data_27635 ####################### # Entry information # ####################### save_entry_information _Saveframe_category entry_information _Entry_title ; Microsecond Protein Dynamics from Combined Bloch-McConnell and Near-Rotary-Resonance R1rho Relaxation-Dispersion MAS NMR ; _BMRB_accession_number 27635 _BMRB_flat_file_name bmr27635.str _Entry_type original _Submission_date 2018-10-03 _Accession_date 2018-10-03 _Entry_origination author _NMR_STAR_version 2.1.1 _Experimental_method NMR _Details . loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Marion Dominique . . 2 Gauto Diego F. . 3 Ayala Isabel . . 4 Hessel Audrey . . 5 Schanda Paul . . stop_ loop_ _Saveframe_category_type _Saveframe_category_type_count T1rho_relaxation 27 stop_ loop_ _Data_type _Data_type_count "T1rho relaxation values" 1539 stop_ loop_ _Revision_date _Revision_keyword _Revision_author _Revision_detail 2019-02-15 update BMRB 'update entry citation' 2019-01-08 original author 'original release' stop_ _Original_release_date 2018-10-03 save_ ############################# # Citation for this entry # ############################# save_entry_citation _Saveframe_category entry_citation _Citation_full . _Citation_title ; Microsecond Protein Dynamics from Combined Bloch-McConnell and Near-Rotary-Resonance R1rho Relaxation-Dispersion MAS NMR ; _Citation_status published _Citation_type journal _CAS_abstract_code . _MEDLINE_UI_code . _PubMed_ID 30444575 loop_ _Author_ordinal _Author_family_name _Author_given_name _Author_middle_initials _Author_family_title 1 Marion Dominique . . 2 Gauto Diego F. . 3 Ayala Isabel . . 4 Giandoreggio-Barranco Karine . . 5 Schanda Paul . . stop_ _Journal_abbreviation Chemphyschem _Journal_volume 20 _Journal_issue 2 _Journal_CSD . _Book_chapter_title . _Book_volume . _Book_series . _Book_ISBN . _Conference_state_province . _Conference_abstract_number . _Page_first 276 _Page_last 284 _Year 2019 _Details . save_ ################################## # Molecular system description # ################################## save_assembly _Saveframe_category molecular_system _Mol_system_name Ubiquitin _Enzyme_commission_number . loop_ _Mol_system_component_name _Mol_label Ubiquitin $Ubiquitin stop_ _System_molecular_weight . _System_physical_state native _System_oligomer_state ? _System_paramagnetic no _System_thiol_state . _Database_query_date . _Details . save_ ######################## # Monomeric polymers # ######################## save_Ubiquitin _Saveframe_category monomeric_polymer _Mol_type polymer _Mol_polymer_class protein _Name_common Ubiquitin _Molecular_mass . _Mol_thiol_state 'not present' _Details . ############################## # Polymer residue sequence # ############################## _Residue_count 76 _Mol_residue_sequence ; MQIFVKTLTGKTITLEVEPS DTIENVKAKIQDKEGIPPDQ QRLIFAGKQLEDGRTLSDYN IQKESTLHLVLRLRGG ; loop_ _Residue_seq_code _Residue_label 1 MET 2 GLN 3 ILE 4 PHE 5 VAL 6 LYS 7 THR 8 LEU 9 THR 10 GLY 11 LYS 12 THR 13 ILE 14 THR 15 LEU 16 GLU 17 VAL 18 GLU 19 PRO 20 SER 21 ASP 22 THR 23 ILE 24 GLU 25 ASN 26 VAL 27 LYS 28 ALA 29 LYS 30 ILE 31 GLN 32 ASP 33 LYS 34 GLU 35 GLY 36 ILE 37 PRO 38 PRO 39 ASP 40 GLN 41 GLN 42 ARG 43 LEU 44 ILE 45 PHE 46 ALA 47 GLY 48 LYS 49 GLN 50 LEU 51 GLU 52 ASP 53 GLY 54 ARG 55 THR 56 LEU 57 SER 58 ASP 59 TYR 60 ASN 61 ILE 62 GLN 63 LYS 64 GLU 65 SER 66 THR 67 LEU 68 HIS 69 LEU 70 VAL 71 LEU 72 ARG 73 LEU 74 ARG 75 GLY 76 GLY stop_ _Sequence_homology_query_date . _Sequence_homology_query_revised_last_date . save_ #################### # Natural source # #################### save_natural_source _Saveframe_category natural_source loop_ _Mol_label _Organism_name_common _NCBI_taxonomy_ID _Superkingdom _Kingdom _Genus _Species $Ubiquitin Human 9606 Eukaryota Metazoa Homo sapiens stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Saveframe_category experimental_source loop_ _Mol_label _Production_method _Host_organism_name_common _Genus _Species _Strain _Vector_name $Ubiquitin 'recombinant technology' . Escherichia coli . pET21b stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Saveframe_category sample _Sample_type microcrystalline _Details 'Ubiquitin crystallized with MPD - Solid State' loop_ _Mol_label _Concentration_value _Concentration_value_units _Isotopic_labeling $Ubiquitin NA mM '[U-100% 15N]' stop_ save_ ############################ # Computer software used # ############################ save_NMRPipe _Saveframe_category software _Name NMRPipe _Version . loop_ _Vendor _Address _Electronic_address 'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax' . . stop_ loop_ _Task 'peak picking' processing stop_ _Details . save_ save_Gamma _Saveframe_category software _Name Gamma _Version . loop_ _Vendor _Address _Electronic_address 'Scott A. Smith' ; ETH - Zurich National High Field Laboratory ; . stop_ loop_ _Task 'Spin evolution simulation' stop_ _Details . save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _Saveframe_category NMR_spectrometer _Manufacturer Agilent _Model INOVA _Field_strength 600 _Details . save_ ############################# # NMR applied experiments # ############################# save_2D_1H-15N_HSQC_1 _Saveframe_category NMR_applied_experiment _Experiment_name '2D 1H-15N HSQC' _Sample_label $sample_1 save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Saveframe_category sample_conditions _Details ; Reprotonation of exchangeable sites in H2O/D2O (50:50) mixture. Crystallization using 2-methylpentane-2,5-diol (MPD) ; loop_ _Variable_type _Variable_value _Variable_value_error _Variable_value_units temperature 273 . K stop_ save_ save_Ubiquitin_R1rho_2.3kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 9.560 0.475 2 3 ILE N 4.515 0.089 3 4 PHE N 2.595 0.058 4 5 VAL N 2.864 0.120 5 6 LYS N 3.225 0.145 6 7 THR N 9.141 0.688 7 10 GLY N 16.181 1.155 8 11 LYS N 20.450 1.368 9 12 THR N 5.099 0.141 10 14 THR N 8.432 0.663 11 15 LEU N 3.521 0.190 12 16 GLU N 3.451 0.083 13 17 VAL N 7.899 0.278 14 18 GLU N 3.041 0.079 15 20 SER N 9.960 0.295 16 21 ASP N 5.612 0.126 17 22 THR N 8.026 0.683 18 23 ILE N 10.753 0.180 19 26 VAL N 4.909 0.347 20 27 LYS N 4.669 0.178 21 32 ASP N 2.646 0.290 22 33 LYS N 2.796 0.079 23 34 GLU N 3.851 0.145 24 35 GLY N 4.643 0.108 25 36 ILE N 4.690 0.093 26 39 ASP N 4.234 0.076 27 40 GLN N 7.348 0.199 28 41 GLN N 8.368 0.199 29 42 ARG N 3.097 0.071 30 44 ILE N 3.444 0.150 31 45 PHE N 2.518 0.112 32 46 ALA N 2.196 0.106 33 47 GLY N 2.666 0.096 34 48 LYS N 2.969 0.091 35 49 GLN N 4.266 0.146 36 50 LEU N 3.329 0.130 37 51 GLU N 11.628 0.412 38 52 ASP N 13.021 0.210 39 53 GLY N 7.491 0.397 40 54 ARG N 10.822 0.580 41 55 THR N 7.092 0.539 42 56 LEU N 3.245 0.159 43 57 SER N 7.616 1.378 44 58 ASP N 4.376 0.331 45 59 TYR N 3.727 0.108 46 60 ASN N 3.852 0.120 47 61 ILE N 3.183 0.092 48 62 GLN N 6.321 0.264 49 63 LYS N 9.970 0.206 50 64 GLU N 4.643 0.108 51 65 SER N 3.772 0.087 52 66 THR N 3.440 0.244 53 67 LEU N 5.141 0.448 54 68 HIS N 3.288 0.268 55 69 LEU N 2.667 0.075 56 70 VAL N 4.871 0.194 57 71 LEU N 7.570 1.433 stop_ save_ save_Ubiquitin_R1rho_2.3kHz_a _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 8.045 0.158 2 3 ILE N 4.257 0.148 3 4 PHE N 2.266 0.132 4 5 VAL N 2.847 0.082 5 6 LYS N 3.002 0.185 6 7 THR N 8.183 0.761 7 10 GLY N 14.663 1.337 8 11 LYS N 19.157 1.281 9 12 THR N 5.008 0.235 10 14 THR N 7.680 0.599 11 15 LEU N 3.073 0.061 12 16 GLU N 3.449 0.119 13 17 VAL N 7.874 0.344 14 18 GLU N 2.692 0.156 15 20 SER N 10.776 0.462 16 21 ASP N 5.435 0.279 17 22 THR N 7.968 0.383 18 23 ILE N 10.299 0.349 19 26 VAL N 4.753 0.196 20 27 LYS N 4.218 0.320 21 32 ASP N 2.252 0.173 22 33 LYS N 2.419 0.173 23 34 GLU N 3.736 0.218 24 35 GLY N 4.604 0.135 25 36 ILE N 4.090 0.153 26 39 ASP N 4.060 0.164 27 40 GLN N 6.798 0.402 28 41 GLN N 8.065 0.315 29 42 ARG N 2.693 0.176 30 44 ILE N 2.903 0.078 31 45 PHE N 2.269 0.046 32 46 ALA N 2.003 0.162 33 47 GLY N 2.496 0.165 34 48 LYS N 2.759 0.111 35 49 GLN N 4.211 0.081 36 50 LEU N 3.245 0.278 37 51 GLU N 11.547 0.228 38 52 ASP N 12.870 0.500 39 53 GLY N 6.780 0.644 40 54 ARG N 10.121 0.338 41 55 THR N 6.983 0.480 42 56 LEU N 3.100 0.297 43 57 SER N 7.102 0.677 44 58 ASP N 4.049 0.800 45 59 TYR N 3.408 0.189 46 60 ASN N 3.498 0.316 47 61 ILE N 3.108 0.160 48 62 GLN N 5.931 0.200 49 63 LYS N 9.709 0.268 50 64 GLU N 4.604 0.135 51 65 SER N 3.689 0.137 52 66 THR N 3.313 0.189 53 67 LEU N 3.726 0.189 54 68 HIS N 3.094 0.161 55 69 LEU N 2.564 0.096 56 70 VAL N 3.705 0.079 57 71 LEU N 13.605 0.352 stop_ save_ save_Ubiquitin_R1rho_2.5kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 7.396 0.141 2 3 ILE N 4.390 0.084 3 4 PHE N 2.478 0.082 4 5 VAL N 2.716 0.091 5 6 LYS N 2.935 0.071 6 7 THR N 9.533 0.600 7 10 GLY N 16.611 1.269 8 11 LYS N 20.747 1.270 9 12 THR N 5.018 0.216 10 14 THR N 8.591 0.561 11 15 LEU N 3.636 0.190 12 16 GLU N 3.448 0.083 13 17 VAL N 7.541 0.219 14 18 GLU N 2.860 0.072 15 20 SER N 9.443 0.365 16 21 ASP N 5.507 0.131 17 22 THR N 8.460 0.635 18 23 ILE N 9.681 0.322 19 26 VAL N 4.706 0.328 20 27 LYS N 4.647 0.369 21 32 ASP N 2.276 0.297 22 33 LYS N 2.740 0.081 23 34 GLU N 3.660 0.107 24 35 GLY N 4.382 0.087 25 36 ILE N 4.585 0.105 26 39 ASP N 4.005 0.099 27 40 GLN N 7.305 0.230 28 41 GLN N 8.217 0.169 29 42 ARG N 3.049 0.074 30 44 ILE N 3.566 0.178 31 45 PHE N 2.582 0.150 32 46 ALA N 2.137 0.196 33 47 GLY N 2.665 0.109 34 48 LYS N 2.945 0.073 35 49 GLN N 4.221 0.086 36 50 LEU N 3.887 0.168 37 51 GLU N 10.299 0.496 38 52 ASP N 12.987 0.447 39 53 GLY N 7.337 0.580 40 54 ARG N 9.766 0.437 41 55 THR N 6.378 0.672 42 56 LEU N 2.599 0.253 43 57 SER N 7.184 0.500 44 58 ASP N 4.833 0.471 45 59 TYR N 3.319 0.081 46 60 ASN N 3.577 0.159 47 61 ILE N 3.022 0.068 48 62 GLN N 6.211 0.280 49 63 LYS N 8.977 0.229 50 64 GLU N 4.382 0.087 51 65 SER N 3.510 0.076 52 66 THR N 3.292 0.191 53 67 LEU N 5.133 0.380 54 68 HIS N 3.281 0.272 55 69 LEU N 2.710 0.047 56 70 VAL N 5.092 0.267 57 71 LEU N 14.124 0.503 stop_ save_ save_Ubiquitin_R1rho_2.5kHz_a _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 10.091 0.440 2 3 ILE N 4.274 0.151 3 4 PHE N 2.205 0.118 4 5 VAL N 2.705 0.051 5 6 LYS N 2.712 0.152 6 7 THR N 8.525 0.568 7 10 GLY N 13.263 1.377 8 11 LYS N 19.305 1.073 9 12 THR N 4.990 0.137 10 14 THR N 7.924 0.510 11 15 LEU N 3.188 0.116 12 16 GLU N 2.663 0.092 13 17 VAL N 7.413 0.352 14 18 GLU N 2.820 0.148 15 20 SER N 10.331 0.236 16 21 ASP N 5.074 0.202 17 22 THR N 7.806 0.392 18 23 ILE N 9.174 0.329 19 26 VAL N 4.452 0.162 20 27 LYS N 4.225 0.181 21 32 ASP N 2.238 0.166 22 33 LYS N 2.441 0.185 23 34 GLU N 3.164 0.196 24 35 GLY N 4.181 0.129 25 36 ILE N 4.031 0.132 26 39 ASP N 3.918 0.170 27 40 GLN N 6.901 0.352 28 41 GLN N 7.987 0.173 29 42 ARG N 2.668 0.170 30 44 ILE N 3.079 0.085 31 45 PHE N 2.212 0.047 32 46 ALA N 1.971 0.112 33 47 GLY N 2.279 0.207 34 48 LYS N 2.793 0.145 35 49 GLN N 4.219 0.146 36 50 LEU N 3.460 0.162 37 51 GLU N 10.060 0.248 38 52 ASP N 12.531 0.338 39 53 GLY N 6.743 0.284 40 54 ARG N 9.643 0.313 41 55 THR N 6.010 0.591 42 56 LEU N 2.575 0.114 43 57 SER N 6.739 0.814 44 58 ASP N 4.537 0.276 45 59 TYR N 3.301 0.166 46 60 ASN N 3.539 0.288 47 61 ILE N 3.013 0.164 48 62 GLN N 5.705 0.143 49 63 LYS N 10.050 0.137 50 64 GLU N 4.181 0.129 