data_25997 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 25997 _Entry.Title ; Solution structure of the J domain of EMCV IRES ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2016-03-16 _Entry.Accession_date 2016-06-10 _Entry.Last_release_date 2016-08-08 _Entry.Original_release_date 2016-08-08 _Entry.Origination author _Entry.NMR_STAR_version 3.1.2.6 _Entry.Original_NMR_STAR_version 3.1.1.99 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype SOLUTION _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.ORCID _Entry_author.Entry_ID 1 Shunsuke Imai . . . . 25997 2 Victoria D'Souza . . . . 25997 3 Gerhard Wagner . . . . 25997 stop_ loop_ _SG_project.SG_project_ID _SG_project.Project_name _SG_project.Full_name_of_center _SG_project.Initial_of_center _SG_project.Entry_ID 1 'not applicable' 'not applicable' . 25997 stop_ loop_ _Struct_keywords.Keywords _Struct_keywords.Text _Struct_keywords.Entry_ID IRES . 25997 'Viral RNA' . 25997 'translation initiation' . 25997 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 25997 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 143 25997 '1H chemical shifts' 154 25997 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 2 . . 2016-10-12 2016-03-16 update BMRB 'update entry citation' 25997 1 . . 2016-08-08 2016-03-16 original author 'original release' 25997 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 25999 'Solution structure of the St domain of EMCV IRES' 25997 BMRB 26000 'Solution structure of the delta-J-delta-K domain of EMCV IRES' 25997 BMRB 26996 'Solution structure of the J-K region of EMCV IRES' 25997 BMRB 26998 'Solution structure of the K domain of EMCV IRES' 25997 PDB 2NBY 'BMRB Entry Tracking System' 25997 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 25997 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 27525590 _Citation.Full_citation . _Citation.Title ; An accurately preorganized IRES RNA structure enables eIF4G capture for initiation of viral translation ; _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'Nat. Struct. Mol. Biol.' _Citation.Journal_name_full . _Citation.Journal_volume 23 _Citation.Journal_issue 9 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 859 _Citation.Page_last 864 _Citation.Year 2016 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.ORCID _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Shunsuke Imai . . . . 25997 1 2 Christopher Hellen . . . . 25997 1 3 Victoria D'Souza . . . . 25997 1 4 Gerhard Wagner . . . . 25997 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 25997 _Assembly.ID 1 _Assembly.Name 'J domain of EMCV IRES' _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 'RNA (39-MER)' 1 $RNA_(39-MER) A . yes native no no . . . 25997 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_RNA_(39-MER) _Entity.Sf_category entity _Entity.Sf_framecode RNA_(39-MER) _Entity.Entry_ID 25997 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name RNA_(39-MER) _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID A _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GGGCAGAAGGUACCCCAUUG UAUGGGAUCUGAUCUGCCC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 39 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method syn _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 12538.552 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 693 G . 25997 1 2 694 G . 25997 1 3 695 G . 25997 1 4 696 C . 25997 1 5 697 A . 25997 1 6 698 G . 25997 1 7 699 A . 25997 1 8 700 A . 25997 1 9 701 G . 25997 1 10 702 G . 25997 1 11 703 U . 25997 1 12 704 A . 25997 1 13 705 C . 25997 1 14 706 C . 25997 1 15 707 C . 25997 1 16 708 C . 25997 1 17 709 A . 25997 1 18 710 U . 25997 1 19 711 U . 25997 1 20 712 G . 25997 1 21 713 U . 25997 1 22 714 A . 25997 1 23 715 U . 25997 1 24 716 G . 25997 1 25 717 G . 25997 1 26 718 G . 25997 1 27 719 A . 25997 1 28 720 U . 25997 1 29 721 C . 25997 1 30 722 U . 25997 1 31 723 G . 25997 1 32 724 A . 25997 1 33 725 U . 25997 1 34 726 C . 25997 1 35 727 U . 25997 1 36 728 G . 25997 1 37 729 C . 25997 1 38 730 C . 