data_27534


#######################
#  Entry information  #
#######################
save_entry_information
   _Entry.Sf_category                    entry_information
   _Entry.Sf_framecode                   entry_information
   _Entry.ID                             27534
   _Entry.Title
;
Solution NMR Structure of PALB2 Colied-coil Domain (PALB2cc)
;
   _Entry.Type                           macromolecule
   _Entry.Version_type                   original
   _Entry.Submission_date                2018-07-05
   _Entry.Accession_date                 2018-07-05
   _Entry.Last_release_date              2018-07-06
   _Entry.Original_release_date          2018-07-06
   _Entry.Origination                    author
   _Entry.Format_name                    .
   _Entry.NMR_STAR_version               3.2.0.16
   _Entry.Original_NMR_STAR_version      3.1
   _Entry.Experimental_method            NMR
   _Entry.Experimental_method_subtype    solution
   _Entry.Source_data_format             .
   _Entry.Source_data_format_version     .
   _Entry.Generated_software_name        .
   _Entry.Generated_software_version     .
   _Entry.Generated_software_ID          .
   _Entry.Generated_software_label       .
   _Entry.Generated_date                 .
   _Entry.DOI                            .
   _Entry.UUID                           .
   _Entry.Related_coordinate_file_name   .
   _Entry.Details                        .
   _Entry.BMRB_internal_directory_name   .

   loop_
      _Entry_author.Ordinal
      _Entry_author.Given_name
      _Entry_author.Family_name
      _Entry_author.First_initial
      _Entry_author.Middle_initials
      _Entry_author.Family_title
      _Entry_author.ORCID
      _Entry_author.Entry_ID

      1   Fei       Song         .   .    .   .   27534
      2   Minxing   Li           .   .    .   .   27534
      3   Gaohua    Liu          .   .    .   .   27534
      4   G.V.T.    Swapna       .   .    .   .   27534
      5   Bing      Xia          .   .    .   .   27534
      6   Samuel    Bunting      .   F.   .   .   27534
      7   Gaetano   Montelione   .   T.   .   .   27534
   stop_

   loop_
      _Entry_src.ID
      _Entry_src.Project_name
      _Entry_src.Organization_full_name
      _Entry_src.Organization_initials
      _Entry_src.Entry_ID

      1   .   'Department of Molecular Biology and Biochemistry, Rutgers, The State University of New Jersey, Piscataway, New Jersey'   .   27534
      2   .   'Center for Advanced Biotechnology and Medicine, Rutgers, The State University of New Jersey, Piscataway, New Jersey'     .   27534
   stop_

   loop_
      _Release.Release_number
      _Release.Format_type
      _Release.Format_version
      _Release.Date
      _Release.Submission_date
      _Release.Type
      _Release.Author
      _Release.Detail
      _Release.Entry_ID

      2   .   .   2019-01-24   2018-07-05   update     BMRB     'update entry citation'   27534
      1   .   .   2018-11-16   2018-07-05   original   author   'original release'        27534
   stop_

   loop_
      _Related_entries.Database_name
      _Related_entries.Database_accession_code
      _Related_entries.Relationship
      _Related_entries.Entry_ID

      BMRB   30493   'chemical shift assignment'   27534
   stop_
save_


###############
#  Citations  #
###############
save_entry_citation
   _Citation.Sf_category                  citations
   _Citation.Sf_framecode                 entry_citation
   _Citation.Entry_ID                     27534
   _Citation.ID                           1
   _Citation.Class                        'entry citation'
   _Citation.CAS_abstract_code            .
   _Citation.MEDLINE_UI_code              .
   _Citation.DOI                          .
   _Citation.PubMed_ID                    30289697
   _Citation.Full_citation                .
   _Citation.Title
;
Antiparallel Coiled-Coil Interactions Mediate the Homodimerization of the DNA Damage-Repair Protein PALB2
;
   _Citation.Status                       published
   _Citation.Type                         journal
   _Citation.Journal_abbrev               Biochemistry
   _Citation.Journal_name_full            .
   _Citation.Journal_volume               57
   _Citation.Journal_issue                47
   _Citation.Journal_ASTM                 .
   _Citation.Journal_ISSN                 .
   _Citation.Journal_CSD                  .
   _Citation.Book_title                   .
   _Citation.Book_chapter_title           .
   _Citation.Book_volume                  .
   _Citation.Book_series                  .
   _Citation.Book_publisher               .
   _Citation.Book_publisher_city          .
   _Citation.Book_ISBN                    .
   _Citation.Conference_title             .
   _Citation.Conference_site              .
   _Citation.Conference_state_province    .
   _Citation.Conference_country           .
   _Citation.Conference_start_date        .
   _Citation.Conference_end_date          .
   _Citation.Conference_abstract_number   .
   _Citation.Thesis_institution           .
   _Citation.Thesis_institution_city      .
   _Citation.Thesis_institution_country   .
   _Citation.WWW_URL                      .
   _Citation.Page_first                   6581
   _Citation.Page_last                    6591
   _Citation.Year                         2018
   _Citation.Details                      .

   loop_
      _Citation_author.Ordinal
      _Citation_author.Given_name
      _Citation_author.Family_name
      _Citation_author.First_initial
      _Citation_author.Middle_initials
      _Citation_author.Family_title
      _Citation_author.ORCID
      _Citation_author.Entry_ID
      _Citation_author.Citation_ID

