 69 69 51773 2 . LEU 70 70 51773 2 . ALA 71 71 51773 2 . GLY 72 72 51773 2 . ASN 73 73 51773 2 . ALA 74 74 51773 2 . ALA 75 75 51773 2 . ARG 76 76 51773 2 . ASP 77 77 51773 2 . ASN 78 78 51773 2 . LYS 79 79 51773 2 . LYS 80 80 51773 2 . THR 81 81 51773 2 . ARG 82 82 51773 2 . ILE 83 83 51773 2 . ILE 84 84 51773 2 . PRO 85 85 51773 2 . ARG 86 86 51773 2 . HIS 87 87 51773 2 . LEU 88 88 51773 2 . GLN 89 89 51773 2 . LEU 90 90 51773 2 . ALA 91 91 51773 2 . ILE 92 92 51773 2 . ARG 93 93 51773 2 . ASN 94 94 51773 2 . ASP 95 95 51773 2 . GLU 96 96 51773 2 . GLU 97 97 51773 2 . LEU 98 98 51773 2 . ASN 99 99 51773 2 . LYS 100 100 51773 2 . LEU 101 101 51773 2 . LEU 102 102 51773 2 . GLY 103 103 51773 2 . ARG 104 104 51773 2 . VAL 105 105 51773 2 . THR 106 106 51773 2 . ILE 107 107 51773 2 . ALA 108 108 51773 2 . GLN 109 109 51773 2 . GLY 110 110 51773 2 . GLY 111 111 51773 2 . VAL 112 112 51773 2 . LEU 113 113 51773 2 . PRO 114 114 51773 2 . ASN 115 115 51773 2 . ILE 116 116 51773 2 . GLN 117 117 51773 2 . ALA 118 118 51773 2 . VAL 119 119 51773 2 . LEU 120 120 51773 2 . LEU 121 121 51773 2 . PRO 122 122 51773 2 . LYS 123 123 51773 2 . LYS 124 124 51773 2 . THR 125 125 51773 2 . GLU 126 126 51773 2 . SER 127 127 51773 2 . HIS 128 128 51773 2 . HIS 129 129 51773 2 . LYS 130 130 51773 2 . ALA 131 131 51773 2 . LYS 132 132 51773 2 . GLY 133 133 51773 2 . LYS 134 134 51773 2 stop_ save_ save_entity_3 _Entity.Sf_category entity _Entity.Sf_framecode entity_3 _Entity.Entry_ID 51773 _Entity.ID 3 _Entity.BMRB_code . _Entity.Name entity_3 _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; AGPGMPEPAKSAPAPKKGSK KAVTKAQKKDGKKRKRSRKE SYSIYVYKVLKQVHPDTGIS SKAMGIMNSFVNDIFERIAG EASRLAHYNKRSTITSREIQ TAVRLLLPGELAKHAVSEGT KAVTKYTSAK ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 130 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'all free' _Entity.Src_method . _Entity.Parent_entity_ID 3 _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 -4 ALA . 51773 3 2 -3 GLY . 51773 3 3 -2 PRO . 51773 3 4 -1 GLY . 51773 3 5 0 MET . 51773 3 6 1 PRO . 51773 3 7 2 GLU . 51773 3 8 3 PRO . 51773 3 9 4 ALA . 51773 3 10 5 LYS . 51773 3 11 6 SER . 51773 3 12 7 ALA . 51773 3 13 8 PRO . 51773 3 14 9 ALA . 51773 3 15 10 PRO . 51773 3 16 11 LYS . 51773 3 17 12 LYS . 51773 3 18 13 GLY . 51773 3 19 14 SER . 51773 3 20 15 LYS . 51773 3 21 16 LYS . 51773 3 22 17 ALA . 51773 3 23 18 VAL . 51773 3 24 19 THR . 51773 3 25 20 LYS . 51773 3 26 21 ALA . 51773 3 27 22 GLN . 51773 3 28 23 LYS . 51773 3 29 24 LYS . 51773 3 30 25 ASP . 51773 3 31 26 GLY . 51773 3 32 27 LYS . 51773 3 33 28 LYS . 51773 3 34 29 ARG . 51773 3 35 30 LYS . 51773 3 36 31 ARG . 51773 3 37 32 SER . 51773 3 38 33 ARG . 51773 3 39 34 LYS . 51773 3 40 35 GLU . 51773 3 41 36 SER . 51773 3 42 37 TYR . 51773 3 43 38 SER . 51773 3 44 39 ILE . 51773 3 45 40 TYR . 51773 3 46 41 VAL . 51773 3 47 42 TYR . 51773 3 48 43 LYS . 51773 3 49 44 VAL . 51773 3 50 45 LEU . 51773 3 51 46 LYS . 51773 3 52 47 GLN . 51773 3 53 48 VAL . 51773 3 54 49 HIS . 51773 3 55 50 PRO . 51773 3 56 51 ASP . 51773 3 57 52 THR . 51773 3 58 53 GLY . 51773 3 59 54 ILE . 51773 3 60 55 SER . 51773 3 61 56 SER . 51773 3 62 57 LYS . 51773 3 63 58 ALA . 51773 3 64 59 MET . 51773 3 65 60 GLY . 51773 3 66 61 ILE . 51773 3 67 62 MET . 51773 3 68 63 ASN . 51773 3 69 64 SER . 51773 3 70 65 PHE . 51773 3 71 66 VAL . 51773 3 72 67 ASN . 51773 3 73 68 ASP . 51773 3 74 69 ILE . 51773 3 75 70 PHE . 51773 3 76 71 GLU . 51773 3 77 72 ARG . 51773 3 78 73 ILE . 51773 3 79 74 ALA . 51773 3 80 75 GLY . 51773 3 81 76 GLU . 51773 3 82 77 ALA . 51773 3 83 78 SER . 51773 3 84 79 ARG . 51773 3 85 80 LEU . 51773 3 86 81 ALA . 51773 3 87 82 HIS . 51773 3 88 83 TYR . 51773 3 89 84 ASN . 51773 3 90 85 LYS . 51773 3 91 86 ARG . 51773 3 92 87 SER . 51773 3 93 88 THR . 51773 3 94 89 ILE . 51773 3 95 90 THR . 51773 3 96 91 SER . 51773 3 97 92 ARG . 51773 3 98 93 GLU . 51773 3 99 94 ILE . 51773 3 100 95 GLN . 51773 3 101 96 THR . 51773 3 102 97 ALA . 51773 3 103 98 VAL . 51773 3 104 99 ARG . 51773 3 105 100 LEU . 51773 3 106 101 LEU . 51773 3 107 102 LEU . 51773 3 108 103 PRO . 51773 3 109 104 GLY . 51773 3 110 105 GLU . 51773 3 111 106 LEU . 51773 3 112 107 ALA . 51773 3 113 108 LYS . 51773 3 114 109 HIS . 51773 3 115 110 ALA . 51773 3 116 111 VAL . 51773 3 117 112 SER . 51773 3 118 113 GLU . 51773 3 119 114 GLY . 51773 3 120 115 THR . 51773 3 121 116 LYS . 51773 3 122 117 ALA . 51773 3 123 118 VAL . 51773 3 124 119 THR . 51773 3 125 120 LYS . 51773 3 126 121 TYR . 51773 3 127 122 THR . 51773 3 128 123 SER . 51773 3 129 124 ALA . 51773 3 130 125 LYS . 51773 3 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . ALA 1 1 51773 3 . GLY 2 2 51773 3 . PRO 3 3 51773 3 . GLY 4 4 51773 3 . MET 5 5 51773 3 . PRO 6 6 51773 3 . GLU 7 7 51773 3 . PRO 8 8 51773 3 . ALA 9 9 51773 3 . LYS 10 10 51773 3 . SER 11 11 51773 3 . ALA 12 12 51773 3 . PRO 13 13 51773 3 . ALA 14 14 51773 3 . PRO 15 15 51773 3 . LYS 16 16 51773 3 . LYS 17 17 51773 3 . GLY 18 18 51773 3 . SER 19 19 51773 3 . LYS 20 20 51773 3 . LYS 21 21 51773 3 . ALA 22 22 51773 3 . VAL 23 23 51773 3 . THR 24 24 51773 3 . LYS 25 25 51773 3 . ALA 26 26 51773 3 . GLN 27 27 51773 3 . LYS 28 28 51773 3 . LYS 29 29 51773 3 . ASP 30 30 51773 3 . GLY 31 31 51773 3 . LYS 32 32 51773 3 . LYS 33 33 51773 3 . ARG 34 34 51773 3 . LYS 35 35 51773 3 . ARG 36 36 51773 3 . SER 37 37 51773 3 . ARG 38 38 51773 3 . LYS 39 39 51773 3 . GLU 40 40 51773 3 . SER 41 41 51773 3 . TYR 42 42 51773 3 . SER 43 43 51773 3 . ILE 44 44 51773 3 . TYR 45 45 51773 3 . VAL 46 46 51773 3 . TYR 47 47 51773 3 . LYS 48 48 51773 3 . VAL 49 49 51773 3 . LEU 50 50 51773 3 . LYS 51 51 51773 3 . GLN 52 52 51773 3 . VAL 53 53 51773 3 . HIS 54 54 51773 3 . PRO 55 55 51773 3 . ASP 56 56 51773 3 . THR 57 57 51773 3 . GLY 58 58 51773 3 . ILE 59 59 51773 3 . SER 60 60 51773 3 . SER 61 61 51773 3 . LYS 62 62 51773 3 . ALA 63 63 51773 3 . MET 64 64 51773 3 . GLY 65 65 51773 3 . ILE 66 66 51773 3 . MET 67 67 51773 3 . ASN 68 68 51773 3 . SER 69 69 51773 3 . PHE 70 70 51773 3 . VAL 71 71 51773 3 . ASN 72 72 51773 3 . ASP 73 73 51773 3 . ILE 74 74 51773 3 . PHE 75 75 51773 3 . GLU 76 76 51773 3 . ARG 77 77 51773 3 . ILE 78 78 51773 3 . ALA 79 79 51773 3 . GLY 80 80 51773 3 . GLU 81 81 51773 3 . ALA 82 82 51773 3 . SER 83 83 51773 3 . ARG 84 84 51773 3 . LEU 85 85 51773 3 . ALA 86 86 51773 3 . HIS 87 87 51773 3 . TYR 88 88 51773 3 . ASN 89 89 51773 3 . LYS 90 90 51773 3 . ARG 91 91 51773 3 . SER 92 92 51773 3 . THR 93 93 51773 3 . ILE 94 94 51773 3 . THR 95 95 51773 3 . SER 96 96 51773 3 . ARG 97 97 51773 3 . GLU 98 98 51773 3 . ILE 99 99 51773 3 . GLN 100 100 51773 3 . THR 101 101 51773 3 . ALA 102 102 51773 3 . VAL 103 103 51773 3 . ARG 104 104 51773 3 . LEU 105 105 51773 3 . LEU 106 106 51773 3 . LEU 107 107 51773 3 . PRO 108 108 51773 3 . GLY 109 109 51773 3 . GLU 110 110 51773 3 . LEU 111 111 51773 3 . ALA 112 112 51773 3 . LYS 113 113 51773 3 . HIS 114 114 51773 3 . ALA 115 115 51773 3 . VAL 116 116 51773 3 . SER 117 117 51773 3 . GLU 118 118 51773 3 . GLY 119 119 51773 3 . THR 120 120 51773 3 . LYS 121 121 51773 3 . ALA 122 122 51773 3 . VAL 123 123 51773 3 . THR 124 124 51773 3 . LYS 125 125 51773 3 . TYR 126 126 51773 3 . THR 127 127 51773 3 . SER 128 128 51773 3 . ALA 129 129 51773 3 . LYS 130 130 51773 3 stop_ save_ #################### # Natural source # #################### save_natural_source_1 _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source_1 _Entity_natural_src_list.Entry_ID 51773 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $entity_1 . 9606 organism . 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 51773 1 2 2 $entity_2 . 9606 organism . 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 51773 1 3 3 $entity_3 . 9606 organism . 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 51773 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source_1 _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source_1 _Entity_experimental_src_list.Entry_ID 51773 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $entity_1 . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli . . . plasmid . . pET . . . 51773 1 2 2 $entity_2 . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli . . . plasmid . . pET . . . 51773 1 3 3 $entity_3 . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli . . . plasmid . . pET . . . 51773 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 51773 _Sample.ID 1 _Sample.Name Sample1 _Sample.Type solution _Sample.Sub_type . _Sample.Details 'CTADC-H2AH2B complex' _Sample.Aggregate_sample_number 1 _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'CTADC of NAP1' '[U-98% 15N]' . . 1 $entity_1 . . 475 350 600 uM . . . . 51773 1 2 H2A 'natural abundance' . . 2 $entity_2 . . 475 350 600 uM . . . . 51773 1 3 H2B 'natural abundance' . . 3 $entity_3 . . 475 350 600 uM . . . . 51773 1 stop_ save_ save_sample_2 _Sample.Sf_category sample _Sample.Sf_framecode sample_2 _Sample.Entry_ID 51773 _Sample.ID 2 _Sample.Name Sample2 _Sample.Type solution _Sample.Sub_type . _Sample.Details 'CTADC-H2AH2B complex' _Sample.Aggregate_sample_number 1 _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'CTADC of NAP1' 'natural abundance' . . 1 $entity_1 . . 475 350 600 uM . . . . 51773 2 2 H2A '[U-98% 15N]' . . 2 $entity_2 . . 475 350 600 uM . . . . 51773 2 3 H2B '[U-98% 15N]' . . 3 $entity_3 . . 475 350 600 uM . . . . 51773 2 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 51773 _Sample_condition_list.ID 1 _Sample_condition_list.Name 'Standard condition' _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 0.2 . M 51773 1 pH 6.0 . pH 51773 1 pressure 1 . atm 51773 1 temperature 293 . K 51773 1 stop_ save_ ############################ # Computer software used # ############################ save_software_1 _Software.Sf_category software _Software.Sf_framecode software_1 _Software.Entry_ID 51773 _Software.ID 1 _Software.Type . _Software.Name Olivia _Software.Version . _Software.DOI . _Software.Details . loop_ _Task.Task _Task.Software_module _Task.Entry_ID _Task.Software_ID 'chemical shift assignment' . 51773 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_NMR_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode NMR_spectrometer_1 _NMR_spectrometer.Entry_ID 51773 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name 'Avance III HD' _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model 'AVANCE III' _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 950 save_ ############################# # NMR applied experiments # ############################# save_experiment_list_1 _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list_1 _Experiment_list.Entry_ID 51773 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NUS_flag _Experiment.Interleaved_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Details _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-15N TROSY' no no no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51773 1 2 '2D 1H-15N TROSY' no no no . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . 1 $NMR_spectrometer_1 . . . . . . . . . . . . . . . . . 51773 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chem_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chem_shift_reference_1 _Chem_shift_reference.Entry_ID 51773 _Chem_shift_reference.ID 1 _Chem_shift_reference.Name Reference1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 DSS 'methyl protons' . . . . ppm 0.00 internal indirect 1.000000000 . . . . . 51773 1 N 15 DSS 'methyl protons' . . . . ppm 0.00 na indirect 0.101329118 . . . . . 51773 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chemical_shifts_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_1 _Assigned_chem_shift_list.Entry_ID 51773 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Name 'CTADN assignment' _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-15N TROSY' . . . 51773 1 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51773 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 1 1 LEU H H 1 8.5840 0.0000 . 1 . . . . . 363 LEU HN . 51773 1 2 . 1 . 1 1 1 LEU N N 15 122.9760 0.0000 . 1 . . . . . 363 LEU N . 51773 1 3 . 1 . 1 2 2 GLY H H 1 8.4660 0.0000 . 1 . . . . . 364 GLY HN . 51773 1 4 . 1 . 1 2 2 GLY N N 15 111.2380 0.0000 . 1 . . . . . 364 GLY N . 51773 1 5 . 1 . 1 3 3 SER H H 1 8.1410 0.0000 . 1 . . . . . 365 SER HN . 51773 1 6 . 1 . 1 3 3 SER N N 15 116.4840 0.0000 . 1 . . . . . 365 SER N . 51773 1 7 . 1 . 1 4 4 GLU H H 1 8.6540 0.0000 . 1 . . . . . 366 GLU HN . 51773 1 8 . 1 . 1 4 4 GLU N N 15 123.5180 0.0000 . 1 . . . . . 366 GLU N . 51773 1 9 . 1 . 1 5 5 GLU H H 1 8.3400 0.0000 . 1 . . . . . 