#******************************************************************* # # $Source: /projects/BMRB/private/cvs/cvsentries/bmr16099/clean/timedomain_data/T6_v2_NC_110508/HBHAcoNH/prosol_History,v $ # # Copyright (c) 1999 # BRUKER ANALYTIK GMBH # D-76287 Rheinstetten, Germany # # All Rights Reserved # # # $Id: prosol_History,v 1.1 2021/02/10 22:19:33 bmrbsvc Exp $ # #******************************************************************* #../conf/instr/spect/prosol/relations/triple #avance-version (07/08/30) # #pulses # P[0]=P90[F1]; # 90 deg pulse F1, 1H P[1]=P90[F1]; # 90 deg pulse F1, 1H P[2]=P90[F1]*2; #180 deg pulse F1, 1H P[3]=P90[F2]; # 90 deg pulse F2, 13C P[4]=P90[F2]*2; #180 deg pulse F2, 13C P[5]=PTOC[F1]*0.66; # 60 deg pulse F1, 1H TOCSY P[6]=PTOC[F1]; # 90 deg pulse F1, 1H, TOCSY P[7]=PTOC[F1]*2; #180 deg pulse F1, 1H, TOCSY P[8]=PSH3[F2]; #adiabatic 180 F2, 13C P[9]=PTOC[F2]; # 90 deg pulse F2, 13C, TOCSY P[10]=PTOC[F2]*2; #180 deg pulse F2, 13C, TOCSY P[11]=PSH8[F1]; # flip-back pulse, F1, 1H P[12]=PSH8[F1]*2; #180 deg sel. F1, 1H (exc. scul) P[13]=PSH4[F2]; # Cali sel. 90 deg, F2, 13C P[14]=PSH6[F2]; # Cali sel.180 deg, F2, 13C P[15]=PSH15[F2]; # 180 deg adiabatic, F2, 13C x-filter # # P[18]=PSH7[F1]; # off-res presat, F1, 1H # # P[21]=P90[F3]; # 90 deg pulse F3, 15N P[22]=P90[F3]*2; #180 deg pulse F3, 15N P[23]=PSH7[F2]; # Calpha sel. 90 deg, F2, 13C P[24]=PSH9[F2]; # Calpha sel. 180 deg, F2, 13C P[25]=PTOC[F3]; # 90 deg pulse, F3, 15N, TOCSY P[26]=PCPDP[F1]; # 90 deg pulse F1, 1H, dec. P[27]=P90[F1]; # WATERGATE pulse, F1, 1H # P[29]=PSH9[F1]; # flip back pulse 2 P[30]=PTOC[F3]*2; #180 deg pulse, F3, 15N, TOCSY P[31]=PSH10[F2]; # Ca or CO decoupling # P[39]=PSH4[F1]; # 90 deg, F1, sf-hmqc H(N) P[40]=PSH6[F1]; # 180 deg, F1, sf-hmqc H(N) P[41]=PSH17[F1]; # 90 deg, F1, best-tripleres. H(N) (pc9) P[42]=PSH19[F1]; # 180 deg, F1, best-tripleres. H(N) (reburp) P[43]=PSH20[F1]; # 90 deg, F1, best-tripleres. H(N) (eburp2) P[44]=PSH22[F1]; # 180 deg, F1, best-tripleres. broadband # P[62]=PUSER5[F3]; # low power decoupling, F3, 15N P[63]=PSH11[F2]; # 180 deg adiabatic decoupling, F2, 13C # #decoupling pulses # PCPD[1]=PCPDP[F1]; # 90 deg pulse F1, 1H, dec. PCPD[2]=PCPDP[F2]; # 90 deg pulse F2, 13C, dec. PCPD[3]=PCPDP[F3]; # 90 deg pulse F3, 15N, dec. PCPD[4]=PCPDP[F4]; # 90 deg pulse F4, 2H, dec. #PCPD[6] #PCPD[7] PCPD[8]=PSH13[F2]; # # power levels # #Pl[0]; PL[1]=PL90[F1]; # high power, F1, 1H PL[2]=PL90[F2]; # high power, F2, 13C PL[3]=PL90[F3]; # high power, F3, 15N PL[4]=PL90[F4]; # high power, F4, 2H #PL[5] # NOT USED #PL[6] # NOT USED #PL[7] # NOT USED #PL[8] # NOT USED PL[9]=PLCW[F1]; # presat power, F1, 1H PL[10]=PLTOC[F1]; # TOCSY power, F1, 1H PL[11]=PLROE[F1]; # ROESY power, F1, 1H PL[12]=PLCPDP[F2]; # dec. power, F2, 13C PL[13]=PLSH13[F2]; # dec. power 2, F2, 13C PL[14]=PLCW[F2]; # low power cw, F2 PL[15]=PLTOC[F2]; # TOCSY power, F2, 13C PL[16]=PLCPDP[F3]; # dec. power, F3, 15N PL[17]=PLCPDP[F4]; # dec. power, F4, 2H PL[18]=PL90[F1]; # WATERGATE