BMRB Entry 7005
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR7005
MolProbity Validation Chart
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NMR-STAR v3 text file.
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Citation: Nygaard, R.; Nielbo, S.; Schwartz, T.; Poulsen, F.. "The PP-Fold Solution Structure of Human Polypeptide YY and Human PYY3-36 As
Determined by NMR" Biochemistry 45, 8350-8357 (2006).
PubMed: 16819834
Assembly members:
Peptide YY, polymer, 35 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
Peptide YY: IKPEAPGEDASPEELNRYYA
SLRHYLNLVTRQRYX
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 204 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Peptide YY | 1 |
Entities:
Entity 1, Peptide YY 35 residues - Formula weight is not available
| 1 | ILE | LYS | PRO | GLU | ALA | PRO | GLY | GLU | ASP | ALA | ||||
| 2 | SER | PRO | GLU | GLU | LEU | ASN | ARG | TYR | TYR | ALA | ||||
| 3 | SER | LEU | ARG | HIS | TYR | LEU | ASN | LEU | VAL | THR | ||||
| 4 | ARG | GLN | ARG | TYR | NH2 |
Samples:
sample_1: Peptide YY 1 mM; NaOH mM; HCl mM; D2O 10%; H2O 90%
sample_cond_1: pH: 4.6; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D DQF COSY | sample_1 | not available | sample_cond_1 |
| 2D TOCSY | sample_1 | not available | sample_cond_1 |
| 2D NOESY | sample_1 | not available | sample_cond_1 |
Software:
NMRPipe - processing
Pronto3D - data analysis
CYANA v1.0 - structure solution
X-PLOR NIH v2.9 - structure solution
CNS v1.1 - refinement
NMR spectrometers:
- Varian INOVA 750 MHz