      1   Fei       Song         .   .    .   .   27534   1
      2   Minxing   Li           .   .    .   .   27534   1
      3   Gaohua    Liu          .   .    .   .   27534   1
      4   G.V.T.    Swapna       .   .    .   .   27534   1
      5   Nourhan   Daigham      .   S.   .   .   27534   1
      6   Bing      Xia          .   .    .   .   27534   1
      7   Gaetano   Montelione   .   T.   .   .   27534   1
      8   Samuel    Bunting      .   F.   .   .   27534   1
   stop_

   loop_
      _Citation_keyword.Keyword
      _Citation_keyword.Entry_ID
      _Citation_keyword.Citation_ID

      Antiparallel                 27534   1
      'Coiled coil'                27534   1
      'Homologous recombination'   27534   1
      PALB2                        27534   1
   stop_
save_


#############################################
#  Molecular system (assembly) description  #
#############################################
save_assembly
   _Assembly.Sf_category                       assembly
   _Assembly.Sf_framecode                      assembly
   _Assembly.Entry_ID                          27534
   _Assembly.ID                                1
   _Assembly.Name                              PALB2cc
   _Assembly.BMRB_code                         .
   _Assembly.Number_of_components              2
   _Assembly.Organic_ligands                   .
   _Assembly.Metal_ions                        .
   _Assembly.Non_standard_bonds                no
   _Assembly.Ambiguous_conformational_states   .
   _Assembly.Ambiguous_chem_comp_sites         .
   _Assembly.Molecules_in_chemical_exchange    .
   _Assembly.Paramagnetic                      no
   _Assembly.Thiol_state                       .
   _Assembly.Molecular_mass                    .
   _Assembly.Enzyme_commission_number          .
   _Assembly.Details                           'The two chains of the homodimer are oriented anti-parallel to each other.'
   _Assembly.DB_query_date                     .
   _Assembly.DB_query_revised_last_date        .

   loop_
      _Entity_assembly.ID
      _Entity_assembly.Entity_assembly_name
      _Entity_assembly.Entity_ID
      _Entity_assembly.Entity_label
      _Entity_assembly.Asym_ID
      _Entity_assembly.PDB_chain_ID
      _Entity_assembly.Experimental_data_reported
      _Entity_assembly.Physical_state
      _Entity_assembly.Conformational_isomer
      _Entity_assembly.Chemical_exchange_state
      _Entity_assembly.Magnetic_equivalence_group_code
      _Entity_assembly.Role
      _Entity_assembly.Details
      _Entity_assembly.Entry_ID
      _Entity_assembly.Assembly_ID

      1   'PALB2cc, chain 1'   1   $PALB2cc   A   .   yes   native   no   no   .   .   .   27534   1
      2   'PALB2cc, chain 2'   1   $PALB2cc   B   .   yes   native   no   no   .   .   .   27534   1
   stop_
save_


    ####################################
    #  Biological polymers and ligands #
    ####################################
save_PALB2cc
   _Entity.Sf_category                       entity
   _Entity.Sf_framecode                      PALB2cc
   _Entity.Entry_ID                          27534
   _Entity.ID                                1
   _Entity.BMRB_code                         .
   _Entity.Name                              PALB2cc
   _Entity.Type                              polymer
   _Entity.Polymer_common_type               .
   _Entity.Polymer_type                      polypeptide(L)
   _Entity.Polymer_type_details              .
   _Entity.Polymer_strand_ID                 .
   _Entity.Polymer_seq_one_letter_code_can   .
   _Entity.Polymer_seq_one_letter_code
;
MEELSGKPLSYAEKEKLKEK
LAFLKKEYSRTLARLQRAKR
AEKAKNSKKAIEDGVPQPEA
LEHHHHHH
;
   _Entity.Target_identifier                 .
   _Entity.Polymer_author_defined_seq        .
   _Entity.Polymer_author_seq_details        .
   _Entity.Ambiguous_conformational_states   no
   _Entity.Ambiguous_chem_comp_sites         no
   _Entity.Nstd_monomer                      no
   _Entity.Nstd_chirality                    no
   _Entity.Nstd_linkage                      no
   _Entity.Nonpolymer_comp_ID                .
   _Entity.Nonpolymer_comp_label             .
   _Entity.Number_of_monomers                68
   _Entity.Number_of_nonpolymer_components   .
   _Entity.Paramagnetic                      no
   _Entity.Thiol_state                       'not present'
   _Entity.Src_method                        .
   _Entity.Parent_entity_ID                  .
   _Entity.Fragment                          .
   _Entity.Mutation                          .
   _Entity.EC_number                         .
   _Entity.Calc_isoelectric_point            .
   _Entity.Formula_weight                    7926.10
   _Entity.Formula_weight_exptl              .
   _Entity.Formula_weight_exptl_meth         .
   _Entity.Details                           .
   _Entity.DB_query_date                     .
   _Entity.DB_query_revised_last_date        .

   loop_
      _Entity_biological_function.Biological_function
      _Entity_biological_function.Entry_ID
      _Entity_biological_function.Entity_ID

      'DNA damage Repair protein; PALB2 = Partner and localizer of BRCA2'                             27534   1
      'coiled-coil domain interacts with BRCA1 as part of the BRCA2-PALB2-BRCA1 DNA repair complex'   27534   1
   stop_

   loop_
      _Entity_comp_index.ID
      _Entity_comp_index.Auth_seq_ID
      _Entity_comp_index.Comp_ID
      _Entity_comp_index.Comp_label
      _Entity_comp_index.Entry_ID
      _Entity_comp_index.Entity_ID

