BMRB Entry 7387

Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR7387

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Title:
PIPdim 18
Deposition date:
2007-04-20
Original release date:
2008-06-12
Authors:
Thwin, M.; Satyanarayanajois, D.; Nagarajarao, L.; Sato, K.; Gopalakrishnakone, P.; Arjunan, P.
Citation:

Citation: Thwin, M.; Satyanarayanajois, D.; Nagarajarao, L.; Sato, K.; Arjunan, P.; Ramapatna, S.; Kumna, P.; Gopalakrishnakone, P.. "Novel peptide inhibitors of human secretory phospholipase A2 with anti-inflammatory activity: solution structure and molecular modeling"  J. Med. Chem. 50, 5938-5950 (2007).
PubMed: 17973469

Assembly members:

Assembly members:
PIP_18, polymer, 18 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: recombinant technology

Entity Sequences (FASTA):

Entity Sequences (FASTA):
PIP_18: VDIHVWDGVVDIHVWDGV

Data sets:
Data typeCount
1H chemical shifts111

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1PIP_181

Entities:

Entity 1, PIP_18 18 residues - Formula weight is not available

1   VALASPILEHISVALTRPASPGLYVALVAL
2   ASPILEHISVALTRPASPGLYVAL

Samples:

sample: PIP_18 2.8 mM; Dimethyl sulfoxide 100%

sample_conditions_1: ionic strength: . .; pressure: 1 atm; temperature: 305 K

Experiments:

NameSampleSample stateSample conditions
2D NOESYsampleisotropicsample_conditions_1
DQF-COSYsampleisotropicsample_conditions_1

Software:

CYANA v2.1, GUNTERT, P. ET AL. - refinement

CYANA v2.1, GUNTERT, P. ET AL. - structure solution

NMR spectrometers:

  • Bruker AVANCE 500 MHz