Content for NMR-STAR saveframe, "heteronucl_T2_relaxation_1"
save_heteronucl_T2_relaxation_1
_Heteronucl_T2_list.Sf_category heteronucl_T2_relaxation
_Heteronucl_T2_list.Sf_framecode heteronucl_T2_relaxation_1
_Heteronucl_T2_list.Entry_ID 52174
_Heteronucl_T2_list.ID 1
_Heteronucl_T2_list.Name 'Apo 600'
_Heteronucl_T2_list.Sample_condition_list_ID 1
_Heteronucl_T2_list.Sample_condition_list_label $sample_conditions_1
_Heteronucl_T2_list.Temp_calibration_method methanol
_Heteronucl_T2_list.Temp_control_method 'no temperature control applied'
_Heteronucl_T2_list.Spectrometer_frequency_1H 600
_Heteronucl_T2_list.T2_coherence_type S(+,-)
_Heteronucl_T2_list.T2_val_units s-1
_Heteronucl_T2_list.Rex_units .
_Heteronucl_T2_list.Details .
_Heteronucl_T2_list.Text_data_format text
_Heteronucl_T2_list.Text_data
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DATA CARRIER_FREQ (MHz)
60.792797
DATA NUCPMG (Hz)
@CARRIER_FREQ 1
33.33 33.33 66.67 66.67 100.00 100.00 133.33 133.33 166.67 200.00 200.00 233.33 233.33 266.67 300.00 333.33 400.00 466.67 500.00 600.00 633.33 800.00 833.33 966.67
DATA ASSIGNMENTS
1 144
2 146
3 147
4 155
5 156
6 174
7 176
8 183
9 185
10 187
11 189
12 213
13 215
14 216
15 219
16 221
17 236
DATA R2 (s-1)
@CARRIER_FREQ 1
1 13.71 14.48 14.67 13.75 13.59 14.34 13.42 13.74 14.28 13.80 13.88 14.11 13.60 14.04 13.37 13.49 13.59 13.47 13.73 14.09 13.48 13.90 13.69 13.23
2 13.89 13.38 13.08 12.88 13.81 13.54 13.08 13.54 12.72 13.34 12.64 13.71 13.30 13.19 12.74 12.81 13.85 13.12 12.81 13.14 13.37 13.17 13.28 12.99
3 14.63 13.14 13.38 13.83 14.22 14.01 13.56 13.57 13.73 12.77 12.97 13.84 13.62 13.75 13.30 12.80 13.41 13.61 13.78 12.96 14.46 12.68 12.77 13.70
4 15.57 15.53 14.93 14.70 14.53 15.19 15.44 15.42 14.91 15.12 14.31 14.82 14.48 15.00 15.41 14.83 14.43 14.92 15.04 14.84 14.63 14.44 14.46 14.29
5 14.11 14.34 14.97 13.99 15.03 13.73 15.10 14.60 14.51 14.51 13.89 14.48 14.96 14.76 13.78 14.68 14.52 13.83 14.15 13.86 14.39 14.23 14.68 13.61
6 16.82 15.66 15.50 16.29 16.04 15.22 15.51 15.44 14.54 15.60 14.63 14.29 15.19 13.94 14.32 14.21 14.18 14.17 14.13 13.80 13.85 13.88 13.97 14.00
7 16.96 17.08 17.56 16.62 16.53 14.99 16.36 15.88 15.02 15.51 15.58 15.27 15.09 15.78 15.38 15.68 15.26 14.50 15.03 15.32 14.95 14.15 15.01 14.90
8 25.93 25.05 24.04 26.20 22.59 24.60 23.28 22.52 22.25 22.36 22.84 20.67 23.04 22.80 21.37 22.57 20.59 22.52 21.43 22.31 21.00 20.38 20.38 23.95
9 15.15 15.31 14.22 14.78 14.83 14.60 15.12 14.37 13.65 13.44 13.98 14.39 13.87 13.54 14.00 13.67 13.69 13.55 13.87 13.77 13.68 13.46 13.57 13.93
10 15.03 15.35 13.91 14.22 13.66 14.39 13.89 14.03 13.30 13.94 14.01 13.80 13.81 14.37 13.95 13.75 13.35 12.99 13.72 12.73 12.32 12.77 12.72 13.32
11 19.28 19.12 19.05 19.04 18.33 18.22 18.28 18.58 18.23 17.67 18.23 18.80 17.51 18.55 17.45 17.90 16.84 17.10 17.44 16.62 16.16 16.25 15.01 15.38
12 15.36 15.40 13.77 14.75 14.85 15.27 15.57 14.93 14.62 14.17 14.77 14.59 14.80 15.15 15.10 14.56 13.85 14.12 13.05 13.58 14.13 13.14 13.42 13.88
13 16.61 17.06 15.92 16.53 15.98 16.43 16.71 16.10 16.71 16.05 16.43 15.73 16.34 16.24 15.18 16.07 15.77 15.05 15.20 14.54 14.51 13.80 14.69 13.75
14 11.18 10.98 11.14 11.04 11.11 10.89 11.36 11.28 11.81 11.17 11.57 10.75 11.61 11.79 11.40 11.42 11.65 11.31 11.25 11.25 11.64 11.70 11.20 11.43
