label list: line no. pc label 283 0xffffffff 1 288 0xffffffff 2 289 0xffffffff LBLSTS2 290 0xffffffff LBLF2 291 0xffffffff LBLSTS1 292 0xffffffff LBLF1 294 0xffffffff 3 pulse program: /opt/topspin/data/pr/nmr/RrR43.002_NC_011608/7/pulseprogram ============== dur0 == line 0 fixdel(1000.000000 usec) setNmr1: 0x10004 dur1 == line 0 fixdel(1000.000000 usec) 'noesyhsqcetgp3d': line 1---> ;noesyhsqcetgp3d 'noesyhsqcetgp3d': line 2---> ;avance-version (04/03/08) 'noesyhsqcetgp3d': line 3---> ;NOESY-HSQC 'noesyhsqcetgp3d': line 4---> ;3D sequence with 'noesyhsqcetgp3d': line 5---> ; homonuclear correlation via dipolar coupling 'noesyhsqcetgp3d': line 6---> ; dipolar coupling may be due to noe or chemical exchange. 'noesyhsqcetgp3d': line 7---> ; H-1/X correlation via double inept transfer 'noesyhsqcetgp3d': line 8---> ;phase sensitive (t1) 'noesyhsqcetgp3d': line 9---> ;phase sensitive using Echo/Antiecho-TPPI gradient selection (t2) 'noesyhsqcetgp3d': line 10---> ;using trim pulses in inept transfer 'noesyhsqcetgp3d': line 11---> ;with decoupling during acquisition 'noesyhsqcetgp3d': line 12---> ;using shaped pulses for inversion on f2 - channel 'noesyhsqcetgp3d': line 13---> ;(use parameterset NOESYHSQCETGP3D) 'noesyhsqcetgp3d': line 14---> ; 'noesyhsqcetgp3d': line 15---> ;A.L. Davis, J. Keeler, E.D. Laue & D. Moskau, J. Magn. Reson. 98, 'noesyhsqcetgp3d': line 16---> ; 207-216 (1992) 'noesyhsqcetgp3d': line 17---> ;A.G. Palmer III, J. Cavanagh, P.E. Wright & M. Rance, J. Magn. 'noesyhsqcetgp3d': line 18---> ; Reson. 93, 151-170 (1991) 'noesyhsqcetgp3d': line 19---> ;L.E. Kay, P. Keifer & T. Saarinen, J. Am. Chem. Soc. 114, 'noesyhsqcetgp3d': line 20---> ; 10663-5 (1992) 'noesyhsqcetgp3d': line 21---> ;J. Schleucher et al., Angew. Chem. 114(10), 1518 (1993) 'Avance.incl': line 1---> ;Avance2.incl 'Avance.incl': line 2---> ; for 1 'Avance.incl': line 3---> ; 'Avance.incl': line 4---> ;avance-version (03/02/17) 'Avance.incl': line 122---> ;$Id: precom.output,v 1.1 2021/02/10 22:37:35 bmrbsvc Exp $ 'Grad.incl': line 1---> ;Grad2.incl - include file for Gradient Spectroscopy 'Grad.incl': line 2---> ; for 1 'Grad.incl': line 3---> ; 'Grad.incl': line 4---> ;avance-version (02/05/31) 'Grad.incl': line 24---> define list EA= 'Grad.incl': line 28---> ;$Id: precom.output,v 1.1 2021/02/10 22:37:35 bmrbsvc Exp $ 'Delay.incl': line 1---> ;Delay.incl - include file for commonly used delays 'Delay.incl': line 2---> ; 'Delay.incl': line 3---> ;version 00/02/07 'Delay.incl': line 6---> ;general delays 'Delay.incl': line 8---> define delay DELTA 'Delay.incl': line 9---> define delay DELTA1 'Delay.incl': line 10---> define delay DELTA2 'Delay.incl': line 11---> define delay DELTA3 'Delay.incl': line 12---> define delay DELTA4 'Delay.incl': line 13---> define delay DELTA5 'Delay.incl': line 14---> define delay DELTA6 'Delay.incl': line 15---> define delay DELTA7 'Delay.incl': line 16---> define delay DELTA8 'Delay.incl': line 18---> define delay TAU 'Delay.incl': line 19---> define delay