BMRB Entry 6348
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR6348
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Citation: van Gammeren, Adriaan; Hulsbergen, Frans; Hollander, Johan; de Groot, Huub. "Residual backbone and side-chain 13C and 15N resonance assignments of the
intrinsic transmembrane light-harvesting 2 protein complex by solid state Magic
Angle Spinning NMR spectroscopy" J. Biomol. NMR 31, 279-293 (2005).
PubMed: 15754054
Assembly members:
alpha-subunit, polymer, 53 residues, Formula weight is not available
Beta-subunit, polymer, 41 residues, Formula weight is not available
RG1, non-polymer, 715.013 Da.
BCL, non-polymer, 911.504 Da.
Natural source: Common Name: purple bacterium Taxonomy ID: 1074 Superkingdom: Bacteria Kingdom: not available Genus/species: Rhodopseudomonas acidophila
Experimental source: Production method: Purified from the natural source
Entity Sequences (FASTA):
alpha-subunit: MNQGKIWTVVNPAIGIPALL
GSVTVIAILVHLAILSHTTW
FPAYWQGGVKKAA
Beta-subunit: ATLTAEQSEELHKYVIDGTR
VFLGLALVAHFLAFSATPWL
H
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 310 |
| 15N chemical shifts | 81 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | Chain 1, Alpha-subunit | 1 |
| 2 | Chain 1, Beta-subunit | 2 |
| 3 | Chain 2, Alpha-subunit | 1 |
| 4 | Chain 2, Beta-subunit | 2 |
| 5 | Chain 3, Alpha-subunit | 1 |
| 6 | Chain 3, Beta-subunit | 2 |
| 7 | Chain 4, Alpha-subunit | 1 |
| 8 | Chain 4, Beta-subunit | 2 |
| 9 | Chain 5, Alpha-subunit | 1 |
| 10 | Chain 5, Beta-subunit | 2 |
| 11 | Chain 6, Alpha-subunit | 1 |
| 12 | Chain 6, Beta-subunit | 2 |
| 13 | Chain 7, Alpha-subunit | 1 |
| 14 | Chain 7, Beta-subunit | 2 |
| 15 | Chain 8, Alpha-subunit | 1 |
| 16 | Chain 8, Beta-subunit | 2 |
| 17 | Chain 9, Alpha-subunit | 1 |
| 18 | Chain 9, Beta-subunit | 2 |
| 19 | bacteriochlorophylls A, 1 | 4 |
| 20 | bacteriochlorophylls A, 2 | 4 |
| 21 | bacteriochlorophylls A, 3 | 4 |
| 22 | rhodopin glucoside, 1 | 3 |
| 23 | rhodopin glucoside, 2 | 3 |
Entities:
Entity 1, Chain 1, Alpha-subunit 53 residues - Formula weight is not available
| 1 | MET | ASN | GLN | GLY | LYS | ILE | TRP | THR | VAL | VAL | ||||
| 2 | ASN | PRO | ALA | ILE | GLY | ILE | PRO | ALA | LEU | LEU | ||||
| 3 | GLY | SER | VAL | THR | VAL | ILE | ALA | ILE | LEU | VAL | ||||
| 4 | HIS | LEU | ALA | ILE | LEU | SER | HIS | THR | THR | TRP | ||||
| 5 | PHE | PRO | ALA | TYR | TRP | GLN | GLY | GLY | VAL | LYS | ||||
| 6 | LYS | ALA | ALA |
Entity 2, Chain 1, Beta-subunit 41 residues - Formula weight is not available
| 1 | ALA | THR | LEU | THR | ALA | GLU | GLN | SER | GLU | GLU | ||||
| 2 | LEU | HIS | LYS | TYR | VAL | ILE | ASP | GLY | THR | ARG | ||||
| 3 | VAL | PHE | LEU | GLY | LEU | ALA | LEU | VAL | ALA | HIS | ||||
| 4 | PHE | LEU | ALA | PHE | SER | ALA | THR | PRO | TRP | LEU | ||||
| 5 | HIS |
Entity 4, bacteriochlorophylls A, 1 - C55 H74 Mg N4 O6 - 911.504 Da.
| 1 | BCL |
Entity 3, rhodopin glucoside, 1 - C46 H66 O6 - 715.013 Da.
| 1 | RG1 |
Samples:
sample_1: alpha-subunit; Beta-subunit
sample_conditions: pH: .; temperature: 253 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| not available | sample_1 | not available | sample_conditions |
Software:
No software information available
NMR spectrometers:
- Bruker AV 750 MHz