data_28027 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 28027 _Entry.Title ; human_CIRBP_68-137 ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2019-10-04 _Entry.Accession_date 2019-10-04 _Entry.Last_release_date 2019-10-04 _Entry.Original_release_date 2019-10-04 _Entry.Origination author _Entry.Format_name . _Entry.NMR_STAR_version 3.2.6.0 _Entry.NMR_STAR_dict_location . _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype solution _Entry.Source_data_format . _Entry.Source_data_format_version . _Entry.Generated_software_name . _Entry.Generated_software_version . _Entry.Generated_software_ID . _Entry.Generated_software_label . _Entry.Generated_date . _Entry.DOI . _Entry.UUID . _Entry.Related_coordinate_file_name . _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Benjamin Bourgeois . . . . 28027 2 Tobias Madl . . . . 28027 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 28027 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '15N chemical shifts' 81 28027 '1H chemical shifts' 81 28027 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2020-04-21 2019-10-04 update BMRB 'update entry citation' 28027 1 . . 2020-04-03 2019-10-04 original author 'original release' 28027 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 28025 'human CIRBP 138-172' 28027 BMRB 28026 'human TNPO1 328-381' 28027 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 28027 _Citation.ID 1 _Citation.Name . _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.PubMed_ID 32234784 _Citation.DOI . _Citation.Full_citation . _Citation.Title ; Nonclassical nuclear localization signals mediate nuclear import of CIRBP ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'Proc. Natl. Acad. Sci. U.S.A.' _Citation.Journal_name_full 'Proceedings of the National Academy of Sciences of the United States of America' _Citation.Journal_volume 117 _Citation.Journal_issue 15 _Citation.Journal_ASTM . _Citation.Journal_ISSN 1091-6490 _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 8503 _Citation.Page_last 8514 _Citation.Year 2020 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Benjamin Bourgeois B. . . . 28027 1 2 Saskia Hutten S. . . . 28027 1 3 Benjamin Gottschalk B. . . . 28027 1 4 Mario Hofweber M. . . . 28027 1 5 Gesa Richter G. . . . 28027 1 6 Julia Sternat J. . . . 28027 1 7 Claudia Abou-Ajram C. . . . 28027 1 8 Christoph Gobl C. . . . 28027 1 9 Gerd Leitinger G. . . . 28027 1 10 Wolfgang Graier W. F. . . 28027 1 11 Dorothee Dormann D. . . . 28027 1 12 Tobias Madl T. . . . 28027 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 28027 _Assembly.ID 1 _Assembly.Name human_CIRBP_38-137 _Assembly.BMRB_code . _Assembly.Number_of_components . _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 CIRBP_68-137 1 $CIRBP A . yes native no no . . . 