BMRB Entry 7389

Click here to enlarge.

PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR7389
MolProbity Validation Chart

NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry

Title:
sPLA2 inhibitor 9
Deposition date:
2007-04-20
Original release date:
2008-02-20
Authors:
Thwin, M.; Satyanarayanajois, D.; Nagarajarao, L.; Sato, K.; Gopalakrishnakone, P.; Arjunan, P.
Citation:

Citation: Thwin, M.; Satyanarayanajois, D.; Nagarajarao, L.; Sato, K.; Arjunan, P.; Ramapatna, S.; Kumna, P.; Gopalakrishnakone, P.. "Novel peptide inhibitors of human secretory phospholipase A2 with antiinflammatory activity: solution structure and molecular modeling."  J. Med. Chem. 50, 5938-5950 (2007).
PubMed: 17973469

Assembly members:

Assembly members:
pip9, polymer, 9 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):

Entity Sequences (FASTA):
pip9: VDIHVWDGV

Data sets:
Data typeCount
1H chemical shifts51

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1pip91

Entities:

Entity 1, pip9 9 residues - Formula weight is not available

1   VALASPILEHISVALTRPASPGLYVAL

Samples:

sample: pip9 4.5 mM; Dimethyl sulfoxide 50%; H2O 50%

sample_conditions_1: ionic strength: . .; pressure: 1 atm; temperature: . K

Experiments:

NameSampleSample stateSample conditions
2D NOESYsampleisotropicsample_conditions_1

Software:

CYANA v2.1, GUNTERT, P. ET AL. - refinement

CYANA v2.1, GUNTERT, P. ET AL. - structure solution

NMR spectrometers:

  • Bruker AVANCE 500 MHz
  • Bruker AVANCE 800 MHz