51 65 SER N 3.487 0.133 52 66 THR N 2.926 0.179 53 67 LEU N 3.525 0.140 54 68 HIS N 2.938 0.155 55 69 LEU N 2.625 0.095 56 70 VAL N 3.781 0.105 57 71 LEU N 14.006 0.537 stop_ save_ save_Ubiquitin_R1rho_3kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 9.268 0.385 2 3 ILE N 4.193 0.116 3 4 PHE N 2.243 0.108 4 5 VAL N 2.569 0.098 5 6 LYS N 2.853 0.108 6 7 THR N 9.141 0.339 7 10 GLY N 16.447 0.993 8 11 LYS N 20.576 1.177 9 12 THR N 4.980 0.235 10 14 THR N 8.170 0.356 11 15 LEU N 3.541 0.163 12 16 GLU N 3.390 0.101 13 17 VAL N 7.283 0.279 14 18 GLU N 2.722 0.059 15 20 SER N 9.533 0.391 16 21 ASP N 5.020 0.085 17 22 THR N 7.559 0.329 18 23 ILE N 8.347 0.152 19 26 VAL N 4.581 0.409 20 27 LYS N 4.373 0.359 21 32 ASP N 2.573 0.284 22 33 LYS N 2.657 0.091 23 34 GLU N 3.542 0.090 24 35 GLY N 4.013 0.067 25 36 ILE N 4.357 0.068 26 39 ASP N 3.791 0.079 27 40 GLN N 7.184 0.175 28 41 GLN N 8.210 0.189 29 42 ARG N 3.112 0.058 30 44 ILE N 3.514 0.179 31 45 PHE N 2.391 0.122 32 46 ALA N 2.181 0.078 33 47 GLY N 2.724 0.101 34 48 LYS N 2.949 0.081 35 49 GLN N 4.214 0.198 36 50 LEU N 3.554 0.206 37 51 GLU N 8.718 0.327 38 52 ASP N 12.887 0.458 39 53 GLY N 6.725 0.472 40 54 ARG N 9.381 0.319 41 55 THR N 6.761 0.459 42 56 LEU N 2.122 0.084 43 57 SER N 6.481 0.315 44 58 ASP N 3.870 0.402 45 59 TYR N 3.223 0.183 46 60 ASN N 3.322 0.101 47 61 ILE N 3.028 0.065 48 62 GLN N 5.559 0.209 49 63 LYS N 9.718 0.203 50 64 GLU N 4.013 0.067 51 65 SER N 3.262 0.084 52 66 THR N 2.597 0.157 53 67 LEU N 5.168 0.379 54 68 HIS N 2.973 0.169 55 69 LEU N 2.554 0.042 56 70 VAL N 4.805 0.214 57 71 LEU N 16.026 0.663 stop_ save_ save_Ubiquitin_R1rho_3kHz_a _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 7.485 0.160 2 3 ILE N 4.058 0.147 3 4 PHE N 2.060 0.061 4 5 VAL N 2.493 0.053 5 6 LYS N 2.642 0.165 6 7 THR N 8.425 0.336 7 10 GLY N 14.306 1.326 8 11 LYS N 19.194 1.061 9 12 THR N 4.724 0.133 10 14 THR N 7.599 0.337 11 15 LEU N 3.100 0.058 12 16 GLU N 2.723 0.096 13 17 VAL N 6.766 0.144 14 18 GLU N 2.469 0.145 15 20 SER N 10.070 0.264 16 21 ASP N 4.953 0.270 17 22 THR N 7.457 0.559 18 23 ILE N 7.722 0.290 19 26 VAL N 4.286 0.156 20 27 LYS N 4.068 0.151 21 32 ASP N 2.195 0.218 22 33 LYS N 2.443 0.151 23 34 GLU N 3.499 0.181 24 35 GLY N 3.750 0.118 25 36 ILE N 4.272 0.101 26 39 ASP N 3.726 0.172 27 40 GLN N 7.072 0.356 28 41 GLN N 7.429 0.312 29 42 ARG N 2.783 0.195 30 44 ILE N 2.834 0.064 31 45 PHE N 2.098 0.046 32 46 ALA N 1.897 0.190 33 47 GLY N 2.419 0.211 34 48 LYS N 2.632 0.112 35 49 GLN N 3.931 0.065 36 50 LEU N 3.427 0.160 37 51 GLU N 8.503 0.171 38 52 ASP N 12.658 0.361 39 53 GLY N 6.489 0.262 40 54 ARG N 9.174 0.287 41 55 THR N 6.631 0.465 42 56 LEU N 2.016 0.266 43 57 SER N 5.970 0.601 44 58 ASP N 3.701 0.173 45 59 TYR N 3.153 0.086 46 60 ASN N 3.197 0.307 47 61 ILE N 2.711 0.170 48 62 GLN N 5.128 0.086 49 63 LYS N 9.200 0.218 50 64 GLU N 3.750 0.118 51 65 SER N 3.222 0.115 52 66 THR N 2.498 0.064 53 67 LEU N 3.634 0.155 54 68 HIS N 2.744 0.315 55 69 LEU N 2.489 0.087 56 70 VAL N 3.582 0.065 57 71 LEU N 14.265 0.513 stop_ save_ save_Ubiquitin_R1rho_3.5kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 9.699 0.425 2 3 ILE N 3.989 0.092 3 4 PHE N 2.153 0.112 4 5 VAL N 2.627 0.106 5 6 LYS N 2.759 0.056 6 7 THR N 8.913 0.253 7 10 GLY N 16.393 0.887 8 11 LYS N 20.450 1.096 9 12 THR N 4.677 0.176 10 14 THR N 7.698 0.264 11 15 LEU N 3.652 0.189 12 16 GLU N 3.292 0.108 13 17 VAL N 6.519 0.271 14 18 GLU N 2.535 0.158 15 20 SER N 9.814 0.204 16 21 ASP N 4.796 0.168 17 22 THR N 7.342 0.582 18 23 ILE N 7.386 0.140 19 26 VAL N 4.529 0.283 20 27 LYS N 3.970 0.327 21 32 ASP N 2.291 0.268 22 33 LYS N 2.652 0.102 23 34 GLU N 3.421 0.087 24 35 GLY N 3.849 0.124 25 36 ILE N 4.117 0.092 26 39 ASP N 3.719 0.160 27 40 GLN N 6.725 0.186 28 41 GLN N 8.170 0.284 29 42 ARG N 3.101 0.092 30 44 ILE N 3.467 0.172 31 45 PHE N 2.398 0.104 32 46 ALA N 2.019 0.165 33 47 GLY N 2.591 0.193 34 48 LYS N 2.692 0.046 35 49 GLN N 4.329 0.110 36 50 LEU N 3.805 0.173 37 51 GLU N 7.943 0.290 38 52 ASP N 12.563 0.417 39 53 GLY N 5.917 0.448 40 54 ARG N 9.116 0.288 41 55 THR N 6.601 0.222 42 56 LEU N 1.921 0.191 43 57 SER N 5.900 0.312 44 58 ASP N 3.489 0.344 45 59 TYR N 2.884 0.086 46 60 ASN N 3.198 0.118 47 61 ILE N 2.868 0.158 48 62 GLN N 5.467 0.185 49 63 LYS N 9.337 0.117 50 64 GLU N 3.849 0.124 51 65 SER N 3.176 0.076 52 66 THR N 2.689 0.154 53 67 LEU N 4.880 0.301 54 68 HIS N 2.761 0.338 55 69 LEU N 2.601 0.053 56 70 VAL N 4.921 0.235 57 71 LEU N 15.244 0.349 stop_ save_ save_Ubiquitin_R1rho_3.5kHz_a _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 7.102 0.106 2 3 ILE N 3.897 0.125 3 4 PHE N 2.103 0.077 4 5 VAL N 2.340 0.052 5 6 LYS N 2.733 0.104 6 7 THR N 8.795 0.312 7 10 GLY N 15.480 1.232 8 11 LYS N 18.116 1.300 9 12 THR N 4.533 0.105 10 14 THR N 7.326 0.210 11 15 LEU N 2.936 0.101 12 16 GLU N 3.114 0.106 13 17 VAL N 6.337 0.136 14 18 GLU N 2.531 0.077 15 20 SER N 9.191 0.273 16 21 ASP N 4.751 0.134 17 22 THR N 6.940 0.235 18 23 ILE N 6.878 0.197 19 26 VAL N 3.965 0.132 20 27 LYS N 3.890 0.151 21 32 ASP N 2.018 0.122 22 33 LYS N 2.521 0.172 23 34 GLU N 3.014 0.215 24 35 GLY N 3.740 0.061 25 36 ILE N 4.049 0.159 26 39 ASP N 3.685 0.078 27 40 GLN N 6.502 0.373 28 41 GLN N 7.994 0.194 29 42 ARG N 3.032 0.157 30 44 ILE N 2.774 0.080 31 45 PHE N 2.083 0.058 32 46 ALA N 2.012 0.079 33 47 GLY N 2.565 0.098 34 48 LYS N 2.668 0.095 35 49 GLN N 3.823 0.089 36 50 LEU N 3.361 0.113 37 51 GLU N 7.770 0.237 38 52 ASP N 11.848 0.223 39 53 GLY N 5.907 0.227 40 54 ARG N 8.873 0.237 41 55 THR N 6.588 0.250 42 56 LEU N 1.845 0.120 43 57 SER N 5.362 0.725 44 58 