367 GLU HN . 51773 1 10 . 1 . 1 5 5 GLU N N 15 121.8600 0.0000 . 1 . . . . . 367 GLU N . 51773 1 11 . 1 . 1 6 6 GLU H H 1 8.3740 0.0000 . 1 . . . . . 368 GLU HN . 51773 1 12 . 1 . 1 6 6 GLU N N 15 122.7580 0.0000 . 1 . . . . . 368 GLU N . 51773 1 13 . 1 . 1 7 7 GLY H H 1 8.4240 0.0000 . 1 . . . . . 369 GLY HN . 51773 1 14 . 1 . 1 7 7 GLY N N 15 110.7800 0.0000 . 1 . . . . . 369 GLY N . 51773 1 15 . 1 . 1 8 8 ASP H H 1 8.2310 0.0000 . 1 . . . . . 370 ASP HN . 51773 1 16 . 1 . 1 8 8 ASP N N 15 121.5050 0.0000 . 1 . . . . . 370 ASP N . 51773 1 17 . 1 . 1 9 9 GLU H H 1 8.5840 0.0000 . 1 . . . . . 371 GLU HN . 51773 1 18 . 1 . 1 9 9 GLU N N 15 121.9570 0.0000 . 1 . . . . . 371 GLU N . 51773 1 19 . 1 . 1 10 10 GLU H H 1 8.3680 0.0000 . 1 . . . . . 372 GLU HN . 51773 1 20 . 1 . 1 10 10 GLU N N 15 120.9860 0.0000 . 1 . . . . . 372 GLU N . 51773 1 21 . 1 . 1 11 11 ASN H H 1 8.1760 0.0000 . 1 . . . . . 373 ASN HN . 51773 1 22 . 1 . 1 11 11 ASN N N 15 118.3810 0.0000 . 1 . . . . . 373 ASN N . 51773 1 23 . 1 . 1 18 18 LYS H H 1 7.9230 0.0000 . 1 . . . . . 380 LYS HN . 51773 1 24 . 1 . 1 18 18 LYS N N 15 118.6700 0.0000 . 1 . . . . . 380 LYS N . 51773 1 25 . 1 . 1 20 20 ASP H H 1 7.2780 0.0000 . 1 . . . . . 382 ASP HN . 51773 1 26 . 1 . 1 20 20 ASP N N 15 121.0950 0.0000 . 1 . . . . . 382 ASP N . 51773 1 27 . 1 . 1 21 21 GLN H H 1 8.0760 0.0000 . 1 . . . . . 383 GLN HN . 51773 1 28 . 1 . 1 21 21 GLN N N 15 121.3500 0.0000 . 1 . . . . . 383 GLN N . 51773 1 29 . 1 . 1 22 22 ASN H H 1 8.4870 0.0000 . 1 . . . . . 384 ASN HN . 51773 1 30 . 1 . 1 22 22 ASN N N 15 121.7420 0.0000 . 1 . . . . . 384 ASN N . 51773 1 31 . 1 . 1 24 24 ALA H H 1 8.3010 0.0000 . 1 . . . . . 386 ALA HN . 51773 1 32 . 1 . 1 24 24 ALA N N 15 125.2920 0.0000 . 1 . . . . . 386 ALA N . 51773 1 33 . 1 . 1 25 25 GLU H H 1 7.8020 0.0000 . 1 . . . . . 387 GLU HN . 51773 1 34 . 1 . 1 25 25 GLU N N 15 125.7800 0.0000 . 1 . . . . . 387 GLU N . 51773 1 stop_ save_ save_assigned_chemical_shifts_2 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_2 _Assigned_chem_shift_list.Entry_ID 51773 _Assigned_chem_shift_list.ID 2 _Assigned_chem_shift_list.Name 'H2A assignment' _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 2 '2D 1H-15N TROSY' . . . 51773 2 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51773 2 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 2 . 2 4 4 GLY H H 1 8.5340 0.0000 . 1 . . . . . -1 GLY HN . 51773 2 2 . 2 . 2 4 4 GLY N N 15 110.4490 0.0000 . 1 . . . . . -1 GLY N . 51773 2 3 . 2 . 2 5 5 MET H H 1 8.2590 0.0000 . 1 . . . . . 0 MET HN . 51773 2 4 . 2 . 2 5 5 MET N N 15 120.9170 0.0000 . 1 . . . . . 0 MET N . 51773 2 5 . 2 . 2 6 6 SER H H 1 8.3810 0.0000 . 1 . . . . . 1 SER HN . 51773 2 6 . 2 . 2 6 6 SER N N 15 117.8680 0.0000 . 1 . . . . . 1 SER N . 51773 2 7 . 2 . 2 7 7 GLY H H 1 8.4060 0.0000 . 1 . . . . . 2 GLY HN . 51773 2 8 . 2 . 2 7 7 GLY N N 15 111.5850 0.0000 . 1 . . . . . 2 GLY N . 51773 2 9 . 2 . 2 8 8 ARG H H 1 8.1570 0.0000 . 1 . . . . . 3 ARG HN . 51773 2 10 . 2 . 2 8 8 ARG N N 15 121.1340 0.0000 . 1 . . . . . 3 ARG N . 51773 2 11 . 2 . 2 9 9 GLY H H 1 8.4180 0.0000 . 1 . . . . . 4 GLY HN . 51773 2 12 . 2 . 2 9 9 GLY N N 15 110.6020 0.0000 . 1 . . . . . 4 GLY N . 51773 2 13 . 2 . 2 10 10 LYS H H 1 8.2030 0.0000 . 1 . . . . . 5 LYS HN . 51773 2 14 . 2 . 2 10 10 LYS N N 15 121.8250 0.0000 . 1 . . . . . 5 LYS N . 51773 2 15 . 2 . 2 11 11 GLN H H 1 8.4630 0.0000 . 1 . . . . . 6 GLN HN . 51773 2 16 . 2 . 2 11 11 GLN N N 15 122.1650 0.0000 . 1 . . . . . 6 GLN N . 51773 2 17 . 2 . 2 12 12 GLY H H 1 8.4060 0.0000 . 1 . . . . . 7 GLY HN . 51773 2 18 . 2 . 2 12 12 GLY N N 15 111.0020 0.0000 . 1 . . . . . 7 GLY N . 51773 2 19 . 2 . 2 13 13 GLY H H 1 8.2590 0.0000 . 1 . . . . . 8 GLY HN . 51773 2 20 . 2 . 2 13 13 GLY N N 15 109.6520 0.0000 . 1 . . . . . 8 GLY N . 51773 2 21 . 2 . 2 14 14 LYS H H 1 8.1750 0.0000 . 1 . . . . . 9 LYS HN . 51773 2 22 . 2 . 2 14 14 LYS N N 15 121.8440 0.0000 . 1 . . . . . 9 LYS N . 51773 2 23 . 2 . 2 15 15 ALA H H 1 8.2640 0.0000 . 1 . . . . . 10 ALA HN . 51773 2 24 . 2 . 2 15 15 ALA N N 15 125.8940 0.0000 . 1 . . . . . 10 ALA N . 51773 2 25 . 2 . 2 16 16 ARG H H 1 8.2580 0.0000 . 1 . . . . . 11 ARG HN . 51773 2 26 . 2 . 2 16 16 ARG N N 15 121.5080 0.0000 . 1 . . . . . 11 ARG N . 51773 2 27 . 2 . 2 17 17 ALA H H 1 8.2290 0.0000 . 1 . . . . . 12 ALA HN . 51773 2 28 . 2 . 2 17 17 ALA N N 15 126.2090 0.0000 . 1 . . . . . 12 ALA N . 51773 2 29 . 2 . 2 18 18 LYS H H 1 8.2380 0.0000 . 1 . . . . . 13 LYS HN . 51773 2 30 . 2 . 2 18 18 LYS N N 15 121.6300 0.0000 . 1 . . . . . 13 LYS N . 51773 2 31 . 2 . 2 19 19 ALA H H 1 8.2720 0.0000 . 1 . . . . . 14 ALA HN . 51773 2 32 . 2 . 2 19 19 ALA N N 15 126.0990 0.0000 . 1 . . . . . 14 ALA N . 51773 2 33 . 2 . 2 20 20 LYS H H 1 8.3520 0.0000 . 1 . . . . . 15 LYS HN . 51773 2 34 . 2 . 2 20 20 LYS N N 15 121.8590 0.0000 . 1 . . . . . 15 LYS N . 51773 2 35 . 2 . 2 21 21 THR H H 1 8.1410 0.0000 . 1 . . . . . 16 THR HN . 51773 2 36 . 2 . 2 21 21 THR N N 15 116.1460 0.0000 . 1 . . . . . 16 THR N . 51773 2 37 . 2 . 2 22 22 ARG H H 1 8.4570 0.0000 . 1 . . . . . 17 ARG HN . 51773 2 38 . 2 . 2 22 22 ARG N N 15 124.3660 0.0000 . 1 . . . . . 17 ARG N . 51773 2 39 . 2 . 2 23 23 SER H H 1 8.4410 0.0000 . 1 . . . . . 18 SER HN . 51773 2 40 . 2 . 2 23 23 SER N N 15 117.7770 0.0000 . 1 . . . . . 18 SER N . 51773 2 41 . 2 . 2 24 24 SER H H 1 8.3800 0.0000 . 1 . . . . . 19 SER HN . 51773 2 42 . 2 . 2 24 24 SER N N 15 119.4140 0.0000 . 1 . . . . . 19 SER N . 51773 2 43 . 2 . 2 25 25 ARG H H 1 8.2920 0.0000 . 1 . . . . . 20 ARG HN . 51773 2 44 . 2 . 2 25 25 ARG N N 15 123.6640 0.0000 . 1 . . . . . 20 ARG N . 51773 2 45 . 2 . 2 27 27 GLY H H 1 7.9990 0.0000 . 1 . . . . . 22 GLY HN . 51773 2 46 . 2 . 2 27 27 GLY N N 15 108.1500 0.0000 . 1 . . . . . 22 GLY N . 51773 2 47 . 2 . 2 28 28 LEU H H 1 8.0150 0.0000 . 1 . . . . . 23 LEU HN . 51773 2 48 . 2 . 2 28 28 LEU N N 15 121.9260 0.0000 . 1 . . . . . 23 LEU N . 51773 2 49 . 2 . 2 32 32 VAL H H 1 8.2260 0.0000 . 1 . . . . . 27 VAL HN . 51773 2 50 . 2 . 2 32 32 VAL N N 15 128.6950 0.0000 . 1 . . . . . 27 VAL N . 51773 2 51 . 2 . 2 33 33 GLY H H 1 8.7680 0.0000 . 1 . . . . . 28 GLY HN . 51773 2 52 . 2 . 2 33 33 GLY N N 15 108.0330 0.0000 . 1 . . . . . 28 GLY N . 51773 2 53 . 2 . 2 34 34 ARG H H 1 7.2140 0.0000 . 1 . . . . . 29 ARG HN . 