data_18892 ####################### # Entry information # ####################### save_entry_information _Entry.Sf_category entry_information _Entry.Sf_framecode entry_information _Entry.ID 18892 _Entry.Title ; Solution structure of the helix II template boundary element from Tetrahymena telomerase RNA ; _Entry.Type macromolecule _Entry.Version_type original _Entry.Submission_date 2012-12-11 _Entry.Accession_date 2012-12-11 _Entry.Last_release_date 2013-01-24 _Entry.Original_release_date 2013-01-24 _Entry.Origination author _Entry.NMR_STAR_version 3.1.1.61 _Entry.Original_NMR_STAR_version 3.1 _Entry.Experimental_method NMR _Entry.Experimental_method_subtype SOLUTION _Entry.Details . _Entry.BMRB_internal_directory_name . loop_ _Entry_author.Ordinal _Entry_author.Given_name _Entry_author.Family_name _Entry_author.First_initial _Entry_author.Middle_initials _Entry_author.Family_title _Entry_author.Entry_ID 1 Darian Cash . D. . 18892 2 Rebecca Richards . J. . 18892 3 Carla Theimer . A. . 18892 4 David Finger . L. . 18892 5 Juli Feigon . . . 18892 stop_ loop_ _SG_project.SG_project_ID _SG_project.Project_name _SG_project.Full_name_of_center _SG_project.Initial_of_center _SG_project.Entry_ID 1 'not applicable' 'not applicable' . 18892 stop_ loop_ _Struct_keywords.Keywords _Struct_keywords.Text _Struct_keywords.Entry_ID biomolecular . 18892 ciliate . 18892 genetic . 18892 holoenzyme . 18892 Models . 18892 Molecular . 18892 'nuclear magnetic resonance' . 18892 'nucleic acid' . 18892 protein . 18892 'protozoan proteins' . 18892 'reverse transcriptase' . 18892 RNA . 18892 secondary . 18892 structure . 18892 telomerase . 18892 template . 18892 tertiary . 18892 'tetrahymena thermophila' . 18892 stop_ loop_ _Data_set.Type _Data_set.Count _Data_set.Entry_ID assigned_chemical_shifts 1 18892 stop_ loop_ _Datum.Type _Datum.Count _Datum.Entry_ID '13C chemical shifts' 151 18892 '15N chemical shifts' 34 18892 '1H chemical shifts' 184 18892 stop_ loop_ _Release.Release_number _Release.Format_type _Release.Format_version _Release.Date _Release.Submission_date _Release.Type _Release.Author _Release.Detail _Release.Entry_ID 1 . . 2013-01-24 2012-12-11 original author . 18892 stop_ loop_ _Related_entries.Database_name _Related_entries.Database_accession_code _Related_entries.Relationship _Related_entries.Entry_ID BMRB 18891 'Solution structure of the Tetrahymena telomerase RNA stem IV terminal loop' 18892 PDB 2M22 'BMRB Entry Tracking System' 18892 stop_ save_ ############### # Citations # ############### save_entry_citation _Citation.Sf_category citations _Citation.Sf_framecode entry_citation _Citation.Entry_ID 18892 _Citation.ID 1 _Citation.Class 'entry citation' _Citation.CAS_abstract_code . _Citation.MEDLINE_UI_code . _Citation.DOI . _Citation.PubMed_ID 16452301 _Citation.Full_citation . _Citation.Title 'Solution structure of the helix II template boundary element from Tetrahymena telomerase RNA' _Citation.Status published _Citation.Type journal _Citation.Journal_abbrev 'Nucleic Acids Res.' _Citation.Journal_name_full . _Citation.Journal_volume 34 _Citation.Journal_issue 3 _Citation.Journal_ASTM . _Citation.Journal_ISSN . _Citation.Journal_CSD . _Citation.Book_title . _Citation.Book_chapter_title . _Citation.Book_volume . _Citation.Book_series . _Citation.Book_publisher . _Citation.Book_publisher_city . _Citation.Book_ISBN . _Citation.Conference_title . _Citation.Conference_site . _Citation.Conference_state_province . _Citation.Conference_country . _Citation.Conference_start_date . _Citation.Conference_end_date . _Citation.Conference_abstract_number . _Citation.Thesis_institution . _Citation.Thesis_institution_city . _Citation.Thesis_institution_country . _Citation.WWW_URL . _Citation.Page_first 816 _Citation.Page_last 825 _Citation.Year 2006 _Citation.Details . loop_ _Citation_author.Ordinal _Citation_author.Given_name _Citation_author.Family_name _Citation_author.First_initial _Citation_author.Middle_initials _Citation_author.Family_title _Citation_author.Entry_ID _Citation_author.Citation_ID 1 Rebecca Richards . J. . 18892 1 2 Carla Theimer . A. . 18892 1 3 David Finger . L. . 18892 1 4 Juli Feigon . . . 18892 1 stop_ save_ ############################################# # Molecular system (assembly) description # ############################################# save_assembly _Assembly.Sf_category assembly _Assembly.Sf_framecode assembly _Assembly.Entry_ID 18892 _Assembly.ID 1 _Assembly.Name 'helix II template boundary element from Tetrahymena telomerase RNA' _Assembly.BMRB_code . _Assembly.Number_of_components 1 _Assembly.Organic_ligands . _Assembly.Metal_ions . _Assembly.Non_standard_bonds . _Assembly.Ambiguous_conformational_states . _Assembly.Ambiguous_chem_comp_sites . _Assembly.Molecules_in_chemical_exchange . _Assembly.Paramagnetic no _Assembly.Thiol_state . _Assembly.Molecular_mass . _Assembly.Enzyme_commission_number . _Assembly.Details . _Assembly.DB_query_date . _Assembly.DB_query_revised_last_date . loop_ _Entity_assembly.ID _Entity_assembly.Entity_assembly_name _Entity_assembly.Entity_ID _Entity_assembly.Entity_label _Entity_assembly.Asym_ID _Entity_assembly.PDB_chain_ID _Entity_assembly.Experimental_data_reported _Entity_assembly.Physical_state _Entity_assembly.Conformational_isomer _Entity_assembly.Chemical_exchange_state _Entity_assembly.Magnetic_equivalence_group_code _Entity_assembly.Role _Entity_assembly.Details _Entity_assembly.Entry_ID _Entity_assembly.Assembly_ID 1 helixII_telo_RNA 1 $helixII_telo_RNA A . yes native no no . . . 