      1    .   MET   .   27534   1
      2    .   GLU   .   27534   1
      3    .   GLU   .   27534   1
      4    .   LEU   .   27534   1
      5    .   SER   .   27534   1
      6    .   GLY   .   27534   1
      7    .   LYS   .   27534   1
      8    .   PRO   .   27534   1
      9    .   LEU   .   27534   1
      10   .   SER   .   27534   1
      11   .   TYR   .   27534   1
      12   .   ALA   .   27534   1
      13   .   GLU   .   27534   1
      14   .   LYS   .   27534   1
      15   .   GLU   .   27534   1
      16   .   LYS   .   27534   1
      17   .   LEU   .   27534   1
      18   .   LYS   .   27534   1
      19   .   GLU   .   27534   1
      20   .   LYS   .   27534   1
      21   .   LEU   .   27534   1
      22   .   ALA   .   27534   1
      23   .   PHE   .   27534   1
      24   .   LEU   .   27534   1
      25   .   LYS   .   27534   1
      26   .   LYS   .   27534   1
      27   .   GLU   .   27534   1
      28   .   TYR   .   27534   1
      29   .   SER   .   27534   1
      30   .   ARG   .   27534   1
      31   .   THR   .   27534   1
      32   .   LEU   .   27534   1
      33   .   ALA   .   27534   1
      34   .   ARG   .   27534   1
      35   .   LEU   .   27534   1
      36   .   GLN   .   27534   1
      37   .   ARG   .   27534   1
      38   .   ALA   .   27534   1
      39   .   LYS   .   27534   1
      40   .   ARG   .   27534   1
      41   .   ALA   .   27534   1
      42   .   GLU   .   27534   1
      43   .   LYS   .   27534   1
      44   .   ALA   .   27534   1
      45   .   LYS   .   27534   1
      46   .   ASN   .   27534   1
      47   .   SER   .   27534   1
      48   .   LYS   .   27534   1
      49   .   LYS   .   27534   1
      50   .   ALA   .   27534   1
      51   .   ILE   .   27534   1
      52   .   GLU   .   27534   1
      53   .   ASP   .   27534   1
      54   .   GLY   .   27534   1
      55   .   VAL   .   27534   1
      56   .   PRO   .   27534   1
      57   .   GLN   .   27534   1
      58   .   PRO   .   27534   1
      59   .   GLU   .   27534   1
      60   .   ALA   .   27534   1
      61   .   LEU   .   27534   1
      62   .   GLU   .   27534   1
      63   .   HIS   .   27534   1
      64   .   HIS   .   27534   1
      65   .   HIS   .   27534   1
      66   .   HIS   .   27534   1
      67   .   HIS   .   27534   1
      68   .   HIS   .   27534   1
   stop_

   loop_
      _Entity_poly_seq.Hetero
      _Entity_poly_seq.Mon_ID
      _Entity_poly_seq.Num
      _Entity_poly_seq.Comp_index_ID
      _Entity_poly_seq.Entry_ID
      _Entity_poly_seq.Entity_ID

      .   MET   1    1    27534   1
      .   GLU   2    2    27534   1
      .   GLU   3    3    27534   1
      .   LEU   4    4    27534   1
      .   SER   5    5    27534   1
      .   GLY   6    6    27534   1
      .   LYS   7    7    27534   1
      .   PRO   8    8    27534   1
      .   LEU   9    9    27534   1
      .   SER   10   10   27534   1
      .   TYR   11   11   27534   1
      .   ALA   12   12   27534   1
      .   GLU   13   13   27534   1
      .   LYS   14   14   27534   1
      .   GLU   15   15   27534   1
      .   LYS   16   16   27534   1
      .   LEU   17   17   27534   1
      .   LYS   18   18   27534   1
      .   GLU   19   19   27534   1
      .   LYS   20   20   27534   1
      .   LEU   21   21   27534   1
      .   ALA   22   22   27534   1
      .   PHE   23   23   27534   1
      .   LEU   24   24   27534   1
      .   LYS   25   25   27534   1
      .   LYS   26   26   27534   1
      .   GLU   27   27   27534   1
      .   TYR   28   28   27534   1
      .   SER   29   29   27534   1
      .   ARG   30   30   27534   1
      .   THR   31   31   27534   1
      .   LEU   32   32   27534   1
      .   ALA   33   33   27534   1
      .   ARG   34   34   27534   1
      .   LEU   35   35   27534   1
      .   GLN   36   36   27534   1
      .   ARG   37   37   27534   1
      .   ALA   38   38   27534   1
      .   LYS   39   39   27534   1
      .   ARG   40   40   27534   1
      .   ALA   41   41   27534   1
      .   GLU   42   42   27534   1
      .   LYS   43   43   27534   1
      .   ALA   44   44   27534   1
      .   LYS   45   45   27534   1
      .   ASN   46   46   27534   1
      .   SER   47   47   27534   1
      .   LYS   48   48   27534   1
      .   LYS   49   49   27534   1
      .   ALA   50   50   27534   1
      .   ILE   51   51   27534   1
      .   GLU   52   52   27534   1
      .   ASP   53   53   27534   1
      .   GLY   54   54   27534   1
      .   VAL   55   55   27534   1
      .   PRO   56   56   27534   1
      .   GLN   57   57   27534   1
      .   PRO   58   58   27534   1
      .   GLU   59   59   27534   1
      .   ALA   60   60   27534   1
      .   LEU   61   61   27534   1
      .   GLU   62   62   27534   1
      .   HIS   63   63   27534   1
      .   HIS   64   64   27534   1
      .   HIS   65   65   27534   1
      .   HIS   66   66   27534   1
      .   HIS   67   67   27534   1
      .   HIS   68   68   27534   1
   stop_
save_