ASP N 3.388 0.183 45 59 TYR N 2.734 0.160 46 60 ASN N 3.070 0.255 47 61 ILE N 2.785 0.061 48 62 GLN N 4.810 0.090 49 63 LYS N 9.158 0.229 50 64 GLU N 3.740 0.061 51 65 SER N 3.147 0.088 52 66 THR N 2.276 0.074 53 67 LEU N 3.463 0.159 54 68 HIS N 2.621 0.159 55 69 LEU N 2.567 0.099 56 70 VAL N 3.544 0.100 57 71 LEU N 14.245 0.597 stop_ save_ save_Ubiquitin_R1rho_4kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 7.669 0.229 2 3 ILE N 3.597 0.077 3 4 PHE N 2.212 0.186 4 5 VAL N 2.248 0.072 5 6 LYS N 3.164 0.081 6 7 THR N 9.009 0.192 7 10 GLY N 16.667 0.969 8 11 LYS N 18.553 1.015 9 12 THR N 4.845 0.144 10 14 THR N 7.199 0.225 11 15 LEU N 3.205 0.085 12 16 GLU N 3.032 0.070 13 17 VAL N 5.537 0.153 14 18 GLU N 2.276 0.072 15 20 SER N 9.940 0.326 16 21 ASP N 4.838 0.127 17 22 THR N 5.181 0.481 18 23 ILE N 6.258 0.178 19 26 VAL N 4.407 0.176 20 27 LYS N 3.146 0.229 21 32 ASP N 1.625 0.244 22 33 LYS N 2.338 0.105 23 34 GLU N 4.189 0.143 24 35 GLY N 3.305 0.140 25 36 ILE N 4.067 0.096 26 39 ASP N 3.918 0.120 27 40 GLN N 6.353 0.324 28 41 GLN N 7.981 0.228 29 42 ARG N 2.561 0.110 30 44 ILE N 2.778 0.078 31 45 PHE N 2.223 0.066 32 46 ALA N 2.832 0.159 33 47 GLY N 2.347 0.158 34 48 LYS N 2.652 0.087 35 49 GLN N 3.845 0.118 36 50 LEU N 2.970 0.066 37 51 GLU N 7.479 0.205 38 52 ASP N 11.534 0.293 39 53 GLY N 5.368 0.353 40 54 ARG N 8.651 0.211 41 55 THR N 5.992 0.161 42 56 LEU N 1.463 0.145 43 57 SER N 7.530 0.804 44 58 ASP N 3.469 0.188 45 59 TYR N 2.621 0.098 46 60 ASN N 3.142 0.156 47 61 ILE N 2.940 0.105 48 62 GLN N 4.581 0.095 49 63 LYS N 8.688 0.190 50 64 GLU N 3.305 0.140 51 65 SER N 3.239 0.101 52 66 THR N 2.079 0.089 53 67 LEU N 3.436 0.207 54 68 HIS N 0.894 0.345 55 69 LEU N 2.387 0.084 56 70 VAL N 3.080 0.113 57 71 LEU N 14.620 0.494 stop_ save_ save_Ubiquitin_R1rho_4.5kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 6.583 0.179 2 3 ILE N 3.873 0.120 3 4 PHE N 1.990 0.058 4 5 VAL N 2.359 0.053 5 6 LYS N 2.786 0.089 6 7 THR N 8.518 0.253 7 10 GLY N 15.601 0.964 8 11 LYS N 19.268 1.129 9 12 THR N 4.333 0.092 10 14 THR N 7.315 0.221 11 15 LEU N 2.997 0.092 12 16 GLU N 3.086 0.064 13 17 VAL N 5.546 0.161 14 18 GLU N 2.211 0.077 15 20 SER N 9.149 0.214 16 21 ASP N 4.550 0.096 17 22 THR N 6.502 0.296 18 23 ILE N 5.848 0.138 19 26 VAL N 3.794 0.159 20 27 LYS N 3.681 0.168 21 32 ASP N 1.946 0.178 22 33 LYS N 2.464 0.090 23 34 GLU N 3.287 0.107 24 35 GLY N 3.556 0.073 25 36 ILE N 3.821 0.084 26 39 ASP N 3.442 0.089 27 40 GLN N 6.761 0.174 28 41 GLN N 7.342 0.157 29 42 ARG N 2.931 0.071 30 44 ILE N 2.756 0.067 31 45 PHE N 2.041 0.052 32 46 ALA N 2.137 0.066 33 47 GLY N 2.672 0.090 34 48 LYS N 2.610 0.073 35 49 GLN N 3.698 0.091 36 50 LEU N 3.550 0.079 37 51 GLU N 6.506 0.143 38 52 ASP N 12.195 0.305 39 53 GLY N 5.811 0.238 40 54 ARG N 7.981 0.185 41 55 THR N 5.945 0.093 42 56 LEU N 1.837 0.138 43 57 SER N 5.063 0.284 44 58 ASP N 3.211 0.308 45 59 TYR N 2.782 0.085 46 60 ASN N 2.916 0.170 47 61 ILE N 2.775 0.073 48 62 GLN N 4.513 0.094 49 63 LYS N 8.718 0.146 50 64 GLU N 3.556 0.073 51 65 SER N 2.899 0.081 52 66 THR N 2.035 0.103 53 67 LEU N 3.479 0.158 54 68 HIS N 2.658 0.124 55 69 LEU N 2.541 0.064 56 70 VAL N 3.550 0.100 57 71 LEU N 13.966 0.259 stop_ save_ save_Ubiquitin_R1rho_5kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 6.566 0.207 2 3 ILE N 3.592 0.135 3 4 PHE N 2.019 0.100 4 5 VAL N 2.474 0.054 5 6 LYS N 2.804 0.153 6 7 THR N 8.547 0.226 7 10 GLY N 14.948 1.046 8 11 LYS N 18.282 0.993 9 12 THR N 4.316 0.126 10 14 THR N 7.013 0.145 11 15 LEU N 2.904 0.074 12 16 GLU N 2.957 0.093 13 17 VAL N 5.144 0.114 14 18 GLU N 2.021 0.100 15 20 SER N 9.058 0.248 16 21 ASP N 4.427 0.120 17 22 THR N 6.549 0.312 18 23 ILE N 5.525 0.143 19 26 VAL N 3.706 0.181 20 27 LYS N 3.766 0.202 21 32 ASP N 2.197 0.143 22 33 LYS N 2.366 0.103 23 34 GLU N 3.204 0.129 24 35 GLY N 3.588 0.068 25 36 ILE N 3.837 0.059 26 39 ASP N 3.470 0.101 27 40 GLN N 6.406 0.217 28 41 GLN N 7.138 0.143 29 42 ARG N 2.899 0.080 30 44 ILE N 2.830 0.093 31 45 PHE N 1.952 0.053 32 46 ALA N 2.160 0.075 33 47 GLY N 2.490 0.095 34 48 LYS N 2.604 0.065 35 49 GLN N 3.664 0.076 36 50 LEU N 3.054 0.069 37 51 GLU N 6.161 0.174 38 52 ASP N 12.019 0.303 39 53 GLY N 5.624 0.289 40 54 ARG N 7.831 0.186 41 55 THR N 5.900 0.132 42 56 LEU N 1.575 0.137 43 57 SER N 5.053 0.351 44 58 ASP N 2.556 0.217 45 59 TYR N 2.583 0.095 46 60 ASN N 2.773 0.163 47 61 ILE N 2.665 0.091 48 62 GLN N 4.371 0.083 49 63 LYS N 8.696 0.119 50 64 GLU N 3.588 0.068 51 65 SER N 2.787 0.071 52 66 THR N 1.920 0.078 53 67 LEU N 3.455 0.203 54 68 HIS N 2.452 0.153 55 69 LEU N 2.402 0.057 56 70 VAL N 3.537 0.080 57 71 LEU N 14.749 0.481 stop_ save_ save_Ubiquitin_R1rho_5.5kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 6.127 0.118 2 3 ILE N 3.627 0.104 3 4 PHE N 1.896 0.091 4 5 VAL N 2.301 0.058 5 6 LYS N 2.734 0.101 6 7 THR N 8.396 0.238 7 10 GLY N 14.837 1.063 8 11 LYS N 18.797 1.261 9 12 THR N 3.986 0.105 10 14 THR N 6.954 0.195 11 15 LEU N 2.917 0.110 12 16 GLU N 2.612 0.114 13 17 VAL N 4.907 0.088 14 18 GLU N 1.955 0.076 15 20 SER N 9.166 0.181 16 21 ASP N 4.344 0.105 17 22 THR N 6.266 0.236 18 23 ILE N 4.997 0.137 19 26 VAL N 3.701 0.188 20 27 LYS N 3.401 0.189 21 32 ASP N 2.158 0.214 22 33 LYS N 2.302 0.084 23 34 GLU N 3.040 0.100 24 35 GLY N 3.412 0.066 25 36 ILE N 3.748 0.074 26 39 ASP N 3.297 0.097 27 40 GLN N 6.227 0.168 28 41 GLN N 7.013 0.170 29 42 ARG N 2.783 0.092 30 44 ILE N 2.789 0.081 31 45 PHE N 1.950 0.049 32 46 ALA N 2.106 0.084 33 47 GLY N 2.559 0.093 34 48 LYS N 2.547 0.065 35 49 GLN N 3.529 0.089 36 50 LEU N 3.077 0.067 37 51 GLU N 6.064 0.163 38 