18892 1 stop_ save_ #################################### # Biological polymers and ligands # #################################### save_helixII_telo_RNA _Entity.Sf_category entity _Entity.Sf_framecode helixII_telo_RNA _Entity.Entry_ID 18892 _Entity.ID 1 _Entity.BMRB_code . _Entity.Name helixII_telo_RNA _Entity.Type polymer _Entity.Polymer_common_type . _Entity.Polymer_type polyribonucleotide _Entity.Polymer_type_details . _Entity.Polymer_strand_ID A _Entity.Polymer_seq_one_letter_code_can . _Entity.Polymer_seq_one_letter_code ; GGCAGAUCUGUAAUAGAACU GCC ; _Entity.Target_identifier . _Entity.Polymer_author_defined_seq . _Entity.Polymer_author_seq_details . _Entity.Ambiguous_conformational_states no _Entity.Ambiguous_chem_comp_sites no _Entity.Nstd_monomer no _Entity.Nstd_chirality no _Entity.Nstd_linkage no _Entity.Nonpolymer_comp_ID . _Entity.Nonpolymer_comp_label . _Entity.Number_of_monomers 23 _Entity.Number_of_nonpolymer_components . _Entity.Paramagnetic no _Entity.Thiol_state 'not present' _Entity.Src_method syn _Entity.Parent_entity_ID . _Entity.Fragment . _Entity.Mutation . _Entity.EC_number . _Entity.Calc_isoelectric_point . _Entity.Formula_weight 7387.508 _Entity.Formula_weight_exptl . _Entity.Formula_weight_exptl_meth . _Entity.Details . _Entity.DB_query_date . _Entity.DB_query_revised_last_date . loop_ _Entity_comp_index.ID _Entity_comp_index.Auth_seq_ID _Entity_comp_index.Comp_ID _Entity_comp_index.Comp_label _Entity_comp_index.Entry_ID _Entity_comp_index.Entity_ID 1 . G . 18892 1 2 . G . 18892 1 3 . C . 18892 1 4 . A . 18892 1 5 . G . 18892 1 6 . A . 18892 1 7 . U . 18892 1 8 . C . 18892 1 9 . U . 18892 1 10 . G . 18892 1 11 . U . 18892 1 12 . A . 18892 1 13 . A . 18892 1 14 . U . 18892 1 15 . A . 18892 1 16 . G . 18892 1 17 . A . 18892 1 18 . A . 18892 1 19 . C . 18892 1 20 . U . 18892 1 21 . G . 18892 1 22 . C . 18892 1 23 . C . 18892 1 stop_ loop_ _Entity_poly_seq.Hetero _Entity_poly_seq.Mon_ID _Entity_poly_seq.Num _Entity_poly_seq.Comp_index_ID _Entity_poly_seq.Entry_ID _Entity_poly_seq.Entity_ID . G 1 1 18892 1 . G 2 2 18892 1 . C 3 3 18892 1 . A 4 4 18892 1 . G 5 5 18892 1 . A 6 6 18892 1 . U 7 7 18892 1 . C 8 8 18892 1 . U 9 9 18892 1 . G 10 10 18892 1 . U 11 11 18892 1 . A 12 12 18892 1 . A 13 13 18892 1 . U 14 14 18892 1 . A 15 15 18892 1 . G 16 16 18892 1 . A 17 17 18892 1 . A 18 18 18892 1 . C 19 19 18892 1 . U 20 20 18892 1 . G 21 21 18892 1 . C 22 22 18892 1 . C 23 23 18892 1 stop_ save_ #################### # Natural source # #################### save_natural_source _Entity_natural_src_list.Sf_category natural_source _Entity_natural_src_list.Sf_framecode natural_source _Entity_natural_src_list.Entry_ID 18892 _Entity_natural_src_list.ID 1 loop_ _Entity_natural_src.ID _Entity_natural_src.Entity_ID _Entity_natural_src.Entity_label _Entity_natural_src.Entity_chimera_segment_ID _Entity_natural_src.NCBI_taxonomy_ID _Entity_natural_src.Type _Entity_natural_src.Common _Entity_natural_src.Organism_name_scientific _Entity_natural_src.Organism_name_common _Entity_natural_src.Organism_acronym _Entity_natural_src.ICTVdb_decimal_code _Entity_natural_src.Superkingdom _Entity_natural_src.Kingdom _Entity_natural_src.Genus _Entity_natural_src.Species _Entity_natural_src.Strain _Entity_natural_src.Variant _Entity_natural_src.Subvariant _Entity_natural_src.Organ _Entity_natural_src.Tissue _Entity_natural_src.Tissue_fraction _Entity_natural_src.Cell_line _Entity_natural_src.Cell_type _Entity_natural_src.ATCC_number _Entity_natural_src.Organelle _Entity_natural_src.Cellular_location _Entity_natural_src.Fragment _Entity_natural_src.Fraction _Entity_natural_src.Secretion _Entity_natural_src.Plasmid _Entity_natural_src.Plasmid_details _Entity_natural_src.Gene_mnemonic _Entity_natural_src.Dev_stage _Entity_natural_src.Details _Entity_natural_src.Citation_ID _Entity_natural_src.Citation_label _Entity_natural_src.Entry_ID _Entity_natural_src.Entity_natural_src_list_ID 1 1 $helixII_telo_RNA . 5911 organism . 'tetrahymena thermophila' 'tetrahymena thermophila' . . Eukaryota . tetrahymena thermophila . . . . . . . . . . . . . . . . . . . . . 18892 1 stop_ save_ ######################### # Experimental source # ######################### save_experimental_source _Entity_experimental_src_list.Sf_category experimental_source _Entity_experimental_src_list.Sf_framecode experimental_source _Entity_experimental_src_list.Entry_ID 18892 _Entity_experimental_src_list.ID 1 loop_ _Entity_experimental_src.ID _Entity_experimental_src.Entity_ID _Entity_experimental_src.Entity_label _Entity_experimental_src.Entity_chimera_segment_ID _Entity_experimental_src.Production_method _Entity_experimental_src.Host_org_scientific_name _Entity_experimental_src.Host_org_name_common _Entity_experimental_src.Host_org_details _Entity_experimental_src.Host_org_NCBI_taxonomy_ID _Entity_experimental_src.Host_org_genus _Entity_experimental_src.Host_org_species _Entity_experimental_src.Host_org_strain _Entity_experimental_src.Host_org_variant _Entity_experimental_src.Host_org_subvariant _Entity_experimental_src.Host_org_organ _Entity_experimental_src.Host_org_tissue _Entity_experimental_src.Host_org_tissue_fraction _Entity_experimental_src.Host_org_cell_line _Entity_experimental_src.Host_org_cell_type _Entity_experimental_src.Host_org_cellular_location _Entity_experimental_src.Host_org_organelle _Entity_experimental_src.Host_org_gene _Entity_experimental_src.Host_org_culture_collection _Entity_experimental_src.Host_org_ATCC_number _Entity_experimental_src.Vector_type _Entity_experimental_src.PDBview_host_org_vector_name _Entity_experimental_src.PDBview_plasmid_name _Entity_experimental_src.Vector_name _Entity_experimental_src.Vector_details _Entity_experimental_src.Vendor_name _Entity_experimental_src.Host_org_dev_stage _Entity_experimental_src.Details _Entity_experimental_src.Citation_ID _Entity_experimental_src.Citation_label _Entity_experimental_src.Entry_ID _Entity_experimental_src.Entity_experimental_src_list_ID 1 1 $helixII_telo_RNA . 'enzymatic synthesis' n/a . . . . . . . . . . . . . . . . . . . . . . . . . 'in vitro transcription using T7 polymerase' . . 18892 1 stop_ save_ ##################################### # Sample contents and methodology # ##################################### ######################## # Sample description # ######################## save_sample_1 _Sample.Sf_category sample _Sample.Sf_framecode sample_1 _Sample.Entry_ID 18892 _Sample.ID 1 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O or 100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 helixII_telo_RNA unlabeled . . 1 $helixII_telo_RNA . . . 0.6 1.0 mM . . . . 18892 1 2 'sodium phosphate' 'natural abundance' . . . . . . 10 . . mM . . . . 18892 1 3 'potassium chloride' 'natural abundance' . . . . . . 30 . . mM . . . . 18892 1 4 EDTA 'natural abundance' . . . . . . 50 . . uM . . . . 18892 1 5 'sodium azide' 'natural abundance' . . . . . . 0.2 . . % . . . . 18892 1 6 H2O 'natural abundance' . . . . . . 90 . . % . . . . 