25997 1 39 731 C . 25997 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . G 1 1 25997 1 . G 2 2 25997 1 . G 3 3 25997 1 . C 4 4 25997 1 . A 5 5 25997 1 . G 6 6 25997 1 . A 7 7 25997 1 . A 8 8 25997 1 . G 9 9 25997 1 . G 10 10 25997 1 . U 11 11 25997 1 . A 12 12 25997 1 . C 13 13 25997 1 . C 14 14 25997 1 . C 15 15 25997 1 . C 16 16 25997 1 . A 17 17 25997 1 . U 18 18 25997 1 . U 19 19 25997 1 . G 20 20 25997 1 . U 21 21 25997 1 . A 22 22 25997 1 . U 23 23 25997 1 . G 24 24 25997 1 . G 25 25 25997 1 . G 26 26 25997 1 . A 27 27 25997 1 . U 28 28 25997 1 . C 29 29 25997 1 . U 30 30 25997 1 . G 31 31 25997 1 . A 32 32 25997 1 . U 33 33 25997 1 . C 34 34 25997 1 . U 35 35 25997 1 . G 36 36 25997 1 . C 37 37 25997 1 . C 38 38 25997 1 . C 39 39 25997 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 25997 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Details _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $RNA_(39-MER) . 12104 virus . 'Encephalomyocarditis virus' 'Encephalomyocarditis virus' . . Viruses . Cardiovirus 'Cardiovirus A' . . . . . . . . . . . . . 25997 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 25997 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Details _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $RNA_(39-MER) . 'enzymatic semisynthesis' . . . . . . . . . . . . . . . . 25997 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 25997 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (39-MER)' 'natural abundance' . . 1 $RNA_(39-MER) . RNA 0.5 . . mM . . . . 25997 1 2 'potassium phosphate' 'natural abundance' . . . . . buffer 10 . . mM . . . . 25997 1 3 'sodium chloride' 'natural abundance' . . . . . salt 10 . . mM . . . . 25997 1 4 D2O [U-2H] . . . . . solvent 100 . . % . . . . 25997 1 stop_ save_ save_sample_2 _Sample.Sf_category sample _Sample.Sf_framecode sample_2 _Sample.Entry_ID 25997 _Sample.ID 2 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (39-MER)' 'natural abundance' . . 1 $RNA_(39-MER) . RNA 0.5 . . mM . . . . 25997 2 2 'potassium phosphate' 'natural abundance' . . . . . buffer 10 . . mM . . . . 25997 2 3 'sodium chloride' 'natural abundance' . . . . . salt 10 . . mM . . . . 25997 2 4 H2O 'natural abundance' . . . . . solvent 90 . . % . . . . 25997 2 5 D2O [U-2H] . . . . . solvent 10 . . % . . . . 25997 2 stop_ save_ save_sample_3 _Sample.Sf_category sample _Sample.Sf_framecode sample_3 _Sample.Entry_ID 25997 _Sample.ID 3 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (39-MER)' '[U-13C; U-15N]-Ade, [U-13C; U-15N]-Cyt' . . 1 $RNA_(39-MER) . RNA 0.5 . . mM . . . . 25997 3 2 'potassium phosphate' 'natural abundance' . . . . . buffer 10 . . mM . . . . 25997 3 3 'sodium chloride' 'natural abundance' . . . . . salt 10 . . mM . . . . 25997 3 4 D2O [U-2H] . . . . . solvent 100 . . % . . . . 25997 3 stop_ save_ save_sample_4 _Sample.Sf_category sample _Sample.Sf_framecode sample_4 _Sample.Entry_ID 25997 _Sample.ID 4 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (39-MER)' '[U-13C; U-15N]-Gua, [U-13C; U-15N]-Ura' . . 1 $RNA_(39-MER) . RNA 0.5 . . mM . . . . 25997 4 2 'potassium phosphate' 'natural abundance' . . . . . buffer 10 . . mM . . . . 25997 4 3 'sodium chloride' 'natural abundance' . . . . . salt 10 . . mM . . . . 25997 4 4 D2O [U-2H] . . . . . solvent 100 . . % . . . . 25997 4 stop_ save_ save_sample_5 _Sample.Sf_category sample _Sample.Sf_framecode sample_5 _Sample.Entry_ID 25997 _Sample.ID 5 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (39-MER)' '[U-13C; U-15N]-Ade, [U-13C; U-15N]-Cyt' . . 1 $RNA_(39-MER) . RNA 0.5 . . mM . . . . 25997 5 2 'potassium phosphate' 'natural abundance' . . . . . buffer 10 . . mM . . . . 25997 5 3 'sodium chloride' 'natural abundance' . . . . . salt 10 . . mM . . . . 25997 5 4 H2O 'natural abundance' . . . . . solvent 90 . . % . . . . 25997 5 5 D2O [U-2H] . . . . . solvent 10 . . % . . . . 25997 5 stop_ save_ save_sample_6 _Sample.Sf_category sample _Sample.Sf_framecode sample_6 _Sample.Entry_ID 25997 _Sample.ID 6 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 'RNA (39-MER)' '[U-13C; U-15N]-Gua, [U-13C; U-15N]-Ura' . . 