51773 2 54 . 2 . 2 34 34 ARG N N 15 122.1030 0.0000 . 1 . . . . . 29 ARG N . 51773 2 55 . 2 . 2 35 35 VAL H H 1 7.7200 0.0000 . 1 . . . . . 30 VAL HN . 51773 2 56 . 2 . 2 35 35 VAL N N 15 119.9430 0.0000 . 1 . . . . . 30 VAL N . 51773 2 57 . 2 . 2 36 36 HIS H H 1 8.7300 0.0000 . 1 . . . . . 31 HIS HN . 51773 2 58 . 2 . 2 36 36 HIS N N 15 120.7110 0.0000 . 1 . . . . . 31 HIS N . 51773 2 59 . 2 . 2 37 37 ARG H H 1 7.9740 0.0000 . 1 . . . . . 32 ARG HN . 51773 2 60 . 2 . 2 37 37 ARG N N 15 118.9910 0.0000 . 1 . . . . . 32 ARG N . 51773 2 61 . 2 . 2 38 38 LEU H H 1 8.3630 0.0000 . 1 . . . . . 33 LEU HN . 51773 2 62 . 2 . 2 38 38 LEU N N 15 120.3280 0.0000 . 1 . . . . . 33 LEU N . 51773 2 63 . 2 . 2 39 39 LEU H H 1 8.4050 0.0000 . 1 . . . . . 34 LEU HN . 51773 2 64 . 2 . 2 39 39 LEU N N 15 120.3240 0.0000 . 1 . . . . . 34 LEU N . 51773 2 65 . 2 . 2 40 40 ARG H H 1 7.9880 0.0000 . 1 . . . . . 35 ARG HN . 51773 2 66 . 2 . 2 40 40 ARG N N 15 118.6500 0.0000 . 1 . . . . . 35 ARG N . 51773 2 67 . 2 . 2 42 42 GLY H H 1 7.5870 0.0000 . 1 . . . . . 37 GLY HN . 51773 2 68 . 2 . 2 42 42 GLY N N 15 104.8660 0.0000 . 1 . . . . . 37 GLY N . 51773 2 69 . 2 . 2 43 43 ASN H H 1 7.8950 0.0000 . 1 . . . . . 38 ASN HN . 51773 2 70 . 2 . 2 43 43 ASN N N 15 116.1050 0.0000 . 1 . . . . . 38 ASN N . 51773 2 71 . 2 . 2 44 44 TYR H H 1 7.7920 0.0000 . 1 . . . . . 39 TYR HN . 51773 2 72 . 2 . 2 44 44 TYR N N 15 117.4800 0.0000 . 1 . . . . . 39 TYR N . 51773 2 73 . 2 . 2 45 45 SER H H 1 7.9910 0.0000 . 1 . . . . . 40 SER HN . 51773 2 74 . 2 . 2 45 45 SER N N 15 112.3500 0.0000 . 1 . . . . . 40 SER N . 51773 2 75 . 2 . 2 46 46 GLU H H 1 8.5040 0.0000 . 1 . . . . . 41 GLU HN . 51773 2 76 . 2 . 2 46 46 GLU N N 15 122.2150 0.0000 . 1 . . . . . 41 GLU N . 51773 2 77 . 2 . 2 47 47 ARG H H 1 8.1060 0.0000 . 1 . . . . . 42 ARG HN . 51773 2 78 . 2 . 2 47 47 ARG N N 15 116.6390 0.0000 . 1 . . . . . 42 ARG N . 51773 2 79 . 2 . 2 48 48 VAL H H 1 8.8660 0.0000 . 1 . . . . . 43 VAL HN . 51773 2 80 . 2 . 2 48 48 VAL N N 15 125.2150 0.0000 . 1 . . . . . 43 VAL N . 51773 2 81 . 2 . 2 49 49 GLY H H 1 9.1030 0.0000 . 1 . . . . . 44 GLY HN . 51773 2 82 . 2 . 2 49 49 GLY N N 15 116.7030 0.0000 . 1 . . . . . 44 GLY N . 51773 2 83 . 2 . 2 50 50 ALA H H 1 8.5110 0.0000 . 1 . . . . . 45 ALA HN . 51773 2 84 . 2 . 2 50 50 ALA N N 15 123.1600 0.0000 . 1 . . . . . 45 ALA N . 51773 2 85 . 2 . 2 51 51 GLY H H 1 8.6310 0.0000 . 1 . . . . . 46 GLY HN . 51773 2 86 . 2 . 2 51 51 GLY N N 15 105.7730 0.0000 . 1 . . . . . 46 GLY N . 51773 2 87 . 2 . 2 52 52 ALA H H 1 7.4450 0.0000 . 1 . . . . . 47 ALA HN . 51773 2 88 . 2 . 2 52 52 ALA N N 15 124.9860 0.0000 . 1 . . . . . 47 ALA N . 51773 2 89 . 2 . 2 54 54 VAL H H 1 6.2720 0.0000 . 1 . . . . . 49 VAL HN . 51773 2 90 . 2 . 2 54 54 VAL N N 15 118.8490 0.0000 . 1 . . . . . 49 VAL N . 51773 2 91 . 2 . 2 55 55 TYR H H 1 7.9120 0.0000 . 1 . . . . . 50 TYR HN . 51773 2 92 . 2 . 2 55 55 TYR N N 15 120.6740 0.0000 . 1 . . . . . 50 TYR N . 51773 2 93 . 2 . 2 56 56 LEU H H 1 8.2720 0.0000 . 1 . . . . . 51 LEU HN . 51773 2 94 . 2 . 2 56 56 LEU N N 15 116.2000 0.0000 . 1 . . . . . 51 LEU N . 51773 2 95 . 2 . 2 57 57 ALA H H 1 8.4310 0.0000 . 1 . . . . . 52 ALA HN . 51773 2 96 . 2 . 2 57 57 ALA N N 15 121.5630 0.0000 . 1 . . . . . 52 ALA N . 51773 2 97 . 2 . 2 58 58 ALA H H 1 7.7870 0.0000 . 1 . . . . . 53 ALA HN . 51773 2 98 . 2 . 2 58 58 ALA N N 15 119.2790 0.0000 . 1 . . . . . 53 ALA N . 51773 2 99 . 2 . 2 59 59 VAL H H 1 7.8940 0.0000 . 1 . . . . . 54 VAL HN . 51773 2 100 . 2 . 2 59 59 VAL N N 15 120.7040 0.0000 . 1 . . . . . 54 VAL N . 51773 2 101 . 2 . 2 60 60 LEU H H 1 8.2750 0.0000 . 1 . . . . . 55 LEU HN . 51773 2 102 . 2 . 2 60 60 LEU N N 15 118.9750 0.0000 . 1 . . . . . 55 LEU N . 51773 2 103 . 2 . 2 62 62 TYR H H 1 7.8560 0.0000 . 1 . . . . . 57 TYR HN . 51773 2 104 . 2 . 2 62 62 TYR N N 15 120.0160 0.0000 . 1 . . . . . 57 TYR N . 51773 2 105 . 2 . 2 63 63 LEU H H 1 8.0110 0.0000 . 1 . . . . . 58 LEU HN . 51773 2 106 . 2 . 2 63 63 LEU N N 15 117.8330 0.0000 . 1 . . . . . 58 LEU N . 51773 2 107 . 2 . 2 66 66 GLU H H 1 7.9580 0.0000 . 1 . . . . . 61 GLU HN . 51773 2 108 . 2 . 2 66 66 GLU N N 15 119.9470 0.0000 . 1 . . . . . 61 GLU N . 51773 2 109 . 2 . 2 67 67 ILE H H 1 7.9380 0.0000 . 1 . . . . . 62 ILE HN . 51773 2 110 . 2 . 2 67 67 ILE N N 15 117.8240 0.0000 . 1 . . . . . 62 ILE N . 51773 2 111 . 2 . 2 69 69 GLU H H 1 9.0200 0.0000 . 1 . . . . . 64 GLU HN . 51773 2 112 . 2 . 2 69 69 GLU N N 15 123.3670 0.0000 . 1 . . . . . 64 GLU N . 51773 2 113 . 2 . 2 70 70 LEU H H 1 7.6270 0.0000 . 1 . . . . . 65 LEU HN . 51773 2 114 . 2 . 2 70 70 LEU N N 15 119.8810 0.0000 . 1 . . . . . 65 LEU N . 51773 2 115 . 2 . 2 71 71 ALA H H 1 9.3510 0.0000 . 1 . . . . . 66 ALA HN . 51773 2 116 . 2 . 2 71 71 ALA N N 15 125.0510 0.0000 . 1 . . . . . 66 ALA N . 51773 2 117 . 2 . 2 72 72 GLY H H 1 8.8100 0.0000 . 1 . . . . . 67 GLY HN . 51773 2 118 . 2 . 2 72 72 GLY N N 15 105.9890 0.0000 . 1 . . . . . 67 GLY N . 51773 2 119 . 2 . 2 73 73 ASN H H 1 7.6580 0.0000 . 1 . . . . . 68 ASN HN . 51773 2 120 . 2 . 2 73 73 ASN N N 15 123.8130 0.0000 . 1 . . . . . 68 ASN N . 51773 2 121 . 2 . 2 74 74 ALA H H 1 7.4550 0.0000 . 1 . . . . . 69 ALA HN . 51773 2 122 . 2 . 2 74 74 ALA N N 15 123.6160 0.0000 . 1 . . . . . 69 ALA N . 51773 2 123 . 2 . 2 75 75 ALA H H 1 7.6850 0.0000 . 1 . . . . . 70 ALA HN . 51773 2 124 . 2 . 2 75 75 ALA N N 15 122.8050 0.0000 . 1 . . . . . 70 ALA N . 51773 2 125 . 2 . 2 76 76 ARG H H 1 7.6940 0.0000 . 1 . . . . . 71 ARG HN . 51773 2 126 . 2 . 2 76 76 ARG N N 15 119.9210 0.0000 . 1 . . . . . 71 ARG N . 51773 2 127 . 2 . 2 77 77 ASP H H 1 8.4920 0.0000 . 1 . . . . . 72 ASP HN . 51773 2 128 . 2 . 2 77 77 ASP N N 15 123.1280 0.0000 . 1 . . . . . 72 ASP N . 51773 2 129 . 2 . 2 78 78 ASN H H 1 7.3410 0.0000 . 1 . . . . . 73 ASN HN . 51773 2 130 . 2 . 2 78 78 ASN N N 15 117.5400 0.0000 . 1 . . . . . 73 ASN N . 51773 2 131 . 2 . 2 79 79 LYS H H 1 8.0950 0.0000 . 1 . . . . . 74 LYS HN . 51773 2 132 . 2 . 2 79 79 LYS N N 15 116.0220 0.0000 . 1 . . . . . 74 LYS N . 51773 2 133 . 2 . 2 80 80 LYS H H 1 8.1480 0.0000 . 1 . . . . . 75 LYS HN . 51773 2 134 . 2 . 2 80 80 LYS N N 15 117.4250 0.0000 . 1 . . . . . 75 LYS N . 51773 2 135 . 2 . 2 81 81 THR H H 1 8.4750 0.0000 . 1 . . . . . 76 THR HN . 51773 2 136 . 2 . 2 81 81 THR N N 15 110.2170 0.0000 . 