18892 1 7 D2O 'natural abundance' . . . . . . 10 . . % . . . . 18892 1 stop_ save_ save_sample_2 _Sample.Sf_category sample _Sample.Sf_framecode sample_2 _Sample.Entry_ID 18892 _Sample.ID 2 _Sample.Type solution _Sample.Sub_type . _Sample.Details . _Sample.Aggregate_sample_number . _Sample.Solvent_system '90% H2O/10% D2O or 100% D2O' _Sample.Preparation_date . _Sample.Preparation_expiration_date . _Sample.Polycrystallization_protocol . _Sample.Single_crystal_protocol . _Sample.Crystal_grow_apparatus . _Sample.Crystal_grow_atmosphere . _Sample.Crystal_grow_details . _Sample.Crystal_grow_method . _Sample.Crystal_grow_method_cit_ID . _Sample.Crystal_grow_pH . _Sample.Crystal_grow_pH_range . _Sample.Crystal_grow_pressure . _Sample.Crystal_grow_pressure_esd . _Sample.Crystal_grow_seeding . _Sample.Crystal_grow_seeding_cit_ID . _Sample.Crystal_grow_temp . _Sample.Crystal_grow_temp_details . _Sample.Crystal_grow_temp_esd . _Sample.Crystal_grow_time . _Sample.Oriented_sample_prep_protocol . _Sample.Lyophilization_cryo_protectant . _Sample.Storage_protocol . loop_ _Sample_component.ID _Sample_component.Mol_common_name _Sample_component.Isotopic_labeling _Sample_component.Assembly_ID _Sample_component.Assembly_label _Sample_component.Entity_ID _Sample_component.Entity_label _Sample_component.Product_ID _Sample_component.Type _Sample_component.Concentration_val _Sample_component.Concentration_val_min _Sample_component.Concentration_val_max _Sample_component.Concentration_val_units _Sample_component.Concentration_val_err _Sample_component.Vendor _Sample_component.Vendor_product_name _Sample_component.Vendor_product_code _Sample_component.Entry_ID _Sample_component.Sample_ID 1 helixII_telo_RNA '13C,15N uniformly labelled' . . 1 $helixII_telo_RNA . . . 0.6 1.0 mM . . . . 18892 2 2 'sodium phosphate' 'natural abundance' . . . . . . 10 . . mM . . . . 18892 2 3 'potassium chloride' 'natural abundance' . . . . . . 30 . . mM . . . . 18892 2 4 EDTA 'natural abundance' . . . . . . 50 . . uM . . . . 18892 2 5 'sodium azide' 'natural abundance' . . . . . . 0.2 . . % . . . . 18892 2 6 H2O 'natural abundance' . . . . . . 90 . . % . . . . 18892 2 7 D2O 'natural abundance' . . . . . . 10 . . % . . . . 18892 2 stop_ save_ ####################### # Sample conditions # ####################### save_sample_conditions_1 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_1 _Sample_condition_list.Entry_ID 18892 _Sample_condition_list.ID 1 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 30 . mM 18892 1 pH 6.3 . pH 18892 1 pressure 1 . atm 18892 1 temperature 298 . K 18892 1 stop_ save_ save_sample_conditions_2 _Sample_condition_list.Sf_category sample_conditions _Sample_condition_list.Sf_framecode sample_conditions_2 _Sample_condition_list.Entry_ID 18892 _Sample_condition_list.ID 2 _Sample_condition_list.Details . loop_ _Sample_condition_variable.Type _Sample_condition_variable.Val _Sample_condition_variable.Val_err _Sample_condition_variable.Val_units _Sample_condition_variable.Entry_ID _Sample_condition_variable.Sample_condition_list_ID 'ionic strength' 30 . mM 18892 2 pH 6.3 . pH 18892 2 pressure 1 . atm 18892 2 temperature 283 . K 18892 2 stop_ save_ ############################ # Computer software used # ############################ save_X-PLOR_NIH _Software.Sf_category software _Software.Sf_framecode X-PLOR_NIH _Software.Entry_ID 18892 _Software.ID 1 _Software.Name 'X-PLOR NIH' _Software.Version 2.9.8 _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Schwieters, Kuszewski, Tjandra and Clore' . . 18892 1 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID refinement 18892 1 'structure solution' 18892 1 stop_ save_ save_SPARKY _Software.Sf_category software _Software.Sf_framecode SPARKY _Software.Entry_ID 18892 _Software.ID 2 _Software.Name SPARKY _Software.Version . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID Goddard . . 18892 2 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID 'data analysis' 18892 2 'peak picking' 18892 2 stop_ save_ save_xwinnmr _Software.Sf_category software _Software.Sf_framecode xwinnmr _Software.Entry_ID 18892 _Software.ID 3 _Software.Name xwinnmr _Software.Version . _Software.Details . loop_ _Vendor.Name _Vendor.Address _Vendor.Electronic_address _Vendor.Entry_ID _Vendor.Software_ID 'Bruker Biospin' . . 18892 3 stop_ loop_ _Task.Task _Task.Entry_ID _Task.Software_ID collection 18892 3 processing 18892 3 stop_ save_ ######################### # Experimental detail # ######################### ################################## # NMR Spectrometer definitions # ################################## save_spectrometer_1 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_1 _NMR_spectrometer.Entry_ID 18892 _NMR_spectrometer.ID 1 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model Avance _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 800 save_ save_spectrometer_2 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_2 _NMR_spectrometer.Entry_ID 18892 _NMR_spectrometer.ID 2 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DRX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 600 save_ save_spectrometer_3 _NMR_spectrometer.Sf_category NMR_spectrometer _NMR_spectrometer.Sf_framecode spectrometer_3 _NMR_spectrometer.Entry_ID 18892 _NMR_spectrometer.ID 3 _NMR_spectrometer.Details . _NMR_spectrometer.Manufacturer Bruker _NMR_spectrometer.Model DRX _NMR_spectrometer.Serial_number . _NMR_spectrometer.Field_strength 500 save_ save_NMR_spectrometer_list _NMR_spectrometer_list.Sf_category NMR_spectrometer_list _NMR_spectrometer_list.Sf_framecode NMR_spectrometer_list _NMR_spectrometer_list.Entry_ID 18892 _NMR_spectrometer_list.ID 1 loop_ _NMR_spectrometer_view.ID _NMR_spectrometer_view.Name _NMR_spectrometer_view.Manufacturer _NMR_spectrometer_view.Model _NMR_spectrometer_view.Serial_number _NMR_spectrometer_view.Field_strength _NMR_spectrometer_view.Details _NMR_spectrometer_view.Citation_ID _NMR_spectrometer_view.Citation_label _NMR_spectrometer_view.Entry_ID _NMR_spectrometer_view.NMR_spectrometer_list_ID 1 spectrometer_1 Bruker Avance . 800 . . . 18892 1 2 spectrometer_2 Bruker DRX . 600 . . . 18892 1 3 spectrometer_3 Bruker DRX . 500 . . . 