1 $RNA_(39-MER) . RNA 0.5 . . mM . . . . 25997 6 2 'potassium phosphate' 'natural abundance' . . . . . buffer 10 . . mM . . . . 25997 6 3 'sodium chloride' 'natural abundance' . . . . . salt 10 . . mM . . . . 25997 6 4 H2O 'natural abundance' . . . . . solvent 90 . . % . . . . 25997 6 5 D2O [U-2H] . . . . . solvent 10 . . % . . . . 25997 6 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 25997 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 20 . mM 25997 1 pH 6.5 . pH 25997 1 pressure 1 . atm 25997 1 temperature 308 . K 25997 1 stop_ save_ save_sample_conditions_2 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_2 _Sample_condition_list.Entry_ID 25997 _Sample_condition_list.ID 2 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 20 . mM 25997 2 pH 6.5 . pH 25997 2 pressure 1 . atm 25997 2 temperature 283 . K 25997 2 stop_ save_ save_sample_conditions_3 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_3 _Sample_condition_list.Entry_ID 25997 _Sample_condition_list.ID 3 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 20 . mM 25997 3 pH 5.5 . pH 25997 3 pressure 1 . atm 25997 3 temperature 283 . K 25997 3 stop_ save_ ############################ # Computer software used # ############################ save_CARA _Software.Sf_category software _Software.Sf_framecode CARA _Software.Entry_ID 25997 _Software.ID 1 _Software.Name CARA _Software.Version . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Keller and Wuthrich' . . 25997 1 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'chemical shift assignment' 25997 1 stop_ save_ save_CYANA _Software.Sf_category software _Software.Sf_framecode CYANA _Software.Entry_ID 25997 _Software.ID 2 _Software.Name CYANA _Software.Version . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Guntert, Mumenthaler and Wuthrich' . . 25997 2 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'structure solution' 25997 2 stop_ save_ save_X-PLOR_NIH _Software.Sf_category software _Software.Sf_framecode X-PLOR_NIH _Software.Entry_ID 25997 _Software.ID 3 _Software.Name X-PLOR_NIH _Software.Version . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Schwieters, Kuszewski, Tjandra and Clore' . . 25997 3 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID refinement 25997 3 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_1 _NMR_spectrometer.Entry_ID 25997 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 800 save_ save_spectrometer_2 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_2 _NMR_spectrometer.Entry_ID 25997 _NMR_spectrometer.ID 2 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 700 save_ save_NMR_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list _NMR_spectrometer_list.Entry_ID 25997 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 spectrometer_1 Bruker Avance . 800 . . . 25997 1 2 spectrometer_2 Bruker Avance . 700 . . . 25997 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 25997 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '2D 1H-1H NOESY' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . . . . . . . . . . . . . . . . . . . 25997 1 2 '2D 1H-1H NOESY' no . . . . . . . . . . 2 $sample_2 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 25997 1 3 '2D 1H-1H NOESY' no . . . . . . . . . . 2 $sample_2 isotropic . . 3 $sample_conditions_3 . . . . . . . . . . . . . . . . . . . . . 25997 1 4 '2D 1H-13C HSQC' no . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . . . . . . . . . . . . . . . . . . . 25997 1 5 '3D 1H-13C NOESY' no . . . . . . . . . . 3 $sample_3 isotropic . . 1 $sample_conditions_1 . . . . . . . . . . . . . . . . . . . . . 25997 1 6 '2D 1H-13C HSQC' no . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . . . . . . . . . . . . . . . . . . . 25997 1 7 '3D 1H-13C NOESY' no . . . . . . . . . . 4 $sample_4 isotropic . . 1 $sample_conditions_1 . . . . . . . . . . . . . . . . . . . . . 25997 1 8 '2D 1H-15N HSQC' no . . . . . . . . . . 