1 . . . . . 76 THR N . 51773 2 137 . 2 . 2 82 82 ARG H H 1 7.0510 0.0000 . 1 . . . . . 77 ARG HN . 51773 2 138 . 2 . 2 82 82 ARG N N 15 119.8510 0.0000 . 1 . . . . . 77 ARG N . 51773 2 139 . 2 . 2 83 83 ILE H H 1 8.4790 0.0000 . 1 . . . . . 78 ILE HN . 51773 2 140 . 2 . 2 83 83 ILE N N 15 125.2840 0.0000 . 1 . . . . . 78 ILE N . 51773 2 141 . 2 . 2 84 84 ILE H H 1 8.9380 0.0000 . 1 . . . . . 79 ILE HN . 51773 2 142 . 2 . 2 84 84 ILE N N 15 125.3280 0.0000 . 1 . . . . . 79 ILE N . 51773 2 143 . 2 . 2 86 86 ARG H H 1 8.3810 0.0000 . 1 . . . . . 81 ARG HN . 51773 2 144 . 2 . 2 86 86 ARG N N 15 116.6640 0.0000 . 1 . . . . . 81 ARG N . 51773 2 145 . 2 . 2 87 87 HIS H H 1 7.3300 0.0000 . 1 . . . . . 82 HIS HN . 51773 2 146 . 2 . 2 87 87 HIS N N 15 118.3550 0.0000 . 1 . . . . . 82 HIS N . 51773 2 147 . 2 . 2 88 88 LEU H H 1 7.0790 0.0000 . 1 . . . . . 83 LEU HN . 51773 2 148 . 2 . 2 88 88 LEU N N 15 117.4750 0.0000 . 1 . . . . . 83 LEU N . 51773 2 149 . 2 . 2 90 90 LEU H H 1 8.1340 0.0000 . 1 . . . . . 85 LEU HN . 51773 2 150 . 2 . 2 90 90 LEU N N 15 120.0380 0.0000 . 1 . . . . . 85 LEU N . 51773 2 151 . 2 . 2 91 91 ALA H H 1 7.7540 0.0000 . 1 . . . . . 86 ALA HN . 51773 2 152 . 2 . 2 91 91 ALA N N 15 120.2350 0.0000 . 1 . . . . . 86 ALA N . 51773 2 153 . 2 . 2 92 92 ILE H H 1 7.5760 0.0000 . 1 . . . . . 87 ILE HN . 51773 2 154 . 2 . 2 92 92 ILE N N 15 114.1770 0.0000 . 1 . . . . . 87 ILE N . 51773 2 155 . 2 . 2 93 93 ARG H H 1 7.8260 0.0000 . 1 . . . . . 88 ARG HN . 51773 2 156 . 2 . 2 93 93 ARG N N 15 115.4320 0.0000 . 1 . . . . . 88 ARG N . 51773 2 157 . 2 . 2 94 94 ASN H H 1 7.6830 0.0000 . 1 . . . . . 89 ASN HN . 51773 2 158 . 2 . 2 94 94 ASN N N 15 113.7980 0.0000 . 1 . . . . . 89 ASN N . 51773 2 159 . 2 . 2 95 95 ASP H H 1 7.3030 0.0000 . 1 . . . . . 90 ASP HN . 51773 2 160 . 2 . 2 95 95 ASP N N 15 122.9440 0.0000 . 1 . . . . . 90 ASP N . 51773 2 161 . 2 . 2 96 96 GLU H H 1 8.8440 0.0000 . 1 . . . . . 91 GLU HN . 51773 2 162 . 2 . 2 96 96 GLU N N 15 126.8460 0.0000 . 1 . . . . . 91 GLU N . 51773 2 163 . 2 . 2 97 97 GLU H H 1 8.0970 0.0000 . 1 . . . . . 92 GLU HN . 51773 2 164 . 2 . 2 97 97 GLU N N 15 118.2150 0.0000 . 1 . . . . . 92 GLU N . 51773 2 165 . 2 . 2 98 98 LEU H H 1 9.1890 0.0000 . 1 . . . . . 93 LEU HN . 51773 2 166 . 2 . 2 98 98 LEU N N 15 121.6100 0.0000 . 1 . . . . . 93 LEU N . 51773 2 167 . 2 . 2 99 99 ASN H H 1 9.0130 0.0000 . 1 . . . . . 94 ASN HN . 51773 2 168 . 2 . 2 99 99 ASN N N 15 119.7590 0.0000 . 1 . . . . . 94 ASN N . 51773 2 169 . 2 . 2 100 100 LYS H H 1 7.5590 0.0000 . 1 . . . . . 95 LYS HN . 51773 2 170 . 2 . 2 100 100 LYS N N 15 120.1400 0.0000 . 1 . . . . . 95 LYS N . 51773 2 171 . 2 . 2 101 101 LEU H H 1 7.8590 0.0000 . 1 . . . . . 96 LEU HN . 51773 2 172 . 2 . 2 101 101 LEU N N 15 119.5820 0.0000 . 1 . . . . . 96 LEU N . 51773 2 173 . 2 . 2 102 102 LEU H H 1 8.6570 0.0000 . 1 . . . . . 97 LEU HN . 51773 2 174 . 2 . 2 102 102 LEU N N 15 116.4230 0.0000 . 1 . . . . . 97 LEU N . 51773 2 175 . 2 . 2 103 103 GLY H H 1 8.0260 0.0000 . 1 . . . . . 98 GLY HN . 51773 2 176 . 2 . 2 103 103 GLY N N 15 110.3390 0.0000 . 1 . . . . . 98 GLY N . 51773 2 177 . 2 . 2 104 104 ARG H H 1 8.1280 0.0000 . 1 . . . . . 99 ARG HN . 51773 2 178 . 2 . 2 104 104 ARG N N 15 118.9740 0.0000 . 1 . . . . . 99 ARG N . 51773 2 179 . 2 . 2 105 105 VAL H H 1 7.7820 0.0000 . 1 . . . . . 100 VAL HN . 51773 2 180 . 2 . 2 105 105 VAL N N 15 121.4780 0.0000 . 1 . . . . . 100 VAL N . 51773 2 181 . 2 . 2 106 106 THR H H 1 8.2680 0.0000 . 1 . . . . . 101 THR HN . 51773 2 182 . 2 . 2 106 106 THR N N 15 120.5200 0.0000 . 1 . . . . . 101 THR N . 51773 2 183 . 2 . 2 107 107 ILE H H 1 8.2010 0.0000 . 1 . . . . . 102 ILE HN . 51773 2 184 . 2 . 2 107 107 ILE N N 15 124.4900 0.0000 . 1 . . . . . 102 ILE N . 51773 2 185 . 2 . 2 108 108 ALA H H 1 8.2090 0.0000 . 1 . . . . . 103 ALA HN . 51773 2 186 . 2 . 2 108 108 ALA N N 15 127.8090 0.0000 . 1 . . . . . 103 ALA N . 51773 2 187 . 2 . 2 109 109 GLN H H 1 8.2710 0.0000 . 1 . . . . . 104 GLN HN . 51773 2 188 . 2 . 2 109 109 GLN N N 15 120.1140 0.0000 . 1 . . . . . 104 GLN N . 51773 2 189 . 2 . 2 110 110 GLY H H 1 8.3290 0.0000 . 1 . . . . . 105 GLY HN . 51773 2 190 . 2 . 2 110 110 GLY N N 15 110.4290 0.0000 . 1 . . . . . 105 GLY N . 51773 2 191 . 2 . 2 111 111 GLY H H 1 8.1840 0.0000 . 1 . . . . . 106 GLY HN . 51773 2 192 . 2 . 2 111 111 GLY N N 15 109.4640 0.0000 . 1 . . . . . 106 GLY N . 51773 2 193 . 2 . 2 112 112 VAL H H 1 7.9430 0.0000 . 1 . . . . . 107 VAL HN . 51773 2 194 . 2 . 2 112 112 VAL N N 15 119.6940 0.0000 . 1 . . . . . 107 VAL N . 51773 2 195 . 2 . 2 113 113 LEU H H 1 8.3240 0.0000 . 1 . . . . . 108 LEU HN . 51773 2 196 . 2 . 2 113 113 LEU N N 15 128.0330 0.0000 . 1 . . . . . 108 LEU N . 51773 2 197 . 2 . 2 115 115 ASN H H 1 8.4060 0.0000 . 1 . . . . . 110 ASN HN . 51773 2 198 . 2 . 2 115 115 ASN N N 15 119.4460 0.0000 . 1 . . . . . 110 ASN N . 51773 2 199 . 2 . 2 116 116 ILE H H 1 8.0530 0.0000 . 1 . . . . . 111 ILE HN . 51773 2 200 . 2 . 2 116 116 ILE N N 15 122.0890 0.0000 . 1 . . . . . 111 ILE N . 51773 2 201 . 2 . 2 117 117 GLN H H 1 8.3230 0.0000 . 1 . . . . . 112 GLN HN . 51773 2 202 . 2 . 2 117 117 GLN N N 15 124.7330 0.0000 . 1 . . . . . 112 GLN N . 51773 2 203 . 2 . 2 118 118 ALA H H 1 8.2030 0.0000 . 1 . . . . . 113 ALA HN . 51773 2 204 . 2 . 2 118 118 ALA N N 15 126.2450 0.0000 . 1 . . . . . 113 ALA N . 51773 2 205 . 2 . 2 119 119 VAL H H 1 8.0010 0.0000 . 1 . . . . . 114 VAL HN . 51773 2 206 . 2 . 2 119 119 VAL N N 15 120.2410 0.0000 . 1 . . . . . 114 VAL N . 51773 2 207 . 2 . 2 120 120 LEU H H 1 8.2030 0.0000 . 1 . . . . . 115 LEU HN . 51773 2 208 . 2 . 2 120 120 LEU N N 15 126.9790 0.0000 . 1 . . . . . 115 LEU N . 51773 2 209 . 2 . 2 121 121 LEU H H 1 8.1530 0.0000 . 1 . . . . . 116 LEU HN . 51773 2 210 . 2 . 2 121 121 LEU N N 15 125.6860 0.0000 . 1 . . . . . 116 LEU N . 51773 2 211 . 2 . 2 123 123 LYS H H 1 8.3360 0.0000 . 1 . . . . . 118 LYS HN . 51773 2 212 . 2 . 2 123 123 LYS N N 15 122.6840 0.0000 . 1 . . . . . 118 LYS N . 51773 2 213 . 2 . 2 124 124 LYS H H 1 8.3860 0.0000 . 1 . . . . . 119 LYS HN . 51773 2 214 . 2 . 2 124 124 LYS N N 15 124.1940 0.0000 . 1 . . . . . 119 LYS N . 51773 2 215 . 2 . 2 125 125 THR H H 1 8.1870 0.0000 . 1 . . . . . 120 THR HN . 51773 2 216 . 2 . 2 125 125 THR N N 15 117.1970 0.0000 . 1 . . . . . 