    ####################
    #  Natural source  #
    ####################
save_natural_source
   _Entity_natural_src_list.Sf_category    natural_source
   _Entity_natural_src_list.Sf_framecode   natural_source
   _Entity_natural_src_list.Entry_ID       27534
   _Entity_natural_src_list.ID             1

   loop_
      _Entity_natural_src.ID
      _Entity_natural_src.Entity_ID
      _Entity_natural_src.Entity_label
      _Entity_natural_src.Entity_chimera_segment_ID
      _Entity_natural_src.NCBI_taxonomy_ID
      _Entity_natural_src.Type
      _Entity_natural_src.Common
      _Entity_natural_src.Organism_name_scientific
      _Entity_natural_src.Organism_name_common
      _Entity_natural_src.Organism_acronym
      _Entity_natural_src.ICTVdb_decimal_code
      _Entity_natural_src.Superkingdom
      _Entity_natural_src.Kingdom
      _Entity_natural_src.Genus
      _Entity_natural_src.Species
      _Entity_natural_src.Strain
      _Entity_natural_src.Variant
      _Entity_natural_src.Organ
      _Entity_natural_src.Tissue
      _Entity_natural_src.Tissue_fraction
      _Entity_natural_src.Cell_line
      _Entity_natural_src.Cell_type
      _Entity_natural_src.ATCC_number
      _Entity_natural_src.Organelle
      _Entity_natural_src.Secretion
      _Entity_natural_src.Plasmid
      _Entity_natural_src.Gene_mnemonic
      _Entity_natural_src.Details
      _Entity_natural_src.Entry_ID
      _Entity_natural_src.Entity_natural_src_list_ID

      1   1   $PALB2cc   .   10090   organism   .   'Mus musculus'   Mouse   .   .   Eukaryota   Metazoa   Mus   musculus   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
   stop_
save_


    #########################
    #  Experimental source  #
    #########################
save_experimental_source
   _Entity_experimental_src_list.Sf_category    experimental_source
   _Entity_experimental_src_list.Sf_framecode   experimental_source
   _Entity_experimental_src_list.Entry_ID       27534
   _Entity_experimental_src_list.ID             1

   loop_
      _Entity_experimental_src.ID
      _Entity_experimental_src.Entity_ID
      _Entity_experimental_src.Entity_label
      _Entity_experimental_src.Entity_chimera_segment_ID
      _Entity_experimental_src.Production_method
      _Entity_experimental_src.Host_org_scientific_name
      _Entity_experimental_src.Host_org_name_common
      _Entity_experimental_src.Host_org_details
      _Entity_experimental_src.Host_org_NCBI_taxonomy_ID
      _Entity_experimental_src.Host_org_genus
      _Entity_experimental_src.Host_org_species
      _Entity_experimental_src.Host_org_strain
      _Entity_experimental_src.Host_org_variant
      _Entity_experimental_src.Host_org_ATCC_number
      _Entity_experimental_src.Vector_type
      _Entity_experimental_src.PDBview_host_org_vector_name
      _Entity_experimental_src.PDBview_plasmid_name
      _Entity_experimental_src.Vector_name
      _Entity_experimental_src.Vector_details
      _Entity_experimental_src.Vendor_name
      _Entity_experimental_src.Details
      _Entity_experimental_src.Entry_ID
      _Entity_experimental_src.Entity_experimental_src_list_ID

      1   1   $PALB2cc   .   'recombinant technology'   'Escherichia coli'   .   .   .   Escherichia   coli   .   .   .   .   .   .   pET21-NESG   .   .   .   27534   1
   stop_
save_


#####################################
#  Sample contents and methodology  #
#####################################
	 
    ########################
    #  Sample description  #
    ########################
save_sample_1
   _Sample.Sf_category                      sample
   _Sample.Sf_framecode                     sample_1
   _Sample.Entry_ID                         27534
   _Sample.ID                               1
   _Sample.Type                             solution
   _Sample.Sub_type                         .
   _Sample.Details                          .
   _Sample.Aggregate_sample_number          .
   _Sample.Solvent_system                   '90% H2O/10% D2O'
   _Sample.Preparation_date                 .
   _Sample.Preparation_expiration_date      .
   _Sample.Polycrystallization_protocol     .
   _Sample.Single_crystal_protocol          .
   _Sample.Crystal_grow_apparatus           .
   _Sample.Crystal_grow_atmosphere          .
   _Sample.Crystal_grow_details             .
   _Sample.Crystal_grow_method              .
   _Sample.Crystal_grow_method_cit_ID       .
   _Sample.Crystal_grow_pH                  .
   _Sample.Crystal_grow_pH_range            .
   _Sample.Crystal_grow_pressure            .
   _Sample.Crystal_grow_pressure_esd        .
   _Sample.Crystal_grow_seeding             .
   _Sample.Crystal_grow_seeding_cit_ID      .
   _Sample.Crystal_grow_temp                .
   _Sample.Crystal_grow_temp_details        .
   _Sample.Crystal_grow_temp_esd            .
   _Sample.Crystal_grow_time                .
   _Sample.Oriented_sample_prep_protocol    .
   _Sample.Lyophilization_cryo_protectant   .
   _Sample.Storage_protocol                 .