5 $sample_5 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 25997 1 9 '2D 1H-15N HSQC' no . . . . . . . . . . 5 $sample_5 isotropic . . 3 $sample_conditions_3 . . . . . . . . . . . . . . . . . . . . . 25997 1 10 '2D 1H-15N HSQC' no . . . . . . . . . . 6 $sample_6 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 25997 1 11 '2D 1H-15N HSQC' no . . . . . . . . . . 6 $sample_6 isotropic . . 3 $sample_conditions_3 . . . . . . . . . . . . . . . . . . . . . 25997 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference_1 _Chem_shift_reference.Entry_ID 25997 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID C 13 DSS 'methyl protons' . . . . ppm 0.00 na indirect 0.251449530 . . . . . 25997 1 H 1 DSS 'methyl protons' . . . . ppm 0 external direct 1 . . . . . 25997 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1 _Assigned_chem_shift_list.Entry_ID 25997 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '2D 1H-1H NOESY' 1 $sample_1 isotropic 25997 1 4 '2D 1H-13C HSQC' 3 $sample_3 isotropic 25997 1 6 '2D 1H-13C HSQC' 4 $sample_4 isotropic 25997 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 G H1' H 1 5.88 0 . 1 . . . A 693 G H1' . 25997 1 2 . 1 1 1 1 G H2' H 1 4.96 0 . 1 . . . A 693 G H2' . 25997 1 3 . 1 1 1 1 G H8 H 1 8.17 0 . 1 . . . A 693 G H8 . 25997 1 4 . 1 1 1 1 G C1' C 13 91.33 0 . 1 . . . A 693 G C1' . 25997 1 5 . 1 1 1 1 G C2' C 13 75.23 0 . 1 . . . A 693 G C2' . 25997 1 6 . 1 1 1 1 G C8 C 13 139.07 0 . 1 . . . A 693 G C8 . 25997 1 7 . 1 1 2 2 G H1' H 1 5.97 0 . 1 . . . A 694 G H1' . 25997 1 8 . 1 1 2 2 G H2' H 1 4.75 0 . 1 . . . A 694 G H2' . 25997 1 9 . 1 1 2 2 G H8 H 1 7.60 0 . 1 . . . A 694 G H8 . 25997 1 10 . 1 1 2 2 G C1' C 13 92.83 0 . 1 . . . A 694 G C1' . 25997 1 11 . 1 1 2 2 G C2' C 13 75.60 0 . 1 . . . A 694 G C2' . 25997 1 12 . 1 1 2 2 G C8 C 13 136.89 0 . 1 . . . A 694 G C8 . 25997 1 13 . 1 1 3 3 G H1' H 1 5.81 0 . 1 . . . A 695 G H1' . 25997 1 14 . 1 1 3 3 G H2' H 1 4.55 0 . 1 . . . A 695 G H2' . 25997 1 15 . 1 1 3 3 G H8 H 1 7.29 0 . 1 . . . A 695 G H8 . 25997 1 16 . 1 1 3 3 G C1' C 13 93.10 0 . 1 . . . A 695 G C1' . 25997 1 17 . 1 1 3 3 G C2' C 13 75.39 0 . 1 . . . A 695 G C2' . 25997 1 18 . 1 1 3 3 G C8 C 13 135.99 0 . 1 . . . A 695 G C8 . 25997 1 19 . 1 1 4 4 C H1' H 1 5.52 0 . 1 . . . A 696 C H1' . 25997 1 20 . 1 1 4 4 C H2' H 1 4.60 0 . 1 . . . A 696 C H2' . 25997 1 21 . 1 1 4 4 C H5 H 1 5.23 0 . 1 . . . A 696 C H5 . 25997 1 22 . 1 1 4 4 C H6 H 1 7.59 0 . 1 . . . A 696 C H6 . 25997 1 23 . 1 1 4 4 C C1' C 13 93.82 0 . 1 . . . A 696 C C1' . 25997 1 24 . 1 1 4 4 C C2' C 13 75.41 0 . 1 . . . A 696 C C2' . 25997 1 25 . 1 1 4 4 C C5 C 13 97.42 0 . 1 . . . A 696 C C5 . 25997 1 26 . 1 1 4 4 C C6 C 13 140.65 0 . 1 . . . A 696 C C6 . 25997 1 27 . 1 1 5 5 A H1' H 1 5.95 0 . 1 . . . A 697 A H1' . 25997 1 28 . 1 1 5 5 A H2 H 1 6.98 0 . 1 . . . A 697 A H2 . 25997 1 29 . 1 1 5 5 A H2' H 1 4.67 0 . 1 . . . A 697 A H2' . 25997 1 30 . 1 1 5 5 A H8 H 1 7.94 0 . 1 . . . A 697 A H8 . 25997 1 31 . 1 1 5 5 A C1' C 13 93.10 0 . 1 . . . A 697 A C1' . 25997 1 32 . 1 1 5 5 A C2 C 13 152.32 0 . 1 . . . A 697 A C2 . 25997 1 33 . 1 1 5 5 A C2' C 13 75.79 0 . 1 . . . A 697 A C2' . 25997 1 34 . 1 1 5 5 A C8 C 13 139.35 0 . 1 . . . A 697 A C8 . 25997 1 35 . 1 1 6 6 G H1' H 1 5.54 0 . 1 . . . A 698 G H1' . 25997 1 36 . 1 1 6 6 G H2' H 1 4.46 0 . 1 . . . A 698 G H2' . 25997 1 37 . 1 1 6 6 G H8 H 1 7.13 0 . 1 . . . A 698 G H8 . 25997 1 38 . 1 1 6 6 G C1' C 13 92.55 0 . 1 . . . A 698 G C1' . 25997 1 39 . 1 1 6 6 G C2' C 13 75.55 0 . 1 . . . A 698 G C2' . 25997 1 40 . 1 1 6 6 G C8 C 13 135.86 0 . 1 . . . A 698 G C8 . 25997 1 41 . 1 1 7 7 A H1' H 1 5.88 0 . 1 . . . A 699 A H1' . 25997 1 42 . 1 1 7 7 A H2 H 1 7.57 0 . 1 . . . A 699 A H2 . 25997 1 43 . 1 1 7 7 A H2' H 1 4.55 0 . 1 . . . A 699 A H2' . 25997 1 44 . 1 1 7 7 A H8 H 1 7.70 0 . 1 . . . A 699 A H8 . 25997 1 45 . 1 1 7 7 A C1' C 13 92.18 0 . 1 . . . A 699 A C1' . 25997 1 46 . 1 1 7 7 A C2 C 13 154.03 0 . 1 . . . A 699 A C2 . 25997 1 47 . 1 1 7 7 A C2' C 13 75.91 0 . 1 . . . A 699 A C2' . 25997 1 48 . 1 1 7 7 A C8 C 13 139.42 0 . 1 . . . A 699 A C8 . 