18892 1 stop_ save_ ############################# # NMR applied experiments # ############################# save_experiment_list _Experiment_list.Sf_category experiment_list _Experiment_list.Sf_framecode experiment_list _Experiment_list.Entry_ID 18892 _Experiment_list.ID 1 _Experiment_list.Details . loop_ _Experiment.ID _Experiment.Name _Experiment.Raw_data_flag _Experiment.NMR_spec_expt_ID _Experiment.NMR_spec_expt_label _Experiment.MS_expt_ID _Experiment.MS_expt_label _Experiment.SAXS_expt_ID _Experiment.SAXS_expt_label _Experiment.FRET_expt_ID _Experiment.FRET_expt_label _Experiment.EMR_expt_ID _Experiment.EMR_expt_label _Experiment.Sample_ID _Experiment.Sample_label _Experiment.Sample_state _Experiment.Sample_volume _Experiment.Sample_volume_units _Experiment.Sample_condition_list_ID _Experiment.Sample_condition_list_label _Experiment.Sample_spinning_rate _Experiment.Sample_angle _Experiment.NMR_tube_type _Experiment.NMR_spectrometer_ID _Experiment.NMR_spectrometer_label _Experiment.NMR_spectrometer_probe_ID _Experiment.NMR_spectrometer_probe_label _Experiment.NMR_spectral_processing_ID _Experiment.NMR_spectral_processing_label _Experiment.Mass_spectrometer_ID _Experiment.Mass_spectrometer_label _Experiment.Xray_instrument_ID _Experiment.Xray_instrument_label _Experiment.Fluorescence_instrument_ID _Experiment.Fluorescence_instrument_label _Experiment.EMR_instrument_ID _Experiment.EMR_instrument_label _Experiment.Chromatographic_system_ID _Experiment.Chromatographic_system_label _Experiment.Chromatographic_column_ID _Experiment.Chromatographic_column_label _Experiment.Entry_ID _Experiment.Experiment_list_ID 1 '11echo and watergate' no . . . . . . . . . . 1 $sample_1 isotropic . . 1 $sample_conditions_1 . . . . . . . . . . . . . . . . . . . . . 18892 1 2 '2D TOCSY' no . . . . . . . . . . 1 $sample_1 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 18892 1 3 '2D NOESY' no . . . . . . . . . . 1 $sample_1 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 18892 1 4 '2D 15N-HMQC, 2D 15N-CPMG-NOESY, 2D JNN-HNN-COSY' no . . . . . . . . . . 2 $sample_2 isotropic . . 1 $sample_conditions_1 . . . . . . . . . . . . . . . . . . . . . 18892 1 5 '2D 13C-HSQCs' no . . . . . . . . . . 2 $sample_2 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 18892 1 6 '2D HCCH COSY, 3D HCCH-TOCSY' no . . . . . . . . . . 2 $sample_2 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 18892 1 7 '3D 1H,13C HMQCs' no . . . . . . . . . . 2 $sample_2 isotropic . . 2 $sample_conditions_2 . . . . . . . . . . . . . . . . . . . . . 18892 1 stop_ save_ #################### # NMR parameters # #################### ############################## # Assigned chemical shifts # ############################## ################################ # Chemical shift referencing # ################################ save_chemical_shift_reference_1 _Chem_shift_reference.Sf_category chem_shift_reference _Chem_shift_reference.Sf_framecode chemical_shift_reference_1 _Chem_shift_reference.Entry_ID 18892 _Chem_shift_reference.ID 1 _Chem_shift_reference.Details . loop_ _Chem_shift_ref.Atom_type _Chem_shift_ref.Atom_isotope_number _Chem_shift_ref.Mol_common_name _Chem_shift_ref.Atom_group _Chem_shift_ref.Concentration_val _Chem_shift_ref.Concentration_units _Chem_shift_ref.Solvent _Chem_shift_ref.Rank _Chem_shift_ref.Chem_shift_units _Chem_shift_ref.Chem_shift_val _Chem_shift_ref.Ref_method _Chem_shift_ref.Ref_type _Chem_shift_ref.Indirect_shift_ratio _Chem_shift_ref.External_ref_loc _Chem_shift_ref.External_ref_sample_geometry _Chem_shift_ref.External_ref_axis _Chem_shift_ref.Indirect_shift_ratio_cit_ID _Chem_shift_ref.Indirect_shift_ratio_cit_label _Chem_shift_ref.Ref_correction_type _Chem_shift_ref.Correction_val _Chem_shift_ref.Correction_val_cit_ID _Chem_shift_ref.Correction_val_cit_label _Chem_shift_ref.Entry_ID _Chem_shift_ref.Chem_shift_reference_ID C 13 DSS 'methyl protons' . . . . ppm 0.00 na indirect 0.251449530 . . . . . . . . . 18892 1 H 1 DSS 'methyl protons' . . . . ppm 0.00 internal direct 1.000000000 . . . . . . . . . 18892 1 N 15 DSS 'methyl protons' . . . . ppm 0.00 na indirect 0.101329118 . . . . . . . . . 18892 1 stop_ save_ ################################### # Assigned chemical shift lists # ################################### ################################################################### # Chemical Shift Ambiguity Index Value Definitions # # # # The values other than 1 are used for those atoms with different # # chemical shifts that cannot be assigned to stereospecific atoms # # or to specific residues or chains. # # # # Index Value Definition # # # # 1 Unique (including isolated methyl protons, # # geminal atoms, and geminal methyl # # groups with identical chemical shifts) # # (e.g. ILE HD11, HD12, HD13 protons) # # 2 Ambiguity of geminal atoms or geminal methyl # # proton groups (e.g. ASP HB2 and HB3 # # protons, LEU CD1 and CD2 carbons, or # # LEU HD11, HD12, HD13 and HD21, HD22, # # HD23 methyl protons) # # 3 Aromatic atoms on opposite sides of # # symmetrical rings (e.g. TYR HE1 and HE2 # # protons) # # 4 Intraresidue ambiguities (e.g. LYS HG and # # HD protons or TRP HZ2 and HZ3 protons) # # 5 Interresidue ambiguities (LYS 12 vs. LYS 27) # # 6 Intermolecular ambiguities (e.g. ASP 31 CA # # in monomer 1 and ASP 31 CA in monomer 2 # # of an asymmetrical homodimer, duplex # # DNA assignments, or other assignments # # that may apply to atoms in one or more # # molecule in the molecular assembly) # # 9 Ambiguous, specific ambiguity not defined # # # ################################################################### save_assigned_chem_shift_list_1 _Assigned_chem_shift_list.Sf_category assigned_chemical_shifts _Assigned_chem_shift_list.Sf_framecode assigned_chem_shift_list_1 _Assigned_chem_shift_list.Entry_ID 18892 _Assigned_chem_shift_list.ID 1 _Assigned_chem_shift_list.Sample_condition_list_ID 1 _Assigned_chem_shift_list.Sample_condition_list_label $sample_conditions_1 _Assigned_chem_shift_list.Chem_shift_reference_ID 1 _Assigned_chem_shift_list.Chem_shift_reference_label $chemical_shift_reference_1 _Assigned_chem_shift_list.Chem_shift_1H_err . _Assigned_chem_shift_list.Chem_shift_13C_err . _Assigned_chem_shift_list.Chem_shift_15N_err . _Assigned_chem_shift_list.Chem_shift_31P_err . _Assigned_chem_shift_list.Chem_shift_2H_err . _Assigned_chem_shift_list.Chem_shift_19F_err . _Assigned_chem_shift_list.Error_derivation_method . _Assigned_chem_shift_list.Details . _Assigned_chem_shift_list.Text_data_format . _Assigned_chem_shift_list.Text_data . loop_ _Chem_shift_experiment.Experiment_ID _Chem_shift_experiment.Experiment_name _Chem_shift_experiment.Sample_ID _Chem_shift_experiment.Sample_label _Chem_shift_experiment.Sample_state _Chem_shift_experiment.Entry_ID _Chem_shift_experiment.Assigned_chem_shift_list_ID 1 '11echo and watergate' . . . 