   loop_
      _Sample_component.ID
      _Sample_component.Mol_common_name
      _Sample_component.Isotopic_labeling
      _Sample_component.Assembly_ID
      _Sample_component.Assembly_label
      _Sample_component.Entity_ID
      _Sample_component.Entity_label
      _Sample_component.Product_ID
      _Sample_component.Type
      _Sample_component.Concentration_val
      _Sample_component.Concentration_val_min
      _Sample_component.Concentration_val_max
      _Sample_component.Concentration_val_units
      _Sample_component.Concentration_val_err
      _Sample_component.Vendor
      _Sample_component.Vendor_product_name
      _Sample_component.Vendor_product_code
      _Sample_component.Entry_ID
      _Sample_component.Sample_ID

      1   PALB2cc              '[U-100% 13C; U-100% 15N]'   .   .   1   $PALB2cc   .   .   1.2    .   .   mM   .   .   .   .   27534   1
      2   MES                  'natural abundance'          .   .   .   .          .   .   20     .   .   mM   .   .   .   .   27534   1
      3   'sodium chloride'    'natural abundance'          .   .   .   .          .   .   200    .   .   mM   .   .   .   .   27534   1
      4   'calcium chloride'   'natural abundance'          .   .   .   .          .   .   5      .   .   mM   .   .   .   .   27534   1
      5   DTT                  'natural abundance'          .   .   .   .          .   .   10     .   .   mM   .   .   .   .   27534   1
      6   'sodium azide'       'natural abundance'          .   .   .   .          .   .   0.02   .   .   %    .   .   .   .   27534   1
      7   H2O                  'natural abundance'          .   .   .   .          .   .   90     .   .   %    .   .   .   .   27534   1
      8   DSS                  'natural abundance'          .   .   .   .          .   .   10     .   .   %    .   .   .   .   27534   1
   stop_
save_

save_sample_2
   _Sample.Sf_category                      sample
   _Sample.Sf_framecode                     sample_2
   _Sample.Entry_ID                         27534
   _Sample.ID                               2
   _Sample.Type                             solution
   _Sample.Sub_type                         .
   _Sample.Details
;
1:2 sample of 13C,15N enriched to unlabeled (natural abundance) protein. 
This sample used to identify the dimer interface in PALB2cc using 
13C filtered NOESY experiments ( pulse sequence: noesyhsqcgpwgx13d).
;
   _Sample.Aggregate_sample_number          .
   _Sample.Solvent_system                   '90% H2O/10% D2O'
   _Sample.Preparation_date                 .
   _Sample.Preparation_expiration_date      .
   _Sample.Polycrystallization_protocol     .
   _Sample.Single_crystal_protocol          .
   _Sample.Crystal_grow_apparatus           .
   _Sample.Crystal_grow_atmosphere          .
   _Sample.Crystal_grow_details             .
   _Sample.Crystal_grow_method              .
   _Sample.Crystal_grow_method_cit_ID       .
   _Sample.Crystal_grow_pH                  .
   _Sample.Crystal_grow_pH_range            .
   _Sample.Crystal_grow_pressure            .
   _Sample.Crystal_grow_pressure_esd        .
   _Sample.Crystal_grow_seeding             .
   _Sample.Crystal_grow_seeding_cit_ID      .
   _Sample.Crystal_grow_temp                .
   _Sample.Crystal_grow_temp_details        .
   _Sample.Crystal_grow_temp_esd            .
   _Sample.Crystal_grow_time                .
   _Sample.Oriented_sample_prep_protocol    .
   _Sample.Lyophilization_cryo_protectant   .
   _Sample.Storage_protocol                 .

   loop_
      _Sample_component.ID
      _Sample_component.Mol_common_name
      _Sample_component.Isotopic_labeling
      _Sample_component.Assembly_ID
      _Sample_component.Assembly_label
      _Sample_component.Entity_ID
      _Sample_component.Entity_label
      _Sample_component.Product_ID
      _Sample_component.Type
      _Sample_component.Concentration_val
      _Sample_component.Concentration_val_min
      _Sample_component.Concentration_val_max
      _Sample_component.Concentration_val_units
      _Sample_component.Concentration_val_err
      _Sample_component.Vendor
      _Sample_component.Vendor_product_name
      _Sample_component.Vendor_product_code
      _Sample_component.Entry_ID
      _Sample_component.Sample_ID

      1   PALB2cc              '[U-100% 13C; U-100% 15N]'   .   .   1   $PALB2cc   .   .   1      .   .   X    .   .   .   .   27534   2
      2   MES                  'natural abundance'          .   .   .   .          .   .   20     .   .   mM   .   .   .   .   27534   2
      3   'sodium chloride'    'natural abundance'          .   .   .   .          .   .   200    .   .   mM   .   .   .   .   27534   2
      4   'calcium chloride'   'natural abundance'          .   .   .   .          .   .   5      .   .   mM   .   .   .   .   27534   2
      5   DTT                  'natural abundance'          .   .   .   .          .   .   10     .   .   mM   .   .   .   .   27534   2
      6   'sodium azide'       'natural abundance'          .   .   .   .          .   .   0.02   .   .   %    .   .   .   .   27534   2
      7   H2O                  'natural abundance'          .   .   .   .          .   .   90     .   .   %    .   .   .   .   27534   2
      8   DSS                  'natural abundance'          .   .   .   .          .   .   10     .   .   %    .   .   .   .   27534   2
      9   PALB2cc              'natural abundance'          .   .   .   .          .   .   2      .   .   X    .   .   .   .   27534   2
   stop_
save_


