# 1 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph"
;fhsqcf3gpph
;avance-version (07/04/04)
;2D H-1/X correlation via double inept transfer
;phase sensitive
;with decoupling during acquisition
;
;S. Mori, C. Abeygunawardana, M. O'Neil-Johnson & P.C.M. van Zijl,
;   J. Magn. Reson. B 108, 94-98 (1995)
;
;$CLASS=HighRes
;$DIM=2D
;$TYPE=
;$SUBTYPE=
;$COMMENT=


# 1 "/opt/topspin/exp/stan/nmr/lists/pp/Avance.incl" 1
;Avance3.incl
;   for AV III
;
;avance-version (07/12/14)
;
;$CLASS=HighRes Incl
;$COMMENT=





























































































































































;$Id: pulseprogram,v 1.1 2021/02/10 23:57:51 bmrbsvc Exp $
# 17 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph" 2

# 1 "/opt/topspin/exp/stan/nmr/lists/pp/Grad.incl" 1
;Grad2.incl  -  include file for Gradient Spectroscopy
;   for 1
;
;avance-version (07/01/17)
;
;$CLASS=HighRes Incl
;$COMMENT=



















define list<gradient> EA=<EA>



;$Id: pulseprogram,v 1.1 2021/02/10 23:57:51 bmrbsvc Exp $
# 18 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph" 2

# 1 "/opt/topspin/exp/stan/nmr/lists/pp/Delay.incl" 1
;Delay.incl  -  include file for commonly used delays
;
;version 00/02/07
;
;$CLASS=HighRes Incl
;$COMMENT=


;general delays

define delay DELTA
define delay DELTA1
define delay DELTA2
define delay DELTA3
define delay DELTA4
define delay DELTA5
define delay DELTA6
define delay DELTA7
define delay DELTA8

define delay TAU
define delay TAU1
define delay TAU2
define delay TAU3
define delay TAU4
define delay TAU5


;delays for centering pulses

define delay CEN_HN1
define delay CEN_HN2
define delay CEN_HN3
define delay CEN_HC1
define delay CEN_HC2
define delay CEN_HC3
define delay CEN_HC4
define delay CEN_HP1
define delay CEN_HP2
define delay CEN_CN1
define delay CEN_CN2
define delay CEN_CN3
define delay CEN_CN4
define delay CEN_CP1
define delay CEN_CP2


;loop counters

define loopcounter COUNTER
define loopcounter SCALEF
define loopcounter FACTOR1
define loopcounter FACTOR2
define loopcounter FACTOR3



;$Id: pulseprogram,v 1.1 2021/02/10 23:57:51 bmrbsvc Exp $
# 19 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph" 2



"p2=p1*2"
"p22=p21*2"
"d11=30m"
"d12=20u"
"d13=4u"
"d26=1s/(cnst4*4)"


"in0=inf1/2"

"d0=3u"


"DELTA=d19-p22/2"
"DELTA1=d26-p16-d16-p27*3-d19*5"
"DELTA2=d26-p16-d16-p27*2-p0-d19*5-8u"
"DELTA4=p21*2/3.1416"


"DELTA3=d0+larger(p2,p14)/2"




"TAU=d26-p16-4u"


# 1 "mc_line 49 file /opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph expanding definition part of mc command before ze"
define delay MCWRK
define delay MCREST
define loopcounter ST1CNT
"ST1CNT = td1 / (2)"
"MCWRK = 0.250000*d1"
"MCREST = d1 - d1"
    dccorr
# 49 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph"
1 ze 
# 1 "mc_line 49 file /opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph expanding definition of mc command after ze"
# 50 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph"
  d11 pl16:f3
# 1 "mc_line 51 file /opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph expanding start label for mc command"
2 MCWRK  * 2 do:f3
LBLSTS1, MCWRK 
LBLF1, MCWRK 
  MCREST
# 52 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph"
3 d12 pl1:f1
  50u setnmr3|0 setnmr0|34|32|33 ctrlgrad 0
  (p1 ph1)
  4u
  p16:gp1
  TAU pl3:f3
  (center (p2 ph1) (p22 ph6):f3 )
  4u
  p16:gp1
  TAU
  (p1 ph2) 
  4u
  p16:gp2
  d16
  (p21 ph3):f3
  DELTA3
  (p22 ph3):f3
  DELTA4
  d0


