BMRB Entry 5463
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PDB ID:
Entry in NMR Restraints Grid
Validation report in NRG-CING
Chem Shift validation: AVS_anomalous, AVS_full
BMRB Entry DOI: doi:10.13018/BMR5463
MolProbity Validation Chart
NMR-STAR file interactive viewer.
NMR-STAR v3 text file.
XML gzip file.
RDF gzip file.
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Citation: Nguyen, M.; Preece, N.; Mahata, M.; Mahata, S.; Tsigelny, I.; O'Connor, D.. "Conformational preferences and activities of peptides from the catecholamine
release-inhibitory (catestatin) region of chromogranin A." Regul. Pept. 118, 75-87 (2004).
PubMed: 14759560
Assembly members:
catestatin chain A, polymer, 21 residues, Formula weight is not available
Natural source: Common Name: Human Taxonomy ID: 9606 Superkingdom: Eukaryota Kingdom: Metazoa Genus/species: Homo sapiens
Experimental source: Production method: chemical synthesis
Entity Sequences (FASTA):
catestatin chain A: SSMKLSFRARAYGFRGPGPQ
L
- assigned_chemical_shifts
| Data type | Count |
| 1H chemical shifts | 122 |
Additional metadata:
Assembly:
| Entity Assembly ID | Entity Name | Entity ID |
|---|---|---|
| 1 | catestatin | 1 |
Entities:
Entity 1, catestatin 21 residues - Formula weight is not available
| 1 | SER | SER | MET | LYS | LEU | SER | PHE | ARG | ALA | ARG | ||||
| 2 | ALA | TYR | GLY | PHE | ARG | GLY | PRO | GLY | PRO | GLN | ||||
| 3 | LEU |
Samples:
sample_1: catestatin chain A mM; D20 90%; H2O 10%
sample_cond_1: pH: 4.9; temperature: 303 K; ionic strength: 6.4 mM; pressure: 1 atm
Experiments:
| Name | Sample | Sample state | Sample conditions |
|---|---|---|---|
| 2D NOESY | not available | not available | not available |
| 2D TOCSY | not available | not available | not available |
Software:
VNMR v5.3F - collection
FELIX v2000 - data analysis
DISCOVER vC - structure solution
NMRARCHITECHT - refinement
NMR spectrometers:
- Varian INOVA 500 MHz