#######################
#  Sample conditions  #
#######################
save_sample_conditions_1
   _Sample_condition_list.Sf_category    sample_conditions
   _Sample_condition_list.Sf_framecode   sample_conditions_1
   _Sample_condition_list.Entry_ID       27534
   _Sample_condition_list.ID             1
   _Sample_condition_list.Details        .

   loop_
      _Sample_condition_variable.Type
      _Sample_condition_variable.Val
      _Sample_condition_variable.Val_err
      _Sample_condition_variable.Val_units
      _Sample_condition_variable.Entry_ID
      _Sample_condition_variable.Sample_condition_list_ID

      'ionic strength'   200   .   mM    27534   1
      pH                 6.5   .   pH    27534   1
      pressure           1     .   atm   27534   1
      temperature        273   .   K     27534   1
   stop_
save_


############################
#  Computer software used  #
############################
save_NMRPipe
   _Software.Sf_category    software
   _Software.Sf_framecode   NMRPipe
   _Software.Entry_ID       27534
   _Software.ID             1
   _Software.Type           .
   _Software.Name           NMRPipe
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax'   .   .   27534   1
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      processing   27534   1
   stop_
save_

save_NMRDraw
   _Software.Sf_category    software
   _Software.Sf_framecode   NMRDraw
   _Software.Entry_ID       27534
   _Software.ID             2
   _Software.Type           .
   _Software.Name           NMRDraw
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Delaglio, Grzesiek, Vuister, Zhu, Pfeifer and Bax'   .   .   27534   2
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      processing   27534   2
   stop_
save_

save_SPARKY
   _Software.Sf_category    software
   _Software.Sf_framecode   SPARKY
   _Software.Entry_ID       27534
   _Software.ID             3
   _Software.Type           .
   _Software.Name           SPARKY
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      Goddard   .   .   27534   3
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      Processing                    27534   3
      'chemical shift assignment'   27534   3
      'peak picking'                27534   3
   stop_
save_

save_TOPSPIN
   _Software.Sf_category    software
   _Software.Sf_framecode   TOPSPIN
   _Software.Entry_ID       27534
   _Software.ID             4
   _Software.Type           .
   _Software.Name           TOPSPIN
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Bruker Biospin'   .   .   27534   4
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      collection   27534   4
   stop_
save_

save_Autoassign
   _Software.Sf_category    software
   _Software.Sf_framecode   Autoassign
   _Software.Entry_ID       27534
   _Software.ID             5
   _Software.Type           .
   _Software.Name           Autoassign
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Zimmerman, Moseley, Kulikowski and Montelione'   .   .   27534   5
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      'chemical shift assignment'   27534   5
      'data analysis'               27534   5
   stop_
save_

save_PINE
   _Software.Sf_category    software
   _Software.Sf_framecode   PINE
   _Software.Entry_ID       27534
   _Software.ID             6
   _Software.Type           .
   _Software.Name           PINE
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Bahrami, Markley, Assadi, and Eghbalnia'   .   .   27534   6
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      'chemical shift assignment'   27534   6
      'data analysis'               27534   6
   stop_
save_

save_CYANA
   _Software.Sf_category    software
   _Software.Sf_framecode   CYANA
   _Software.Entry_ID       27534
   _Software.ID             7
   _Software.Type           .
   _Software.Name           CYANA
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Guntert, Mumenthaler and Wuthrich'   .   .   27534   7
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      'geometry optimization'   27534   7
      refinement                27534   7
      'structure solution'      27534   7
   stop_
save_

save_CNS
   _Software.Sf_category    software
   _Software.Sf_framecode   CNS
   _Software.Entry_ID       27534
   _Software.ID             8
   _Software.Type           .
   _Software.Name           CNS
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Brunger, Adams, Clore, Gros, Nilges and Read'   .   .   27534   8
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      'geometry optimization'   27534   8
      refinement                27534   8
      'structure solution'      27534   8
   stop_
save_

save_AVS
   _Software.Sf_category    software
   _Software.Sf_framecode   AVS
   _Software.Entry_ID       27534
   _Software.ID             9
   _Software.Type           .
   _Software.Name           AVS
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Moseley and Montelione'   .   .   27534   9
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      'chemical shift assignment'   27534   9
      'data analysis'               27534   9
   stop_
save_

save_TALOS
   _Software.Sf_category    software
   _Software.Sf_framecode   TALOS
   _Software.Entry_ID       27534
   _Software.ID             10
   _Software.Type           .
   _Software.Name           TALOS
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Cornilescu, Delaglio and Bax'   .   .   27534   10
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      'data analysis'   27534   10
   stop_
save_

save_PSVS
   _Software.Sf_category    software
   _Software.Sf_framecode   PSVS
   _Software.Entry_ID       27534
   _Software.ID             11
   _Software.Type           .
   _Software.Name           PSVS
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'Bhattacharya and Montelione'   .   .   27534   11
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      validation   27534   11
   stop_
save_

save_xeasy
   _Software.Sf_category    software
   _Software.Sf_framecode   xeasy
   _Software.Entry_ID       27534
   _Software.ID             12
   _Software.Type           .
   _Software.Name           xeasy
   _Software.Version        .
   _Software.DOI            .
   _Software.Details        .

   loop_
      _Vendor.Name
      _Vendor.Address
      _Vendor.Electronic_address
      _Vendor.Entry_ID
      _Vendor.Software_ID