120 THR N . 51773 2 217 . 2 . 2 126 126 GLU H H 1 8.4240 0.0000 . 1 . . . . . 121 GLU HN . 51773 2 218 . 2 . 2 126 126 GLU N N 15 124.5780 0.0000 . 1 . . . . . 121 GLU N . 51773 2 219 . 2 . 2 127 127 SER H H 1 8.3480 0.0000 . 1 . . . . . 122 SER HN . 51773 2 220 . 2 . 2 127 127 SER N N 15 118.1140 0.0000 . 1 . . . . . 122 SER N . 51773 2 221 . 2 . 2 130 130 LYS H H 1 8.3270 0.0000 . 1 . . . . . 125 LYS HN . 51773 2 222 . 2 . 2 130 130 LYS N N 15 124.3710 0.0000 . 1 . . . . . 125 LYS N . 51773 2 223 . 2 . 2 131 131 ALA H H 1 8.3550 0.0000 . 1 . . . . . 126 ALA HN . 51773 2 224 . 2 . 2 131 131 ALA N N 15 126.7870 0.0000 . 1 . . . . . 126 ALA N . 51773 2 225 . 2 . 2 132 132 LYS H H 1 8.3130 0.0000 . 1 . . . . . 127 LYS HN . 51773 2 226 . 2 . 2 132 132 LYS N N 15 121.9130 0.0000 . 1 . . . . . 127 LYS N . 51773 2 227 . 2 . 2 133 133 GLY H H 1 8.3790 0.0000 . 1 . . . . . 128 GLY HN . 51773 2 228 . 2 . 2 133 133 GLY N N 15 111.7880 0.0000 . 1 . . . . . 128 GLY N . 51773 2 229 . 2 . 2 134 134 LYS H H 1 7.7880 0.0000 . 1 . . . . . 129 LYS HN . 51773 2 230 . 2 . 2 134 134 LYS N N 15 126.6790 0.0000 . 1 . . . . . 129 LYS N . 51773 2 stop_ save_ save_assigned_chemical_shifts_3 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chemical_shifts_3 _Assigned_chem_shift_list.Entry_ID 51773 _Assigned_chem_shift_list.ID 3 _Assigned_chem_shift_list.Name 'H2B assignment' _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chem_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 2 '2D 1H-15N TROSY' . . . 51773 3 stop_ loop_ _Chem_shift_software.Software_ID _Chem_shift_software.Software_label _Chem_shift_software.Method_ID _Chem_shift_software.Method_label _Chem_shift_software.Entry_ID _Chem_shift_software.Assigned_chem_shift_list_ID 1 $software_1 . . 51773 3 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 3 . 3 4 4 GLY H H 1 8.5340 0.0000 . 1 . . . . . -1 GLY HN . 51773 3 2 . 3 . 3 4 4 GLY N N 15 110.7280 0.0000 . 1 . . . . . -1 GLY N . 51773 3 3 . 3 . 3 5 5 MET H H 1 8.1010 0.0000 . 1 . . . . . 0 MET HN . 51773 3 4 . 3 . 3 5 5 MET N N 15 121.8800 0.0000 . 1 . . . . . 0 MET N . 51773 3 5 . 3 . 3 7 7 GLU H H 1 8.4380 0.0000 . 1 . . . . . 2 GLU HN . 51773 3 6 . 3 . 3 7 7 GLU N N 15 123.4960 0.0000 . 1 . . . . . 2 GLU N . 51773 3 7 . 3 . 3 9 9 ALA H H 1 8.3570 0.0000 . 1 . . . . . 4 ALA HN . 51773 3 8 . 3 . 3 9 9 ALA N N 15 124.8560 0.0000 . 1 . . . . . 4 ALA N . 51773 3 9 . 3 . 3 10 10 LYS H H 1 8.2810 0.0000 . 1 . . . . . 5 LYS HN . 51773 3 10 . 3 . 3 10 10 LYS N N 15 121.5860 0.0000 . 1 . . . . . 5 LYS N . 51773 3 11 . 3 . 3 11 11 SER H H 1 8.1980 0.0000 . 1 . . . . . 6 SER HN . 51773 3 12 . 3 . 3 11 11 SER N N 15 117.6960 0.0000 . 1 . . . . . 6 SER N . 51773 3 13 . 3 . 3 12 12 ALA H H 1 8.2660 0.0000 . 1 . . . . . 7 ALA HN . 51773 3 14 . 3 . 3 12 12 ALA N N 15 127.8500 0.0000 . 1 . . . . . 7 ALA N . 51773 3 15 . 3 . 3 14 14 ALA H H 1 8.3470 0.0000 . 1 . . . . . 9 ALA HN . 51773 3 16 . 3 . 3 14 14 ALA N N 15 126.5270 0.0000 . 1 . . . . . 9 ALA N . 51773 3 17 . 3 . 3 16 16 LYS H H 1 8.3870 0.0000 . 1 . . . . . 11 LYS HN . 51773 3 18 . 3 . 3 16 16 LYS N N 15 122.8350 0.0000 . 1 . . . . . 11 LYS N . 51773 3 19 . 3 . 3 17 17 LYS H H 1 8.3890 0.0000 . 1 . . . . . 12 LYS HN . 51773 3 20 . 3 . 3 17 17 LYS N N 15 124.1480 0.0000 . 1 . . . . . 12 LYS N . 51773 3 21 . 3 . 3 18 18 GLY H H 1 8.4410 0.0000 . 1 . . . . . 13 GLY HN . 51773 3 22 . 3 . 3 18 18 GLY N N 15 111.5360 0.0000 . 1 . . . . . 13 GLY N . 51773 3 23 . 3 . 3 19 19 SER H H 1 8.1460 0.0000 . 1 . . . . . 14 SER HN . 51773 3 24 . 3 . 3 19 19 SER N N 15 116.5100 0.0000 . 1 . . . . . 14 SER N . 51773 3 25 . 3 . 3 20 20 LYS H H 1 8.3740 0.0000 . 1 . . . . . 15 LYS HN . 51773 3 26 . 3 . 3 20 20 LYS N N 15 124.2260 0.0000 . 1 . . . . . 15 LYS N . 51773 3 27 . 3 . 3 21 21 LYS H H 1 8.2500 0.0000 . 1 . . . . . 16 LYS HN . 51773 3 28 . 3 . 3 21 21 LYS N N 15 123.9860 0.0000 . 1 . . . . . 16 LYS N . 51773 3 29 . 3 . 3 22 22 ALA H H 1 8.2920 0.0000 . 1 . . . . . 17 ALA HN . 51773 3 30 . 3 . 3 22 22 ALA N N 15 126.8630 0.0000 . 1 . . . . . 17 ALA N . 51773 3 31 . 3 . 3 23 23 VAL H H 1 8.1730 0.0000 . 1 . . . . . 18 VAL HN . 51773 3 32 . 3 . 3 23 23 VAL N N 15 121.1720 0.0000 . 1 . . . . . 18 VAL N . 51773 3 33 . 3 . 3 24 24 THR H H 1 8.2210 0.0000 . 1 . . . . . 19 THR HN . 51773 3 34 . 3 . 3 24 24 THR N N 15 119.8750 0.0000 . 1 . . . . . 19 THR N . 51773 3 35 . 3 . 3 25 25 LYS H H 1 8.3380 0.0000 . 1 . . . . . 20 LYS HN . 51773 3 36 . 3 . 3 25 25 LYS N N 15 125.1850 0.0000 . 1 . . . . . 20 LYS N . 51773 3 37 . 3 . 3 26 26 ALA H H 1 8.2740 0.0000 . 1 . . . . . 21 ALA HN . 51773 3 38 . 3 . 3 26 26 ALA N N 15 126.2120 0.0000 . 1 . . . . . 21 ALA N . 51773 3 39 . 3 . 3 27 27 GLN H H 1 8.3070 0.0000 . 1 . . . . . 22 GLN HN . 51773 3 40 . 3 . 3 27 27 GLN N N 15 121.0160 0.0000 . 1 . . . . . 22 GLN N . 51773 3 41 . 3 . 3 28 28 LYS H H 1 8.3480 0.0000 . 1 . . . . . 23 LYS HN . 51773 3 42 . 3 . 3 28 28 LYS N N 15 124.2310 0.0000 . 1 . . . . . 23 LYS N . 51773 3 43 . 3 . 3 29 29 LYS H H 1 8.3670 0.0000 . 1 . . . . . 24 LYS HN . 51773 3 44 . 3 . 3 29 29 LYS N N 15 124.3130 0.0000 . 1 . . . . . 24 LYS N . 51773 3 45 . 3 . 3 30 30 ASP H H 1 8.3150 0.0000 . 1 . . . . . 25 ASP HN . 51773 3 46 . 3 . 3 30 30 ASP N N 15 122.4230 0.0000 . 1 . . . . . 25 ASP N . 51773 3 47 . 3 . 3 31 31 GLY H H 1 8.3000 0.0000 . 1 . . . . . 26 GLY HN . 51773 3 48 . 3 . 3 31 31 GLY N N 15 110.3390 0.0000 . 1 . . . . . 26 GLY N . 51773 3 49 . 3 . 3 32 32 LYS H H 1 8.1420 0.0000 . 1 . . . . . 27 LYS HN . 51773 3 50 . 3 . 3 32 32 LYS N N 15 121.6100 0.0000 . 1 . . . . . 27 LYS N . 51773 3 51 . 3 . 3 33 33 LYS H H 1 8.2120 0.0000 . 1 . . . . . 28 LYS HN . 51773 3 52 . 3 . 3 33 33 LYS N N 15 123.1200 0.0000 . 1 . . . . . 28 LYS N . 51773 3 53 . 3 . 3 34 34 ARG H H 1 8.3990 0.0000 . 1 . . . . . 29 ARG HN . 51773 3 54 . 3 . 3 34 34 ARG N N 15 124.0280 0.0000 . 1 . . . . . 29 ARG N . 51773 3 55 . 3 . 3 35 35 LYS H H 1 8.2740 0.0000 . 1 . . . . . 30 LYS HN . 51773 3 56 . 3 . 3 35 35 LYS N N 15 123.6320 0.0000 . 1 . . . . . 30 LYS N . 51773 3 57 . 3 . 3 36 36 ARG H H 1 8.2850 0.0000 . 1 . . . . . 31 ARG HN . 51773 3 58 . 3 . 3 36 36 ARG N N 15 123.5650 0.0000 . 1 . . . . . 31 ARG N . 51773 3 59 . 3 . 3 37 37 SER H H 1 8.3910 0.0000 . 1 . . . . . 32 SER HN . 51773 3 60 . 3 . 3 37 37 SER N N 15 118.8970 0.0000 . 1 . . . . . 