28027 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_CIRBP _Entity.Sf_category entity _Entity.Sf_framecode CIRBP _Entity.Entry_ID 28027 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name CIRBP _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polypeptide(L) _Entity.Polymer_type_details . _Entity.Polymer_strand_ID . _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; MKHHHHHHPMSDYDIPTTEN LYFQGAMGNGKSVDGRQIRV DQAGKSSDNRSRGYRGGSAG GRGFFRGGRGRGRGFSRGGG DRGYGGNRFESRSGGYGG ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 98 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'all free' _Entity.Src_method . _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight . _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 40 MET . 28027 1 2 41 LYS . 28027 1 3 42 HIS . 28027 1 4 43 HIS . 28027 1 5 44 HIS . 28027 1 6 45 HIS . 28027 1 7 46 HIS . 28027 1 8 47 HIS . 28027 1 9 48 PRO . 28027 1 10 49 MET . 28027 1 11 50 SER . 28027 1 12 51 ASP . 28027 1 13 52 TYR . 28027 1 14 53 ASP . 28027 1 15 54 ILE . 28027 1 16 55 PRO . 28027 1 17 56 THR . 28027 1 18 57 THR . 28027 1 19 58 GLU . 28027 1 20 59 ASN . 28027 1 21 60 LEU . 28027 1 22 61 TYR . 28027 1 23 62 PHE . 28027 1 24 63 GLN . 28027 1 25 64 GLY . 28027 1 26 65 ALA . 28027 1 27 66 MET . 28027 1 28 67 GLY . 28027 1 29 68 ASN . 28027 1 30 69 GLY . 28027 1 31 70 LYS . 28027 1 32 71 SER . 28027 1 33 72 VAL . 28027 1 34 73 ASP . 28027 1 35 74 GLY . 28027 1 36 75 ARG . 28027 1 37 76 GLN . 28027 1 38 77 ILE . 28027 1 39 78 ARG . 28027 1 40 79 VAL . 28027 1 41 80 ASP . 28027 1 42 81 GLN . 28027 1 43 82 ALA . 28027 1 44 83 GLY . 28027 1 45 84 LYS . 28027 1 46 85 SER . 28027 1 47 86 SER . 28027 1 48 87 ASP . 28027 1 49 88 ASN . 28027 1 50 89 ARG . 28027 1 51 90 SER . 28027 1 52 91 ARG . 28027 1 53 92 GLY . 28027 1 54 93 TYR . 28027 1 55 94 ARG . 28027 1 56 95 GLY . 28027 1 57 96 GLY . 28027 1 58 97 SER . 28027 1 59 98 ALA . 28027 1 60 99 GLY . 28027 1 61 100 GLY . 28027 1 62 101 ARG . 28027 1 63 102 GLY . 28027 1 64 103 PHE . 28027 1 65 104 PHE . 28027 1 66 105 ARG . 28027 1 67 106 GLY . 28027 1 68 107 GLY . 28027 1 69 108 ARG . 28027 1 70 109 GLY . 28027 1 71 110 ARG . 28027 1 72 111 GLY . 28027 1 73 112 ARG . 28027 1 74 113 GLY . 28027 1 75 114 PHE . 28027 1 76 115 SER . 28027 1 77 116 ARG . 28027 1 78 117 GLY . 28027 1 79 118 GLY . 28027 1 80 119 GLY . 28027 1 81 120 ASP . 28027 1 82 121 ARG . 28027 1 83 122 GLY . 28027 1 84 123 TYR . 28027 1 85 124 GLY . 28027 1 86 125 GLY . 28027 1 87 126 ASN . 28027 1 88 127 ARG . 28027 1 89 128 PHE . 28027 1 90 129 GLU . 28027 1 91 130 SER . 28027 1 92 131 ARG . 28027 1 93 132 SER . 28027 1 94 133 GLY . 28027 1 95 134 GLY . 28027 1 96 135 TYR . 28027 1 97 136 GLY . 28027 1 98 137 GLY . 