18892 1 3 '2D NOESY' . . . 18892 1 5 '2D 13C-HSQCs' . . . 18892 1 6 '2D HCCH COSY, 3D HCCH-TOCSY' . . . 18892 1 stop_ loop_ _Atom_chem_shift.ID _Atom_chem_shift.Assembly_atom_ID _Atom_chem_shift.Entity_assembly_ID _Atom_chem_shift.Entity_ID _Atom_chem_shift.Comp_index_ID _Atom_chem_shift.Seq_ID _Atom_chem_shift.Comp_ID _Atom_chem_shift.Atom_ID _Atom_chem_shift.Atom_type _Atom_chem_shift.Atom_isotope_number _Atom_chem_shift.Val _Atom_chem_shift.Val_err _Atom_chem_shift.Assign_fig_of_merit _Atom_chem_shift.Ambiguity_code _Atom_chem_shift.Occupancy _Atom_chem_shift.Resonance_ID _Atom_chem_shift.Auth_entity_assembly_ID _Atom_chem_shift.Auth_asym_ID _Atom_chem_shift.Auth_seq_ID _Atom_chem_shift.Auth_comp_ID _Atom_chem_shift.Auth_atom_ID _Atom_chem_shift.Details _Atom_chem_shift.Entry_ID _Atom_chem_shift.Assigned_chem_shift_list_ID 1 . 1 1 1 1 G H1 H 1 12.982 . . 1 . . . A 1 G H1 . 18892 1 2 . 1 1 1 1 G H1' H 1 5.836 . . 1 . . . A 1 G H1' . 18892 1 3 . 1 1 1 1 G H2' H 1 4.974 . . 1 . . . A 1 G H2' . 18892 1 4 . 1 1 1 1 G H3' H 1 4.754 . . 1 . . . A 1 G H3' . 18892 1 5 . 1 1 1 1 G H4' H 1 4.599 . . 1 . . . A 1 G H4' . 18892 1 6 . 1 1 1 1 G H5' H 1 4.420 . . 2 . . . A 1 G H5' . 18892 1 7 . 1 1 1 1 G H5'' H 1 4.299 . . 2 . . . A 1 G H5'' . 18892 1 8 . 1 1 1 1 G H8 H 1 8.144 . . 1 . . . A 1 G H8 . 18892 1 9 . 1 1 1 1 G C1' C 13 90.591 . . 1 . . . A 1 G C1' . 18892 1 10 . 1 1 1 1 G C2' C 13 74.830 . . 1 . . . A 1 G C2' . 18892 1 11 . 1 1 1 1 G C3' C 13 75.033 . . 1 . . . A 1 G C3' . 18892 1 12 . 1 1 1 1 G C4' C 13 83.695 . . 1 . . . A 1 G C4' . 18892 1 13 . 1 1 1 1 G C5' C 13 67.454 . . 1 . . . A 1 G C5' . 18892 1 14 . 1 1 1 1 G C8 C 13 139.015 . . 1 . . . A 1 G C8 . 18892 1 15 . 1 1 1 1 G N1 N 15 147.034 . . 1 . . . A 1 G N1 . 18892 1 16 . 1 1 2 2 G H1 H 1 13.358 . . 1 . . . A 2 G H1 . 18892 1 17 . 1 1 2 2 G H1' H 1 5.928 . . 1 . . . A 2 G H1' . 18892 1 18 . 1 1 2 2 G H2' H 1 4.617 . . 1 . . . A 2 G H2' . 18892 1 19 . 1 1 2 2 G H3' H 1 4.510 . . 1 . . . A 2 G H3' . 18892 1 20 . 1 1 2 2 G H4' H 1 4.558 . . 1 . . . A 2 G H4' . 18892 1 21 . 1 1 2 2 G H5' H 1 4.348 . . 2 . . . A 2 G H5' . 18892 1 22 . 1 1 2 2 G H5'' H 1 4.166 . . 2 . . . A 2 G H5'' . 18892 1 23 . 1 1 2 2 G H8 H 1 7.644 . . 1 . . . A 2 G H8 . 18892 1 24 . 1 1 2 2 G C1' C 13 92.928 . . 1 . . . A 2 G C1' . 18892 1 25 . 1 1 2 2 G C2' C 13 75.287 . . 1 . . . A 2 G C2' . 18892 1 26 . 1 1 2 2 G C4' C 13 82.378 . . 1 . . . A 2 G C4' . 18892 1 27 . 1 1 2 2 G C5' C 13 67.219 . . 1 . . . A 2 G C5' . 18892 1 28 . 1 1 2 2 G C8 C 13 136.898 . . 1 . . . A 2 G C8 . 18892 1 29 . 1 1 2 2 G N1 N 15 148.085 . . 1 . . . A 2 G N1 . 18892 1 30 . 1 1 3 3 C H1' H 1 5.552 . . 1 . . . A 3 C H1' . 18892 1 31 . 1 1 3 3 C H2' H 1 4.670 . . 1 . . . A 3 C H2' . 18892 1 32 . 1 1 3 3 C H3' H 1 4.574 . . 1 . . . A 3 C H3' . 18892 1 33 . 1 1 3 3 C H4' H 1 4.467 . . 1 . . . A 3 C H4' . 18892 1 34 . 1 1 3 3 C H5 H 1 5.273 . . 1 . . . A 3 C H5 . 18892 1 35 . 1 1 3 3 C H5' H 1 4.614 . . 2 . . . A 3 C H5' . 18892 1 36 . 1 1 3 3 C H5'' H 1 4.160 . . 2 . . . A 3 C H5'' . 18892 1 37 . 1 1 3 3 C H6 H 1 7.661 . . 1 . . . A 3 C H6 . 18892 1 38 . 1 1 3 3 C C1' C 13 93.750 . . 1 . . . A 3 C C1' . 18892 1 39 . 1 1 3 3 C C2' C 13 75.439 . . 1 . . . A 3 C C2' . 18892 1 40 . 1 1 3 3 C C3' C 13 72.236 . . 1 . . . A 3 C C3' . 18892 1 41 . 1 1 3 3 C C4' C 13 81.958 . . 1 . . . A 3 C C4' . 18892 1 42 . 1 1 3 3 C C5 C 13 97.384 . . 1 . . . A 3 C C5 . 18892 1 43 . 1 1 3 3 C C5' C 13 64.679 . . 1 . . . A 3 C C5' . 18892 1 44 . 1 1 3 3 C C6 C 13 140.588 . . 1 . . . A 3 C C6 . 18892 1 45 . 1 1 3 3 C N4 N 15 97.744 . . 1 . . . A 3 C N4 . 18892 1 46 . 1 1 4 4 A H1' H 1 5.953 . . 1 . . . A 4 A H1' . 18892 1 47 . 1 1 4 4 A H2 H 1 6.924 . . 1 . . . A 4 A H2 . 18892 1 48 . 1 1 4 4 A H2' H 1 4.737 . . 1 . . . A 4 A H2' . 18892 1 49 . 1 1 4 4 A H3' H 1 4.658 . . 1 . . . A 4 A H3' . 18892 1 50 . 1 1 4 4 A H5' H 1 4.548 . . 2 . . . A 4 A H5' . 18892 1 51 . 1 1 4 4 A H5'' H 1 4.204 . . 2 . . . A 4 A H5'' . 18892 1 52 . 1 1 4 4 A H8 H 1 7.942 . . 1 . . . A 4 A H8 . 18892 1 53 . 1 1 4 4 A C1' C 13 93.140 . . 1 . . . A 4 A C1' . 18892 1 54 . 1 1 4 4 A C2 C 13 152.139 . . 1 . . . A 4 A C2 . 18892 1 55 . 1 1 4 4 A C2' C 13 75.641 . . 1 . . . A 4 A C2' . 18892 1 56 . 1 1 4 4 A C3' C 13 73.126 . . 1 . . . A 4 A C3' . 18892 1 57 . 1 1 4 4 A C5' C 13 65.986 . . 1 . . . A 4 A C5' . 18892 1 58 . 1 1 4 4 A C8 C 13 139.288 . . 1 . . . A 4 A C8 . 18892 1 59 . 1 1 4 4 A N1 N 15 213.002 . . 1 . . . A 4 A N1 . 18892 1 60 . 1 1 4 4 A N3 N 15 219.714 . . 1 . . . A 4 A N3 . 18892 1 61 . 1 1 4 4 A N6 N 15 82.137 . . 1 . . . A 4 A N6 . 18892 1 62 . 1 1 5 5 G H1 H 1 12.839 . . 1 . . . A 5 G H1 . 18892 1 63 . 1 1 5 5 G H1' H 1 5.516 . . 1 . . . A 5 G H1' . 18892 1 64 . 1 1 5 5 G H2' H 1 4.495 . . 1 . . . A 5 G H2' . 18892 1 65 . 1 1 5 5 G H3' H 1 4.642 . . 1 . . . A 5 G H3' . 18892 1 66 . 1 1 5 5 G H4' H 1 4.468 . . 1 . . . A 5 G H4' . 18892 1 67 . 1 1 5 5 G H5' H 1 4.550 . . 2 . . . A 5 G H5' . 18892 1 68 . 1 1 5 5 G H5'' H 1 4.108 . . 2 . . . A 5 G H5'' . 18892 1 69 . 1 1 5 5 G H8 H 1 7.143 . . 1 . . . A 5 G H8 . 18892 1 70 . 1 1 5 5 G C1' C 13 92.805 . . 1 . . . A 5 G C1' . 18892 1 71 . 1 1 5 5 G C2' C 13 75.152 . . 1 . . . A 5 G C2' . 18892 1 72 . 1 1 5 5 G C3' C 13 75.280 . . 1 . . . A 5 G C3' . 18892 1 73 . 1 1 5 5 G C4' C 13 82.164 . . 1 . . . A 5 G C4' . 18892 1 74 . 1 1 5 5 G C5' C 13 65.349 . . 1 . . . A 5 G C5' . 18892 1 75 . 1 1 5 5 G C8 C 13 135.938 . . 1 . . . A 5 G C8 . 18892 1 76 . 1 1 5 5 G N1 N 15 147.420 . . 1 . . . A 5 G N1 . 18892 1 77 . 1 1 5 5 G N2 N 15 73.510 . . 1 . . . A 5 G N2 . 18892 1 78 . 1 1 6 6 A H1' H 1 6.043 . . 1 . . . A 6 A H1' . 18892 1 79 . 1 1 6 6 A H2 H 1 8.558 . . 1 . . . A 6 A H2 . 18892 1 80 . 1 1 6 6 A H2' H 1 4.575 . . 1 . . . A 6 A H2' . 