32 SER N . 51773 3 61 . 3 . 3 38 38 ARG H H 1 8.4510 0.0000 . 1 . . . . . 33 ARG HN . 51773 3 62 . 3 . 3 38 38 ARG N N 15 124.4350 0.0000 . 1 . . . . . 33 ARG N . 51773 3 63 . 3 . 3 39 39 LYS H H 1 8.3540 0.0000 . 1 . . . . . 34 LYS HN . 51773 3 64 . 3 . 3 39 39 LYS N N 15 124.4220 0.0000 . 1 . . . . . 34 LYS N . 51773 3 65 . 3 . 3 40 40 GLU H H 1 8.2060 0.0000 . 1 . . . . . 35 GLU HN . 51773 3 66 . 3 . 3 40 40 GLU N N 15 123.7040 0.0000 . 1 . . . . . 35 GLU N . 51773 3 67 . 3 . 3 41 41 SER H H 1 8.5800 0.0000 . 1 . . . . . 36 SER HN . 51773 3 68 . 3 . 3 41 41 SER N N 15 117.3500 0.0000 . 1 . . . . . 36 SER N . 51773 3 69 . 3 . 3 42 42 TYR H H 1 7.9660 0.0000 . 1 . . . . . 37 TYR HN . 51773 3 70 . 3 . 3 42 42 TYR N N 15 118.5910 0.0000 . 1 . . . . . 37 TYR N . 51773 3 71 . 3 . 3 48 48 LYS H H 1 7.4350 0.0000 . 1 . . . . . 43 LYS HN . 51773 3 72 . 3 . 3 48 48 LYS N N 15 118.3070 0.0000 . 1 . . . . . 43 LYS N . 51773 3 73 . 3 . 3 49 49 VAL H H 1 7.9340 0.0000 . 1 . . . . . 44 VAL HN . 51773 3 74 . 3 . 3 49 49 VAL N N 15 120.7230 0.0000 . 1 . . . . . 44 VAL N . 51773 3 75 . 3 . 3 50 50 LEU H H 1 8.5210 0.0000 . 1 . . . . . 45 LEU HN . 51773 3 76 . 3 . 3 50 50 LEU N N 15 122.2710 0.0000 . 1 . . . . . 45 LEU N . 51773 3 77 . 3 . 3 51 51 LYS H H 1 7.6750 0.0000 . 1 . . . . . 46 LYS HN . 51773 3 78 . 3 . 3 51 51 LYS N N 15 115.2400 0.0000 . 1 . . . . . 46 LYS N . 51773 3 79 . 3 . 3 52 52 GLN H H 1 7.2630 0.0000 . 1 . . . . . 47 GLN HN . 51773 3 80 . 3 . 3 52 52 GLN N N 15 115.7390 0.0000 . 1 . . . . . 47 GLN N . 51773 3 81 . 3 . 3 53 53 VAL H H 1 7.6550 0.0000 . 1 . . . . . 48 VAL HN . 51773 3 82 . 3 . 3 53 53 VAL N N 15 114.1700 0.0000 . 1 . . . . . 48 VAL N . 51773 3 83 . 3 . 3 54 54 HIS H H 1 8.8500 0.0000 . 1 . . . . . 49 HIS HN . 51773 3 84 . 3 . 3 54 54 HIS N N 15 119.3910 0.0000 . 1 . . . . . 49 HIS N . 51773 3 85 . 3 . 3 56 56 ASP H H 1 8.3320 0.0000 . 1 . . . . . 51 ASP HN . 51773 3 86 . 3 . 3 56 56 ASP N N 15 116.0950 0.0000 . 1 . . . . . 51 ASP N . 51773 3 87 . 3 . 3 57 57 THR H H 1 7.7990 0.0000 . 1 . . . . . 52 THR HN . 51773 3 88 . 3 . 3 57 57 THR N N 15 119.5350 0.0000 . 1 . . . . . 52 THR N . 51773 3 89 . 3 . 3 58 58 GLY H H 1 8.5220 0.0000 . 1 . . . . . 53 GLY HN . 51773 3 90 . 3 . 3 58 58 GLY N N 15 113.5960 0.0000 . 1 . . . . . 53 GLY N . 51773 3 91 . 3 . 3 59 59 ILE H H 1 8.7920 0.0000 . 1 . . . . . 54 ILE HN . 51773 3 92 . 3 . 3 59 59 ILE N N 15 118.4230 0.0000 . 1 . . . . . 54 ILE N . 51773 3 93 . 3 . 3 60 60 SER H H 1 8.9570 0.0000 . 1 . . . . . 55 SER HN . 51773 3 94 . 3 . 3 60 60 SER N N 15 125.3110 0.0000 . 1 . . . . . 55 SER N . 51773 3 95 . 3 . 3 61 61 SER H H 1 9.1160 0.0000 . 1 . . . . . 56 SER HN . 51773 3 96 . 3 . 3 61 61 SER N N 15 119.2360 0.0000 . 1 . . . . . 56 SER N . 51773 3 97 . 3 . 3 63 63 ALA H H 1 7.5720 0.0000 . 1 . . . . . 58 ALA HN . 51773 3 98 . 3 . 3 63 63 ALA N N 15 121.9730 0.0000 . 1 . . . . . 58 ALA N . 51773 3 99 . 3 . 3 64 64 MET H H 1 8.7520 0.0000 . 1 . . . . . 59 MET HN . 51773 3 100 . 3 . 3 64 64 MET N N 15 120.6360 0.0000 . 1 . . . . . 59 MET N . 51773 3 101 . 3 . 3 65 65 GLY H H 1 7.9760 0.0000 . 1 . . . . . 60 GLY HN . 51773 3 102 . 3 . 3 65 65 GLY N N 15 107.9820 0.0000 . 1 . . . . . 60 GLY N . 51773 3 103 . 3 . 3 66 66 ILE H H 1 7.2780 0.0000 . 1 . . . . . 61 ILE HN . 51773 3 104 . 3 . 3 66 66 ILE N N 15 124.3610 0.0000 . 1 . . . . . 61 ILE N . 51773 3 105 . 3 . 3 67 67 MET H H 1 7.9470 0.0000 . 1 . . . . . 62 MET HN . 51773 3 106 . 3 . 3 67 67 MET N N 15 118.7350 0.0000 . 1 . . . . . 62 MET N . 51773 3 107 . 3 . 3 68 68 ASN H H 1 8.6320 0.0000 . 1 . . . . . 63 ASN HN . 51773 3 108 . 3 . 3 68 68 ASN N N 15 118.0440 0.0000 . 1 . . . . . 63 ASN N . 51773 3 109 . 3 . 3 69 69 SER H H 1 8.0540 0.0000 . 1 . . . . . 64 SER HN . 51773 3 110 . 3 . 3 69 69 SER N N 15 119.4660 0.0000 . 1 . . . . . 64 SER N . 51773 3 111 . 3 . 3 70 70 PHE H H 1 8.4140 0.0000 . 1 . . . . . 65 PHE HN . 51773 3 112 . 3 . 3 70 70 PHE N N 15 122.8300 0.0000 . 1 . . . . . 65 PHE N . 51773 3 113 . 3 . 3 71 71 VAL H H 1 8.4310 0.0000 . 1 . . . . . 66 VAL HN . 51773 3 114 . 3 . 3 71 71 VAL N N 15 118.9870 0.0000 . 1 . . . . . 66 VAL N . 51773 3 115 . 3 . 3 72 72 ASN H H 1 8.0200 0.0000 . 1 . . . . . 67 ASN HN . 51773 3 116 . 3 . 3 72 72 ASN N N 15 115.9130 0.0000 . 1 . . . . . 67 ASN N . 51773 3 117 . 3 . 3 73 73 ASP H H 1 8.1770 0.0000 . 1 . . . . . 68 ASP HN . 51773 3 118 . 3 . 3 73 73 ASP N N 15 120.1660 0.0000 . 1 . . . . . 68 ASP N . 51773 3 119 . 3 . 3 74 74 ILE H H 1 8.3450 0.0000 . 1 . . . . . 69 ILE HN . 51773 3 120 . 3 . 3 74 74 ILE N N 15 118.7840 0.0000 . 1 . . . . . 69 ILE N . 51773 3 121 . 3 . 3 75 75 PHE H H 1 8.5390 0.0000 . 1 . . . . . 70 PHE HN . 51773 3 122 . 3 . 3 75 75 PHE N N 15 120.4250 0.0000 . 1 . . . . . 70 PHE N . 51773 3 123 . 3 . 3 76 76 GLU H H 1 8.3740 0.0000 . 1 . . . . . 71 GLU HN . 51773 3 124 . 3 . 3 76 76 GLU N N 15 118.0660 0.0000 . 1 . . . . . 71 GLU N . 51773 3 125 . 3 . 3 77 77 ARG H H 1 8.4180 0.0000 . 1 . . . . . 72 ARG HN . 51773 3 126 . 3 . 3 77 77 ARG N N 15 120.3170 0.0000 . 1 . . . . . 72 ARG N . 51773 3 127 . 3 . 3 78 78 ILE H H 1 8.2470 0.0000 . 1 . . . . . 73 ILE HN . 51773 3 128 . 3 . 3 78 78 ILE N N 15 119.5770 0.0000 . 1 . . . . . 73 ILE N . 51773 3 129 . 3 . 3 79 79 ALA H H 1 8.6780 0.0000 . 1 . . . . . 74 ALA HN . 51773 3 130 . 3 . 3 79 79 ALA N N 15 122.4580 0.0000 . 1 . . . . . 74 ALA N . 51773 3 131 . 3 . 3 80 80 GLY H H 1 8.1050 0.0000 . 1 . . . . . 75 GLY HN . 51773 3 132 . 3 . 3 80 80 GLY N N 15 104.3750 0.0000 . 1 . . . . . 75 GLY N . 51773 3 133 . 3 . 3 81 81 GLU H H 1 7.5920 0.0000 . 1 . . . . . 76 GLU HN . 51773 3 134 . 3 . 3 81 81 GLU N N 15 124.6030 0.0000 . 1 . . . . . 76 GLU N . 51773 3 135 . 3 . 3 82 82 ALA H H 1 8.7010 0.0000 . 1 . . . . . 77 ALA HN . 51773 3 136 . 3 . 3 82 82 ALA N N 15 122.2920 0.0000 . 1 . . . . . 77 ALA N . 51773 3 137 . 3 . 3 83 83 SER H H 1 8.1980 0.0000 . 1 . . . . . 78 SER HN . 51773 3 138 . 3 . 3 83 83 SER N N 15 111.4640 0.0000 . 1 . . . . . 78 SER N . 51773 3 139 . 3 . 3 84 84 ARG H H 1 7.8100 0.0000 . 1 . . . . . 79 ARG HN . 51773 3 140 . 3 . 3 84 84 ARG N N 15 123.4730 0.0000 . 1 . . . . . 79 ARG N . 51773 3 141 . 3 . 3 85 85 LEU H H 1 8.3370 0.0000 . 1 . . . . . 80 LEU HN . 51773 3 142 . 3 . 3 85 85 LEU N N 15 120.3270 0.0000 . 1 . . . . . 80 LEU N . 51773 3 143 . 3 . 