28027 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . MET 1 1 28027 1 . LYS 2 2 28027 1 . HIS 3 3 28027 1 . HIS 4 4 28027 1 . HIS 5 5 28027 1 . HIS 6 6 28027 1 . HIS 7 7 28027 1 . HIS 8 8 28027 1 . PRO 9 9 28027 1 . MET 10 10 28027 1 . SER 11 11 28027 1 . ASP 12 12 28027 1 . TYR 13 13 28027 1 . ASP 14 14 28027 1 . ILE 15 15 28027 1 . PRO 16 16 28027 1 . THR 17 17 28027 1 . THR 18 18 28027 1 . GLU 19 19 28027 1 . ASN 20 20 28027 1 . LEU 21 21 28027 1 . TYR 22 22 28027 1 . PHE 23 23 28027 1 . GLN 24 24 28027 1 . GLY 25 25 28027 1 . ALA 26 26 28027 1 . MET 27 27 28027 1 . GLY 28 28 28027 1 . ASN 29 29 28027 1 . GLY 30 30 28027 1 . LYS 31 31 28027 1 . SER 32 32 28027 1 . VAL 33 33 28027 1 . ASP 34 34 28027 1 . GLY 35 35 28027 1 . ARG 36 36 28027 1 . GLN 37 37 28027 1 . ILE 38 38 28027 1 . ARG 39 39 28027 1 . VAL 40 40 28027 1 . ASP 41 41 28027 1 . GLN 42 42 28027 1 . ALA 43 43 28027 1 . GLY 44 44 28027 1 . LYS 45 45 28027 1 . SER 46 46 28027 1 . SER 47 47 28027 1 . ASP 48 48 28027 1 . ASN 49 49 28027 1 . ARG 50 50 28027 1 . SER 51 51 28027 1 . ARG 52 52 28027 1 . GLY 53 53 28027 1 . TYR 54 54 28027 1 . ARG 55 55 28027 1 . GLY 56 56 28027 1 . GLY 57 57 28027 1 . SER 58 58 28027 1 . ALA 59 59 28027 1 . GLY 60 60 28027 1 . GLY 61 61 28027 1 . ARG 62 62 28027 1 . GLY 63 63 28027 1 . PHE 64 64 28027 1 . PHE 65 65 28027 1 . ARG 66 66 28027 1 . GLY 67 67 28027 1 . GLY 68 68 28027 1 . ARG 69 69 28027 1 . GLY 70 70 28027 1 . ARG 71 71 28027 1 . GLY 72 72 28027 1 . ARG 73 73 28027 1 . GLY 74 74 28027 1 . PHE 75 75 28027 1 . SER 76 76 28027 1 . ARG 77 77 28027 1 . GLY 78 78 28027 1 . GLY 79 79 28027 1 . GLY 80 80 28027 1 . ASP 81 81 28027 1 . ARG 82 82 28027 1 . GLY 83 83 28027 1 . TYR 84 84 28027 1 . GLY 85 85 28027 1 . GLY 86 86 28027 1 . ASN 87 87 28027 1 . ARG 88 88 28027 1 . PHE 89 89 28027 1 . GLU 90 90 28027 1 . SER 91 91 28027 1 . ARG 92 92 28027 1 . SER 93 93 28027 1 . GLY 94 94 28027 1 . GLY 95 95 28027 1 . TYR 96 96 28027 1 . GLY 97 97 28027 1 . GLY 98 98 28027 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 28027 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $CIRBP . 9606 organism . 'Homo sapiens' Human . . Eukaryota Metazoa Homo sapiens . . . . . . . . . . . . . 28027 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 28027 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $CIRBP . 'recombinant technology' 'Escherichia coli' . . . Escherichia coli . . . . . . pETM-11 . . . 28027 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 28027 _Sample.ID 1 _Sample.Name . _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 CIRBP '[U-99% 13C; U-99% 15N]' . . 1 $CIRBP . . 500 . . uM . . . . 28027 1 2 D2O '[U-100% 2H]' . . . . . . 10 . . % . . . . 28027 1 3 TRIS 'natural abundance' . . . . . . 50 . . mM . . . . 28027 1 4 'sodium chloride' 'natural abundance' . . . . . . 