25997 1 49 . 1 1 8 8 A H1' H 1 5.67 0 . 1 . . . A 700 A H1' . 25997 1 50 . 1 1 8 8 A H2 H 1 7.84 0 . 1 . . . A 700 A H2 . 25997 1 51 . 1 1 8 8 A H2' H 1 4.50 0 . 1 . . . A 700 A H2' . 25997 1 52 . 1 1 8 8 A H8 H 1 7.75 0 . 1 . . . A 700 A H8 . 25997 1 53 . 1 1 8 8 A C1' C 13 92.05 0 . 1 . . . A 700 A C1' . 25997 1 54 . 1 1 8 8 A C2 C 13 154.76 0 . 1 . . . A 700 A C2 . 25997 1 55 . 1 1 8 8 A C2' C 13 74.15 0 . 1 . . . A 700 A C2' . 25997 1 56 . 1 1 8 8 A C8 C 13 139.85 0 . 1 . . . A 700 A C8 . 25997 1 57 . 1 1 9 9 G H1' H 1 5.14 0 . 1 . . . A 701 G H1' . 25997 1 58 . 1 1 9 9 G H2' H 1 4.46 0 . 1 . . . A 701 G H2' . 25997 1 59 . 1 1 9 9 G H3' H 1 4.27 0 . 1 . . . A 701 G H3' . 25997 1 60 . 1 1 9 9 G H8 H 1 7.49 0 . 1 . . . A 701 G H8 . 25997 1 61 . 1 1 9 9 G C1' C 13 90.94 0 . 1 . . . A 701 G C1' . 25997 1 62 . 1 1 9 9 G C2' C 13 75.31 0 . 1 . . . A 701 G C2' . 25997 1 63 . 1 1 9 9 G C8 C 13 137.64 0 . 1 . . . A 701 G C8 . 25997 1 64 . 1 1 10 10 G H1' H 1 5.75 0 . 1 . . . A 702 G H1' . 25997 1 65 . 1 1 10 10 G H2' H 1 4.65 0 . 1 . . . A 702 G H2' . 25997 1 66 . 1 1 10 10 G H8 H 1 7.61 0 . 1 . . . A 702 G H8 . 25997 1 67 . 1 1 10 10 G C1' C 13 90.36 0 . 1 . . . A 702 G C1' . 25997 1 68 . 1 1 10 10 G C2' C 13 75.67 0 . 1 . . . A 702 G C2' . 25997 1 69 . 1 1 11 11 U H1' H 1 5.89 0 . 1 . . . A 703 U H1' . 25997 1 70 . 1 1 11 11 U H2' H 1 4.49 0 . 1 . . . A 703 U H2' . 25997 1 71 . 1 1 11 11 U H5 H 1 5.79 0 . 1 . . . A 703 U H5 . 25997 1 72 . 1 1 11 11 U H6 H 1 7.80 0 . 1 . . . A 703 U H6 . 25997 1 73 . 1 1 11 11 U C1' C 13 92.46 0 . 1 . . . A 703 U C1' . 25997 1 74 . 1 1 11 11 U C2' C 13 75.93 0 . 1 . . . A 703 U C2' . 25997 1 75 . 1 1 11 11 U C5 C 13 105.21 0 . 1 . . . A 703 U C5 . 25997 1 76 . 1 1 11 11 U C6 C 13 143.18 0 . 1 . . . A 703 U C6 . 25997 1 77 . 1 1 12 12 A H1' H 1 5.93 0 . 1 . . . A 704 A H1' . 25997 1 78 . 1 1 12 12 A H2 H 1 7.89 0 . 1 . . . A 704 A H2 . 25997 1 79 . 1 1 12 12 A H2' H 1 4.88 0 . 1 . . . A 704 A H2' . 25997 1 80 . 1 1 12 12 A H5' H 1 4.25 0 . 2 . . . A 704 A H5' . 25997 1 81 . 1 1 12 12 A H5'' H 1 4.48 0 . 2 . . . A 704 A H5'' . 25997 1 82 . 1 1 12 12 A H8 H 1 8.16 0 . 1 . . . A 704 A H8 . 25997 1 83 . 1 1 12 12 A C1' C 13 93.13 0 . 1 . . . A 704 A C1' . 25997 1 84 . 1 1 12 12 A C2 C 13 154.16 0 . 1 . . . A 704 A C2 . 25997 1 85 . 1 1 12 12 A C2' C 13 75.46 0 . 1 . . . A 704 A C2' . 25997 1 86 . 1 1 12 12 A C5' C 13 66.65 0 . 1 . . . A 704 A C5' . 25997 1 87 . 1 1 12 12 A C8 C 13 141.39 0 . 1 . . . A 704 A C8 . 25997 1 88 . 1 1 13 13 C H1' H 1 5.51 0 . 1 . . . A 705 C H1' . 25997 1 89 . 1 1 13 13 C H2' H 1 4.25 0 . 1 . . . A 705 C H2' . 25997 1 90 . 1 1 13 13 C H5 H 1 5.60 0 . 1 . . . A 705 C H5 . 25997 1 91 . 1 1 13 13 C H6 H 1 7.77 0 . 1 . . . A 705 C H6 . 25997 1 92 . 1 1 13 13 C C1' C 13 93.34 0 . 1 . . . A 705 C C1' . 25997 1 93 . 1 1 13 13 C C2' C 13 75.78 0 . 1 . . . A 705 C C2' . 25997 1 94 . 1 1 13 13 C C5 C 13 97.67 0 . 1 . . . A 705 C C5 . 25997 1 95 . 1 1 13 13 C C6 C 13 141.62 0 . 1 . . . A 705 C C6 . 25997 1 96 . 1 1 14 14 C H1' H 1 5.65 0 . 1 . . . A 706 C H1' . 25997 1 97 . 1 1 14 14 C H2' H 1 4.39 0 . 1 . . . A 706 C H2' . 25997 1 98 . 1 1 14 14 C H5 H 1 5.69 0 . 1 . . . A 706 C H5 . 25997 1 99 . 1 1 14 14 C H6 H 1 7.81 0 . 1 . . . A 706 C H6 . 25997 1 100 . 1 1 14 14 C C1' C 13 93.69 0 . 1 . . . A 706 C C1' . 25997 1 101 . 1 1 14 14 C C2' C 13 75.63 0 . 1 . . . A 706 C C2' . 25997 1 102 . 1 1 14 14 C C5 C 13 98.40 0 . 1 . . . A 706 C C5 . 25997 1 103 . 1 1 14 14 C C6 C 13 141.93 0 . 1 . . . A 706 C C6 . 25997 1 104 . 1 1 15 15 C H1' H 1 5.46 0 . 1 . . . A 707 C H1' . 25997 1 105 . 1 1 15 15 C H2' H 1 4.04 0 . 1 . . . A 707 C H2' . 25997 1 106 . 1 1 15 15 C H5 H 1 5.53 0 . 1 . . . A 707 C H5 . 25997 1 107 . 1 1 15 15 C H6 H 1 7.83 0 . 1 . . . A 707 C H6 . 25997 1 108 . 1 1 15 15 C C1' C 13 94.32 0 . 1 . . . A 707 C C1' . 25997 1 109 . 1 1 15 15 C C2' C 13 67.58 0 . 1 . . . A 707 C C2' . 25997 1 110 . 1 1 15 15 C C5 C 13 98.11 0 . 1 . . . A 707 C C5 . 25997 1 111 . 1 1 15 15 C C6 C 13 141.72 0 . 1 . . . A 707 C C6 . 25997 1 112 . 