18892 1 81 . 1 1 6 6 A H3' H 1 4.614 . . 1 . . . A 6 A H3' . 18892 1 82 . 1 1 6 6 A H4' H 1 4.552 . . 1 . . . A 6 A H4' . 18892 1 83 . 1 1 6 6 A H5' H 1 4.554 . . 2 . . . A 6 A H5' . 18892 1 84 . 1 1 6 6 A H5'' H 1 4.184 . . 2 . . . A 6 A H5'' . 18892 1 85 . 1 1 6 6 A H8 H 1 7.986 . . 1 . . . A 6 A H8 . 18892 1 86 . 1 1 6 6 A C1' C 13 91.950 . . 1 . . . A 6 A C1' . 18892 1 87 . 1 1 6 6 A C2 C 13 156.037 . . 1 . . . A 6 A C2 . 18892 1 88 . 1 1 6 6 A C2' C 13 76.187 . . 1 . . . A 6 A C2' . 18892 1 89 . 1 1 6 6 A C3' C 13 73.460 . . 1 . . . A 6 A C3' . 18892 1 90 . 1 1 6 6 A C4' C 13 82.330 . . 1 . . . A 6 A C4' . 18892 1 91 . 1 1 6 6 A C5' C 13 65.506 . . 1 . . . A 6 A C5' . 18892 1 92 . 1 1 6 6 A C8 C 13 139.013 . . 1 . . . A 6 A C8 . 18892 1 93 . 1 1 6 6 A N1 N 15 212.627 . . 1 . . . A 6 A N1 . 18892 1 94 . 1 1 6 6 A N3 N 15 229.202 . . 1 . . . A 6 A N3 . 18892 1 95 . 1 1 7 7 U H1' H 1 5.505 . . 1 . . . A 7 U H1' . 18892 1 96 . 1 1 7 7 U H2' H 1 4.261 . . 1 . . . A 7 U H2' . 18892 1 97 . 1 1 7 7 U H3 H 1 13.400 . . 1 . . . A 7 U H3 . 18892 1 98 . 1 1 7 7 U H3' H 1 4.282 . . 1 . . . A 7 U H3' . 18892 1 99 . 1 1 7 7 U H4' H 1 4.495 . . 1 . . . A 7 U H4' . 18892 1 100 . 1 1 7 7 U H5 H 1 5.062 . . 1 . . . A 7 U H5 . 18892 1 101 . 1 1 7 7 U H5' H 1 4.391 . . 2 . . . A 7 U H5' . 18892 1 102 . 1 1 7 7 U H5'' H 1 4.063 . . 2 . . . A 7 U H5'' . 18892 1 103 . 1 1 7 7 U H6 H 1 7.253 . . 1 . . . A 7 U H6 . 18892 1 104 . 1 1 7 7 U C1' C 13 94.431 . . 1 . . . A 7 U C1' . 18892 1 105 . 1 1 7 7 U C2' C 13 75.561 . . 1 . . . A 7 U C2' . 18892 1 106 . 1 1 7 7 U C3' C 13 73.215 . . 1 . . . A 7 U C3' . 18892 1 107 . 1 1 7 7 U C4' C 13 83.611 . . 1 . . . A 7 U C4' . 18892 1 108 . 1 1 7 7 U C5 C 13 103.537 . . 1 . . . A 7 U C5 . 18892 1 109 . 1 1 7 7 U C5' C 13 66.428 . . 1 . . . A 7 U C5' . 18892 1 110 . 1 1 7 7 U C6 C 13 141.408 . . 1 . . . A 7 U C6 . 18892 1 111 . 1 1 7 7 U N3 N 15 162.034 . . 1 . . . A 7 U N3 . 18892 1 112 . 1 1 8 8 C H1' H 1 5.547 . . 1 . . . A 8 C H1' . 18892 1 113 . 1 1 8 8 C H2' H 1 4.405 . . 1 . . . A 8 C H2' . 18892 1 114 . 1 1 8 8 C H3' H 1 4.574 . . 1 . . . A 8 C H3' . 18892 1 115 . 1 1 8 8 C H4' H 1 4.468 . . 1 . . . A 8 C H4' . 18892 1 116 . 1 1 8 8 C H5 H 1 5.545 . . 1 . . . A 8 C H5 . 18892 1 117 . 1 1 8 8 C H6 H 1 7.806 . . 1 . . . A 8 C H6 . 18892 1 118 . 1 1 8 8 C C1' C 13 94.094 . . 1 . . . A 8 C C1' . 18892 1 119 . 1 1 8 8 C C2' C 13 75.467 . . 1 . . . A 8 C C2' . 18892 1 120 . 1 1 8 8 C C3' C 13 72.227 . . 1 . . . A 8 C C3' . 18892 1 121 . 1 1 8 8 C C4' C 13 81.970 . . 1 . . . A 8 C C4' . 18892 1 122 . 1 1 8 8 C C5 C 13 97.249 . . 1 . . . A 8 C C5 . 18892 1 123 . 1 1 8 8 C C6 C 13 141.544 . . 1 . . . A 8 C C6 . 18892 1 124 . 1 1 8 8 C N4 N 15 97.279 . . 1 . . . A 8 C N4 . 18892 1 125 . 1 1 9 9 U H1' H 1 5.505 . . 1 . . . A 9 U H1' . 18892 1 126 . 1 1 9 9 U H2' H 1 4.433 . . 1 . . . A 9 U H2' . 18892 1 127 . 1 1 9 9 U H3 H 1 13.079 . . 1 . . . A 9 U H3 . 18892 1 128 . 1 1 9 9 U H3' H 1 4.448 . . 1 . . . A 9 U H3' . 18892 1 129 . 1 1 9 9 U H4' H 1 4.518 . . 1 . . . A 9 U H4' . 18892 1 130 . 1 1 9 9 U H5 H 1 5.326 . . 1 . . . A 9 U H5 . 18892 1 131 . 1 1 9 9 U H5' H 1 4.525 . . 2 . . . A 9 U H5' . 18892 1 132 . 1 1 9 9 U H5'' H 1 4.104 . . 2 . . . A 9 U H5'' . 18892 1 133 . 1 1 9 9 U H6 H 1 7.639 . . 1 . . . A 9 U H6 . 18892 1 134 . 1 1 9 9 U C1' C 13 93.615 . . 1 . . . A 9 U C1' . 18892 1 135 . 1 1 9 9 U C2' C 13 75.558 . . 1 . . . A 9 U C2' . 18892 1 136 . 1 1 9 9 U C3' C 13 72.319 . . 1 . . . A 9 U C3' . 18892 1 137 . 1 1 9 9 U C4' C 13 82.661 . . 1 . . . A 9 U C4' . 18892 1 138 . 1 1 9 9 U C5 C 13 103.742 . . 1 . . . A 9 U C5 . 18892 1 139 . 1 1 9 9 U C5' C 13 64.995 . . 1 . . . A 9 U C5' . 18892 1 140 . 1 1 9 9 U C6 C 13 141.066 . . 1 . . . A 9 U C6 . 18892 1 141 . 1 1 9 9 U N3 N 15 160.303 . . 1 . . . A 9 U N3 . 18892 1 142 . 1 1 10 10 G H1 H 1 10.333 . . 1 . . . A 10 G H1 . 18892 1 143 . 1 1 10 10 G H1' H 1 5.503 . . 1 . . . A 10 G H1' . 18892 1 144 . 1 1 10 10 G H2' H 1 4.504 . . 1 . . . A 10 G H2' . 18892 1 145 . 1 1 10 10 G H3' H 1 4.626 . . 1 . . . A 10 G H3' . 18892 1 146 . 1 1 10 10 G H4' H 1 4.496 . . 1 . . . A 10 G H4' . 18892 1 147 . 1 1 10 10 G H5' H 1 4.388 . . 2 . . . A 10 G H5' . 18892 1 148 . 1 1 10 10 G H5'' H 1 4.117 . . 2 . . . A 10 G H5'' . 18892 1 149 . 1 1 10 10 G H8 H 1 7.827 . . 1 . . . A 10 G H8 . 18892 1 150 . 1 1 10 10 G C1' C 13 90.859 . . 1 . . . A 10 G C1' . 18892 1 151 . 1 1 10 10 G C2' C 13 75.556 . . 1 . . . A 10 G C2' . 18892 1 152 . 1 1 10 10 G C4' C 13 83.642 . . 1 . . . A 10 G C4' . 18892 1 153 . 1 1 10 10 G C5' C 13 66.421 . . 1 . . . A 10 G C5' . 18892 1 154 . 1 1 10 10 G C8 C 13 137.576 . . 1 . . . A 10 G C8 . 18892 1 155 . 1 1 10 10 G N1 N 15 145.276 . . 1 . . . A 10 G N1 . 18892 1 156 . 1 1 11 11 U H1' H 1 5.691 . . 1 . . . A 11 U H1' . 18892 1 157 . 1 1 11 11 U H2' H 1 4.461 . . 1 . . . A 11 U H2' . 18892 1 158 . 1 1 11 11 U H3' H 1 4.480 . . 1 . . . A 11 U H3' . 18892 1 159 . 1 1 11 11 U H4' H 1 4.218 . . 1 . . . A 11 U H4' . 18892 1 160 . 1 1 11 11 U H5 H 1 5.493 . . 1 . . . A 11 U H5 . 18892 1 161 . 1 1 11 11 U H5' H 1 4.186 . . 2 . . . A 11 U H5' . 18892 1 162 . 1 1 11 11 U H5'' H 1 4.048 . . 2 . . . A 11 U H5'' . 18892 1 163 . 1 1 11 11 U H6 H 1 7.604 . . 1 . . . A 11 U H6 . 18892 1 164 . 1 1 11 11 U C1' C 13 91.335 . . 1 . . . A 11 U C1' . 18892 1 165 . 1 1 11 11 U C2' C 13 75.234 . . 1 . . . A 11 U C2' . 18892 1 166 . 1 1 11 11 U C3' C 13 75.703 . . 1 . . . A 11 U C3' . 18892 1 167 . 1 1 11 11 U C4' C 13 84.081 . . 1 . . . A 11 U C4' . 18892 1 168 . 1 1 11 11 U C5 C 13 104.083 . . 1 . . . A 11 U C5 . 18892 1 169 . 1 1 11 11 U C5' C 13 66.621 . . 1 . . . A 11 U C5' . 18892 1 170 . 1 1 11 11 U C6 C 13 143.253 . . 1 . . . A 11 U C6 . 18892 1 171 . 1 1 12 12 A H1' H 1 5.663 . . 1 . . . A 12 A H1' . 18892 1 172 . 1 1 12 12 A H2 H 1 7.973 . . 1 . . . A 12 A H2 . 18892 1 173 . 1 1 12 12 A H2' H 1 4.538 . . 1 . . . A 12 A H2' . 18892 1 174 . 1 1 12 12 A H3' H 1 4.647 . . 1 . . . A 12 A H3' . 18892 1 175 . 1 1 12 12 A H4' H 1 4.206 . . 1 . . . A 12 A H4' . 18892 1 176 . 1 1 12 12 A H5' H 1 3.923 . . 2 . . . A 12 A H5' . 18892 1 177 . 1 1 12 12 A H5'' H 1 3.849 . . 2 . . . A 12 A H5'' . 18892 1 178 . 1 1 12 12 A H8 H 1 8.118 . . 1 . . . A 12 A H8 . 18892 1 179 . 1 1 12 12 A C1' C 13 90.762 . . 