BMRB Entry 5452

Chem Shift validation: AVS_full
BMRB Entry DOI: doi:10.13018/BMR5452

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Title:
pKa determinations for AAPE
Deposition date:
2002-07-04
Original release date:
2003-03-20
Authors:
Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John
Citation:

Citation: Song, Jikui; Laskowski, Michael; Qasim, Mohammad; Markley, John. "NMR Determination of pKa Values for Asp, Glu, His, and Lys Mutants at Each Variable Contiguous Enzyme-inhibitor Contact Position of the Turkey Ovomucoid Third Domain"  Biochemistry 42, 2847-2856 (2003).
PubMed: 12627950

Assembly members:

Assembly members:
Suc-PPAD-pna, polymer, 4 residues, Formula weight is not available

Natural source:

Natural source:   Common Name: not available   Taxonomy ID: not available   Superkingdom: not available   Kingdom: not available   Genus/species: not available not available

Experimental source:

Experimental source:   Production method: chemical synthesis

Entity Sequences (FASTA):

Entity Sequences (FASTA):
Suc-PPAD-pna: AAPE

Data sets:
  • pKa_value_data_set
  • pH_NMR_param_list
Data typeCount
pKa values1
pH NMR parameter values13

Additional metadata:

  • Assembly
  • Samples and Experiments
  • Software
  • Spectrometers
  • Hide all

Assembly:

Entity Assembly IDEntity NameEntity ID
1AAPE1

Entities:

Entity 1, AAPE 4 residues - Formula weight is not available

1   ALAALAPROGLU

Samples:

sample_1: Suc-PPAD-pna 2 mM; KCl 100 mM; DSS 0.4 mM

conditions_set_1: pH: .; temperature: 298 K; ionic strength: 100 mM

Experiments:

NameSampleSample stateSample conditions
TOCSYsample_1not availableconditions_set_1

Software:

No software information available

NMR spectrometers:

  • Bruker DMX 500 MHz