150 . . mM . . . . 28027 1 5 TCEP 'natural abundance' . . . . . . 2 . . mM . . . . 28027 1 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 28027 _Sample_condition_list.ID 1 _Sample_condition_list.Name . _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 0.15 . M 28027 1 pH 6.7 . pH 28027 1 pressure 1 . atm 28027 1 temperature 298 . K 28027 1 stop_ save_ ############################ # Computer software used # ############################ save_CCPN _Software.Sf_category software _Software.Sf_framecode CCPN _Software.Entry_ID 28027 _Software.ID 1 _Software.Type . _Software.Name CCPN _Software.Version . _Software.DOI . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Bruker Biospin' . . 28027 1 CCPN . . 28027 1 'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax' . . 28027 1 stop_ loop_ _Task.Software_module _Task.Task _Task.Entry_ID _Task.Software_ID . collection 28027 1 . 'peak picking' 28027 1 . processing 28027 1 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_1 _NMR_spectrometer.Entry_ID 28027 _NMR_spectrometer.ID 1 _NMR_spectrometer.Name . _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_NMR_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list _NMR_spectrometer_list.Entry_ID 28027 _NMR_spectrometer_list.ID 1 _NMR_spectrometer_list.Name . loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 spectrometer_1 Bruker Avance . 600 . . . 28027 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 28027 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-15N HSQC' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 28027 1 2 '3D HNCACB' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 28027 1 3 '3D CBCA(CO)NH' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 28027 1 4 '3D HN(CA)NNH' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . 1 $spectrometer_1 . . . . . . . . . . . . . . . . 28027 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference_1 _Chem_shift_reference.Entry_ID 28027 _Chem_shift_reference.ID 1 _Chem_shift_reference.Name . _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID H 1 water protons . . . . ppm 4.707 na indirect 1 . . . . . 28027 1 N 15 '[15N] ammonium chloride' nitrogen . . . . ppm 117 na indirect 1 . . . . . 28027 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1 _Assigned_chem_shift_list.Entry_ID 28027 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Name . _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-15N HSQC' . . . 28027 1 2 '3D HNCACB' . . . 28027 1 3 '3D CBCA(CO)NH' . . . 28027 1 4 '3D HN(CA)NNH' . . . 28027 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_assembly_asym_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Ambiguity_set_ID _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 . 