1 . . . A 12 A C1' . 18892 1 180 . 1 1 12 12 A C2 C 13 154.738 . . 1 . . . A 12 A C2 . 18892 1 181 . 1 1 12 12 A C2' C 13 76.793 . . 1 . . . A 12 A C2' . 18892 1 182 . 1 1 12 12 A C3' C 13 76.154 . . 1 . . . A 12 A C3' . 18892 1 183 . 1 1 12 12 A C4' C 13 84.266 . . 1 . . . A 12 A C4' . 18892 1 184 . 1 1 12 12 A C5' C 13 66.506 . . 1 . . . A 12 A C5' . 18892 1 185 . 1 1 12 12 A C8 C 13 141.618 . . 1 . . . A 12 A C8 . 18892 1 186 . 1 1 12 12 A N1 N 15 215.927 . . 1 . . . A 12 A N1 . 18892 1 187 . 1 1 12 12 A N3 N 15 223.315 . . 1 . . . A 12 A N3 . 18892 1 188 . 1 1 13 13 A H1' H 1 5.937 . . 1 . . . A 13 A H1' . 18892 1 189 . 1 1 13 13 A H2 H 1 7.947 . . 1 . . . A 13 A H2 . 18892 1 190 . 1 1 13 13 A H2' H 1 4.884 . . 1 . . . A 13 A H2' . 18892 1 191 . 1 1 13 13 A H3' H 1 5.050 . . 1 . . . A 13 A H3' . 18892 1 192 . 1 1 13 13 A H4' H 1 4.484 . . 1 . . . A 13 A H4' . 18892 1 193 . 1 1 13 13 A H5' H 1 4.347 . . 2 . . . A 13 A H5' . 18892 1 194 . 1 1 13 13 A H5'' H 1 4.164 . . 2 . . . A 13 A H5'' . 18892 1 195 . 1 1 13 13 A H8 H 1 8.096 . . 1 . . . A 13 A H8 . 18892 1 196 . 1 1 13 13 A C1' C 13 91.277 . . 1 . . . A 13 A C1' . 18892 1 197 . 1 1 13 13 A C2 C 13 154.736 . . 1 . . . A 13 A C2 . 18892 1 198 . 1 1 13 13 A C2' C 13 75.543 . . 1 . . . A 13 A C2' . 18892 1 199 . 1 1 13 13 A C3' C 13 75.404 . . 1 . . . A 13 A C3' . 18892 1 200 . 1 1 13 13 A C4' C 13 84.368 . . 1 . . . A 13 A C4' . 18892 1 201 . 1 1 13 13 A C5' C 13 67.231 . . 1 . . . A 13 A C5' . 18892 1 202 . 1 1 13 13 A C8 C 13 142.299 . . 1 . . . A 13 A C8 . 18892 1 203 . 1 1 13 13 A N1 N 15 216.677 . . 1 . . . A 13 A N1 . 18892 1 204 . 1 1 13 13 A N3 N 15 226.090 . . 1 . . . A 13 A N3 . 18892 1 205 . 1 1 14 14 U H1' H 1 5.970 . . 1 . . . A 14 U H1' . 18892 1 206 . 1 1 14 14 U H2' H 1 4.472 . . 1 . . . A 14 U H2' . 18892 1 207 . 1 1 14 14 U H3' H 1 4.738 . . 1 . . . A 14 U H3' . 18892 1 208 . 1 1 14 14 U H4' H 1 4.537 . . 1 . . . A 14 U H4' . 18892 1 209 . 1 1 14 14 U H5 H 1 5.805 . . 1 . . . A 14 U H5 . 18892 1 210 . 1 1 14 14 U H5' H 1 4.427 . . 2 . . . A 14 U H5' . 18892 1 211 . 1 1 14 14 U H5'' H 1 4.262 . . 2 . . . A 14 U H5'' . 18892 1 212 . 1 1 14 14 U H6 H 1 7.750 . . 1 . . . A 14 U H6 . 18892 1 213 . 1 1 14 14 U C1' C 13 91.207 . . 1 . . . A 14 U C1' . 18892 1 214 . 1 1 14 14 U C2' C 13 75.649 . . 1 . . . A 14 U C2' . 18892 1 215 . 1 1 14 14 U C3' C 13 75.603 . . 1 . . . A 14 U C3' . 18892 1 216 . 1 1 14 14 U C4' C 13 84.336 . . 1 . . . A 14 U C4' . 18892 1 217 . 1 1 14 14 U C5 C 13 105.039 . . 1 . . . A 14 U C5 . 18892 1 218 . 1 1 14 14 U C5' C 13 67.009 . . 1 . . . A 14 U C5' . 18892 1 219 . 1 1 14 14 U C6 C 13 143.185 . . 1 . . . A 14 U C6 . 18892 1 220 . 1 1 15 15 A H1' H 1 5.182 . . 1 . . . A 15 A H1' . 18892 1 221 . 1 1 15 15 A H2 H 1 7.407 . . 1 . . . A 15 A H2 . 18892 1 222 . 1 1 15 15 A H2' H 1 4.717 . . 1 . . . A 15 A H2' . 18892 1 223 . 1 1 15 15 A H3' H 1 4.490 . . 1 . . . A 15 A H3' . 18892 1 224 . 1 1 15 15 A H4' H 1 4.491 . . 1 . . . A 15 A H4' . 18892 1 225 . 1 1 15 15 A H5' H 1 4.413 . . 2 . . . A 15 A H5' . 18892 1 226 . 1 1 15 15 A H5'' H 1 4.293 . . 2 . . . A 15 A H5'' . 18892 1 227 . 1 1 15 15 A H8 H 1 8.259 . . 1 . . . A 15 A H8 . 18892 1 228 . 1 1 15 15 A C1' C 13 93.014 . . 1 . . . A 15 A C1' . 18892 1 229 . 1 1 15 15 A C2 C 13 153.026 . . 1 . . . A 15 A C2 . 18892 1 230 . 1 1 15 15 A C2' C 13 75.157 . . 1 . . . A 15 A C2' . 18892 1 231 . 1 1 15 15 A C3' C 13 74.203 . . 1 . . . A 15 A C3' . 18892 1 232 . 1 1 15 15 A C4' C 13 83.017 . . 1 . . . A 15 A C4' . 18892 1 233 . 1 1 15 15 A C5' C 13 67.380 . . 1 . . . A 15 A C5' . 18892 1 234 . 1 1 15 15 A C8 C 13 140.791 . . 1 . . . A 15 A C8 . 18892 1 235 . 1 1 15 15 A N1 N 15 213.489 . . 1 . . . A 15 A N1 . 18892 1 236 . 1 1 15 15 A N3 N 15 220.614 . . 1 . . . A 15 A N3 . 18892 1 237 . 1 1 15 15 A N6 N 15 78.619 . . 1 . . . A 15 A N6 . 18892 1 238 . 1 1 16 16 G H1 H 1 12.408 . . 1 . . . A 16 G H1 . 18892 1 239 . 1 1 16 16 G H1' H 1 5.540 . . 1 . . . A 16 G H1' . 18892 1 240 . 1 1 16 16 G H2' H 1 4.599 . . 1 . . . A 16 G H2' . 18892 1 241 . 1 1 16 16 G H3' H 1 4.474 . . 1 . . . A 16 G H3' . 18892 1 242 . 1 1 16 16 G H4' H 1 4.467 . . 1 . . . A 16 G H4' . 18892 1 243 . 1 1 16 16 G H5' H 1 4.423 . . 2 . . . A 16 G H5' . 18892 1 244 . 1 1 16 16 G H5'' H 1 4.096 . . 2 . . . A 16 G H5'' . 18892 1 245 . 1 1 16 16 G H8 H 1 7.108 . . 1 . . . A 16 G H8 . 18892 1 246 . 1 1 16 16 G C1' C 13 92.736 . . 1 . . . A 16 G C1' . 18892 1 247 . 1 1 16 16 G C2' C 13 75.242 . . 1 . . . A 16 G C2' . 18892 1 248 . 1 1 16 16 G C3' C 13 72.623 . . 1 . . . A 16 G C3' . 18892 1 249 . 1 1 16 16 G C4' C 13 81.996 . . 1 . . . A 16 G C4' . 18892 1 250 . 1 1 16 16 G C5' C 13 65.912 . . 1 . . . A 16 G C5' . 18892 1 251 . 1 1 16 16 G C8 C 13 136.073 . . 1 . . . A 16 G C8 . 18892 1 252 . 1 1 16 16 G N1 N 15 146.454 . . 1 . . . A 16 G N1 . 18892 1 253 . 1 1 16 16 G N2 N 15 74.074 . . 1 . . . A 16 G N2 . 18892 1 254 . 1 1 17 17 A H1' H 1 5.867 . . 1 . . . A 17 A H1' . 18892 1 255 . 1 1 17 17 A H2 H 1 7.306 . . 1 . . . A 17 A H2 . 18892 1 256 . 1 1 17 17 A H2' H 1 4.599 . . 1 . . . A 17 A H2' . 18892 1 257 . 1 1 17 17 A H3' H 1 4.705 . . 1 . . . A 17 A H3' . 18892 1 258 . 1 1 17 17 A H4' H 1 4.502 . . 1 . . . A 17 A H4' . 18892 1 259 . 1 1 17 17 A H5' H 1 4.614 . . 2 . . . A 17 A H5' . 18892 1 260 . 1 1 17 17 A H5'' H 1 4.167 . . 2 . . . A 17 A H5'' . 18892 1 261 . 1 1 17 17 A H8 H 1 7.618 . . 1 . . . A 17 A H8 . 18892 1 262 . 1 1 17 17 A C1' C 13 93.204 . . 1 . . . A 17 A C1' . 18892 1 263 . 1 1 17 17 A C2 C 13 153.441 . . 1 . . . A 17 A C2 . 18892 1 264 . 1 1 17 17 A C2' C 13 75.668 . . 1 . . . A 17 A C2' . 18892 1 265 . 1 1 17 17 A C3' C 13 72.734 . . 1 . . . A 17 A C3' . 18892 1 266 . 1 1 17 17 A C4' C 13 82.293 . . 1 . . . A 17 A C4' . 18892 1 267 . 1 1 17 17 A C5' C 13 65.010 . . 1 . . . A 17 A C5' . 18892 1 268 . 1 1 17 17 A C8 C 13 139.082 . . 1 . . . A 17 A C8 . 18892 1 269 . 1 1 17 17 A N1 N 15 210.977 . . 1 . . . A 17 A N1 . 18892 1 270 . 1 1 17 17 A N3 N 15 221.927 . . 1 . . . A 17 A N3 . 18892 1 271 . 1 1 17 17 A N6 N 15 82.790 . . 1 . . . A 17 A N6 . 18892 1 272 . 1 1 18 18 A H1' H 1 5.918 . . 1 . . . A 18 A H1' . 18892 1 273 . 1 1 18 18 A H2 H 1 8.496 . . 1 . . . A 18 A H2 . 18892 1 274 . 1 1 18 18 A H2' H 1 4.549 . . 1 . . . A 18 A H2' . 