TAU1 'Delay.incl': line 20---> define delay TAU2 'Delay.incl': line 21---> define delay TAU3 'Delay.incl': line 22---> define delay TAU4 'Delay.incl': line 23---> define delay TAU5 'Delay.incl': line 26---> ;delays for centering pulses 'Delay.incl': line 28---> define delay CEN_HN1 'Delay.incl': line 29---> define delay CEN_HN2 'Delay.incl': line 30---> define delay CEN_HN3 'Delay.incl': line 31---> define delay CEN_HC1 'Delay.incl': line 32---> define delay CEN_HC2 'Delay.incl': line 33---> define delay CEN_HC3 'Delay.incl': line 34---> define delay CEN_HC4 'Delay.incl': line 35---> define delay CEN_HP1 'Delay.incl': line 36---> define delay CEN_HP2 'Delay.incl': line 37---> define delay CEN_CN1 'Delay.incl': line 38---> define delay CEN_CN2 'Delay.incl': line 39---> define delay CEN_CN3 'Delay.incl': line 40---> define delay CEN_CN4 'Delay.incl': line 41---> define delay CEN_CP1 'Delay.incl': line 42---> define delay CEN_CP2 'Delay.incl': line 45---> ;loop counters 'Delay.incl': line 47---> define loopcounter COUNTER 'Delay.incl': line 48---> define loopcounter SCALEF 'Delay.incl': line 49---> define loopcounter FACTOR1 'Delay.incl': line 50---> define loopcounter FACTOR2 'Delay.incl': line 51---> define loopcounter FACTOR3 'Delay.incl': line 55---> ;$Id: precom.output,v 1.1 2021/02/10 22:37:35 bmrbsvc Exp $ 'noesyhsqcetgp3d': line 30---> "p2=p1*2" 'noesyhsqcetgp3d': line 32---> "p4=p3*2" 'noesyhsqcetgp3d': line 34---> "d0=3u" 'noesyhsqcetgp3d': line 36---> "d4=1s/(cnst2*4)" 'noesyhsqcetgp3d': line 38---> "d10=3u" 'noesyhsqcetgp3d': line 40---> "d11=30m" 'noesyhsqcetgp3d': line 42---> "d12=20u" 'noesyhsqcetgp3d': line 45---> "DELTA2=d4-larger(p2,p14)/2-p16-8u" 'noesyhsqcetgp3d': line 46---> "DELTA3=d4-larger(p2,p14)/2" 'noesyhsqcetgp3d': line 49---> "DELTA=larger(p14,p22)+d0*2" 'noesyhsqcetgp3d': line 50---> "DELTA1=p16+d16+larger(p2,p22)+d10*2" 'noesyhsqcetgp3d': line 57---> aqseq 321 'noesyhsqcetgp3d': line 60, expandi line 1---> ; dimension 3 aq-mode (F2) Echo-Antiecho (F1) States-TPPI F2->F1 'noesyhsqcetgp3d': line 60, expandi line 2---> define delay MCWRK 'noesyhsqcetgp3d': line 60, expandi line 3---> define delay MCREST 'noesyhsqcetgp3d': line 60, expandi line 4---> define loopcounter ST1CNT 'noesyhsqcetgp3d': line 60, expandi line 5---> "ST1CNT = td1 / (2)" 'noesyhsqcetgp3d': line 60, expandi line 6---> define loopcounter ST2CNT 'noesyhsqcetgp3d': line 60, expandi line 7---> "ST2CNT = td2 / (2)" 'noesyhsqcetgp3d': line 60, expandi line 8---> "MCWRK = 0.111111*d1" 'noesyhsqcetgp3d': line 60, expandi line 9---> "MCREST = d1 - d1" 'noesyhsqcetgp3d': line 60---> 1 ze dur2 == line 283 fixdel(3000.000000 usec) EVENT-EOSZ ze1 'noesyhsqcetgp3d': line 61---> d11 pl12:f2 dur3 == line 286 d11 channel 2: set power PL12 'noesyhsqcetgp3d': line 62, expandi line 1---> 2 MCWRK do:f2 dur4 == line 288 MCWRK channel 2: DO 'noesyhsqcetgp3d': line 62, expandi line 2---> LBLSTS2, MCWRK * 4 dur5 == line 289 MCWRK * 4 'noesyhsqcetgp3d': line 62, expandi line 3---> LBLF2, MCWRK * 3 dur6 == line 290 MCWRK * 3 'noesyhsqcetgp3d': line 62, expandi line 4---> LBLSTS1, MCWRK dur7 == line 291 MCWRK 'noesyhsqcetgp3d': line 62, expandi line 5---> LBLF1, MCREST dur8 == line 292 MCREST 'noesyhsqcetgp3d': line 63---> 3 d12 pl0:f2 dur9 == line 294 d12 channel 2: set power PL0 'noesyhsqcetgp3d': line 64---> (p1 ph7) Begin of PTList: lalign { dur10 == line 295 p1 SPF1 phase(7,0) } End of PTList 'noesyhsqcetgp3d': line 65---> DELTA dur11 == line 296 DELTA 'noesyhsqcetgp3d': line 66---> (p2 ph8) Begin of PTList: lalign { dur12 == line 297 p2 SPF1 phase(8,0) } End of PTList 'noesyhsqcetgp3d': line 67---> d0 dur13 == line 298 d0 'noesyhsqcetgp3d': line 70---> (center (p14:sp3 ph1):f2 (p22 ph1):f3 ) Begin of PTList: center { dur14 == line 301 p14 Shape SPF2 channel 2: shape pulse 3 via ptr -1 phase(1,0) } { dur15 == line 301 p22 SPF3 phase(1,0) } End of PTList 'noesyhsqcetgp3d': line 75---> d0 dur16 == line 306 d0 'noesyhsqcetgp3d': line 76---> (p1 ph1):f1 Begin of PTList: lalign { dur17 == line 307 p1 SPF1 phase(1,0) } End of PTList 'noesyhsqcetgp3d': line 77---> d8 dur18 == line 308 d8 'noesyhsqcetgp3d': line 78---> (p1 ph1):f1 Begin of PTList: lalign { dur19 == line 309 p1 SPF1 phase(1,0) } End of PTList 'noesyhsqcetgp3d': line 79---> DELTA3 pl0:f2 dur20 == line 310 DELTA3 channel 2: set power PL0 'noesyhsqcetgp3d': line 80---> 4u dur21 == line 311 fixdel(4.000000 usec) 'noesyhsqcetgp3d': line 81---> (center (p2 ph1) (p14:sp3 ph6):f2 ) Begin of PTList: center { dur22 == line 312 p2 SPF1 phase(1,0) } { dur23 == line 312 p14 Shape SPF2 channel 2: shape pulse 3 via ptr -1 phase(6,0) } End of PTList 'noesyhsqcetgp3d': line 82---> 4u dur24 == line 313 fixdel(4.000000 usec) 'noesyhsqcetgp3d': line 83---> DELTA3 pl2:f2 setnmr3|0 setnmr0|34|32|33 dur25 == line 314 DELTA3 setRcp2: 0x7 setNmr1: 0x1 channel 2: set power PL2 'noesyhsqcetgp3d': line 84---> p28 ph1 dur26 == line 315 p28 phase(1,0) 'noesyhsqcetgp3d': line 85---> 4u dur27 == line 316 fixdel(4.000000 usec) 'noesyhsqcetgp3d': line 86---> (p1 ph2) (p3 ph3):f2 Begin of PTList: lalign { dur28 == line 317 p1 SPF1 phase(2,0) } { dur29 == line 317 p3 SPF2 phase(3,0) } End of PTList 'noesyhsqcetgp3d': line 87---> d10 dur30 == line 318 d10 'noesyhsqcetgp3d': line 90---> (center (p2 ph5) (p22 ph1):f3 ) Begin of PTList: center { dur31 == line 321 p2 SPF1 phase(5,0) } { dur32 == line 321 p22 SPF3 phase(1,0) } End of PTList 'noesyhsqcetgp3d': line 95---> d10 dur33 == line 326 d10 'noesyhsqcetgp3d': line 96---> p16:gp1*EA dur34 == line 327 p16 NEXTGRAD 'noesyhsqcetgp3d': line 97---> d16 dur35 == line 328 d16 'noesyhsqcetgp3d': line 98---> (p4 ph4):f2 Begin of PTList: lalign { dur36 == line 329 p4 SPF2 phase(4,0) } End of PTList 'noesyhsqcetgp3d': line 99---> DELTA1 dur37 == line 330 DELTA1 'noesyhsqcetgp3d': line 100---> (ralign (p1 ph1) (p3 ph4):f2 ) Begin of PTList: ralign { dur38 == line 331 p1 SPF1 phase(1,0) } { dur39 == line 331 p3 SPF2 phase(4,0) } End of PTList 'noesyhsqcetgp3d': line 101---> DELTA3 pl0:f2 