52 ASP N 11.891 0.233 39 53 GLY N 5.504 0.277 40 54 ARG N 7.776 0.189 41 55 THR N 5.784 0.142 42 56 LEU N 1.364 0.123 43 57 SER N 4.693 0.285 44 58 ASP N 2.512 0.187 45 59 TYR N 2.479 0.097 46 60 ASN N 2.531 0.154 47 61 ILE N 2.577 0.072 48 62 GLN N 4.348 0.080 49 63 LYS N 8.361 0.123 50 64 GLU N 3.412 0.066 51 65 SER N 2.796 0.070 52 66 THR N 1.942 0.076 53 67 LEU N 3.339 0.143 54 68 HIS N 2.573 0.150 55 69 LEU N 2.302 0.052 56 70 VAL N 3.476 0.112 57 71 LEU N 14.684 0.371 stop_ save_ save_Ubiquitin_R1rho_6kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 5.974 0.162 2 3 ILE N 3.549 0.111 3 4 PHE N 1.877 0.068 4 5 VAL N 2.247 0.053 5 6 LYS N 2.633 0.095 6 7 THR N 8.361 0.238 7 10 GLY N 14.837 0.729 8 11 LYS N 18.692 0.856 9 12 THR N 3.845 0.128 10 14 THR N 6.831 0.190 11 15 LEU N 2.779 0.072 12 16 GLU N 2.711 0.118 13 17 VAL N 4.568 0.085 14 18 GLU N 1.947 0.081 15 20 SER N 8.905 0.195 16 21 ASP N 4.214 0.095 17 22 THR N 5.967 0.231 18 23 ILE N 4.919 0.177 19 26 VAL N 3.630 0.156 20 27 LYS N 3.320 0.184 21 32 ASP N 2.145 0.273 22 33 LYS N 2.260 0.089 23 34 GLU N 3.138 0.099 24 35 GLY N 3.385 0.069 25 36 ILE N 3.762 0.085 26 39 ASP N 3.212 0.089 27 40 GLN N 6.250 0.180 28 41 GLN N 6.969 0.152 29 42 ARG N 2.774 0.126 30 44 ILE N 2.786 0.057 31 45 PHE N 1.801 0.042 32 46 ALA N 2.085 0.081 33 47 GLY N 2.577 0.090 34 48 LYS N 2.670 0.071 35 49 GLN N 3.532 0.090 36 50 LEU N 3.063 0.074 37 51 GLU N 5.865 0.159 38 52 ASP N 12.151 0.294 39 53 GLY N 5.643 0.248 40 54 ARG N 7.651 0.232 41 55 THR N 5.692 0.098 42 56 LEU N 1.445 0.132 43 57 SER N 4.803 0.295 44 58 ASP N 2.482 0.181 45 59 TYR N 2.591 0.088 46 60 ASN N 2.591 0.157 47 61 ILE N 2.508 0.071 48 62 GLN N 4.216 0.074 49 63 LYS N 8.299 0.146 50 64 GLU N 3.385 0.069 51 65 SER N 2.652 0.085 52 66 THR N 1.943 0.067 53 67 LEU N 3.365 0.175 54 68 HIS N 2.567 0.157 55 69 LEU N 2.309 0.054 56 70 VAL N 3.487 0.091 57 71 LEU N 13.333 0.384 stop_ save_ save_Ubiquitin_R1rho_8kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 5.627 0.146 2 3 ILE N 3.305 0.096 3 4 PHE N 1.820 0.092 4 5 VAL N 2.170 0.053 5 6 LYS N 2.550 0.078 6 7 THR N 7.987 0.260 7 10 GLY N 14.368 0.896 8 11 LYS N 17.762 0.827 9 12 THR N 3.573 0.115 10 14 THR N 6.515 0.228 11 15 LEU N 2.729 0.058 12 16 GLU N 2.544 0.074 13 17 VAL N 3.970 0.112 14 18 GLU N 1.817 0.105 15 20 SER N 8.368 0.151 16 21 ASP N 3.914 0.092 17 22 THR N 5.714 0.230 18 23 ILE N 4.371 0.166 19 26 VAL N 3.520 0.159 20 27 LYS N 3.214 0.169 21 32 ASP N 2.019 0.196 22 33 LYS N 2.289 0.112 23 34 GLU N 3.100 0.110 24 35 GLY N 3.160 0.064 25 36 ILE N 3.764 0.072 26 39 ASP N 3.219 0.074 27 40 GLN N 5.921 0.188 28 41 GLN N 6.983 0.233 29 42 ARG N 2.735 0.158 30 44 ILE N 2.641 0.074 31 45 PHE N 1.766 0.057 32 46 ALA N 1.874 0.095 33 47 GLY N 2.545 0.095 34 48 LYS N 2.454 0.088 35 49 GLN N 3.446 0.079 36 50 LEU N 2.835 0.060 37 51 GLU N 5.543 0.152 38 52 ASP N 12.210 0.247 39 53 GLY N 5.516 0.260 40 54 ARG N 7.746 0.169 41 55 THR N 5.464 0.107 42 56 LEU N 1.422 0.128 43 57 SER N 4.730 0.327 44 58 ASP N 2.286 0.212 45 59 TYR N 2.511 0.110 46 60 ASN N 2.470 0.153 47 61 ILE N 2.435 0.076 48 62 GLN N 4.037 0.067 49 63 LYS N 7.987 0.107 50 64 GLU N 3.160 0.064 51 65 SER N 2.682 0.082 52 66 THR N 1.741 0.099 53 67 LEU N 3.348 0.190 54 68 HIS N 2.546 0.166 55 69 LEU N 2.207 0.047 56 70 VAL N 3.473 0.097 57 71 LEU N 13.227 0.416 stop_ save_ save_Ubiquitin_R1rho_10kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 5.896 0.211 2 3 ILE N 3.212 0.102 3 4 PHE N 1.770 0.093 4 5 VAL N 2.449 0.071 5 6 LYS N 2.451 0.111 6 7 THR N 7.628 0.221 7 10 GLY N 14.204 0.876 8 11 LYS N 17.212 0.883 9 12 THR N 3.490 0.083 10 14 THR N 6.262 0.156 11 15 LEU N 2.679 0.066 12 16 GLU N 2.476 0.084 13 17 VAL N 3.979 0.086 14 18 GLU N 1.688 0.096 15 20 SER N 8.319 0.185 16 21 ASP N 3.865 0.111 17 22 THR N 5.685 0.249 18 23 ILE N 4.188 0.106 19 26 VAL N 3.289 0.172 20 27 LYS N 3.185 0.170 21 32 ASP N 2.438 0.173 22 33 LYS N 2.361 0.096 23 34 GLU N 2.949 0.105 24 35 GLY N 3.164 0.065 25 36 ILE N 3.667 0.088 26 39 ASP N 2.986 0.079 27 40 GLN N 6.120 0.204 28 41 GLN N 6.770 0.136 29 42 ARG N 2.716 0.121 30 44 ILE N 2.588 0.080 31 45 PHE N 1.830 0.047 32 46 ALA N 1.872 0.084 33 47 GLY N 2.422 0.084 34 48 LYS N 2.399 0.083 35 49 GLN N 3.436 0.076 36 50 LEU N 2.850 0.064 37 51 GLU N 5.498 0.144 38 52 ASP N 12.165 0.303 39 53 GLY N 5.219 0.264 40 54 ARG N 7.868 0.200 41 55 THR N 5.417 0.112 42 56 LEU N 1.282 0.141 43 57 SER N 4.399 0.296 44 58 ASP N 2.047 0.212 45 59 TYR N 2.519 0.088 46 60 ASN N 2.139 0.166 47 61 ILE N 2.493 0.089 48 62 GLN N 4.016 0.070 49 63 LYS N 7.855 0.114 50 64 GLU N 3.164 0.065 51 65 SER N 2.671 0.076 52 66 THR N 1.719 0.091 53 67 LEU N 3.250 0.160 54 68 HIS N 2.675 0.162 55 69 LEU N 2.229 0.065 56 70 VAL N 3.226 0.066 57 71 LEU N 11.737 0.371 stop_ save_ save_Ubiquitin_R1rho_12kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 5.862 0.185 2 3 ILE N 3.205 0.106 3 4 PHE N 1.692 0.091 4 5 VAL N 2.304 0.073 5 6 LYS N 2.438 0.098 6 7 THR N 7.704 0.218 7 10 GLY N 14.706 0.792 8 11 LYS N 17.241 1.037 9 12 THR N 3.343 0.094 10 14 THR N 6.341 0.187 11 15 LEU N 2.800 0.082 12 16 GLU N 2.509 0.086 13 17 VAL N 4.087 0.120 14 18 GLU N 1.718 0.106 15 20 SER N 7.943 0.177 16 21 ASP N 3.896 0.125 17 22 THR N 5.540 0.236 18 23 ILE N 3.973 0.120 19 26 VAL N 3.674 0.201 20 27 LYS N 3.191 0.220 21 32 ASP N 2.057 0.137 22 33 LYS N 2.205 0.115 23 34 GLU N 2.860 0.105 24 35 GLY N 3.164 0.085 25 36 ILE N 3.514 0.084 26 39 ASP N 3.097 0.088 27 40 GLN N 5.800 0.224 28 41 GLN N 6.557 0.129 29 42 ARG N 2.695 0.097 30 44 ILE N 2.729 0.094 31 45 PHE N 2.007 0.055 