1 1 16 16 C H1' H 1 5.45 0 . 1 . . . A 708 C H1' . 25997 1 113 . 1 1 16 16 C H2' H 1 4.46 0 . 1 . . . A 708 C H2' . 25997 1 114 . 1 1 16 16 C H5 H 1 5.52 0 . 1 . . . A 708 C H5 . 25997 1 115 . 1 1 16 16 C H6 H 1 7.77 0 . 1 . . . A 708 C H6 . 25997 1 116 . 1 1 16 16 C C1' C 13 94.15 0 . 1 . . . A 708 C C1' . 25997 1 117 . 1 1 16 16 C C2' C 13 75.24 0 . 1 . . . A 708 C C2' . 25997 1 118 . 1 1 16 16 C C5 C 13 97.49 0 . 1 . . . A 708 C C5 . 25997 1 119 . 1 1 16 16 C C6 C 13 141.37 0 . 1 . . . A 708 C C6 . 25997 1 120 . 1 1 17 17 A H1' H 1 5.96 0 . 1 . . . A 709 A H1' . 25997 1 121 . 1 1 17 17 A H2 H 1 7.48 0 . 1 . . . A 709 A H2 . 25997 1 122 . 1 1 17 17 A H2' H 1 4.39 0 . 1 . . . A 709 A H2' . 25997 1 123 . 1 1 17 17 A H8 H 1 8.06 0 . 1 . . . A 709 A H8 . 25997 1 124 . 1 1 17 17 A C1' C 13 93.15 0 . 1 . . . A 709 A C1' . 25997 1 125 . 1 1 17 17 A C2 C 13 153.84 0 . 1 . . . A 709 A C2 . 25997 1 126 . 1 1 17 17 A C2' C 13 75.86 0 . 1 . . . A 709 A C2' . 25997 1 127 . 1 1 17 17 A C8 C 13 139.64 0 . 1 . . . A 709 A C8 . 25997 1 128 . 1 1 18 18 U H1' H 1 5.67 0 . 1 . . . A 710 U H1' . 25997 1 129 . 1 1 18 18 U H2' H 1 4.26 0 . 1 . . . A 710 U H2' . 25997 1 130 . 1 1 18 18 U H5 H 1 5.21 0 . 1 . . . A 710 U H5 . 25997 1 131 . 1 1 18 18 U H6 H 1 7.39 0 . 1 . . . A 710 U H6 . 25997 1 132 . 1 1 18 18 U C1' C 13 90.47 0 . 1 . . . A 710 U C1' . 25997 1 133 . 1 1 18 18 U C2' C 13 75.75 0 . 1 . . . A 710 U C2' . 25997 1 134 . 1 1 18 18 U C5 C 13 104.45 0 . 1 . . . A 710 U C5 . 25997 1 135 . 1 1 18 18 U C6 C 13 141.63 0 . 1 . . . A 710 U C6 . 25997 1 136 . 1 1 19 19 U H1' H 1 5.87 0 . 1 . . . A 711 U H1' . 25997 1 137 . 1 1 19 19 U H2' H 1 4.36 0 . 1 . . . A 711 U H2' . 25997 1 138 . 1 1 19 19 U H5 H 1 5.86 0 . 1 . . . A 711 U H5 . 25997 1 139 . 1 1 19 19 U H6 H 1 7.86 0 . 1 . . . A 711 U H6 . 25997 1 140 . 1 1 19 19 U C1' C 13 90.89 0 . 1 . . . A 711 U C1' . 25997 1 141 . 1 1 19 19 U C2' C 13 76.19 0 . 1 . . . A 711 U C2' . 25997 1 142 . 1 1 19 19 U C5 C 13 105.05 0 . 1 . . . A 711 U C5 . 25997 1 143 . 1 1 19 19 U C6 C 13 143.53 0 . 1 . . . A 711 U C6 . 25997 1 144 . 1 1 20 20 G H1' H 1 5.40 0 . 1 . . . A 712 G H1' . 25997 1 145 . 1 1 20 20 G H2' H 1 4.42 0 . 1 . . . A 712 G H2' . 25997 1 146 . 1 1 20 20 G H3' H 1 4.59 0 . 1 . . . A 712 G H3' . 25997 1 147 . 1 1 20 20 G H4' H 1 3.87 0 . 1 . . . A 712 G H4' . 25997 1 148 . 1 1 20 20 G H5' H 1 3.99 0 . 2 . . . A 712 G H5' . 25997 1 149 . 1 1 20 20 G H5'' H 1 4.13 0 . 2 . . . A 712 G H5'' . 25997 1 150 . 1 1 20 20 G H8 H 1 7.84 0 . 1 . . . A 712 G H8 . 25997 1 151 . 1 1 20 20 G C1' C 13 89.20 0 . 1 . . . A 712 G C1' . 25997 1 152 . 1 1 20 20 G C2' C 13 77.00 0 . 1 . . . A 712 G C2' . 25997 1 153 . 1 1 20 20 G C4' C 13 86.08 0 . 1 . . . A 712 G C4' . 25997 1 154 . 1 1 20 20 G C5' C 13 68.06 0 . 1 . . . A 712 G C5' . 25997 1 155 . 1 1 20 20 G C8 C 13 140.06 0 . 1 . . . A 712 G C8 . 25997 1 156 . 1 1 21 21 U H1' H 1 5.88 0 . 1 . . . A 713 U H1' . 25997 1 157 . 1 1 21 21 U H2' H 1 4.33 0 . 1 . . . A 713 U H2' . 25997 1 158 . 1 1 21 21 U H3' H 1 4.70 0 . 1 . . . A 713 U H3' . 25997 1 159 . 1 1 21 21 U H4' H 1 4.43 0 . 1 . . . A 713 U H4' . 25997 1 160 . 1 1 21 21 U H5 H 1 5.86 0 . 1 . . . A 713 U H5 . 25997 1 161 . 1 1 21 21 U H5' H 1 3.98 0 . 2 . . . A 713 U H5' . 25997 1 162 . 1 1 21 21 U H5'' H 1 3.92 0 . 2 . . . A 713 U H5'' . 25997 1 163 . 1 1 21 21 U H6 H 1 7.74 0 . 1 . . . A 713 U H6 . 25997 1 164 . 1 1 21 21 U C1' C 13 90.05 0 . 1 . . . A 713 U C1' . 25997 1 165 . 1 1 21 21 U C2' C 13 75.70 0 . 1 . . . A 713 U C2' . 25997 1 166 . 1 1 21 21 U C3' C 13 77.58 0 . 1 . . . A 713 U C3' . 25997 1 167 . 1 1 21 21 U C5 C 13 105.52 0 . 1 . . . A 713 U C5 . 25997 1 168 . 1 1 21 21 U C5' C 13 68.08 0 . 1 . . . A 713 U C5' . 25997 1 169 . 1 1 21 21 U C6 C 13 143.94 0 . 1 . . . A 713 U C6 . 25997 1 170 . 1 1 22 22 A H1' H 1 5.92 0 . 1 . . . A 714 A H1' . 25997 1 171 . 1 1 22 22 A H2 H 1 7.94 0 . 1 . . . A 714 A H2 . 25997 1 172 . 1 1 22 22 A H2' H 1 4.87 0 . 1 . . . A 714 A H2' . 25997 1 173 . 1 1 22 22 A H3' H 1 4.76 0 . 1 . . . A 714 A H3' . 25997 1 174 . 