18892 1 275 . 1 1 18 18 A H3' H 1 4.565 . . 1 . . . A 18 A H3' . 18892 1 276 . 1 1 18 18 A H4' H 1 4.556 . . 1 . . . A 18 A H4' . 18892 1 277 . 1 1 18 18 A H5' H 1 4.545 . . 2 . . . A 18 A H5' . 18892 1 278 . 1 1 18 18 A H5'' H 1 4.183 . . 2 . . . A 18 A H5'' . 18892 1 279 . 1 1 18 18 A H8 H 1 7.916 . . 1 . . . A 18 A H8 . 18892 1 280 . 1 1 18 18 A C1' C 13 91.702 . . 1 . . . A 18 A C1' . 18892 1 281 . 1 1 18 18 A C2 C 13 155.832 . . 1 . . . A 18 A C2 . 18892 1 282 . 1 1 18 18 A C2' C 13 76.162 . . 1 . . . A 18 A C2' . 18892 1 283 . 1 1 18 18 A C3' C 13 73.741 . . 1 . . . A 18 A C3' . 18892 1 284 . 1 1 18 18 A C4' C 13 82.391 . . 1 . . . A 18 A C4' . 18892 1 285 . 1 1 18 18 A C5' C 13 65.706 . . 1 . . . A 18 A C5' . 18892 1 286 . 1 1 18 18 A C8 C 13 138.741 . . 1 . . . A 18 A C8 . 18892 1 287 . 1 1 18 18 A N1 N 15 212.027 . . 1 . . . A 18 A N1 . 18892 1 288 . 1 1 18 18 A N3 N 15 231.077 . . 1 . . . A 18 A N3 . 18892 1 289 . 1 1 18 18 A N6 N 15 80.389 . . 1 . . . A 18 A N6 . 18892 1 290 . 1 1 19 19 C H1' H 1 5.454 . . 1 . . . A 19 C H1' . 18892 1 291 . 1 1 19 19 C H2' H 1 4.362 . . 1 . . . A 19 C H2' . 18892 1 292 . 1 1 19 19 C H3' H 1 4.229 . . 1 . . . A 19 C H3' . 18892 1 293 . 1 1 19 19 C H4' H 1 4.501 . . 1 . . . A 19 C H4' . 18892 1 294 . 1 1 19 19 C H5 H 1 5.156 . . 1 . . . A 19 C H5 . 18892 1 295 . 1 1 19 19 C H5' H 1 4.388 . . 2 . . . A 19 C H5' . 18892 1 296 . 1 1 19 19 C H5'' H 1 4.065 . . 2 . . . A 19 C H5'' . 18892 1 297 . 1 1 19 19 C H6 H 1 7.113 . . 1 . . . A 19 C H6 . 18892 1 298 . 1 1 19 19 C C1' C 13 94.918 . . 1 . . . A 19 C C1' . 18892 1 299 . 1 1 19 19 C C2' C 13 75.331 . . 1 . . . A 19 C C2' . 18892 1 300 . 1 1 19 19 C C3' C 13 73.134 . . 1 . . . A 19 C C3' . 18892 1 301 . 1 1 19 19 C C4' C 13 82.485 . . 1 . . . A 19 C C4' . 18892 1 302 . 1 1 19 19 C C5 C 13 98.032 . . 1 . . . A 19 C C5 . 18892 1 303 . 1 1 19 19 C C5' C 13 66.565 . . 1 . . . A 19 C C5' . 18892 1 304 . 1 1 19 19 C C6 C 13 140.722 . . 1 . . . A 19 C C6 . 18892 1 305 . 1 1 19 19 C N4 N 15 96.376 . . 1 . . . A 19 C N4 . 18892 1 306 . 1 1 20 20 U H1' H 1 5.518 . . 1 . . . A 20 U H1' . 18892 1 307 . 1 1 20 20 U H2' H 1 4.641 . . 1 . . . A 20 U H2' . 18892 1 308 . 1 1 20 20 U H3 H 1 13.627 . . 1 . . . A 20 U H3 . 18892 1 309 . 1 1 20 20 U H3' H 1 4.571 . . 1 . . . A 20 U H3' . 18892 1 310 . 1 1 20 20 U H4' H 1 4.468 . . 1 . . . A 20 U H4' . 18892 1 311 . 1 1 20 20 U H5 H 1 5.295 . . 1 . . . A 20 U H5 . 18892 1 312 . 1 1 20 20 U H5' H 1 4.391 . . 2 . . . A 20 U H5' . 18892 1 313 . 1 1 20 20 U H5'' H 1 4.120 . . 2 . . . A 20 U H5'' . 18892 1 314 . 1 1 20 20 U H6 H 1 7.881 . . 1 . . . A 20 U H6 . 18892 1 315 . 1 1 20 20 U C1' C 13 93.471 . . 1 . . . A 20 U C1' . 18892 1 316 . 1 1 20 20 U C2' C 13 75.231 . . 1 . . . A 20 U C2' . 18892 1 317 . 1 1 20 20 U C3' C 13 72.919 . . 1 . . . A 20 U C3' . 18892 1 318 . 1 1 20 20 U C4' C 13 82.164 . . 1 . . . A 20 U C4' . 18892 1 319 . 1 1 20 20 U C5 C 13 103.401 . . 1 . . . A 20 U C5 . 18892 1 320 . 1 1 20 20 U C5' C 13 66.448 . . 1 . . . A 20 U C5' . 18892 1 321 . 1 1 20 20 U C6 C 13 141.748 . . 1 . . . A 20 U C6 . 18892 1 322 . 1 1 20 20 U N3 N 15 162.202 . . 1 . . . A 20 U N3 . 18892 1 323 . 1 1 21 21 G H1 H 1 12.504 . . 1 . . . A 21 G H1 . 18892 1 324 . 1 1 21 21 G H1' H 1 5.792 . . 1 . . . A 21 G H1' . 18892 1 325 . 1 1 21 21 G H2' H 1 4.535 . . 1 . . . A 21 G H2' . 18892 1 326 . 1 1 21 21 G H3' H 1 4.615 . . 1 . . . A 21 G H3' . 18892 1 327 . 1 1 21 21 G H4' H 1 4.523 . . 1 . . . A 21 G H4' . 18892 1 328 . 1 1 21 21 G H5' H 1 4.553 . . 2 . . . A 21 G H5' . 18892 1 329 . 1 1 21 21 G H5'' H 1 4.174 . . 2 . . . A 21 G H5'' . 18892 1 330 . 1 1 21 21 G H8 H 1 7.749 . . 1 . . . A 21 G H8 . 18892 1 331 . 1 1 21 21 G C1' C 13 92.784 . . 1 . . . A 21 G C1' . 18892 1 332 . 1 1 21 21 G C2' C 13 75.253 . . 1 . . . A 21 G C2' . 18892 1 333 . 1 1 21 21 G C3' C 13 72.699 . . 1 . . . A 21 G C3' . 18892 1 334 . 1 1 21 21 G C4' C 13 81.966 . . 1 . . . A 21 G C4' . 18892 1 335 . 1 1 21 21 G C5' C 13 65.480 . . 1 . . . A 21 G C5' . 18892 1 336 . 1 1 21 21 G C8 C 13 136.349 . . 1 . . . A 21 G C8 . 18892 1 337 . 1 1 21 21 G N1 N 15 147.253 . . 1 . . . A 21 G N1 . 18892 1 338 . 1 1 21 21 G N2 N 15 74.544 . . 1 . . . A 21 G N2 . 18892 1 339 . 1 1 22 22 C H1' H 1 5.505 . . 1 . . . A 22 C H1' . 18892 1 340 . 1 1 22 22 C H2' H 1 4.524 . . 1 . . . A 22 C H2' . 18892 1 341 . 1 1 22 22 C H3' H 1 4.470 . . 1 . . . A 22 C H3' . 18892 1 342 . 1 1 22 22 C H4' H 1 4.411 . . 1 . . . A 22 C H4' . 18892 1 343 . 1 1 22 22 C H5 H 1 5.199 . . 1 . . . A 22 C H5 . 18892 1 344 . 1 1 22 22 C H5' H 1 4.605 . . 2 . . . A 22 C H5' . 18892 1 345 . 1 1 22 22 C H5'' H 1 4.075 . . 2 . . . A 22 C H5'' . 18892 1 346 . 1 1 22 22 C H6 H 1 7.687 . . 1 . . . A 22 C H6 . 18892 1 347 . 1 1 22 22 C C1' C 13 94.051 . . 1 . . . A 22 C C1' . 18892 1 348 . 1 1 22 22 C C2' C 13 75.973 . . 1 . . . A 22 C C2' . 18892 1 349 . 1 1 22 22 C C3' C 13 71.985 . . 1 . . . A 22 C C3' . 18892 1 350 . 1 1 22 22 C C4' C 13 82.175 . . 1 . . . A 22 C C4' . 18892 1 351 . 1 1 22 22 C C5 C 13 96.836 . . 1 . . . A 22 C C5 . 18892 1 352 . 1 1 22 22 C C5' C 13 64.556 . . 1 . . . A 22 C C5' . 18892 1 353 . 1 1 22 22 C C6 C 13 141.136 . . 1 . . . A 22 C C6 . 18892 1 354 . 1 1 22 22 C N4 N 15 98.897 . . 1 . . . A 22 C N4 . 18892 1 355 . 1 1 23 23 C H1' H 1 5.775 . . 1 . . . A 23 C H1' . 18892 1 356 . 1 1 23 23 C H2' H 1 4.036 . . 1 . . . A 23 C H2' . 18892 1 357 . 1 1 23 23 C H3' H 1 4.207 . . 1 . . . A 23 C H3' . 18892 1 358 . 1 1 23 23 C H4' H 1 4.189 . . 1 . . . A 23 C H4' . 18892 1 359 . 1 1 23 23 C H5 H 1 5.516 . . 1 . . . A 23 C H5 . 18892 1 360 . 1 1 23 23 C H5' H 1 4.508 . . 2 . . . A 23 C H5' . 18892 1 361 . 1 1 23 23 C H5'' H 1 4.047 . . 2 . . . A 23 C H5'' . 18892 1 362 . 1 1 23 23 C H6 H 1 7.675 . . 1 . . . A 23 C H6 . 18892 1 363 . 1 1 23 23 C C1' C 13 92.850 . . 1 . . . A 23 C C1' . 18892 1 364 . 1 1 23 23 C C2' C 13 77.483 . . 1 . . . A 23 C C2' . 18892 1 365 . 1 1 23 23 C C3' C 13 69.609 . . 1 . . . A 23 C C3' . 18892 1 366 . 1 1 23 23 C C4' C 13 83.480 . . 1 . . . A 23 C C4' . 18892 1 367 . 1 1 23 23 C C5 C 13 98.152 . . 1 . . . A 23 C C5 . 18892 1 368 . 1 1 23 23 C C5' C 13 65.124 . . 1 . . . A 23 C C5' . 18892 1 369 . 1 1 23 23 C C6 C 13 141.683 . . 1 . . . A 23 C C6 . 18892 1 stop_ save_