32 46 ALA N 1.858 0.110 33 47 GLY N 2.494 0.100 34 48 LYS N 2.388 0.089 35 49 GLN N 3.382 0.101 36 50 LEU N 2.886 0.064 37 51 GLU N 5.453 0.119 38 52 ASP N 12.626 0.268 39 53 GLY N 5.643 0.307 40 54 ARG N 8.375 0.182 41 55 THR N 5.488 0.145 42 56 LEU N 1.533 0.141 43 57 SER N 4.552 0.317 44 58 ASP N 2.332 0.244 45 59 TYR N 2.425 0.109 46 60 ASN N 2.363 0.166 47 61 ILE N 2.438 0.094 48 62 GLN N 4.114 0.073 49 63 LYS N 7.680 0.141 50 64 GLU N 3.164 0.085 51 65 SER N 2.665 0.070 52 66 THR N 1.650 0.086 53 67 LEU N 3.360 0.174 54 68 HIS N 2.630 0.158 55 69 LEU N 2.281 0.062 56 70 VAL N 3.392 0.124 57 71 LEU N 11.737 0.364 stop_ save_ save_Ubiquitin_R1rho_15kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 5.708 0.292 2 3 ILE N 3.150 0.080 3 4 PHE N 1.502 0.076 4 5 VAL N 2.112 0.096 5 6 LYS N 2.143 0.079 6 7 THR N 6.812 0.213 7 10 GLY N 13.889 0.959 8 11 LYS N 16.639 0.725 9 12 THR N 3.470 0.098 10 14 THR N 6.053 0.137 11 15 LEU N 2.551 0.099 12 16 GLU N 1.780 0.184 13 17 VAL N 3.453 0.089 14 18 GLU N 1.631 0.114 15 20 SER N 7.508 0.227 16 21 ASP N 3.614 0.098 17 22 THR N 5.417 0.196 18 23 ILE N 3.957 0.155 19 26 VAL N 3.628 0.196 20 27 LYS N 2.979 0.208 21 32 ASP N 1.803 0.148 22 33 LYS N 2.039 0.087 23 34 GLU N 2.928 0.095 24 35 GLY N 2.906 0.067 25 36 ILE N 3.368 0.072 26 39 ASP N 2.705 0.075 27 40 GLN N 5.402 0.180 28 41 GLN N 6.180 0.150 29 42 ARG N 2.743 0.097 30 44 ILE N 2.575 0.076 31 45 PHE N 1.749 0.052 32 46 ALA N 1.749 0.080 33 47 GLY N 2.533 0.089 34 48 LYS N 2.393 0.086 35 49 GLN N 3.151 0.107 36 50 LEU N 2.737 0.051 37 51 GLU N 5.195 0.137 38 52 ASP N 13.193 0.465 39 53 GLY N 5.314 0.286 40 54 ARG N 9.434 0.221 41 55 THR N 5.400 0.122 42 56 LEU N 1.287 0.131 43 57 SER N 4.095 0.318 44 58 ASP N 2.033 0.230 45 59 TYR N 2.438 0.092 46 60 ASN N 2.143 0.150 47 61 ILE N 2.283 0.084 48 62 GLN N 3.827 0.079 49 63 LYS N 6.959 0.108 50 64 GLU N 2.906 0.067 51 65 SER N 2.565 0.070 52 66 THR N 1.771 0.110 53 67 LEU N 3.215 0.194 54 68 HIS N 2.428 0.139 55 69 LEU N 2.089 0.051 56 70 VAL N 3.052 0.069 57 71 LEU N 10.870 0.625 stop_ save_ save_Ubiquitin_R1rho_20kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 7.380 0.269 2 3 ILE N 3.675 0.268 3 4 PHE N 2.602 0.206 4 5 VAL N 3.133 0.183 5 6 LYS N 2.159 0.314 6 7 THR N 8.319 0.269 7 10 GLY N 16.863 0.990 8 11 LYS N 19.194 0.814 9 12 THR N 4.373 0.180 10 14 THR N 7.102 0.183 11 15 LEU N 3.824 0.245 12 16 GLU N 2.918 0.214 13 17 VAL N 4.505 0.221 14 18 GLU N 2.097 0.290 15 20 SER N 9.124 0.275 16 21 ASP N 4.780 0.263 17 22 THR N 6.698 0.440 18 23 ILE N 5.163 0.263 19 26 VAL N 4.878 0.481 20 27 LYS N 4.274 0.413 21 32 ASP N 2.783 0.392 22 33 LYS N 2.753 0.255 23 34 GLU N 3.320 0.280 24 35 GLY N 3.621 0.175 25 36 ILE N 3.929 0.184 26 39 ASP N 3.602 0.195 27 40 GLN N 6.361 0.348 28 41 GLN N 7.087 0.324 29 42 ARG N 3.668 0.286 30 44 ILE N 3.672 0.208 31 45 PHE N 2.865 0.181 32 46 ALA N 2.202 0.206 33 47 GLY N 3.128 0.230 34 48 LYS N 3.103 0.150 35 49 GLN N 4.011 0.227 36 50 LEU N 3.885 0.161 37 51 GLU N 6.831 0.356 38 52 ASP N 17.794 0.887 39 53 GLY N 6.757 0.699 40 54 ARG N 13.986 0.536 41 55 THR N 6.887 0.220 42 56 LEU N 2.012 0.314 43 57 SER N 5.476 0.706 44 58 ASP N 3.283 0.509 45 59 TYR N 2.937 0.269 46 60 ASN N 4.013 0.402 47 61 ILE N 3.230 0.225 48 62 GLN N 5.015 0.169 49 63 LYS N 5.659 0.261 50 64 GLU N 3.621 0.175 51 65 SER N 3.300 0.331 52 66 THR N 2.222 0.297 53 67 LEU N 5.081 0.429 54 68 HIS N 2.221 0.294 55 69 LEU N 2.706 0.126 56 70 VAL N 4.533 0.285 57 71 LEU N 12.690 0.496 stop_ save_ save_Ubiquitin_R1rho_22kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 7.474 0.409 2 3 ILE N 2.971 0.264 3 4 PHE N 2.360 0.192 4 5 VAL N 2.919 0.220 5 6 LYS N 1.797 0.437 6 7 THR N 7.541 0.246 7 10 GLY N 16.584 1.026 8 11 LYS N 18.657 0.922 9 12 THR N 4.452 0.259 10 14 THR N 6.930 0.207 11 15 LEU N 3.401 0.190 12 16 GLU N 3.283 0.189 13 17 VAL N 4.335 0.327 14 18 GLU N 1.941 0.280 15 20 SER N 8.104 0.349 16 21 ASP N 3.940 0.216 17 22 THR N 6.693 0.560 18 23 ILE N 4.861 0.286 19 26 VAL N 4.195 0.502 20 27 LYS N 3.038 0.489 21 32 ASP N 2.049 0.623 22 33 LYS N 2.380 0.352 23 34 GLU N 2.870 0.317 24 35 GLY N 3.384 0.174 25 36 ILE N 3.946 0.226 26 39 ASP N 3.189 0.207 27 40 GLN N 5.302 0.408 28 41 GLN N 7.102 0.284 29 42 ARG N 3.220 0.447 30 44 ILE N 3.170 0.283 31 45 PHE N 2.408 0.134 32 46 ALA N 1.821 0.248 33 47 GLY N 2.812 0.242 34 48 LYS N 2.970 0.235 35 49 GLN N 3.522 0.274 36 50 LEU N 3.499 0.148 37 51 GLU N 6.831 0.330 38 52 ASP N 18.315 0.711 39 53 GLY N 5.984 0.640 40 54 ARG N 15.361 0.687 41 55 THR N 6.940 0.224 42 56 LEU N 1.451 0.392 43 57 SER N 4.342 0.864 44 58 ASP N 2.768 0.593 45 59 TYR N 2.373 0.248 46 60 ASN N 3.448 0.463 47 61 ILE N 3.027 0.238 48 62 GLN N 4.792 0.230 49 63 LYS N 5.227 0.285 50 64 GLU N 3.384 0.174 51 65 SER N 2.938 0.167 52 66 THR N 1.914 0.388 53 67 LEU N 4.955 0.373 54 68 HIS N 1.779 0.406 55 69 LEU N 2.395 0.176 56 70 VAL N 4.254 0.227 57 71 LEU N 11.976 0.545 stop_ save_ save_Ubiquitin_R1rho_24kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 8.104 0.462 2 3 ILE N 2.919 0.229 3 4 PHE N 2.478 0.220 4 5 VAL N 2.825 0.133 5 6 LYS N 2.028 0.301 6 7 THR N 7.375 0.257 7 10 GLY N 16.556 0.726 8 11 LYS N 16.667 0.575 9 12 THR N 4.519 0.256 10 14 THR N 6.892 0.274 11 15 LEU N 3.280 0.203 12 16 GLU N 3.291 0.334 13 17 VAL N 4.581 0.354 14 18 GLU N 1.590 0.169 15 20 SER N 8.006 0.222 16 21 ASP N 4.141 0.244 17 22 THR N 7.042 0.491 18 23 ILE N 5.543 0.282 19 26 VAL N 4.411 0.582 20 27 LYS N 3.272 0.430 21 32 ASP N 2.631 0.627 22 33 LYS N 2.702 0.289 23 34 GLU N 2.818 0.348 24 35 GLY N 3.477 0.206 25 36 ILE N 3.820 