1 1 22 22 A H4' H 1 4.61 0 . 1 . . . A 714 A H4' . 25997 1 175 . 1 1 22 22 A H5' H 1 4.27 0 . 2 . . . A 714 A H5' . 25997 1 176 . 1 1 22 22 A H5'' H 1 4.30 0 . 2 . . . A 714 A H5'' . 25997 1 177 . 1 1 22 22 A H8 H 1 8.45 0 . 1 . . . A 714 A H8 . 25997 1 178 . 1 1 22 22 A C1' C 13 89.65 0 . 1 . . . A 714 A C1' . 25997 1 179 . 1 1 22 22 A C2 C 13 154.83 0 . 1 . . . A 714 A C2 . 25997 1 180 . 1 1 22 22 A C2' C 13 75.08 0 . 1 . . . A 714 A C2' . 25997 1 181 . 1 1 22 22 A C3' C 13 76.43 0 . 1 . . . A 714 A C3' . 25997 1 182 . 1 1 22 22 A C4' C 13 84.65 0 . 1 . . . A 714 A C4' . 25997 1 183 . 1 1 22 22 A C5' C 13 68.32 0 . 1 . . . A 714 A C5' . 25997 1 184 . 1 1 22 22 A C8 C 13 141.39 0 . 1 . . . A 714 A C8 . 25997 1 185 . 1 1 23 23 U H1' H 1 5.85 0 . 1 . . . A 715 U H1' . 25997 1 186 . 1 1 23 23 U H2' H 1 4.68 0 . 1 . . . A 715 U H2' . 25997 1 187 . 1 1 23 23 U H5 H 1 5.20 0 . 1 . . . A 715 U H5 . 25997 1 188 . 1 1 23 23 U H6 H 1 7.74 0 . 1 . . . A 715 U H6 . 25997 1 189 . 1 1 23 23 U C1' C 13 93.26 0 . 1 . . . A 715 U C1' . 25997 1 190 . 1 1 23 23 U C2' C 13 75.20 0 . 1 . . . A 715 U C2' . 25997 1 191 . 1 1 23 23 U C5 C 13 103.62 0 . 1 . . . A 715 U C5 . 25997 1 192 . 1 1 23 23 U C6 C 13 142.52 0 . 1 . . . A 715 U C6 . 25997 1 193 . 1 1 24 24 G H1' H 1 5.93 0 . 1 . . . A 716 G H1' . 25997 1 194 . 1 1 24 24 G H2' H 1 4.66 0 . 1 . . . A 716 G H2' . 25997 1 195 . 1 1 24 24 G H8 H 1 7.76 0 . 1 . . . A 716 G H8 . 25997 1 196 . 1 1 24 24 G C1' C 13 92.47 0 . 1 . . . A 716 G C1' . 25997 1 197 . 1 1 24 24 G C2' C 13 75.60 0 . 1 . . . A 716 G C2' . 25997 1 198 . 1 1 24 24 G C8 C 13 136.48 0 . 1 . . . A 716 G C8 . 25997 1 199 . 1 1 25 25 G H1' H 1 5.72 0 . 1 . . . A 717 G H1' . 25997 1 200 . 1 1 25 25 G H2' H 1 4.47 0 . 1 . . . A 717 G H2' . 25997 1 201 . 1 1 25 25 G H8 H 1 7.20 0 . 1 . . . A 717 G H8 . 25997 1 202 . 1 1 25 25 G C1' C 13 92.71 0 . 1 . . . A 717 G C1' . 25997 1 203 . 1 1 25 25 G C2' C 13 72.99 0 . 1 . . . A 717 G C2' . 25997 1 204 . 1 1 25 25 G C8 C 13 135.89 0 . 1 . . . A 717 G C8 . 25997 1 205 . 1 1 26 26 G H1' H 1 5.74 0 . 1 . . . A 718 G H1' . 25997 1 206 . 1 1 26 26 G H2' H 1 4.61 0 . 1 . . . A 718 G H2' . 25997 1 207 . 1 1 26 26 G H8 H 1 7.11 0 . 1 . . . A 718 G H8 . 25997 1 208 . 1 1 26 26 G C1' C 13 92.98 0 . 1 . . . A 718 G C1' . 25997 1 209 . 1 1 26 26 G C2' C 13 75.55 0 . 1 . . . A 718 G C2' . 25997 1 210 . 1 1 26 26 G C8 C 13 136.27 0 . 1 . . . A 718 G C8 . 25997 1 211 . 1 1 27 27 A H1' H 1 6.05 0 . 1 . . . A 719 A H1' . 25997 1 212 . 1 1 27 27 A H2 H 1 8.16 0 . 1 . . . A 719 A H2 . 25997 1 213 . 1 1 27 27 A H2' H 1 4.62 0 . 1 . . . A 719 A H2' . 25997 1 214 . 1 1 27 27 A H8 H 1 7.85 0 . 1 . . . A 719 A H8 . 25997 1 215 . 1 1 27 27 A C1' C 13 93.27 0 . 1 . . . A 719 A C1' . 25997 1 216 . 1 1 27 27 A C2' C 13 75.80 0 . 1 . . . A 719 A C2' . 25997 1 217 . 1 1 27 27 A C8 C 13 140.76 0 . 1 . . . A 719 A C8 . 25997 1 218 . 1 1 28 28 U H1' H 1 5.40 0 . 1 . . . A 720 U H1' . 25997 1 219 . 1 1 28 28 U H2' H 1 4.32 0 . 1 . . . A 720 U H2' . 25997 1 220 . 1 1 28 28 U H5 H 1 5.33 0 . 1 . . . A 720 U H5 . 25997 1 221 . 1 1 28 28 U H6 H 1 7.58 0 . 1 . . . A 720 U H6 . 25997 1 222 . 1 1 28 28 U C1' C 13 93.40 0 . 1 . . . A 720 U C1' . 25997 1 223 . 1 1 28 28 U C2' C 13 75.48 0 . 1 . . . A 720 U C2' . 25997 1 224 . 1 1 28 28 U C5 C 13 103.43 0 . 1 . . . A 720 U C5 . 25997 1 225 . 1 1 28 28 U C6 C 13 141.20 0 . 1 . . . A 720 U C6 . 25997 1 226 . 1 1 29 29 C H1' H 1 5.59 0 . 1 . . . A 721 C H1' . 25997 1 227 . 1 1 29 29 C H2' H 1 4.42 0 . 1 . . . A 721 C H2' . 25997 1 228 . 1 1 29 29 C H5 H 1 5.63 0 . 1 . . . A 721 C H5 . 25997 1 229 . 1 1 29 29 C H6 H 1 7.79 0 . 1 . . . A 721 C H6 . 25997 1 230 . 1 1 29 29 C C1' C 13 93.40 0 . 1 . . . A 721 C C1' . 25997 1 231 . 1 1 29 29 C C2' C 13 75.61 0 . 1 . . . A 721 C C2' . 25997 1 232 . 1 1 29 29 C C5 C 13 97.97 0 . 1 . . . A 721 C C5 . 25997 1 233 . 1 1 29 29 C C6 C 13 141.82 0 . 1 . . . A 721 C C6 . 25997 1 234 . 1 1 30 30 U H1' H 1 5.52 0 . 1 . . . A 722 U H1' . 25997 1 235 . 1 1 30 30 U H2' H 1 4.14 0 . 1 . . . A 722 U H2' . 25997 1 236 . 