1 10 10 MET H H 1 8.648 . . . . . . . . 49 M HN . 28027 1 2 . 1 . 1 10 10 MET N N 15 120.302 . . . . . . . . 49 M N . 28027 1 3 . 1 . 1 11 11 SER H H 1 8.189 . . . . . . . . 50 S HN . 28027 1 4 . 1 . 1 11 11 SER N N 15 116.090 . . . . . . . . 50 S N . 28027 1 5 . 1 . 1 12 12 ASP H H 1 8.249 . . . . . . . . 51 D HN . 28027 1 6 . 1 . 1 12 12 ASP N N 15 121.779 . . . . . . . . 51 D N . 28027 1 7 . 1 . 1 13 13 TYR H H 1 7.823 . . . . . . . . 52 Y HN . 28027 1 8 . 1 . 1 13 13 TYR N N 15 118.789 . . . . . . . . 52 Y N . 28027 1 9 . 1 . 1 14 14 ASP H H 1 8.071 . . . . . . . . 53 D HN . 28027 1 10 . 1 . 1 14 14 ASP N N 15 121.599 . . . . . . . . 53 D N . 28027 1 11 . 1 . 1 15 15 ILE H H 1 7.839 . . . . . . . . 54 I HN . 28027 1 12 . 1 . 1 15 15 ILE N N 15 122.175 . . . . . . . . 54 I N . 28027 1 13 . 1 . 1 17 17 THR H H 1 8.220 . . . . . . . . 56 T HN . 28027 1 14 . 1 . 1 17 17 THR N N 15 114.495 . . . . . . . . 56 T N . 28027 1 15 . 1 . 1 18 18 THR H H 1 8.015 . . . . . . . . 57 T HN . 28027 1 16 . 1 . 1 18 18 THR N N 15 115.235 . . . . . . . . 57 T N . 28027 1 17 . 1 . 1 19 19 GLU H H 1 8.307 . . . . . . . . 58 E HN . 28027 1 18 . 1 . 1 19 19 GLU N N 15 122.636 . . . . . . . . 58 E N . 28027 1 19 . 1 . 1 20 20 ASN H H 1 8.301 . . . . . . . . 59 N HN . 28027 1 20 . 1 . 1 20 20 ASN N N 15 119.338 . . . . . . . . 59 N N . 28027 1 21 . 1 . 1 21 21 LEU H H 1 7.959 . . . . . . . . 60 L HN . 28027 1 22 . 1 . 1 21 21 LEU N N 15 122.128 . . . . . . . . 60 L N . 28027 1 23 . 1 . 1 22 22 TYR H H 1 7.894 . . . . . . . . 61 Y HN . 28027 1 24 . 1 . 1 22 22 TYR N N 15 119.485 . . . . . . . . 61 Y N . 28027 1 25 . 1 . 1 23 23 PHE H H 1 7.906 . . . . . . . . 62 F HN . 28027 1 26 . 1 . 1 23 23 PHE N N 15 121.297 . . . . . . . . 62 F N . 28027 1 27 . 1 . 1 24 24 GLN H H 1 7.670 . . . . . . . . 63 Q HN . 28027 1 28 . 1 . 1 24 24 GLN N N 15 126.010 . . . . . . . . 63 Q N . 28027 1 29 . 1 . 1 27 27 MET H H 1 8.476 . . . . . . . . 66 M HN . 28027 1 30 . 1 . 1 27 27 MET N N 15 119.232 . . . . . . . . 66 M N . 28027 1 31 . 1 . 1 28 28 GLY H H 1 8.258 . . . . . . . . 67 G HN . 28027 1 32 . 1 . 1 28 28 GLY N N 15 110.037 . . . . . . . . 67 G N . 28027 1 33 . 1 . 1 29 29 ASN H H 1 7.906 . . . . . . . . 68 N HN . 28027 1 34 . 1 . 1 29 29 ASN N N 15 124.123 . . . . . . . . 68 N N . 28027 1 35 . 1 . 1 30 30 GLY H H 1 8.213 . . . . . . . . 69 G HN . 28027 1 36 . 1 . 1 30 30 GLY N N 15 113.905 . . . . . . . . 69 G N . 28027 1 37 . 1 . 1 31 31 LYS H H 1 8.195 . . . . . . . . 70 K HN . 28027 1 38 . 1 . 1 31 31 LYS N N 15 120.365 . . . . . . . . 70 K N . 28027 1 39 . 1 . 1 32 32 SER H H 1 8.308 . . . . . . . . 71 S HN . 28027 1 40 . 1 . 1 32 32 SER N N 15 117.006 . . . . . . . . 71 S N . 28027 1 41 . 1 . 1 33 33 VAL H H 1 8.190 . . . . . . . . 72 V HN . 28027 1 42 . 1 . 