0.161 26 39 ASP N 3.557 0.235 27 40 GLN N 5.462 0.447 28 41 GLN N 7.435 0.213 29 42 ARG N 3.413 0.350 30 44 ILE N 3.383 0.364 31 45 PHE N 2.508 0.130 32 46 ALA N 1.922 0.179 33 47 GLY N 2.900 0.261 34 48 LYS N 2.765 0.139 35 49 GLN N 3.807 0.191 36 50 LEU N 3.597 0.157 37 51 GLU N 7.174 0.391 38 52 ASP N 20.284 0.667 39 53 GLY N 6.849 0.662 40 54 ARG N 17.921 1.015 41 55 THR N 7.513 0.284 42 56 LEU N 1.740 0.322 43 57 SER N 3.535 0.752 44 58 ASP N 2.055 0.582 45 59 TYR N 2.901 0.314 46 60 ASN N 3.274 0.361 47 61 ILE N 2.805 0.204 48 62 GLN N 4.995 0.188 49 63 LYS N 5.322 0.238 50 64 GLU N 3.477 0.206 51 65 SER N 3.117 0.205 52 66 THR N 2.286 0.461 53 67 LEU N 5.359 0.435 54 68 HIS N 2.336 0.377 55 69 LEU N 2.527 0.130 56 70 VAL N 4.124 0.220 57 71 LEU N 11.186 0.415 stop_ save_ save_Ubiquitin_R1rho_26kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 8.446 0.392 2 3 ILE N 3.059 0.281 3 4 PHE N 2.573 0.238 4 5 VAL N 2.722 0.188 5 6 LYS N 2.320 0.233 6 7 THR N 6.378 0.332 7 10 GLY N 15.221 0.894 8 11 LYS N 16.779 0.507 9 12 THR N 5.198 0.331 10 14 THR N 6.671 0.219 11 15 LEU N 3.900 0.246 12 16 GLU N 3.018 0.236 13 17 VAL N 3.786 0.248 14 18 GLU N 2.241 0.355 15 20 SER N 8.110 0.243 16 21 ASP N 4.037 0.277 17 22 THR N 7.513 0.723 18 23 ILE N 5.510 0.310 19 26 VAL N 5.945 0.792 20 27 LYS N 3.630 0.524 21 32 ASP N 2.745 0.461 22 33 LYS N 2.485 0.277 23 34 GLU N 2.939 0.284 24 35 GLY N 3.400 0.252 25 36 ILE N 3.601 0.244 26 39 ASP N 3.607 0.328 27 40 GLN N 5.441 0.499 28 41 GLN N 6.940 0.346 29 42 ARG N 2.614 0.323 30 44 ILE N 3.432 0.262 31 45 PHE N 2.182 0.162 32 46 ALA N 2.311 0.258 33 47 GLY N 3.587 0.290 34 48 LYS N 2.771 0.177 35 49 GLN N 3.536 0.175 36 50 LEU N 3.730 0.181 37 51 GLU N 7.210 0.284 38 52 ASP N 22.883 0.869 39 53 GLY N 7.468 0.705 40 54 ARG N 21.367 1.109 41 55 THR N 8.503 0.266 42 56 LEU N 2.713 0.352 43 57 SER N 4.124 0.874 44 58 ASP N 2.729 0.671 45 59 TYR N 2.955 0.303 46 60 ASN N 3.452 0.575 47 61 ILE N 3.008 0.310 48 62 GLN N 5.467 0.199 49 63 LYS N 7.530 0.200 50 64 GLU N 3.400 0.252 51 65 SER N 3.069 0.153 52 66 THR N 2.353 0.530 53 67 LEU N 5.485 0.422 54 68 HIS N 2.763 0.359 55 69 LEU N 2.348 0.199 56 70 VAL N 4.433 0.318 57 71 LEU N 12.048 0.478 stop_ save_ save_Ubiquitin_R1rho_28kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 9.542 0.629 2 3 ILE N 3.519 0.305 3 4 PHE N 3.162 0.260 4 5 VAL N 2.334 0.279 5 6 LYS N 2.782 0.426 6 7 THR N 7.424 0.376 7 10 GLY N 13.587 1.080 8 11 LYS N 15.267 1.040 9 12 THR N 6.752 0.404 10 14 THR N 7.435 0.333 11 15 LEU N 4.946 0.390 12 16 GLU N 3.575 0.237 13 17 VAL N 7.728 0.649 14 18 GLU N 2.949 0.415 15 20 SER N 8.299 0.521 16 21 ASP N 4.396 0.326 17 22 THR N 13.227 1.377 18 23 ILE N 7.429 0.289 19 26 VAL N 6.313 0.896 20 27 LYS N 3.170 0.632 21 32 ASP N 6.575 1.102 22 33 LYS N 3.064 0.492 23 34 GLU N 4.645 0.737 24 35 GLY N 4.664 0.337 25 36 ILE N 4.415 0.499 26 39 ASP N 4.367 0.313 27 40 GLN N 5.305 0.628 28 41 GLN N 5.770 0.560 29 42 ARG N 2.465 0.384 30 44 ILE N 4.090 0.283 31 45 PHE N 3.436 0.371 32 46 ALA N 4.888 0.617 33 47 GLY N 3.347 0.401 34 48 LYS N 3.560 0.514 35 49 GLN N 4.161 0.512 36 50 LEU N 3.444 0.308 37 51 GLU N 9.124 0.499 38 52 ASP N 27.624 1.702 39 53 GLY N 9.050 0.975 40 54 ARG N 22.676 1.388 41 55 THR N 9.662 0.414 42 56 LEU N 2.236 0.542 43 57 SER N 3.635 1.189 44 58 ASP N 3.228 1.136 45 59 TYR N 4.838 0.582 46 60 ASN N 3.216 0.613 47 61 ILE N 3.455 0.315 48 62 GLN N 6.039 0.256 49 63 LYS N 6.039 0.442 50 64 GLU N 4.664 0.337 51 65 SER N 4.390 0.481 52 66 THR N 3.197 0.396 53 67 LEU N 5.522 0.601 54 68 HIS N 1.962 0.519 55 69 LEU N 2.750 0.234 56 70 VAL N 4.114 0.242 57 71 LEU N 11.062 0.477 stop_ save_ save_Ubiquitin_R1rho_30kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 11.050 0.449 2 3 ILE N 3.293 0.294 3 4 PHE N 3.785 0.423 4 5 VAL N 2.259 0.435 5 6 LYS N 3.338 0.310 6 7 THR N 181.818 2041950000.000 7 10 GLY N 12.987 1.052 8 11 LYS N 16.556 1.170 9 12 THR N 7.097 0.448 10 14 THR N 6.807 0.360 11 15 LEU N 4.102 0.255 12 16 GLU N 3.652 0.246 13 17 VAL N 5.112 0.264 14 18 GLU N 2.430 0.289 15 20 SER N 7.899 0.329 16 21 ASP N 4.550 0.350 17 22 THR N 10.941 0.819 18 23 ILE N 8.658 0.495 19 26 VAL N 6.329 0.822 20 27 LYS N 5.485 0.538 21 32 ASP N 4.225 0.705 22 33 LYS N 2.901 0.391 23 34 GLU N 4.124 0.430 24 35 GLY N 3.965 0.361 25 36 ILE N 3.488 0.168 26 39 ASP N 4.423 0.347 27 40 GLN N 5.501 0.538 28 41 GLN N 7.148 0.451 29 42 ARG N 2.186 0.593 30 44 ILE N 3.965 0.365 31 45 PHE N 2.769 0.226 32 46 ALA N 3.366 0.313 33 47 GLY N 3.922 0.514 34 48 LYS N 3.118 0.342 35 49 GLN N 3.808 0.307 36 50 LEU N 4.144 0.212 37 51 GLU N 9.940 0.486 38 52 ASP N 34.483 1.593 39 53 GLY N 9.980 1.463 40 54 ARG N 28.490 2.216 41 55 THR N 9.814 0.394 42 56 LEU N 2.586 0.663 43 57 SER N 5.299 1.868 44 58 ASP N 3.854 0.927 45 59 TYR N 4.308 0.447 46 60 ASN N 4.029 0.702 47 61 ILE N 3.433 0.381 48 62 GLN N 6.460 0.261 49 63 LYS N 6.127 0.519 50 64 GLU N 3.965 0.361 51 65 SER N 3.549 0.312 52 66 THR N 4.776 0.638 53 67 LEU N 6.711 0.648 54 68 HIS N 4.068 0.794 55 69 LEU N 2.826 0.250 56 70 VAL N 5.094 0.318 57 71 LEU N 9.970 0.368 stop_ save_ save_Ubiquitin_R1rho_31kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 12.225 0.692 2 3 ILE N 3.560 0.383 3 4 PHE N 3.837 0.554 4 5 VAL N 2.758 0.348 5 6 LYS N 4.143 0.319 6 7 THR N 6.614 0.436 7 10 GLY N 13.774 1.080 8 11 LYS N 16.978 0.888 9 12 THR N 8.071 0.473 10 14 THR N 7.812 0.331 11 15 LEU N 4.878 0.428 12 16 GLU N 3.871 0.358 13 17 VAL N 5.333 0.547 14 18 GLU N 3.167 0.487 15 20 SER N 9.328 0.479 16 21 ASP N 4.367 0.522 17 22 THR N 11.990 1.048 18 23 ILE N 10.060 