dur40 == line 332 DELTA3 channel 2: set power PL0 'noesyhsqcetgp3d': line 102---> (center (p2 ph1) (p14:sp3 ph1):f2 ) Begin of PTList: center { dur41 == line 333 p2 SPF1 phase(1,0) } { dur42 == line 333 p14 Shape SPF2 channel 2: shape pulse 3 via ptr -1 phase(1,0) } End of PTList 'noesyhsqcetgp3d': line 103---> 4u dur43 == line 334 fixdel(4.000000 usec) 'noesyhsqcetgp3d': line 104---> p16:gp2 dur44 == line 335 p16 NEXTGRAD 'noesyhsqcetgp3d': line 105---> DELTA2 pl12:f2 dur45 == line 336 DELTA2 channel 2: set power PL12 'noesyhsqcetgp3d': line 106---> 4u setnmr3^0 setnmr0^34^32^33 dur46 == line 337 fixdel(4.000000 usec) clrRcp2: 0x7 clrNmr1: 0x1 'noesyhsqcetgp3d': line 107---> go=2 ph31 cpd2:f2 Begin of PTList: lalign { dur47 == line 338 de1 dur48 == line 338 fixdel(4.000000 usec) ADCGO RCU 1 channel 1: SY receive phase(31,8) receive + phase (0,8) } { dur49 == line 338 derx dur50 == line 338 fixdel(3.000000 usec) setNmr1: 0x200 } { dur51 == line 338 deadc dur52 == line 338 fixdel(2.000000 usec) setNmr1: 0x10100 phase(41,0) PHADDO PHREF } { dur53 == line 338 depa dur54 == line 338 fixdel(4.000000 usec) setNmr1: 0x400 dur55 == line 338 aq channel 1: CPDSNG prog 29 (CPDPRG30)via ptr 0 channel 2: CPD prog 1 (CPDPRG2)via ptr 0 dur56 == line 338 fixdel(2500.000000 usec) dur57 == line 338 fixdel(500.000000 usec) clrNmr1: 0x30700 channel 1: Dwell off channel 1: SY transmit EVENT-EOSZ eos1 loop to 'noesyhsqcetgp3d': line 62, expandi line 1 times ns (ns+ds) } End of PTList 'noesyhsqcetgp3d': line 108, expandi line 1---> MCWRK do:f2 wr #0 if #0 zd igrad EA 'noesyhsqcetgp3d': line 108, expandi line 2---> lo to LBLSTS2 times 2 dur58 == line 340 MCWRK channel 2: DO EVENT-EOSZ zd1 AQBUS-WR RCU 1 wrif 0 loop to 'noesyhsqcetgp3d': line 62, expandi line 2 times 2 'noesyhsqcetgp3d': line 108, expandi line 3---> MCWRK id10 MCWRK ip3*2 MCWRK ip6*2 MCWRK ip31*2 'noesyhsqcetgp3d': line 108, expandi line 4---> lo to LBLF2 times ST2CNT dur59 == line 342 MCWRK EVENT-ID 10 dur60 == line 342 MCWRK IRPTIPH 3 IRPTIFC3 dur61 == line 342 MCWRK IRPTIPH 6 IRPTIFC3 dur62 == line 342 MCWRK IRPTIPH 31 IRPTIFC3 loop to 'noesyhsqcetgp3d': line 62, expandi line 3 times l127 'noesyhsqcetgp3d': line 108, expandi line 5---> MCWRK rd10 MCWRK ip7 MCWRK ip8 'noesyhsqcetgp3d': line 108, expandi line 6---> lo to LBLSTS1 times 2 dur63 == line 344 MCWRK EVENT-RD 10 dur64 == line 344 MCWRK IRPTIPH 7 dur65 == line 344 MCWRK IRPTIPH 8 loop to 'noesyhsqcetgp3d': line 62, expandi line 4 times 2 'noesyhsqcetgp3d': line 108, expandi line 7---> MCWRK id0 'noesyhsqcetgp3d': line 108, expandi line 8---> lo to LBLF1 times ST1CNT dur66 == line 346 MCWRK EVENT-ID 0 loop to 'noesyhsqcetgp3d': line 62, expandi line 5 times l126 'noesyhsqcetgp3d': line 111---> exit 'noesyhsqcetgp3d': line 112---> dur67 == line 349 fixdel(50000.000000 usec) dur68 == line 349 fixdel(10000.000000 usec) EVENT-EOSZ esc0 dur69 == line 349 fixdel(10000.000000 usec) phase program no. 33: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0x8000 = 180.00 