1 33 33 VAL N N 15 121.310 . . . . . . . . 72 V N . 28027 1 43 . 1 . 1 34 34 ASP H H 1 8.265 . . . . . . . . 73 D HN . 28027 1 44 . 1 . 1 34 34 ASP N N 15 123.069 . . . . . . . . 73 D N . 28027 1 45 . 1 . 1 35 35 GLY H H 1 8.279 . . . . . . . . 74 G HN . 28027 1 46 . 1 . 1 35 35 GLY N N 15 109.462 . . . . . . . . 74 G N . 28027 1 47 . 1 . 1 36 36 ARG H H 1 8.022 . . . . . . . . 75 R HN . 28027 1 48 . 1 . 1 36 36 ARG N N 15 120.063 . . . . . . . . 75 R N . 28027 1 49 . 1 . 1 37 37 GLN H H 1 8.315 . . . . . . . . 76 Q HN . 28027 1 50 . 1 . 1 37 37 GLN N N 15 121.028 . . . . . . . . 76 Q N . 28027 1 51 . 1 . 1 38 38 ILE H H 1 8.098 . . . . . . . . 77 I HN . 28027 1 52 . 1 . 1 38 38 ILE N N 15 122.600 . . . . . . . . 77 I N . 28027 1 53 . 1 . 1 39 39 ARG H H 1 8.337 . . . . . . . . 78 R HN . 28027 1 54 . 1 . 1 39 39 ARG N N 15 125.612 . . . . . . . . 78 R N . 28027 1 55 . 1 . 1 40 40 VAL H H 1 8.209 . . . . . . . . 79 V HN . 28027 1 56 . 1 . 1 40 40 VAL N N 15 121.835 . . . . . . . . 79 V N . 28027 1 57 . 1 . 1 41 41 ASP H H 1 8.387 . . . . . . . . 80 D HN . 28027 1 58 . 1 . 1 41 41 ASP N N 15 123.549 . . . . . . . . 80 D N . 28027 1 59 . 1 . 1 42 42 GLN H H 1 8.242 . . . . . . . . 81 Q HN . 28027 1 60 . 1 . 1 42 42 GLN N N 15 120.755 . . . . . . . . 81 Q N . 28027 1 61 . 1 . 1 43 43 ALA H H 1 8.230 . . . . . . . . 82 A HN . 28027 1 62 . 1 . 1 43 43 ALA N N 15 124.498 . . . . . . . . 82 A N . 28027 1 63 . 1 . 1 44 44 GLY H H 1 8.259 . . . . . . . . 83 G HN . 28027 1 64 . 1 . 1 44 44 GLY N N 15 107.954 . . . . . . . . 83 G N . 28027 1 65 . 1 . 1 45 45 LYS H H 1 8.060 . . . . . . . . 84 K HN . 28027 1 66 . 1 . 1 45 45 LYS N N 15 120.622 . . . . . . . . 84 K N . 28027 1 67 . 1 . 1 46 46 SER H H 1 8.342 . . . . . . . . 85 S HN . 28027 1 68 . 1 . 1 46 46 SER N N 15 116.969 . . . . . . . . 85 S N . 28027 1 69 . 1 . 1 47 47 SER H H 1 8.300 . . . . . . . . 86 S HN . 28027 1 70 . 1 . 1 47 47 SER N N 15 117.556 . . . . . . . . 86 S N . 28027 1 71 . 1 . 1 48 48 ASP H H 1 8.205 . . . . . . . . 87 D HN . 28027 1 72 . 1 . 1 48 48 ASP N N 15 122.030 . . . . . . . . 87 D N . 28027 1 73 . 1 . 1 49 49 ASN H H 1 8.293 . . . . . . . . 88 N HN . 28027 1 74 . 1 . 1 49 49 ASN N N 15 119.499 . . . . . . . . 88 N N . 28027 1 75 . 1 . 1 50 50 ARG H H 1 8.208 . . . . . . . . 89 R HN . 28027 1 76 . 1 . 1 50 50 ARG N N 15 120.641 . . . . . . . . 89 R N . 28027 1 77 . 1 . 1 51 51 SER H H 1 8.188 . . . . . . . . 90 S HN . 28027 1 78 . 1 . 1 51 51 SER N N 15 116.020 . . . . . . . . 90 S N . 28027 1 79 . 1 . 1 52 52 ARG H H 1 8.198 . . . . . . . . 91 R HN . 28027 1 80 . 1 . 1 52 52 ARG N N 15 122.450 . . . . . . . . 91 R N . 28027 1 81 . 1 . 1 53 53 GLY H H 1 8.223 . . . . . . . . 92 G HN . 28027 1 82 . 1 . 1 53 53 GLY N N 15 109.068 . . . . . . . . 92 G N . 28027 1 83 . 1 . 