      'C. Bartels, T.-h. Xia, M. Billeter, P. Guntert, and K. Wuthrich'   .   .   27534   12
   stop_

   loop_
      _Task.Task
      _Task.Entry_ID
      _Task.Software_ID

      'chemical shift assignment'   27534   12
      'data analysis'               27534   12
   stop_
save_


#########################
#  Experimental detail  #
#########################

    ##################################
    #  NMR Spectrometer definitions  #
    ##################################
save_spectrometer_1
   _NMR_spectrometer.Sf_category      NMR_spectrometer
   _NMR_spectrometer.Sf_framecode     spectrometer_1
   _NMR_spectrometer.Entry_ID         27534
   _NMR_spectrometer.ID               1
   _NMR_spectrometer.Details          cryo-probe
   _NMR_spectrometer.Manufacturer     Bruker
   _NMR_spectrometer.Model            Avance
   _NMR_spectrometer.Serial_number    .
   _NMR_spectrometer.Field_strength   800
save_

save_NMR_spectrometer_list
   _NMR_spectrometer_list.Sf_category    NMR_spectrometer_list
   _NMR_spectrometer_list.Sf_framecode   NMR_spectrometer_list
   _NMR_spectrometer_list.Entry_ID       27534
   _NMR_spectrometer_list.ID             1

   loop_
      _NMR_spectrometer_view.ID
      _NMR_spectrometer_view.Name
      _NMR_spectrometer_view.Manufacturer
      _NMR_spectrometer_view.Model
      _NMR_spectrometer_view.Serial_number
      _NMR_spectrometer_view.Field_strength
      _NMR_spectrometer_view.Details
      _NMR_spectrometer_view.Citation_ID
      _NMR_spectrometer_view.Citation_label
      _NMR_spectrometer_view.Entry_ID
      _NMR_spectrometer_view.NMR_spectrometer_list_ID

      1   spectrometer_1   Bruker   Avance   .   800   cryo-probe   .   .   27534   1
   stop_
save_


    #############################
    #  NMR applied experiments  #
    #############################
save_experiment_list
   _Experiment_list.Sf_category    experiment_list
   _Experiment_list.Sf_framecode   experiment_list
   _Experiment_list.Entry_ID       27534
   _Experiment_list.ID             1
   _Experiment_list.Details        .

   loop_
      _Experiment.ID
      _Experiment.Name
      _Experiment.Raw_data_flag
      _Experiment.NMR_spec_expt_ID
      _Experiment.NMR_spec_expt_label
      _Experiment.MS_expt_ID
      _Experiment.MS_expt_label
      _Experiment.SAXS_expt_ID
      _Experiment.SAXS_expt_label
      _Experiment.FRET_expt_ID
      _Experiment.FRET_expt_label
      _Experiment.EMR_expt_ID
      _Experiment.EMR_expt_label
      _Experiment.Sample_ID
      _Experiment.Sample_label
      _Experiment.Sample_state
      _Experiment.Sample_volume
      _Experiment.Sample_volume_units
      _Experiment.Sample_condition_list_ID
      _Experiment.Sample_condition_list_label
      _Experiment.Sample_spinning_rate
      _Experiment.Sample_angle
      _Experiment.NMR_tube_type
      _Experiment.NMR_spectrometer_ID
      _Experiment.NMR_spectrometer_label
      _Experiment.NMR_spectrometer_probe_ID
      _Experiment.NMR_spectrometer_probe_label
      _Experiment.NMR_spectral_processing_ID
      _Experiment.NMR_spectral_processing_label
      _Experiment.Mass_spectrometer_ID
      _Experiment.Mass_spectrometer_label
      _Experiment.Xray_instrument_ID
      _Experiment.Xray_instrument_label
      _Experiment.Fluorescence_instrument_ID
      _Experiment.Fluorescence_instrument_label
      _Experiment.EMR_instrument_ID
      _Experiment.EMR_instrument_label
      _Experiment.Chromatographic_system_ID
      _Experiment.Chromatographic_system_label
      _Experiment.Chromatographic_column_ID
      _Experiment.Chromatographic_column_label
      _Experiment.Entry_ID
      _Experiment.Experiment_list_ID

      1    '2D TROSY-HSQC'                                                       yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      2    '3D TROSY-HNCOCA'                                                     yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      3    '3D TROSY-HNCA'                                                       yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      4    '3D TROSY-HNCOCACB'                                                   yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      5    '3D TROSY-HNCACB'                                                     yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      6    '3D TROSY-HNCO'                                                       yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      7    '3D TROSY-HBHACONH'                                                   yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      8    '3D HCCH-TOCSY'                                                       yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      9    '3D CCH-TOCSY'                                                        yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      10   '2D 1H-13C HSQC aliphatic'                                            yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      11   'AROMATIC CCH-TOCSY'                                                  yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      12   '3D 1H 13C NOESY'                                                     yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      13   '3D simultaneous 13C-aromatic,13C-aliphatic,15N edited 1H-1H NOESY'   yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      14   '3D 1H-13C NOESY aromatic'                                            yes   .   .   .   .   .   .   .   .   .   .   1   $sample_1   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
      15   'X-filtered noesy (pulse sequence: noesyhsqcgpwgx13d)'                yes   .   .   .   .   .   .   .   .   .   .   2   $sample_2   isotropic   .   .   1   $sample_conditions_1   .   .   .   1   $spectrometer_1   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   .   27534   1
   stop_
save_