  (center (p2 ph5) (p14:sp3 ph1):f2 )




  d0
  DELTA4
  (p22 ph4):f3
  DELTA3
  (p21 ph4):f3
  4u
  p16:gp2
  d16
  (p1 ph7) 
  DELTA1
  p16:gp3
  d16 pl18:f1
  p27*0.231 ph8
  d19*2
  p27*0.692 ph8
  d19*2
  p27*1.462 ph8
  DELTA
  (p22 ph1):f3
  DELTA
  p27*1.462 ph9
  d19*2
  p27*0.692 ph9
  d19*2
  p0*0.231 ph9
  4u
  p16:gp3
  d16
  4u setnmr3^0 setnmr0^34^32^33 ctrlgrad 7
  DELTA2 pl16:f3
  go=2 ph31 cpd3:f3
# 1 "mc_line 109 file /opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph expanding mc command in line"
  MCWRK  do:f3 wr #0 if #0 zd ip3  MCWRK  ip6
  lo to LBLSTS1 times 2
  MCWRK id0
  lo to LBLF1 times ST1CNT
  MCWRK
# 110 "/opt/topspin/exp/stan/nmr/lists/pp/fhsqcf3gpph"
exit 
  

ph1=0
ph2=1
ph3=0 2
ph4=0 0 0 0 2 2 2 2
ph5=0 0 2 2
ph6=0
ph7=2
ph8=1
ph9=3
ph31=0 2 0 2 2 0 2 0


;pl1 : f1 channel - power level for pulse (default)
;pl3 : f3 channel - power level for pulse (default)
;pl16: f3 channel - power level for CPD/BB decoupling
;pl18: f1 channel - power level for 3-9-19-pulse (watergate)
;sp3: f2 channel - shaped pulse 180 degree (adiabatic)
;p0 : f1 channel -  90 degree pulse at pl18
;                      use for fine adjustment
;p1 : f1 channel -  90 degree high power pulse
;p2 : f1 channel - 180 degree high power pulse
;p14: f2 channel - 180 degree shaped pulse for inversion (adiabatic)
;p16: homospoil/gradient pulse
;p21: f3 channel -  90 degree high power pulse
;p22: f3 channel - 180 degree high power pulse
;p27: f1 channel -  90 degree pulse at pl18
;d0 : incremented delay (2D)                         [3 usec]
;d1 : relaxation delay; 1-5 * T1
;d11: delay for disk I/O                             [30 msec]
;d12: delay for power switching                      [20 usec]
;d13: short delay                                    [4 usec]
;d16: delay for homospoil/gradient recovery
;d19: delay for binomial water suppression
;     d19 = (1/(2*d)), d = distance of next null (in Hz)
;d26 : 1/(4J(YH))
;cnst4: = J(YH)
;inf1: 1/SW(X) = 2 * DW(X)
;in0: 1/(2 * SW(X)) = DW(X)
;nd0: 2
;NS: 8 * n
;DS: 16
;td1: number of experiments
;FnMODE: States-TPPI (or TPPI)
;cpd3: decoupling according to sequence defined by cpdprg3
;pcpd3: f3 channel - 90 degree pulse for decoupling sequence


;use gradient ratio:          gp 1 : gp 2 : gp 3
;                               50 :   80 :   30

;for z-only gradients:
;gpz1: 50%
;gpz2: 80%
;gpz3: 30%


;for magic angle gradients (MAG) with xyz-gradientsystem use instead:

;gpx1: 20%
;gpx2: 10%
;gpx3: 15%*k

;gpy1: 40%
;gpy2: 0%
;gpy3: 15%*k

;gpz1: 20%
;gpz2: 0%
;gpz3: 15%

;   with k = calibration constant from 1D magic angle gradient
;      calibration

;use gradient files:   
;gpnam1: SINE.100
;gpnam2: SINE.100
;gpnam3: SINE.100


                                          ;preprocessor-flags-start
;1: for C-13 and N-15 labeled samples start experiment with 
;             option -DLABEL_CN (eda: ZGOPTNS)
                                          ;preprocessor-flags-end



;$Id: pulseprogram,v 1.1 2021/02/10 23:57:51 bmrbsvc Exp $