1 54 54 TYR H H 1 7.979 . . . . . . . . 93 Y HN . 28027 1 84 . 1 . 1 54 54 TYR N N 15 120.484 . . . . . . . . 93 Y N . 28027 1 85 . 1 . 1 55 55 ARG H H 1 8.261 . . . . . . . . 94 R HN . 28027 1 86 . 1 . 1 55 55 ARG N N 15 124.047 . . . . . . . . 94 R N . 28027 1 87 . 1 . 1 56 56 GLY H H 1 7.650 . . . . . . . . 95 G HN . 28027 1 88 . 1 . 1 56 56 GLY N N 15 108.926 . . . . . . . . 95 G N . 28027 1 89 . 1 . 1 57 57 GLY H H 1 8.149 . . . . . . . . 96 G HN . 28027 1 90 . 1 . 1 57 57 GLY N N 15 108.569 . . . . . . . . 96 G N . 28027 1 91 . 1 . 1 58 58 SER H H 1 8.213 . . . . . . . . 97 S HN . 28027 1 92 . 1 . 1 58 58 SER N N 15 115.770 . . . . . . . . 97 S N . 28027 1 93 . 1 . 1 59 59 ALA H H 1 8.342 . . . . . . . . 98 A HN . 28027 1 94 . 1 . 1 59 59 ALA N N 15 125.842 . . . . . . . . 98 A N . 28027 1 95 . 1 . 1 60 60 GLY H H 1 8.187 . . . . . . . . 99 G HN . 28027 1 96 . 1 . 1 60 60 GLY N N 15 107.763 . . . . . . . . 99 G N . 28027 1 97 . 1 . 1 61 61 GLY H H 1 8.115 . . . . . . . . 100 G HN . 28027 1 98 . 1 . 1 61 61 GLY N N 15 108.465 . . . . . . . . 100 G N . 28027 1 99 . 1 . 1 62 62 ARG H H 1 8.152 . . . . . . . . 101 R HN . 28027 1 100 . 1 . 1 62 62 ARG N N 15 120.141 . . . . . . . . 101 R N . 28027 1 101 . 1 . 1 63 63 GLY H H 1 8.300 . . . . . . . . 102 G HN . 28027 1 102 . 1 . 1 63 63 GLY N N 15 109.328 . . . . . . . . 102 G N . 28027 1 103 . 1 . 1 64 64 PHE H H 1 7.927 . . . . . . . . 103 F HN . 28027 1 104 . 1 . 1 64 64 PHE N N 15 119.893 . . . . . . . . 103 F N . 28027 1 105 . 1 . 1 65 65 PHE H H 1 8.167 . . . . . . . . 104 F HN . 28027 1 106 . 1 . 1 65 65 PHE N N 15 122.011 . . . . . . . . 104 F N . 28027 1 107 . 1 . 1 66 66 ARG H H 1 8.190 . . . . . . . . 105 R HN . 28027 1 108 . 1 . 1 66 66 ARG N N 15 123.553 . . . . . . . . 105 R N . 28027 1 109 . 1 . 1 67 67 GLY H H 1 7.815 . . . . . . . . 106 G HN . 28027 1 110 . 1 . 1 67 67 GLY N N 15 109.218 . . . . . . . . 106 G N . 28027 1 111 . 1 . 1 68 68 GLY H H 1 8.133 . . . . . . . . 107 G HN . 28027 1 112 . 1 . 1 68 68 GLY N N 15 108.516 . . . . . . . . 107 G N . 28027 1 113 . 1 . 1 74 74 GLY H H 1 8.338 . . . . . . . . 113 G HN . 28027 1 114 . 1 . 1 74 74 GLY N N 15 109.570 . . . . . . . . 113 G N . 28027 1 115 . 1 . 1 75 75 PHE H H 1 8.001 . . . . . . . . 114 F HN . 28027 1 116 . 1 . 1 75 75 PHE N N 15 119.821 . . . . . . . . 114 F N . 28027 1 117 . 1 . 1 76 76 SER H H 1 8.190 . . . . . . . . 115 S HN . 28027 1 118 . 1 . 1 76 76 SER N N 15 117.400 . . . . . . . . 115 S N . 28027 1 119 . 1 . 1 77 77 ARG H H 1 8.317 . . . . . . . . 116 R HN . 28027 1 120 . 1 . 1 77 77 ARG N N 15 123.065 . . . . . . . . 116 R N . 28027 1 121 . 1 . 1 78 78 GLY H H 1 8.346 . . . . . . . . 117 G HN . 28027 1 122 . 1 . 1 78 78 GLY N N 15 109.806 . . . . . . . . 117 G N . 28027 1 123 . 1 . 