save_2D_TROSY-HSQC
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    2D_TROSY-HSQC
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              1
   _NMR_spec_expt.Name                            '2D TROSY-HSQC'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      'TROSY-N15 HSQC'   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   1
   stop_
save_

save_2D_1H-13C_HSQC_aliphatic
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    2D_1H-13C_HSQC_aliphatic
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              2
   _NMR_spec_expt.Name                            '2D 1H-13C HSQC aliphatic'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      'C13 HSQC ALIPHATIC'   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   2
   stop_
save_

save_3D_TROSY-HNCOCA
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_TROSY-HNCOCA
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              3
   _NMR_spec_expt.Name                            '3D TROSY-HNCOCA'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      HNCOCA   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   3
   stop_
save_

save_3D_TROSY-HNCA
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_TROSY-HNCA
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              4
   _NMR_spec_expt.Name                            '3D TROSY-HNCA'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      HNCA   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   4
   stop_
save_

save_3D_TROSY-HNCOCACB
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_TROSY-HNCOCACB
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              5
   _NMR_spec_expt.Name                            '3D TROSY-HNCOCACB'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      HNCOCACB   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   5
   stop_
save_

save_3D_TROSY-HNCACB
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_TROSY-HNCACB
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              6
   _NMR_spec_expt.Name                            '3D TROSY-HNCACB'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      HNCACB   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   6
   stop_
save_

save_3D_TROSY-HNCO
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_TROSY-HNCO
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              7
   _NMR_spec_expt.Name                            '3D TROSY-HNCO'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      HNCO   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   7
   stop_
save_

save_3D_TROSY-HBHACONH
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_TROSY-HBHACONH
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              8
   _NMR_spec_expt.Name                            '3D TROSY-HBHACONH'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      HBHACONH   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   8
   stop_
save_

save_3D_HCCH-TOCSY
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_HCCH-TOCSY
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              9
   _NMR_spec_expt.Name                            '3D CCH-TOCSY'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      HCCH-TOCSY   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   9
   stop_
save_

save_3D_CCH-TOCSY
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_CCH-TOCSY
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              10
   _NMR_spec_expt.Name                            '3D CCH-TOCSY'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      CCH-TOCSY   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   10
   stop_
save_

save_AROMATIC_CCH-TOCSY
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    AROMATIC_CCH-TOCSY
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              11
   _NMR_spec_expt.Name                            'AROMATIC CCH-TOCSY'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      'AROMATIC CCH-TOCSY'   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   11
   stop_
save_

save_3D_1H_13C_NOESY
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_1H_13C_NOESY
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              12
   _NMR_spec_expt.Name                            '3D 1H 13C NOESY'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      '3D 1H 13C NOESY'   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   12
   stop_
save_

save_NMR_spectrometer_expt_1
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    NMR_spectrometer_expt_1
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              13
   _NMR_spec_expt.Name                            '3D simultaneous 13C-aromatic,13C-aliphatic,15N edited 1H-1H NOESY'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      SIMNOESY   'time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   13
   stop_
save_

save_3D_1H-13C_NOESY_aromatic
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    3D_1H-13C_NOESY_aromatic
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              14
   _NMR_spec_expt.Name                            '3D 1H-13C NOESY aromatic'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      'C13 NOESY AROMATIC'   'Time-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   14
   stop_
save_

save_X-filtered_noesy_(pulse_sequence_noesyhsqcgpwgx13d)
   _NMR_spec_expt.Sf_category                     NMR_spectrometer_expt
   _NMR_spec_expt.Sf_framecode                    X-filtered_noesy_(pulse_sequence_noesyhsqcgpwgx13d)
   _NMR_spec_expt.Entry_ID                        27534
   _NMR_spec_expt.ID                              15
   _NMR_spec_expt.Name                            'X-filtered noesy (pulse sequence: noesyhsqcgpwgx13d)'
   _NMR_spec_expt.Type                            .
   _NMR_spec_expt.Sample_volume                   .
   _NMR_spec_expt.Sample_volume_units             .
   _NMR_spec_expt.NMR_tube_type                   .
   _NMR_spec_expt.Sample_spinning_rate            .
   _NMR_spec_expt.Sample_angle                    .
   _NMR_spec_expt.NMR_spectrometer_ID             1
   _NMR_spec_expt.NMR_spectrometer_label          $spectrometer_1
   _NMR_spec_expt.NMR_spectrometer_probe_ID       .
   _NMR_spec_expt.NMR_spectrometer_probe_label    .
   _NMR_spec_expt.Carrier_freq_switch_time        .
   _NMR_spec_expt.Software_ID                     .
   _NMR_spec_expt.Software_label                  .
   _NMR_spec_expt.Method_ID                       .
   _NMR_spec_expt.Method_label                    .
   _NMR_spec_expt.Pulse_seq_accession_BMRB_code   .
   _NMR_spec_expt.Details                         .

   loop_
      _NMR_experiment_file.Name
      _NMR_experiment_file.Type
      _NMR_experiment_file.Directory_path
      _NMR_experiment_file.Byte_order
      _NMR_experiment_file.Bytes_per_data_point
      _NMR_experiment_file.File_header_size
      _NMR_experiment_file.Record_header_size
      _NMR_experiment_file.Record_trailer_size
      _NMR_experiment_file.Compression_algorithm
      _NMR_experiment_file.Details
      _NMR_experiment_file.Entry_ID
      _NMR_experiment_file.NMR_spec_expt_ID

      'XFD NOESY'   'TIme-domain (raw spectral data)'   .   .   .   .   .   .   .   FID   27534   15
   stop_
save_