3 87 87 HIS H H 1 8.0100 0.0000 . 1 . . . . . 82 HIS HN . 51773 3 144 . 3 . 3 87 87 HIS N N 15 115.4350 0.0000 . 1 . . . . . 82 HIS N . 51773 3 145 . 3 . 3 89 89 ASN H H 1 7.6110 0.0000 . 1 . . . . . 84 ASN HN . 51773 3 146 . 3 . 3 89 89 ASN N N 15 115.9690 0.0000 . 1 . . . . . 84 ASN N . 51773 3 147 . 3 . 3 91 91 ARG H H 1 8.3610 0.0000 . 1 . . . . . 86 ARG HN . 51773 3 148 . 3 . 3 91 91 ARG N N 15 118.1480 0.0000 . 1 . . . . . 86 ARG N . 51773 3 149 . 3 . 3 92 92 SER H H 1 8.4840 0.0000 . 1 . . . . . 87 SER HN . 51773 3 150 . 3 . 3 92 92 SER N N 15 118.2370 0.0000 . 1 . . . . . 87 SER N . 51773 3 151 . 3 . 3 93 93 THR H H 1 7.4930 0.0000 . 1 . . . . . 88 THR HN . 51773 3 152 . 3 . 3 93 93 THR N N 15 116.6270 0.0000 . 1 . . . . . 88 THR N . 51773 3 153 . 3 . 3 94 94 ILE H H 1 7.6710 0.0000 . 1 . . . . . 89 ILE HN . 51773 3 154 . 3 . 3 94 94 ILE N N 15 124.5240 0.0000 . 1 . . . . . 89 ILE N . 51773 3 155 . 3 . 3 95 95 THR H H 1 9.2520 0.0000 . 1 . . . . . 90 THR HN . 51773 3 156 . 3 . 3 95 95 THR N N 15 121.3840 0.0000 . 1 . . . . . 90 THR N . 51773 3 157 . 3 . 3 96 96 SER H H 1 8.9760 0.0000 . 1 . . . . . 91 SER HN . 51773 3 158 . 3 . 3 96 96 SER N N 15 117.3980 0.0000 . 1 . . . . . 91 SER N . 51773 3 159 . 3 . 3 97 97 ARG H H 1 7.7960 0.0000 . 1 . . . . . 92 ARG HN . 51773 3 160 . 3 . 3 97 97 ARG N N 15 122.7350 0.0000 . 1 . . . . . 92 ARG N . 51773 3 161 . 3 . 3 98 98 GLU H H 1 7.4030 0.0000 . 1 . . . . . 93 GLU HN . 51773 3 162 . 3 . 3 98 98 GLU N N 15 119.6910 0.0000 . 1 . . . . . 93 GLU N . 51773 3 163 . 3 . 3 99 99 ILE H H 1 7.1010 0.0000 . 1 . . . . . 94 ILE HN . 51773 3 164 . 3 . 3 99 99 ILE N N 15 116.5810 0.0000 . 1 . . . . . 94 ILE N . 51773 3 165 . 3 . 3 100 100 GLN H H 1 7.8740 0.0000 . 1 . . . . . 95 GLN HN . 51773 3 166 . 3 . 3 100 100 GLN N N 15 119.9620 0.0000 . 1 . . . . . 95 GLN N . 51773 3 167 . 3 . 3 101 101 THR H H 1 8.0790 0.0000 . 1 . . . . . 96 THR HN . 51773 3 168 . 3 . 3 101 101 THR N N 15 116.0670 0.0000 . 1 . . . . . 96 THR N . 51773 3 169 . 3 . 3 102 102 ALA H H 1 7.8540 0.0000 . 1 . . . . . 97 ALA HN . 51773 3 170 . 3 . 3 102 102 ALA N N 15 123.5030 0.0000 . 1 . . . . . 97 ALA N . 51773 3 171 . 3 . 3 103 103 VAL H H 1 8.4340 0.0000 . 1 . . . . . 98 VAL HN . 51773 3 172 . 3 . 3 103 103 VAL N N 15 118.2180 0.0000 . 1 . . . . . 98 VAL N . 51773 3 173 . 3 . 3 104 104 ARG H H 1 7.8070 0.0000 . 1 . . . . . 99 ARG HN . 51773 3 174 . 3 . 3 104 104 ARG N N 15 117.4420 0.0000 . 1 . . . . . 99 ARG N . 51773 3 175 . 3 . 3 105 105 LEU H H 1 7.7540 0.0000 . 1 . . . . . 100 LEU HN . 51773 3 176 . 3 . 3 105 105 LEU N N 15 118.2420 0.0000 . 1 . . . . . 100 LEU N . 51773 3 177 . 3 . 3 106 106 LEU H H 1 7.8510 0.0000 . 1 . . . . . 101 LEU HN . 51773 3 178 . 3 . 3 106 106 LEU N N 15 117.8220 0.0000 . 1 . . . . . 101 LEU N . 51773 3 179 . 3 . 3 107 107 LEU H H 1 8.1500 0.0000 . 1 . . . . . 102 LEU HN . 51773 3 180 . 3 . 3 107 107 LEU N N 15 120.5250 0.0000 . 1 . . . . . 102 LEU N . 51773 3 181 . 3 . 3 109 109 GLY H H 1 8.0890 0.0000 . 1 . . . . . 104 GLY HN . 51773 3 182 . 3 . 3 109 109 GLY N N 15 105.5380 0.0000 . 1 . . . . . 104 GLY N . 51773 3 183 . 3 . 3 110 110 GLU H H 1 10.2550 0.0000 . 1 . . . . . 105 GLU HN . 51773 3 184 . 3 . 3 110 110 GLU N N 15 129.5310 0.0000 . 1 . . . . . 105 GLU N . 51773 3 185 . 3 . 3 111 111 LEU H H 1 8.8930 0.0000 . 1 . . . . . 106 LEU HN . 51773 3 186 . 3 . 3 111 111 LEU N N 15 123.8130 0.0000 . 1 . . . . . 106 LEU N . 51773 3 187 . 3 . 3 112 112 ALA H H 1 7.9100 0.0000 . 1 . . . . . 107 ALA HN . 51773 3 188 . 3 . 3 112 112 ALA N N 15 119.4410 0.0000 . 1 . . . . . 107 ALA N . 51773 3 189 . 3 . 3 113 113 LYS H H 1 7.3240 0.0000 . 1 . . . . . 108 LYS HN . 51773 3 190 . 3 . 3 113 113 LYS N N 15 117.1360 0.0000 . 1 . . . . . 108 LYS N . 51773 3 191 . 3 . 3 114 114 HIS H H 1 8.0620 0.0000 . 1 . . . . . 109 HIS HN . 51773 3 192 . 3 . 3 114 114 HIS N N 15 118.0170 0.0000 . 1 . . . . . 109 HIS N . 51773 3 193 . 3 . 3 115 115 ALA H H 1 8.6270 0.0000 . 1 . . . . . 110 ALA HN . 51773 3 194 . 3 . 3 115 115 ALA N N 15 123.7680 0.0000 . 1 . . . . . 110 ALA N . 51773 3 195 . 3 . 3 116 116 VAL H H 1 8.2150 0.0000 . 1 . . . . . 111 VAL HN . 51773 3 196 . 3 . 3 116 116 VAL N N 15 117.3750 0.0000 . 1 . . . . . 111 VAL N . 51773 3 197 . 3 . 3 117 117 SER H H 1 7.4360 0.0000 . 1 . . . . . 112 SER HN . 51773 3 198 . 3 . 3 117 117 SER N N 15 117.8160 0.0000 . 1 . . . . . 112 SER N . 51773 3 199 . 3 . 3 118 118 GLU H H 1 8.0930 0.0000 . 1 . . . . . 113 GLU HN . 51773 3 200 . 3 . 3 118 118 GLU N N 15 119.8550 0.0000 . 1 . . . . . 113 GLU N . 51773 3 201 . 3 . 3 119 119 GLY H H 1 8.6220 0.0000 . 1 . . . . . 114 GLY HN . 51773 3 202 . 3 . 3 119 119 GLY N N 15 109.8530 0.0000 . 1 . . . . . 114 GLY N . 51773 3 203 . 3 . 3 120 120 THR H H 1 7.9340 0.0000 . 1 . . . . . 115 THR HN . 51773 3 204 . 3 . 3 120 120 THR N N 15 117.0200 0.0000 . 1 . . . . . 115 THR N . 51773 3 205 . 3 . 3 121 121 LYS H H 1 7.8870 0.0000 . 1 . . . . . 116 LYS HN . 51773 3 206 . 3 . 3 121 121 LYS N N 15 123.2790 0.0000 . 1 . . . . . 116 LYS N . 51773 3 207 . 3 . 3 122 122 ALA H H 1 7.6440 0.0000 . 1 . . . . . 117 ALA HN . 51773 3 208 . 3 . 3 122 122 ALA N N 15 121.9150 0.0000 . 1 . . . . . 117 ALA N . 51773 3 209 . 3 . 3 123 123 VAL H H 1 8.0520 0.0000 . 1 . . . . . 118 VAL HN . 51773 3 210 . 3 . 3 123 123 VAL N N 15 118.2260 0.0000 . 1 . . . . . 118 VAL N . 51773 3 211 . 3 . 3 125 125 LYS H H 1 7.8530 0.0000 . 1 . . . . . 120 LYS HN . 51773 3 212 . 3 . 3 125 125 LYS N N 15 121.8640 0.0000 . 1 . . . . . 120 LYS N . 51773 3 213 . 3 . 3 126 126 TYR H H 1 8.2110 0.0000 . 1 . . . . . 121 TYR HN . 51773 3 214 . 3 . 3 126 126 TYR N N 15 118.6520 0.0000 . 1 . . . . . 121 TYR N . 51773 3 215 . 3 . 3 127 127 THR H H 1 7.9650 0.0000 . 1 . . . . . 122 THR HN . 51773 3 216 . 3 . 3 127 127 THR N N 15 112.4530 0.0000 . 1 . . . . . 122 THR N . 51773 3 217 . 3 . 3 128 128 SER H H 1 7.8800 0.0000 . 1 . . . . . 123 SER HN . 51773 3 218 . 3 . 3 128 128 SER N N 15 117.7420 0.0000 . 1 . . . . . 123 SER N . 51773 3 219 . 3 . 3 129 129 ALA H H 1 7.9880 0.0000 . 1 . . . . . 124 ALA HN . 51773 3 220 . 3 . 3 129 129 ALA N N 15 126.8230 0.0000 . 1 . . . . . 124 ALA N . 51773 3 221 . 3 . 3 130 130 LYS H H 1 7.8050 0.0000 . 1 . . . . . 125 LYS HN . 51773 3 222 . 3 . 3 130 130 LYS N N 15 126.4390 0.0000 . 1 . . . . . 125 LYS N . 51773 3 stop_ save_