15 21.03 22.45 21.43 21.47 21.75 23.07 22.11 22.95 21.34 20.99 20.66 22.78 21.86 21.84 20.37 21.45 21.06 20.15 20.77 20.13 19.29 18.69 19.50 17.53
16 15.70 15.23 15.16 14.28 13.97 14.29 14.65 14.08 14.77 14.25 14.15 14.17 14.11 14.16 13.63 14.83 14.11 13.77 13.78 14.80 13.99 13.85 14.22 14.01
17 15.81 16.38 15.76 15.46 15.54 14.90 15.66 14.82 14.63 15.68 14.07 15.43 15.30 14.59 14.92 14.93 14.90 14.36 13.98 14.61 14.35 13.96 14.74 14.52
DATA R2ERRORS (s-1)
@CARRIER_FREQ 1
1 0.46 0.48 0.48 0.46 0.45 0.47 0.45 0.46 0.47 0.46 0.46 0.47 0.45 0.47 0.45 0.45 0.45 0.45 0.46 0.47 0.45 0.46 0.46 0.45
2 0.36 0.35 0.35 0.34 0.36 0.35 0.35 0.35 0.34 0.35 0.34 0.36 0.35 0.35 0.34 0.34 0.36 0.35 0.34 0.35 0.35 0.35 0.35 0.34
3 0.51 0.48 0.48 0.49 0.50 0.50 0.49 0.49 0.49 0.47 0.47 0.49 0.49 0.49 0.48 0.47 0.48 0.49 0.49 0.47 0.51 0.46 0.47 0.49
4 0.50 0.50 0.49 0.48 0.48 0.49 0.50 0.50 0.49 0.49 0.47 0.48 0.48 0.49 0.50 0.48 0.48 0.49 0.49 0.49 0.48 0.48 0.48 0.47
5 0.54 0.55 0.57 0.54 0.57 0.53 0.57 0.56 0.56 0.56 0.54 0.56 0.57 0.56 0.54 0.56 0.56 0.54 0.55 0.54 0.55 0.55 0.56 0.53
6 0.71 0.66 0.66 0.69 0.68 0.65 0.66 0.66 0.63 0.66 0.63 0.62 0.65 0.61 0.62 0.62 0.62 0.62 0.61 0.60 0.61 0.61 0.61 0.61
7 0.82 0.82 0.84 0.80 0.80 0.74 0.79 0.77 0.74 0.76 0.76 0.75 0.74 0.77 0.75 0.76 0.75 0.72 0.74 0.75 0.74 0.71 0.74 0.73
8 1.40 1.33 1.26 1.42 1.16 1.30 1.20 1.15 1.13 1.14 1.17 1.04 1.19 1.17 1.08 1.16 1.03 1.15 1.08 1.14 1.06 1.02 1.02 1.25
9 0.38 0.38 0.36 0.37 0.37 0.37 0.38 0.36 0.35 0.35 0.36 0.36 0.35 0.35 0.36 0.35 0.35 0.35 0.35 0.35 0.35 0.35 0.35 0.36
10 0.32 0.33 0.31 0.31 0.30 0.31 0.31 0.31 0.30 0.31 0.31 0.30 0.30 0.31 0.31 0.30 0.30 0.29 0.30 0.29 0.28 0.29 0.29 0.30
11 0.43 0.42 0.42 0.42 0.41 0.40 0.40 0.41 0.40 0.39 0.40 0.42 0.39 0.41 0.39 0.40 0.37 0.38 0.39 0.37 0.36 0.36 0.34 0.35
12 0.48 0.48 0.45 0.47 0.47 0.48 0.49 0.47 0.47 0.45 0.47 0.46 0.47 0.48 0.48 0.46 0.45 0.45 0.43 0.44 0.45 0.43 0.44 0.45
13 0.38 0.39 0.37 0.38 0.37 0.38 0.39 0.37 0.39 0.37 0.38 0.37 0.38 0.38 0.36 0.37 0.37 0.35 0.36 0.35 0.35 0.33 0.35 0.33
14 0.30 0.30 0.30 0.30 0.30 0.30 0.30 0.30 0.31 0.30 0.31 0.29 0.31 0.31 0.30 0.30 0.31 0.30 0.30 0.30 0.31 0.31 0.30 0.30
15 0.70 0.76 0.71 0.72 0.73 0.78 0.74 0.78 0.71 0.70 0.68 0.77 0.73 0.73 0.67 0.71 0.70 0.66 0.69 0.66 0.63 0.61 0.64 0.58
16 0.46 0.45 0.45 0.43 0.42 0.43 0.44 0.42 0.44 0.43 0.43 0.43 0.42 0.43 0.41 0.44 0.42 0.42 0.42 0.44 0.42 0.42 0.43 0.42
17 0.50 0.52 0.50 0.49 0.49 0.48 0.50 0.48 0.47 0.50 0.46 0.49 0.49 0.47 0.48 0.48 0.48 0.46 0.46 0.47 0.46 0.46 0.47 0.47
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loop_
_Heteronucl_T2_experiment.Experiment_ID
_Heteronucl_T2_experiment.Experiment_name
_Heteronucl_T2_experiment.Sample_ID
_Heteronucl_T2_experiment.Sample_label
_Heteronucl_T2_experiment.Sample_state
_Heteronucl_T2_experiment.Entry_ID
_Heteronucl_T2_experiment.Heteronucl_T2_list_ID
1 '1H-15N CPMG' . . . 52174 1
stop_
loop_
_Heteronucl_T2_software.Software_ID
_Heteronucl_T2_software.Software_label
_Heteronucl_T2_software.Method_ID
_Heteronucl_T2_software.Method_label
_Heteronucl_T2_software.Entry_ID
_Heteronucl_T2_software.Heteronucl_T2_list_ID
1 $software_1 . . 52174 1
2 $software_2 . . 52174 1
stop_
save_