degrees 3: 0x8000 = 180.00 degrees phase program no. 34: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0x8000 = 180.00 degrees 3: 0x8000 = 180.00 degrees 4: 0x4000 = 90.00 degrees 5: 0x4000 = 90.00 degrees 6: 0xc000 = 270.00 degrees 7: 0xc000 = 270.00 degrees phase program no. 36: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 37: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x4000 = 90.00 degrees phase program no. 38: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x8000 = 180.00 degrees phase program no. 39: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0xc000 = 270.00 degrees phase program no. 41: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 1: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 2: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x4000 = 90.00 degrees phase program no. 3: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0x8000 = 180.00 degrees phase program no. 4: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0 = 0.00 degrees 3: 0 = 0.00 degrees 4: 0 = 0.00 degrees 5: 0 = 0.00 degrees 6: 0 = 0.00 degrees 7: 0 = 0.00 degrees 8: 0x8000 = 180.00 degrees 9: 0x8000 = 180.00 degrees 10: 0x8000 = 180.00 degrees 11: 0x8000 = 180.00 degrees 12: 0x8000 = 180.00 degrees 13: 0x8000 = 180.00 degrees 14: 0x8000 = 180.00 degrees 15: 0x8000 = 180.00 degrees phase program no. 5: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0x8000 = 180.00 degrees 3: 0x8000 = 180.00 degrees phase program no. 6: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees phase program no. 7: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0 = 0.00 degrees 2: 0 = 0.00 degrees 3: 0 = 0.00 degrees 4: 0x8000 = 180.00 degrees 5: 0x8000 = 180.00 degrees 6: 0x8000 = 180.00 degrees 7: 0x8000 = 180.00 degrees phase program no. 8: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0x4000 = 90.00 degrees 1: 0x4000 = 90.00 degrees 2: 0x4000 = 90.00 degrees 3: 0x4000 = 90.00 degrees 4: 0xc000 = 270.00 degrees 5: 0xc000 = 270.00 degrees 6: 0xc000 = 270.00 degrees 7: 0xc000 = 270.00 degrees phase program no. 31: Fraction: 4.000000 Increment: 0x4000 = 90.00 degrees 0: 0 = 0.00 degrees 1: 0x8000 = 180.00 degrees 2: 0 = 0.00 degrees 3: 0x8000 = 180.00 degrees 4: 0x8000 = 180.00 degrees 5: 0 = 0.00 degrees 6: 0x8000 = 180.00 degrees 7: 0 = 0.00 degrees 8: 0x8000 = 180.00 degrees 9: 0 = 0.00 degrees 10: 0x8000 = 180.00 degrees 11: 0 = 0.00 degrees 12: 0 = 0.00 degrees 13: 0x8000 = 180.00 degrees 14: 0 = 0.00 degrees 15: 0x8000 = 180.00 degrees file list: ================================================= filename actlineno offset ================================================= noesyhsqcetgp3d 1 1 Avance.incl 25 25 noesyhsqcetgp3d 148 125 Grad.incl 150 150 noesyhsqcetgp3d 179 155 Delay.incl 181 181 noesyhsqcetgp3d 237 212 noesyhsqcetgp3d expandi 272 212 noesyhsqcetgp3d 282 223 noesyhsqcetgp3d expandi 284 223 noesyhsqcetgp3d 285 225 noesyhsqcetgp3d expandi 287 225 noesyhsqcetgp3d 293 231 noesyhsqcetgp3d expandi 339 231 noesyhsqcetgp3d 348 238