1 1 30 30 U H5 H 1 5.57 0 . 1 . . . A 722 U H5 . 25997 1 237 . 1 1 30 30 U H6 H 1 7.65 0 . 1 . . . A 722 U H6 . 25997 1 238 . 1 1 30 30 U C1' C 13 93.51 0 . 1 . . . A 722 U C1' . 25997 1 239 . 1 1 30 30 U C2' C 13 75.51 0 . 1 . . . A 722 U C2' . 25997 1 240 . 1 1 30 30 U C5 C 13 104.70 0 . 1 . . . A 722 U C5 . 25997 1 241 . 1 1 30 30 U C6 C 13 141.47 0 . 1 . . . A 722 U C6 . 25997 1 242 . 1 1 31 31 G H1' H 1 5.56 0 . 1 . . . A 723 G H1' . 25997 1 243 . 1 1 31 31 G H2' H 1 4.54 0 . 1 . . . A 723 G H2' . 25997 1 244 . 1 1 31 31 G H3' H 1 4.79 0 . 1 . . . A 723 G H3' . 25997 1 245 . 1 1 31 31 G H8 H 1 7.83 0 . 1 . . . A 723 G H8 . 25997 1 246 . 1 1 31 31 G C1' C 13 90.02 0 . 1 . . . A 723 G C1' . 25997 1 247 . 1 1 31 31 G C2' C 13 75.97 0 . 1 . . . A 723 G C2' . 25997 1 248 . 1 1 31 31 G C3' C 13 75.64 0 . 1 . . . A 723 G C3' . 25997 1 249 . 1 1 31 31 G C8 C 13 138.67 0 . 1 . . . A 723 G C8 . 25997 1 250 . 1 1 32 32 A H1' H 1 5.97 0 . 1 . . . A 724 A H1' . 25997 1 251 . 1 1 32 32 A H2 H 1 7.87 0 . 1 . . . A 724 A H2 . 25997 1 252 . 1 1 32 32 A H2' H 1 4.75 0 . 1 . . . A 724 A H2' . 25997 1 253 . 1 1 32 32 A H8 H 1 8.29 0 . 1 . . . A 724 A H8 . 25997 1 254 . 1 1 32 32 A C1' C 13 90.11 0 . 1 . . . A 724 A C1' . 25997 1 255 . 1 1 32 32 A C2 C 13 154.91 0 . 1 . . . A 724 A C2 . 25997 1 256 . 1 1 32 32 A C2' C 13 76.16 0 . 1 . . . A 724 A C2' . 25997 1 257 . 1 1 32 32 A C8 C 13 141.55 0 . 1 . . . A 724 A C8 . 25997 1 258 . 1 1 33 33 U H1' H 1 5.61 0 . 1 . . . A 725 U H1' . 25997 1 259 . 1 1 33 33 U H2' H 1 4.59 0 . 1 . . . A 725 U H2' . 25997 1 260 . 1 1 33 33 U H5 H 1 5.80 0 . 1 . . . A 725 U H5 . 25997 1 261 . 1 1 33 33 U H6 H 1 7.91 0 . 1 . . . A 725 U H6 . 25997 1 262 . 1 1 33 33 U C1' C 13 92.21 0 . 1 . . . A 725 U C1' . 25997 1 263 . 1 1 33 33 U C2' C 13 75.13 0 . 1 . . . A 725 U C2' . 25997 1 264 . 1 1 33 33 U C5 C 13 104.55 0 . 1 . . . A 725 U C5 . 25997 1 265 . 1 1 33 33 U C6 C 13 143.11 0 . 1 . . . A 725 U C6 . 25997 1 266 . 1 1 34 34 C H1' H 1 5.53 0 . 1 . . . A 726 C H1' . 25997 1 267 . 1 1 34 34 C H2' H 1 4.42 0 . 1 . . . A 726 C H2' . 25997 1 268 . 1 1 34 34 C H5 H 1 5.78 0 . 1 . . . A 726 C H5 . 25997 1 269 . 1 1 34 34 C H6 H 1 7.85 0 . 1 . . . A 726 C H6 . 25997 1 270 . 1 1 34 34 C C1' C 13 94.42 0 . 1 . . . A 726 C C1' . 25997 1 271 . 1 1 34 34 C C2' C 13 75.36 0 . 1 . . . A 726 C C2' . 25997 1 272 . 1 1 34 34 C C5 C 13 97.92 0 . 1 . . . A 726 C C5 . 25997 1 273 . 1 1 34 34 C C6 C 13 142.12 0 . 1 . . . A 726 C C6 . 25997 1 274 . 1 1 35 35 U H1' H 1 5.50 0 . 1 . . . A 727 U H1' . 25997 1 275 . 1 1 35 35 U H2' H 1 4.60 0 . 1 . . . A 727 U H2' . 25997 1 276 . 1 1 35 35 U H5 H 1 5.44 0 . 1 . . . A 727 U H5 . 25997 1 277 . 1 1 35 35 U H6 H 1 7.90 0 . 1 . . . A 727 U H6 . 25997 1 278 . 1 1 35 35 U C1' C 13 93.51 0 . 1 . . . A 727 U C1' . 25997 1 279 . 1 1 35 35 U C2' C 13 75.27 0 . 1 . . . A 727 U C2' . 25997 1 280 . 1 1 35 35 U C5 C 13 103.63 0 . 1 . . . A 727 U C5 . 25997 1 281 . 1 1 35 35 U C6 C 13 141.84 0 . 1 . . . A 727 U C6 . 25997 1 282 . 1 1 36 36 G H1' H 1 5.82 0 . 1 . . . A 728 G H1' . 25997 1 283 . 1 1 36 36 G H2' H 1 4.73 0 . 1 . . . A 728 G H2' . 25997 1 284 . 1 1 36 36 G H8 H 1 7.81 0 . 1 . . . A 728 G H8 . 25997 1 285 . 1 1 36 36 G C1' C 13 92.58 0 . 1 . . . A 728 G C1' . 25997 1 286 . 1 1 36 36 G C8 C 13 136.42 0 . 1 . . . A 728 G C8 . 25997 1 287 . 1 1 37 37 C H1' H 1 5.49 0 . 1 . . . A 729 C H1' . 25997 1 288 . 1 1 37 37 C H2' H 1 4.36 0 . 1 . . . A 729 C H2' . 25997 1 289 . 1 1 37 37 C H5 H 1 5.25 0 . 1 . . . A 729 C H5 . 25997 1 290 . 1 1 37 37 C H6 H 1 7.71 0 . 1 . . . A 729 C H6 . 25997 1 291 . 1 1 37 37 C C1' C 13 93.82 0 . 1 . . . A 729 C C1' . 25997 1 292 . 1 1 37 37 C C5 C 13 96.97 0 . 1 . . . A 729 C C5 . 25997 1 293 . 1 1 37 37 C C6 C 13 141.11 0 . 1 . . . A 729 C C6 . 25997 1 294 . 1 1 38 38 C H5 H 1 5.50 0 . 1 . . . A 730 C H5 . 25997 1 295 . 1 1 38 38 C H6 H 1 7.79 0 . 1 . . . A 730 C H6 . 25997 1 296 . 1 1 38 38 C C5 C 13 97.70 0 . 1 . . . A 730 C C5 . 25997 1 297 . 1 1 38 38 C C6 C 13 141.40 0 . 1 . . . A 730 C C6 . 25997 1 stop_ save_