BMRB Entry 5587
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5587
MolProbity Validation Chart
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NMR-STAR v3 text file.
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Citation: Znosko, B.; Burkard, M.; Krugh, T.; Turner, D.. "Molecular Recognition in Purine-Rich Internal Loops: Thermodynamic, Structural,
and Dynamic Consequences of Purine for Adenine Substitutions in 5'(rGGCAAGCCU)2" Biochemistry 41, 14978-14987 (2002).
PubMed: 1245247
Assembly members:
na, polymer, 9 residues, Formula weight is not available
Natural source: Common Name: not available Taxonomy ID: not available Superkingdom: not available Kingdom: not available Genus/species: not available not available
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
na: GGCAXGCCU
- assigned_chemical_shifts
| Data type | Count |
| 31P chemical shifts | 8 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | 5'-R(*GP*GP*CP*AP*(P5P)P*GP*CP*CP*U)-3' | 1 |
Entities:
Entity 1, 5'-R(*GP*GP*CP*AP*(P5P)P*GP*CP*CP*U)-3' 9 residues - Formula weight is not available
| 1 | G | G | C | A | P5P | G | C | C | U |
Samples:
sample_1: na 1 mM; NaCl 80 mM; phosphate buffer 10 mM; EDTA 0.5 mM; H2O 90%; D2O 10%
sample_2: na 2 mM; NaCl 80 mM; phosphate buffer 10 mM; EDTA 0.5 mM; D2O 99.996%
sample_cond_1: pH: 6.5; pressure: 1 atm; temperature: 273 K
sample_cond_2: pH: 7.7; pressure: 1 atm; temperature: 303 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D NOESY | not available | not available | not available |
Software:
VNMR v5.2 - collection
FELIX v2000 - data analysis
DISCOVER v95.0 - structure solution
NMR spectrometers:
- Varian INOVA 500 MHz