power, F1, 1H PL[19]=PLCPDP[F1]; # dec. power, F1, 1H #PL[20] # DANTE-Z #PL[21] #PL[22] PL[23]=PLTOC[F3]; # TOCSY power, F3, 15N (t2) PL[24]=PLHD[F2]; # HD decoupling, F2 PL[25]=PLUSER1[F3]; # T1rho power, F3, 15N PL[26]=PLUSER5[F3]; # low power decoupling, F3, 15N #PL[27] # Shaka Spinlock PL[28]=PLSH10[F2]; # Ca or CO decoupling #PL[29] # NOT USED PL[30]=PLCPDP[F2]; # dec. power, F2, 13C (=pl12) PL[31]=PLUSER2[F2]; # dec. power, F2, 13C, cw bilev # # shapes # #SP[0]=[]; # SP[1]=PLSH8[F1]; # flip-back pulse, F1, 1H SP[2]=PLSH4[F2]; # Cali sel. 90 deg, F2, 13C SP[3]=PLSH6[F2]; # Cali sel. 180 deg, F2, 13C SP[4]=PLSH4[F2]; # Cali sel. 90 deg, F2, 13C off SP[5]=PLSH6[F2]; # Cali sel. 180 deg, F2, 13C off SP[6]=PLSH5[F2]; # Cali sel. 90 deg, F2, 13C off, tr SP[7]=PLSH6[F2]; # Cali sel. 180 deg, F2, 13C SP[8]=PLSH5[F2]; # Cali sel. 90 deg, F2, 13C, tr SP[9]=PLSH9[F2]; # Calpha sel.180 deg, F2, 13C SP[10]=PLSH7[F2]; # Calpha sel. 90 deg, F2, 13C SP[11]=PLSH9[F1]; # flip-back pulse, F1, H SP[12]=PLSH8[F2]; # Calpha sel. 90 deg, F2, 13C, tr SP[13]=PLSH3[F2]; # adiabatic 180 deg, F2, 13C SP[14]=PLSH12[F2]; # adiab. bilev dec., F2, 13C SP[15]=PLSH10[F2]; # CO/Ca sel.dec. 180 deg, F2, 13C SP[16]=PLSH9[F2]; # Calpha sel.180 deg, F2, 13C SP[17]=PLSH9[F2]; # Calpha sel.180 deg, F2, 13C SP[18]=PLSH15[F2]; # adiabatic 180 deg, F2, 13C, x-filter # SP[23]=PLSH4[F1]; # H(N) 90 deg, F1, 1H SP[24]=PLSH6[F1]; # H(N) 180 deg, F1, 1H SP[25]=PLSH17[F1]; # H(N) 90 deg, F1, 1H SP[26]=PLSH19[F1]; # H(N) 180 deg, F1, 1H SP[27]=PLSH18[F1]; # H(N) 90 deg, F1, 1H tr SP[28]=PLSH20[F1]; # H(N) 90 deg, F1, 1H SP[29]=PLSH21[F1]; # H(N) 90 deg, F1, 1H tr SP[30]=PLSH22[F1]; # H(N) 180 deg, F1, 1H SP[31]=PLSH11[F2]; # adiab. dec., F2, 13C # #SPNAM0=[]; SPNAM1=PNSH8[F1]; SPNAM2=PNSH4[F2]; SPNAM3=PNSH6[F2]; SPNAM4=PNSH4[F2]; SPNAM5=PNSH6[F2]; SPNAM6=PNSH5[F2]; SPNAM7=PNSH6[F2]; SPNAM8=PNSH5[F2]; SPNAM9=PNSH9[F2]; SPNAM10=PNSH7[F2]; SPNAM11=PNSH9[F1]; SPNAM12=PNSH8[F2]; SPNAM13=PNSH3[F2]; SPNAM14=PNSH12[F2]; SPNAM15=PNSH10[F2]; SPNAM16=PNSH9[F2]; SPNAM17=PNSH9[F2]; SPNAM18=PNSH15[F2]; # SPNAM23=PNSH4[F1]; SPNAM24=PNSH6[F1]; SPNAM25=PNSH17[F1]; SPNAM26=PNSH19[F1]; SPNAM27=PNSH18[F1]; SPNAM28=PNSH20[F1]; SPNAM29=PNSH21[F1]; SPNAM30=PNSH22[F1]; SPNAM31=PNSH11[F2]; # #Alignment # #SPOAL[0]=[]; SPOAL[1]=PASH8[F1]; SPOAL[2]=PASH4[F2]; SPOAL[3]=PASH6[F2]; SPOAL[4]=PASH4[F2]; SPOAL[5]=PASH6[F2]; SPOAL[6]=PASH5[F2]; SPOAL[7]=PASH6[F2]; SPOAL[8]=PASH5[F2]; SPOAL[9]=PASH9[F2]; SPOAL[10]=PASH7[F2]; SPOAL[11]=PASH9[F1]; SPOAL[12]=PASH8[F2]; SPOAL[13]=PASH3[F2]; SPOAL[14]=PASH12[F2]; SPOAL[15]=PASH10[F2]; SPOAL[16]=PASH9[F2]; SPOAL[17]=PASH9[F2]; SPOAL[18]=PASH15[F2]; # SPOAL[23]=PASH4[F1]; SPOAL[24]=PASH6[F1]; SPOAL[25]=PASH17[F1]; SPOAL[26]=PASH19[F1]; SPOAL[27]=PASH18[F1]; SPOAL[28]=PASH20[F1]; SPOAL[29]=PASH21[F1]; SPOAL[30]=PASH22[F1]; SPOAL[31]=PASH11[F2]; # #Delays # D[9]=TTOC[F1]; D[15]=TTOC[F2]; # #misc # D[16]=D_grad; P[16]=P_grad1; P[17]=P_mlev; P[19]=P_grad2; P[20]=P_mlev; P[28]=P_hsqc;