0.481 19 26 VAL N 6.623 1.009 20 27 LYS N 4.158 1.059 21 32 ASP N 4.062 1.168 22 33 LYS N 2.300 0.608 23 34 GLU N 3.855 0.509 24 35 GLY N 4.666 0.366 25 36 ILE N 3.541 0.274 26 39 ASP N 4.352 0.366 27 40 GLN N 5.155 0.792 28 41 GLN N 6.192 0.469 29 42 ARG N 3.189 0.570 30 44 ILE N 4.448 0.425 31 45 PHE N 3.389 0.281 32 46 ALA N 3.882 0.448 33 47 GLY N 4.488 0.504 34 48 LYS N 3.438 0.296 35 49 GLN N 3.932 0.367 36 50 LEU N 4.701 0.198 37 51 GLU N 11.236 0.494 38 52 ASP N 33.223 1.755 39 53 GLY N 8.658 1.440 40 54 ARG N 29.412 2.292 41 55 THR N 11.261 0.602 42 56 LEU N 2.967 0.762 43 57 SER N 4.202 1.700 44 58 ASP N 3.631 1.262 45 59 TYR N 3.788 0.380 46 60 ASN N 3.915 0.799 47 61 ILE N 3.264 0.424 48 62 GLN N 7.326 0.346 49 63 LYS N 7.547 0.446 50 64 GLU N 4.666 0.366 51 65 SER N 3.554 0.206 52 66 THR N 5.453 0.733 53 67 LEU N 7.899 0.774 54 68 HIS N 4.995 0.984 55 69 LEU N 3.493 0.275 56 70 VAL N 5.744 0.388 57 71 LEU N 10.650 0.840 stop_ save_ save_Ubiquitin_R1rho_32kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 13.947 0.918 2 3 ILE N 3.318 0.450 3 4 PHE N 2.364 0.557 4 5 VAL N 3.066 0.417 5 6 LYS N 1.886 0.771 6 7 THR N 8.150 0.608 7 10 GLY N 14.025 1.363 8 11 LYS N 15.649 0.847 9 12 THR N 9.058 0.627 10 14 THR N 7.716 0.290 11 15 LEU N 5.299 0.505 12 16 GLU N 3.698 0.470 13 17 VAL N 6.105 0.586 14 18 GLU N 3.928 0.887 15 20 SER N 9.497 0.565 16 21 ASP N 6.588 0.768 17 22 THR N 12.788 1.282 18 23 ILE N 10.101 0.726 19 26 VAL N 7.215 2.890 20 27 LYS N 4.225 1.381 21 32 ASP N 4.202 1.341 22 33 LYS N 3.540 0.757 23 34 GLU N 3.772 0.812 24 35 GLY N 3.885 0.497 25 36 ILE N 4.437 0.444 26 39 ASP N 4.545 0.513 27 40 GLN N 5.942 0.824 28 41 GLN N 7.077 0.637 29 42 ARG N 2.118 0.655 30 44 ILE N 5.092 0.416 31 45 PHE N 3.550 0.387 32 46 ALA N 3.540 0.571 33 47 GLY N 4.757 0.937 34 48 LYS N 3.121 0.442 35 49 GLN N 5.650 0.369 36 50 LEU N 6.711 0.411 37 51 GLU N 12.255 0.961 38 52 ASP N 36.900 1.961 39 53 GLY N 9.597 1.664 40 54 ARG N 32.787 2.494 41 55 THR N 12.547 0.496 42 56 LEU N 2.070 2.097 43 57 SER N 6.207 2.572 44 58 ASP N 3.221 2.510 45 59 TYR N 4.102 0.596 46 60 ASN N 4.766 1.117 47 61 ILE N 3.771 0.891 48 62 GLN N 8.143 0.503 49 63 LYS N 8.651 0.384 50 64 GLU N 3.885 0.497 51 65 SER N 3.937 0.460 52 66 THR N 7.148 0.864 53 67 LEU N 8.850 0.967 54 68 HIS N 3.292 1.393 55 69 LEU N 3.401 0.373 56 70 VAL N 6.105 0.449 57 71 LEU N 12.376 0.809 stop_ save_ save_Ubiquitin_R1rho_32.5kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 17.065 0.804 2 3 ILE N 4.075 0.467 3 4 PHE N 6.297 0.471 4 5 VAL N 3.034 0.601 5 6 LYS N 3.807 0.884 6 7 THR N 7.220 0.908 7 10 GLY N 13.021 1.546 8 11 LYS N 14.472 1.483 9 12 THR N 10.132 0.777 10 14 THR N 8.873 0.448 11 15 LEU N 6.024 0.519 12 16 GLU N 3.630 0.455 13 17 VAL N 5.587 0.838 14 18 GLU N 4.129 0.831 15 20 SER N 9.804 0.857 16 21 ASP N 5.311 0.669 17 22 THR N 14.577 2.112 18 23 ILE N 13.158 0.871 19 26 VAL N 7.541 1.558 20 27 LYS N 2.890 1.661 21 32 ASP N 5.609 1.744 22 33 LYS N 4.225 1.050 23 34 GLU N 4.904 0.981 24 35 GLY N 4.699 0.704 25 36 ILE N 4.562 0.397 26 39 ASP N 5.988 0.586 27 40 GLN N 5.747 1.251 28 41 GLN N 6.684 0.986 29 42 ARG N 3.415 0.822 30 44 ILE N 6.031 0.682 31 45 PHE N 4.511 0.439 32 46 ALA N 3.466 0.722 33 47 GLY N 4.719 1.109 34 48 LYS N 4.085 0.711 35 49 GLN N 5.216 0.499 36 50 LEU N 5.513 0.561 37 51 GLU N 14.727 1.078 38 52 ASP N 40.323 2.309 39 53 GLY N 13.227 2.301 40 54 ARG N 35.971 3.028 41 55 THR N 12.739 0.743 42 56 LEU N 3.801 1.221 43 57 SER N 3.194 1456.780 44 58 ASP N 6.892 2.126 45 59 TYR N 4.869 1.132 46 60 ASN N 5.543 1.357 47 61 ILE N 4.496 0.653 48 62 GLN N 8.913 0.594 49 63 LYS N 8.084 0.641 50 64 GLU N 4.699 0.704 51 65 SER N 5.441 0.448 52 66 THR N 7.587 0.974 53 67 LEU N 10.320 1.161 54 68 HIS N 7.163 1.561 55 69 LEU N 3.978 0.524 56 70 VAL N 7.582 0.764 57 71 LEU N 11.682 0.882 stop_ save_ save_Ubiquitin_R1rho_33kHz _Saveframe_category T1rho_relaxation _Details . loop_ _Sample_label $sample_1 stop_ _Sample_conditions_label $sample_conditions_1 _Spectrometer_frequency_1H 600 _T1rho_coherence_type S(+,-) _T1rho_value_units ms-1 _Text_data_format . _Text_data . loop_ _T1rho_ID _Residue_seq_code _Residue_label _Atom_name _T1rho_value _T1rho_value_error 1 2 GLN N 15.649 0.808 2 3 ILE N 4.184 0.540 3 4 PHE N 5.838 0.446 4 5 VAL N 2.072 0.863 5 6 LYS N 4.902 0.700 6 7 THR N 7.289 0.565 7 10 GLY N 15.949 1.608 8 11 LYS N 17.153 1.330 9 12 THR N 10.846 0.886 10 14 THR N 9.025 0.445 11 15 LEU N 5.845 0.488 12 16 GLU N 4.778 0.465 13 17 VAL N 6.562 0.625 14 18 GLU N 3.953 0.603 15 20 SER N 10.482 0.814 16 21 ASP N 5.757 0.773 17 22 THR N 15.060 1.907 18 23 ILE N 12.165 0.990 19 26 VAL N 8.489 1.715 20 27 LYS N 3.469 1.574 21 32 ASP N 6.653 1.493 22 33 LYS N 2.462 0.711 23 34 GLU N 3.808 0.754 24 35 GLY N 4.943 0.553 25 36 ILE N 4.216 0.451 26 39 ASP N 4.137 0.726 27 40 GLN N 5.522 1.314 28 41 GLN N 8.425 0.764 29 42 ARG N 2.846 0.785 30 44 ILE N 5.568 0.531 31 45 PHE N 3.751 0.367 32 46 ALA N 4.636 0.701 33 47 GLY N 4.625 0.829 34 48 LYS N 2.844 0.402 35 49 GLN N 5.705 0.442 36 50 LEU N 4.673 0.346 37 51 GLU N 14.124 0.894 38 52 ASP N 33.223 1.777 39 53 GLY N 11.547 2.152 40 54 ARG N 34.014 2.626 41 55 THR N 13.263 0.728 42 56 LEU N 3.652 1.173 43 57 SER N 5.084 3.594 44 58 ASP N 6.676 2.176 45 59 TYR N 4.527 0.678 46 60 ASN N 5.233 1.153 47 61 ILE N 4.134 0.573 48 62 GLN N 8.795 0.475 49 63 LYS N 8.333 0.564 50 64 GLU N 4.943 0.553 51 65 SER N 5.260 0.522 52 66 THR N 6.583 0.702 53 67 LEU N 10.132 1.140 54 68 HIS N 6.807 1.626 55 69 LEU N 3.404 0.397 56 70 VAL N 6.447 0.570 57 71 LEU N 11.614 0.989 stop_ save_