BMRB Entry 5472
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_anomalous, AVS_full, LACS
BMRB Entry DOI: doi:10.13018/BMR5472
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
All files associated with the entry
Citation: Song, Jikui; Laskowski, Michael; Qasim, Mohammod; Markley, John. "Two Conformational States of Turkey Ovomucoid Third Domain at low pH:
Three-dimensional Structures, Internal Dynamics, and Interconversion
Kinetics and Thermodynamics" Biochemistry 42, 6380-6391 (2003).
PubMed: 12767219
Assembly members:
Ovomucoid Third Domain, polymer, 56 residues, Formula weight is not available
Natural source: Common Name: Turkey Taxonomy ID: 9103 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Meleagris gallopavo
Experimental source: Production method: recombinant technology
Entity Sequences (FASTA):
Ovomucoid Third Domain: LAAVSVDCSEYPKDACTLEY
RPLCGSDNKTYGNKCNFCNA
VVESNGTLTLSHFGKC
- assigned_chemical_shifts
| Data type | Count |
| 13C chemical shifts | 205 |
| 15N chemical shifts | 60 |
| 1H chemical shifts | 332 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | P5-OMTKY3 C state | 1 |
Entities:
Entity 1, P5-OMTKY3 C state 56 residues - Formula weight is not available
| 1 | LEU | ALA | ALA | VAL | SER | VAL | ASP | CYS | SER | GLU | ||||
| 2 | TYR | PRO | LYS | ASP | ALA | CYS | THR | LEU | GLU | TYR | ||||
| 3 | ARG | PRO | LEU | CYS | GLY | SER | ASP | ASN | LYS | THR | ||||
| 4 | TYR | GLY | ASN | LYS | CYS | ASN | PHE | CYS | ASN | ALA | ||||
| 5 | VAL | VAL | GLU | SER | ASN | GLY | THR | LEU | THR | LEU | ||||
| 6 | SER | HIS | PHE | GLY | LYS | CYS |
Samples:
Sample_1: Ovomucoid Third Domain, [U-13C; U-15N], 2 mM
condition_1: pH: 2.5; temperature: 298 K
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 1H-15N NOESY | not available | not available | not available |
| 15N-TOCSY | not available | not available | not available |
| 1H-1H NOESY | not available | not available | not available |
| HNCA | not available | not available | not available |
| HNCOCA | not available | not available | not available |
| HNCACB | not available | not available | not available |
| CCONH | not available | not available | not available |
| HCCONH | not available | not available | not available |
| HCCHCOSY | not available | not available | not available |
| 13C-NOESY HNCO | not available | not available | not available |
| 3h-HNCO | not available | not available | not available |
| 1H-15N TOCSY | not available | not available | not available |
| HN(CO)CA | not available | not available | not available |
| HNCO | not available | not available | not available |
Software:
FELIX v95 -
NMR spectrometers:
- Bruker DMX 500 MHz
- Bruker AMX 600 MHz
- Bruker DMX 750 MHz
Related Database Links:
| BMRB | 1374 1375 4068 42 4864 4865 507 5411 5440 5448 5449 5473 5518 5520 |
| PDB | |
| SWISS-PROT | P52245 P68436 |
Download HSQC peak lists in one of the following formats:
CSV: Backbone
or all simulated peaks
SPARKY: Backbone
or all simulated peaks