1 79 79 GLY H H 1 8.205 . . . . . . . . 118 G HN . 28027 1 124 . 1 . 1 79 79 GLY N N 15 108.703 . . . . . . . . 118 G N . 28027 1 125 . 1 . 1 80 80 GLY H H 1 8.242 . . . . . . . . 119 G HN . 28027 1 126 . 1 . 1 80 80 GLY N N 15 108.791 . . . . . . . . 119 G N . 28027 1 127 . 1 . 1 81 81 ASP H H 1 8.199 . . . . . . . . 120 D HN . 28027 1 128 . 1 . 1 81 81 ASP N N 15 120.331 . . . . . . . . 120 D N . 28027 1 129 . 1 . 1 82 82 ARG H H 1 8.248 . . . . . . . . 121 R HN . 28027 1 130 . 1 . 1 82 82 ARG N N 15 120.821 . . . . . . . . 121 R N . 28027 1 131 . 1 . 1 83 83 GLY H H 1 8.251 . . . . . . . . 122 G HN . 28027 1 132 . 1 . 1 83 83 GLY N N 15 108.828 . . . . . . . . 122 G N . 28027 1 133 . 1 . 1 84 84 TYR H H 1 8.016 . . . . . . . . 123 Y HN . 28027 1 134 . 1 . 1 84 84 TYR N N 15 119.980 . . . . . . . . 123 Y N . 28027 1 135 . 1 . 1 85 85 GLY H H 1 8.371 . . . . . . . . 124 G HN . 28027 1 136 . 1 . 1 85 85 GLY N N 15 111.072 . . . . . . . . 124 G N . 28027 1 137 . 1 . 1 86 86 GLY H H 1 7.849 . . . . . . . . 125 G HN . 28027 1 138 . 1 . 1 86 86 GLY N N 15 108.220 . . . . . . . . 125 G N . 28027 1 139 . 1 . 1 87 87 ASN H H 1 8.237 . . . . . . . . 126 N HN . 28027 1 140 . 1 . 1 87 87 ASN N N 15 118.414 . . . . . . . . 126 N N . 28027 1 141 . 1 . 1 88 88 ARG H H 1 8.178 . . . . . . . . 127 R HN . 28027 1 142 . 1 . 1 88 88 ARG N N 15 121.076 . . . . . . . . 127 R N . 28027 1 143 . 1 . 1 89 89 PHE H H 1 8.153 . . . . . . . . 128 F HN . 28027 1 144 . 1 . 1 89 89 PHE N N 15 120.340 . . . . . . . . 128 F N . 28027 1 145 . 1 . 1 90 90 GLU H H 1 8.166 . . . . . . . . 129 E HN . 28027 1 146 . 1 . 1 90 90 GLU N N 15 122.005 . . . . . . . . 129 E N . 28027 1 147 . 1 . 1 91 91 SER H H 1 8.226 . . . . . . . . 130 S HN . 28027 1 148 . 1 . 1 91 91 SER N N 15 116.875 . . . . . . . . 130 S N . 28027 1 149 . 1 . 1 92 92 ARG H H 1 8.337 . . . . . . . . 131 R HN . 28027 1 150 . 1 . 1 92 92 ARG N N 15 122.995 . . . . . . . . 131 R N . 28027 1 151 . 1 . 1 93 93 SER H H 1 8.277 . . . . . . . . 132 S HN . 28027 1 152 . 1 . 1 93 93 SER N N 15 116.607 . . . . . . . . 132 S N . 28027 1 153 . 1 . 1 94 94 GLY H H 1 8.327 . . . . . . . . 133 G HN . 28027 1 154 . 1 . 1 94 94 GLY N N 15 110.822 . . . . . . . . 133 G N . 28027 1 155 . 1 . 1 95 95 GLY H H 1 8.107 . . . . . . . . 134 G HN . 28027 1 156 . 1 . 1 95 95 GLY N N 15 108.365 . . . . . . . . 134 G N . 28027 1 157 . 1 . 1 96 96 TYR H H 1 8.085 . . . . . . . . 135 Y HN . 28027 1 158 . 1 . 1 96 96 TYR N N 15 120.193 . . . . . . . . 135 Y N . 28027 1 159 . 1 . 1 97 97 GLY H H 1 8.324 . . . . . . . . 136 G HN . 28027 1 160 . 1 . 1 97 97 GLY N N 15 111.706 . . . . . . . . 136 G N . 28027 1 161 . 1 . 1 98 98 GLY H H 1 7.486 . . . . . . . . 137 G HN . 28027 1 162 . 1 . 1 98 98 GLY N N 15 114.795 . . . . . . . . 137 G N . 28027 1 stop_ save_